#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:48:17 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181195 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/74/2227485.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227485_Fobs loop_ _publ_author_name 'Arderne, Charmaine' 'Kruger, Gert J.' _publ_section_title ; Ethane-1,2-diammonium dibromide: a redetermination at 100K ; _journal_coeditor_code HB5586 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2470 _journal_volume 66 _journal_year 2010 _space_group_IT_number 12 _symmetry_space_group_name_Hall '-C 2y' _symmetry_space_group_name_H-M 'C 1 2/m 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.323 _cell_angle_gamma 90.000 _cell_length_a 15.1442 _cell_length_b 4.7598 _cell_length_c 4.8146 _exptl_crystal_F_000 212.00 _reflns_d_resolution_high 0.7470 _cod_data_source_file hb5586Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' mo_gk08_0m in C2/m at 100K' _shelx_refln_list_code 4 _shelx_f_calc_maximum 154.95 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' '-x, -y, -z' 'x, -y, z' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 338.68 393.03 11.42 o 4 0 0 11363.41 12466.97 272.10 o 6 0 0 10724.99 11392.55 316.87 o 8 0 0 1828.38 2047.82 44.98 o 10 0 0 7452.16 7884.57 142.34 o 12 0 0 270.06 290.86 4.83 o 14 0 0 1952.70 2081.25 28.55 o 16 0 0 2276.91 2402.84 36.37 o 18 0 0 212.50 223.98 14.02 o 1 1 0 902.29 1015.71 12.97 o 3 1 0 11991.74 12637.95 165.67 o 5 1 0 31.70 29.43 0.69 o 7 1 0 5092.88 5334.26 47.01 o 9 1 0 3703.15 3959.71 33.29 o 11 1 0 874.02 925.34 9.03 o 13 1 0 5318.13 5534.65 58.70 o 15 1 0 33.59 43.04 1.22 o 17 1 0 1902.79 1925.48 24.17 o 19 1 0 1402.12 1441.47 34.18 o 0 2 0 17496.37 16901.51 417.57 o 2 2 0 570.32 542.16 6.52 o 4 2 0 7079.59 6997.44 75.04 o 6 2 0 6222.48 6150.97 63.02 o 8 2 0 970.05 993.06 11.14 o 10 2 0 5669.15 5656.09 66.23 o 12 2 0 236.93 248.62 4.01 o 14 2 0 1535.07 1552.74 23.75 o 16 2 0 1859.15 1861.86 25.75 o 18 2 0 163.24 167.85 3.78 o 1 3 0 1309.07 1267.29 14.04 o 3 3 0 5868.22 5726.12 61.29 o 5 3 0 28.93 34.82 1.07 o 7 3 0 3779.85 3832.36 39.28 o 9 3 0 2165.70 2220.19 27.67 o 11 3 0 643.98 650.22 8.76 o 13 3 0 3567.69 3607.96 49.53 o 15 3 0 19.76 24.36 1.98 o 17 3 0 1348.43 1356.24 19.20 o 0 4 0 6442.07 6752.66 118.00 o 2 4 0 288.36 285.69 4.68 o 4 4 0 2969.19 2999.67 34.29 o 6 4 0 2931.85 2924.49 41.92 o 8 4 0 437.98 460.07 6.18 o 10 4 0 2963.20 3045.86 42.93 o 12 4 0 139.24 140.17 3.82 o 14 4 0 858.81 857.62 14.07 o 1 5 0 527.09 554.50 8.27 o 3 5 0 2552.41 2617.11 38.00 o 5 5 0 5.35 3.92 2.00 o 7 5 0 1604.99 1721.89 31.92 o 9 5 0 988.62 1044.65 17.58 o 11 5 0 297.20 311.48 6.44 o 0 6 0 2433.73 2572.42 44.19 o 2 6 0 100.14 110.74 3.43 o 4 6 0 1098.88 1177.59 18.70 o 6 6 0 1153.92 1219.71 29.93 o -20 0 1 978.66 1006.31 38.93 o -18 0 1 2167.74 2175.78 34.35 o -16 0 1 3.24 8.37 1.23 o -14 0 1 4043.19 4039.77 55.08 o -12 0 1 1836.72 1872.12 23.01 o -10 0 1 3336.86 3390.94 38.67 o -8 0 1 4410.34 4335.58 49.61 o -6 0 1 178.10 192.31 2.20 o -4 0 1 10839.13 11063.66 231.58 o -2 0 1 2197.94 2332.38 31.46 o 0 0 1 728.15 818.23 9.99 o 2 0 1 10174.31 10438.55 137.96 o 4 0 1 1213.27 1275.23 17.54 o 6 0 1 6299.29 6415.93 109.91 o 8 0 1 3961.83 4021.91 87.57 o 10 0 1 239.71 244.75 5.05 o 12 0 1 6418.00 6293.04 113.45 o 14 0 1 170.99 175.61 7.04 o 16 0 1 1821.37 1775.14 39.76 o 18 0 1 1709.16 1701.12 38.39 o -19 1 1 302.27 307.90 4.51 o -17 1 1 1446.00 1449.64 16.42 o -15 1 1 2384.92 2436.21 25.27 o -13 1 1 151.29 158.67 2.12 o -11 1 1 5287.37 5305.78 50.33 o -9 1 1 2702.85 2788.04 25.41 o -7 1 1 7175.57 7157.12 62.73 o -5 1 1 9318.48 9293.49 81.05 o -3 1 1 56.73 51.65 1.00 o -1 1 1 24008.35 24481.90 541.55 o 1 1 1 2186.58 2207.70 29.36 o 3 1 1 9359.93 9447.00 97.99 o 5 1 1 7680.99 7676.39 77.32 o 7 1 1 319.91 330.94 3.36 o 9 1 1 7562.39 7733.81 83.16 o 11 1 1 427.93 432.12 6.51 o 13 1 1 1278.32 1299.74 18.29 o 15 1 1 2462.34 2456.78 37.51 o 17 1 1 49.33 48.31 2.40 o -18 2 1 1798.39 1805.68 23.44 o -16 2 1 0.66 5.72 1.86 o -14 2 1 3491.68 3489.44 41.39 o -12 2 1 1440.65 1443.29 17.38 o -10 2 1 2425.84 2459.58 32.53 o -8 2 1 4255.46 4192.18 42.87 o -6 2 1 49.08 49.94 0.99 o -4 2 1 7474.13 7302.26 73.95 o -2 2 1 2051.09 1945.22 23.93 o 0 2 1 983.65 927.40 10.12 o 2 2 1 7550.97 7151.56 77.35 o 4 2 1 457.21 471.51 5.12 o 6 2 1 4758.86 4589.18 49.57 o 8 2 1 3187.67 3109.42 39.33 o 10 2 1 313.36 305.63 4.45 o 12 2 1 4970.56 4995.61 62.78 o 14 2 1 143.54 149.19 2.93 o 16 2 1 1555.35 1505.60 23.25 o 18 2 1 1388.88 1406.20 32.18 o -17 3 1 1002.63 992.53 14.37 o -15 3 1 1519.59 1533.71 19.84 o -13 3 1 86.32 88.56 2.38 o -11 3 1 3404.41 3370.85 42.62 o -9 3 1 1337.49 1320.23 17.07 o -7 3 1 3463.50 3408.67 34.64 o -5 3 1 4821.58 4503.58 47.91 o -3 3 1 56.37 56.43 1.59 o -1 3 1 9185.84 8528.20 95.74 o 1 3 1 1178.55 1109.47 12.89 o 3 3 1 3851.78 3754.07 45.08 o 5 3 1 4531.65 4321.89 44.15 o 7 3 1 157.27 160.88 2.66 o 9 3 1 4460.46 4350.79 54.95 o 11 3 1 369.57 349.21 5.62 o 13 3 1 877.04 860.69 12.40 o 15 3 1 1665.49 1603.52 22.48 o -14 4 1 1960.91 1916.70 26.96 o -12 4 1 819.83 826.09 11.24 o -10 4 1 1255.50 1264.66 16.65 o -8 4 1 2342.31 2276.34 31.21 o -6 4 1 32.24 40.96 1.55 o -4 4 1 3583.59 3509.17 39.17 o -2 4 1 1220.04 1192.36 12.53 o 0 4 1 589.67 573.91 6.69 o 2 4 1 3711.25 3563.31 38.23 o 4 4 1 191.40 193.14 2.86 o 6 4 1 2518.13 2485.59 29.54 o 8 4 1 1645.64 1633.65 21.22 o 10 4 1 182.40 175.00 3.69 o 12 4 1 2760.36 2724.90 43.33 o 14 4 1 80.34 84.77 2.93 o -11 5 1 1554.34 1593.61 32.55 o -9 5 1 607.22 607.90 11.00 o -7 5 1 1603.84 1574.82 22.06 o -5 5 1 1968.32 1950.13 30.11 o -3 5 1 35.81 41.82 1.71 o -1 5 1 3674.92 3757.37 40.45 o 1 5 1 475.58 464.38 5.79 o 3 5 1 1662.97 1662.74 21.33 o 5 5 1 1891.74 1873.21 26.11 o 7 5 1 64.95 74.00 2.81 o 9 5 1 2098.28 2061.41 31.48 o 11 5 1 155.20 157.24 4.69 o -6 6 1 17.01 16.93 2.54 o -4 6 1 1336.04 1422.94 25.20 o -2 6 1 474.25 513.65 8.03 o 0 6 1 210.73 229.28 6.05 o 2 6 1 1388.49 1466.65 20.86 o 4 6 1 84.25 85.37 3.42 o -20 0 2 326.65 325.89 6.46 o -18 0 2 788.00 770.34 12.90 o -16 0 2 2728.37 2742.72 43.40 o -14 0 2 50.47 55.84 2.18 o -12 0 2 4050.44 4039.63 55.22 o -10 0 2 3058.65 3121.16 37.17 o -8 0 2 4231.32 4184.75 45.26 o -6 0 2 9342.33 9176.50 107.56 o -4 0 2 34.78 29.61 1.85 o -2 0 2 13510.30 13829.48 251.34 o 0 0 2 4345.17 4352.87 61.39 o 2 0 2 7809.85 7739.73 87.81 o 4 0 2 6029.30 5932.27 94.56 o 6 0 2 3.95 3.13 0.62 o 8 0 2 6785.36 6631.69 80.16 o 10 0 2 770.66 786.35 12.07 o 12 0 2 970.24 976.68 21.99 o 14 0 2 2284.40 2338.86 56.87 o 16 0 2 5.02 5.55 1.63 o -19 1 2 2110.03 2139.24 26.39 o -17 1 2 4.79 5.41 1.34 o -15 1 2 2596.68 2553.05 26.49 o -13 1 2 2234.12 2201.87 22.90 o -11 1 2 1836.34 1849.85 19.29 o -9 1 2 4292.29 4225.88 37.54 o -7 1 2 289.09 286.79 2.72 o -5 1 2 5674.96 5838.64 54.53 o -3 1 2 3998.16 3846.71 38.91 o -1 1 2 828.89 842.52 10.38 o 1 1 2 6363.16 6295.50 59.96 o 3 1 2 1960.77 2016.62 21.95 o 5 1 2 4993.52 5128.92 51.50 o 7 1 2 3879.64 4040.16 40.55 o 9 1 2 59.41 67.11 1.53 o 11 1 2 5315.03 5407.88 61.98 o 13 1 2 492.94 507.68 6.38 o 15 1 2 1615.59 1619.27 24.78 o 17 1 2 1547.94 1531.62 24.36 o -18 2 2 648.00 642.84 9.52 o -16 2 2 2208.52 2221.48 30.05 o -14 2 2 35.91 45.96 2.42 o -12 2 2 3146.42 3151.05 43.65 o -10 2 2 2458.60 2462.54 26.08 o -8 2 2 3152.02 3182.61 26.86 o -6 2 2 6377.51 6216.42 81.64 o -4 2 2 2.19 2.97 0.62 o -2 2 2 9705.07 9388.92 169.39 o 0 2 2 2815.15 2736.53 29.28 o 2 2 2 4385.39 4384.79 42.69 o 4 2 2 5283.97 5155.57 50.21 o 6 2 2 2.18 6.00 1.19 o 8 2 2 5242.83 5170.60 65.15 o 10 2 2 722.21 718.51 9.60 o 12 2 2 796.28 798.38 10.64 o 14 2 2 1932.04 1902.62 26.44 o 16 2 2 4.28 7.83 1.95 o -17 3 2 3.49 5.75 1.76 o -15 3 2 1810.20 1792.80 23.14 o -13 3 2 1513.63 1512.25 19.59 o -11 3 2 1238.65 1209.63 14.82 o -9 3 2 2847.12 2777.87 32.60 o -7 3 2 192.78 197.56 3.77 o -5 3 2 3840.29 3723.51 36.53 o -3 3 2 2172.63 2061.21 21.14 o -1 3 2 505.85 492.61 5.74 o 1 3 2 4292.48 4168.82 44.43 o 3 3 2 757.68 778.41 9.25 o 5 3 2 2976.50 2971.21 36.43 o 7 3 2 2442.70 2433.67 31.11 o 9 3 2 62.09 65.64 2.17 o 11 3 2 3453.74 3385.28 43.02 o 13 3 2 320.25 310.60 5.32 o 15 3 2 1105.68 1071.88 15.41 o -14 4 2 20.66 28.84 2.28 o -12 4 2 1740.65 1704.31 22.17 o -10 4 2 1252.92 1220.53 15.97 o -8 4 2 1611.71 1562.01 18.75 o -6 4 2 3158.74 2966.41 42.81 o -4 4 2 0.37 1.25 0.97 o -2 4 2 4416.72 4298.57 43.72 o 0 4 2 1352.64 1273.97 13.35 o 2 4 2 2034.95 2006.51 21.78 o 4 4 2 2724.35 2581.17 33.96 o 6 4 2 0.28 2.75 1.68 o 8 4 2 2835.59 2722.17 46.48 o 10 4 2 414.03 375.19 6.82 o 12 4 2 453.98 433.51 7.66 o -11 5 2 543.07 545.97 8.95 o -9 5 2 1338.54 1318.26 29.53 o -7 5 2 91.19 96.84 2.76 o -5 5 2 1588.40 1575.45 17.45 o -3 5 2 1097.30 1062.81 11.43 o -1 5 2 237.96 232.67 3.46 o 1 5 2 1853.45 1841.72 21.48 o 3 5 2 379.94 377.78 5.85 o 5 5 2 1381.33 1363.07 22.58 o 7 5 2 1118.14 1082.43 22.11 o 9 5 2 25.23 36.52 5.86 o -2 6 2 1653.75 1737.90 23.72 o 0 6 2 511.56 522.46 7.81 o -18 0 3 33.68 33.47 3.20 o -16 0 3 1707.52 1691.55 27.13 o -14 0 3 2272.82 2219.83 35.33 o -12 0 3 799.40 791.49 11.80 o -10 0 3 4097.74 3964.01 54.39 o -8 0 3 421.49 416.10 4.93 o -6 0 3 3088.28 3126.53 38.87 o -4 0 3 4927.28 4896.44 60.70 o -2 0 3 413.11 436.59 6.60 o 0 0 3 4943.84 4887.81 55.37 o 2 0 3 2395.13 2461.48 28.05 o 4 0 3 3234.41 3274.86 43.78 o 6 0 3 4313.38 4341.11 64.79 o 8 0 3 8.08 16.41 1.52 o 10 0 3 4040.12 4007.45 59.79 o 12 0 3 1009.75 1019.63 15.82 o 14 0 3 1430.93 1473.54 22.66 o -19 1 3 309.19 306.07 5.31 o -17 1 3 2308.82 2317.42 26.15 o -15 1 3 0.01 1.08 1.30 o -13 1 3 2632.33 2601.51 27.68 o -11 1 3 2507.18 2478.76 24.56 o -9 1 3 1694.60 1721.75 14.89 o -7 1 3 6880.90 6778.30 57.76 o -5 1 3 8.56 15.21 0.94 o -3 1 3 6562.29 6656.71 58.50 o -1 1 3 3950.91 3956.48 34.81 o 1 1 3 3425.63 3493.96 31.89 o 3 1 3 4912.38 4818.66 43.91 o 5 1 3 41.02 44.28 1.31 o 7 1 3 4236.80 4177.50 46.52 o 9 1 3 1223.72 1238.34 14.18 o 11 1 3 672.14 680.45 8.14 o 13 1 3 1666.47 1684.92 18.19 o 15 1 3 107.04 111.07 2.34 o -18 2 3 22.82 31.00 2.07 o -16 2 3 1394.50 1376.18 17.37 o -14 2 3 1904.38 1897.50 20.39 o -12 2 3 729.38 733.07 8.80 o -10 2 3 3164.96 3058.10 40.74 o -8 2 3 348.19 366.55 3.92 o -6 2 3 2634.72 2689.06 25.25 o -4 2 3 3523.07 3520.00 34.83 o -2 2 3 347.35 352.28 4.54 o 0 2 3 3788.96 3761.04 35.84 o 2 2 3 1708.43 1726.32 15.98 o 4 2 3 2615.33 2616.32 26.76 o 6 2 3 3192.89 3190.17 38.96 o 8 2 3 4.18 11.52 1.56 o 10 2 3 3315.06 3309.86 45.03 o 12 2 3 790.91 801.66 11.69 o 14 2 3 1148.74 1157.90 17.99 o -15 3 3 0.01 0.75 1.76 o -13 3 3 1720.62 1679.62 20.38 o -11 3 3 1754.14 1703.04 21.83 o -9 3 3 1131.91 1129.35 15.14 o -7 3 3 4300.51 4245.57 56.00 o -5 3 3 18.65 25.26 1.44 o -3 3 3 4148.69 4140.88 41.32 o -1 3 3 2538.68 2524.31 24.30 o 1 3 3 2020.17 2001.93 20.50 o 3 3 3 3282.17 3201.45 44.47 o 5 3 3 45.62 44.61 2.01 o 7 3 3 2948.30 2844.69 38.92 o 9 3 3 833.74 843.95 12.33 o 11 3 3 448.71 452.60 9.05 o 13 3 3 1200.95 1187.89 18.51 o -14 4 3 1082.62 1036.82 17.42 o -12 4 3 402.10 380.61 8.19 o -10 4 3 1767.97 1693.58 27.57 o -8 4 3 194.81 208.28 3.99 o -6 4 3 1420.62 1477.23 16.67 o -4 4 3 1897.11 1904.79 22.25 o -2 4 3 185.34 199.26 3.47 o 0 4 3 2075.19 2065.44 20.07 o 2 4 3 858.04 845.12 10.55 o 4 4 3 1410.86 1395.83 19.68 o 6 4 3 1742.12 1720.68 24.06 o 8 4 3 3.01 7.00 2.31 o 10 4 3 1873.08 1858.53 28.83 o -9 5 3 523.19 550.48 8.19 o -7 5 3 1979.71 2036.66 37.81 o -5 5 3 4.06 10.09 1.87 o -3 5 3 1835.98 1914.47 19.99 o -1 5 3 1101.88 1102.68 12.54 o 1 5 3 897.00 917.14 11.25 o 3 5 3 1506.63 1501.53 22.07 o 5 5 3 17.00 20.64 2.35 o -18 0 4 1782.68 1832.82 29.71 o -16 0 4 50.92 55.03 2.92 o -14 0 4 1889.91 1869.44 30.02 o -12 0 4 1998.97 1972.08 31.53 o -10 0 4 604.26 608.97 8.64 o -8 0 4 5514.74 5512.02 68.64 o -6 0 4 83.27 82.09 2.21 o -4 0 4 3925.01 3926.19 53.22 o -2 0 4 3508.76 3502.16 43.74 o 0 0 4 1515.68 1580.61 18.29 o 2 0 4 4298.12 4338.06 54.07 o 4 0 4 106.88 96.39 2.49 o 6 0 4 2517.35 2437.38 36.75 o 8 0 4 1599.46 1639.08 25.09 o 10 0 4 444.12 460.03 7.98 o 12 0 4 1239.25 1244.06 19.49 o -17 1 4 997.41 979.82 11.70 o -15 1 4 1689.91 1647.47 18.87 o -13 1 4 206.14 208.63 3.19 o -11 1 4 3017.67 2867.25 30.56 o -9 1 4 434.72 439.61 4.79 o -7 1 4 1399.45 1406.30 12.35 o -5 1 4 3834.00 3864.23 34.12 o -3 1 4 82.60 96.21 1.54 o -1 1 4 3192.14 3254.14 28.76 o 1 1 4 1914.46 1936.25 18.27 o 3 1 4 1440.41 1418.79 15.65 o 5 1 4 3662.22 3534.57 38.14 o 7 1 4 3.02 3.40 1.36 o 9 1 4 2428.23 2360.21 27.30 o 11 1 4 1247.97 1236.22 14.75 o -16 2 4 45.07 47.05 2.90 o -14 2 4 1579.11 1504.22 18.85 o -12 2 4 1669.39 1627.73 20.25 o -10 2 4 476.60 474.42 7.06 o -8 2 4 4667.92 4669.06 46.15 o -6 2 4 59.42 67.42 2.15 o -4 2 4 3107.84 3132.96 31.14 o -2 2 4 3054.00 3036.22 32.05 o 0 2 4 1322.91 1338.91 12.16 o 2 2 4 3472.79 3470.65 37.41 o 4 2 4 106.10 98.25 2.33 o 6 2 4 2174.69 2107.85 26.13 o 8 2 4 1312.55 1322.48 16.75 o 10 2 4 375.24 380.55 5.72 o -13 3 4 144.01 143.65 3.40 o -11 3 4 2030.38 1947.51 27.02 o -9 3 4 266.71 273.28 4.81 o -7 3 4 886.59 915.80 10.71 o -5 3 4 2538.49 2577.68 25.35 o -3 3 4 69.77 77.48 2.02 o -1 3 4 1978.58 2013.43 19.59 o 1 3 4 1280.18 1261.38 13.35 o 3 3 4 977.02 972.22 11.79 o 5 3 4 2362.70 2320.56 28.72 o 7 3 4 3.88 3.04 1.75 o 9 3 4 1656.71 1620.90 20.52 o -10 4 4 273.13 279.74 4.97 o -8 4 4 2610.84 2629.54 34.29 o -6 4 4 34.90 41.42 1.93 o -4 4 4 1728.39 1734.54 18.15 o -2 4 4 1677.27 1696.45 18.77 o 0 4 4 714.47 723.01 8.54 o 2 4 4 1961.29 1963.31 22.99 o 4 4 4 60.57 64.20 2.48 o 6 4 4 1245.09 1218.11 17.21 o -14 0 5 13.68 18.02 2.63 o -12 0 5 2223.80 2210.59 42.48 o -10 0 5 431.97 425.42 7.27 o -8 0 5 620.01 632.31 10.59 o -6 0 5 2881.98 2908.84 36.75 o -4 0 5 0.55 16.44 2.25 o -2 0 5 2234.91 2273.74 35.45 o 0 0 5 1525.85 1503.51 24.20 o 2 0 5 526.55 519.70 10.57 o 4 0 5 3166.56 3044.30 45.89 o 6 0 5 28.60 40.80 2.87 o 8 0 5 1510.14 1432.64 22.40 o -15 1 5 1204.02 1208.87 15.06 o -13 1 5 1337.51 1267.54 15.72 o -11 1 5 118.13 121.65 2.85 o -9 1 5 3755.52 3773.78 37.54 o -7 1 5 181.39 195.87 2.76 o -5 1 5 2107.22 2153.76 20.46 o -3 1 5 2576.29 2606.84 26.12 o -1 1 5 475.41 493.72 5.55 o 1 1 5 3189.37 3182.94 35.95 o 3 1 5 143.49 152.49 3.24 o 5 1 5 1240.89 1178.16 14.17 o 7 1 5 1483.62 1491.30 17.74 o 9 1 5 198.96 207.29 3.75 o -12 2 5 1851.89 1781.54 24.56 o -10 2 5 336.02 330.12 5.66 o -8 2 5 475.26 477.16 6.37 o -6 2 5 2371.60 2453.78 23.25 o -4 2 5 0.53 12.85 1.41 o -2 2 5 1791.61 1816.78 19.45 o 0 2 5 1253.39 1270.22 14.35 o 2 2 5 408.35 426.07 5.57 o 4 2 5 2639.72 2608.01 30.29 o 6 2 5 23.73 30.96 2.03 o -11 3 5 79.09 84.70 3.14 o -9 3 5 2658.18 2617.92 34.28 o -7 3 5 117.02 130.88 3.01 o -5 3 5 1454.97 1461.12 14.16 o -3 3 5 1777.66 1811.11 19.43 o -1 3 5 336.86 350.99 5.41 o 1 3 5 2221.17 2216.26 24.44 o 3 3 5 91.27 109.05 2.99 o 5 3 5 863.64 836.75 10.57 o -4 4 5 0.35 7.20 1.95 o -2 4 5 1020.75 1053.73 18.55 o -10 0 6 2407.14 2507.71 47.55 o -8 0 6 322.22 322.49 6.46 o -6 0 6 1283.00 1331.80 19.83 o -4 0 6 1762.09 1801.00 29.12 o -2 0 6 82.97 82.93 3.87 o 0 0 6 2389.80 2374.66 43.11 o 2 0 6 165.86 158.13 5.40 o -9 1 6 236.28 236.41 4.49 o -7 1 6 1625.25 1681.36 18.62 o -5 1 6 77.02 84.90 2.55 o -3 1 6 1344.50 1399.03 16.28 o -1 1 6 985.14 946.07 12.16 o 1 1 6 102.21 98.74 3.40 o -6 2 6 1106.68 1131.85 12.96 o -4 2 6 1434.76 1437.97 18.21 o -2 2 6 67.94 70.34 2.93 o 0 2 6 2026.36 2048.80 40.38 o