#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/74/2227487.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227487_Fobs loop_ _publ_author_name 'Fairuz, Zainal A.' 'Aiyub, Zaharah' 'Abdullah, Zanariah' 'Ng, Seik Weng' 'Tiekink, Edward R. T.' _publ_section_title ; Tetra-\m-acetato-\k^8^O:O'-bis{[N-(4-chlorophenyl)-4-methylpyridin-2-amine-\kN^1^]copper(II)} ; _journal_coeditor_code HB5589 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1049 _journal_page_last m1050 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 109.901 _cell_angle_gamma 90.000 _cell_length_a 11.7430 _cell_length_b 15.6191 _cell_length_c 9.9866 _exptl_crystal_F_000 820.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file hb5589Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 212.94 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 18619.88 20647.94 880.68 o 2 0 0 120.69 92.40 9.27 o 3 0 0 271.65 337.60 23.31 o 4 0 0 4197.12 5066.10 222.31 o 5 0 0 2102.92 2225.08 97.88 o 6 0 0 43.71 34.84 14.16 o 7 0 0 4937.01 5134.65 218.21 o 8 0 0 18991.84 19531.70 798.76 o 9 0 0 1567.37 1494.50 78.24 o 10 0 0 13.20 -18.52 20.59 o 11 0 0 1176.25 962.80 93.59 o 12 0 0 362.20 298.84 57.63 o 13 0 0 154.06 104.72 31.51 o 14 0 0 110.01 131.40 35.25 o 1 1 0 42.18 109.27 15.80 o 2 1 0 39.33 77.83 6.04 o 3 1 0 4634.35 5018.28 157.75 o 4 1 0 5539.60 6550.89 189.80 o 5 1 0 614.82 647.27 26.43 o 6 1 0 47.32 86.81 11.69 o 7 1 0 496.16 466.25 25.10 o 8 1 0 1230.13 1378.88 50.90 o 9 1 0 591.63 692.89 47.94 o 10 1 0 76.28 62.59 20.85 o 11 1 0 11.14 -22.43 25.10 o 12 1 0 101.59 90.90 24.11 o 13 1 0 336.95 287.49 28.19 o 14 1 0 22.15 3.63 20.96 o 0 2 0 19615.68 19065.63 631.67 o 1 2 0 18308.89 17853.82 721.71 o 2 2 0 281.76 226.14 13.35 o 3 2 0 206.03 262.05 16.47 o 4 2 0 96.78 165.48 11.62 o 5 2 0 1668.23 1749.36 56.26 o 6 2 0 3189.90 3047.01 94.05 o 7 2 0 4762.00 4625.48 139.70 o 8 2 0 1881.28 1868.05 64.19 o 9 2 0 501.36 489.81 34.83 o 10 2 0 1.26 -14.96 18.45 o 11 2 0 33.78 34.40 17.40 o 12 2 0 15.07 42.15 24.21 o 13 2 0 265.89 202.11 34.40 o 14 2 0 812.11 595.84 73.01 o 1 3 0 8714.31 9238.08 531.45 o 2 3 0 35.62 27.70 5.30 o 3 3 0 444.62 355.88 26.00 o 4 3 0 42.36 22.43 8.49 o 5 3 0 1513.93 1941.17 61.93 o 6 3 0 8.95 16.41 10.02 o 7 3 0 361.10 490.40 30.69 o 8 3 0 41.59 49.14 18.51 o 9 3 0 81.79 75.57 20.80 o 10 3 0 724.88 714.41 50.88 o 11 3 0 170.40 126.69 19.62 o 12 3 0 5.50 -10.48 24.45 o 13 3 0 31.70 43.09 23.83 o 14 3 0 30.73 35.83 26.15 o 0 4 0 8505.94 9460.83 315.59 o 1 4 0 22864.10 23553.20 964.01 o 2 4 0 1589.40 1298.64 71.80 o 3 4 0 6838.56 7084.90 252.36 o 4 4 0 68.80 54.87 14.15 o 5 4 0 340.45 521.01 42.73 o 6 4 0 3481.41 3617.23 131.22 o 7 4 0 3634.52 3434.15 126.90 o 8 4 0 900.35 823.21 45.51 o 9 4 0 1663.51 1709.84 64.09 o 10 4 0 7.69 6.30 15.02 o 11 4 0 3.23 21.45 17.18 o 12 4 0 308.90 336.14 51.51 o 13 4 0 233.37 154.40 28.79 o 14 4 0 337.84 389.45 51.03 o 1 5 0 575.62 638.44 24.01 o 2 5 0 2168.69 2000.64 87.60 o 3 5 0 228.96 173.62 11.98 o 4 5 0 1609.29 1597.43 51.48 o 5 5 0 30.67 20.80 9.42 o 6 5 0 7.42 9.84 9.80 o 7 5 0 14.55 19.25 11.80 o 8 5 0 226.31 272.18 21.52 o 9 5 0 739.81 712.45 57.92 o 10 5 0 154.26 170.89 20.66 o 11 5 0 753.46 724.72 38.85 o 12 5 0 521.50 540.66 68.53 o 13 5 0 40.57 61.89 24.95 o 0 6 0 10.86 39.91 7.30 o 1 6 0 44.10 19.98 7.71 o 2 6 0 1771.54 1732.26 77.91 o 3 6 0 284.67 314.17 15.21 o 4 6 0 140.86 139.03 15.60 o 5 6 0 349.70 351.60 23.36 o 6 6 0 1091.96 1173.23 54.42 o 7 6 0 1221.78 1253.77 46.55 o 8 6 0 629.76 684.57 35.74 o 9 6 0 103.57 102.68 18.03 o 10 6 0 237.53 226.07 23.06 o 11 6 0 49.59 9.67 18.92 o 12 6 0 154.35 151.54 26.47 o 13 6 0 251.84 226.98 65.00 o 1 7 0 1027.12 1161.85 39.91 o 2 7 0 3183.46 3192.34 136.78 o 3 7 0 3996.30 4050.77 172.55 o 4 7 0 1763.77 1536.06 58.68 o 5 7 0 4981.85 5074.44 151.47 o 6 7 0 205.05 204.72 26.62 o 7 7 0 59.28 68.33 22.53 o 8 7 0 5.61 15.50 13.67 o 9 7 0 22.11 16.48 14.53 o 10 7 0 242.21 290.70 25.32 o 11 7 0 352.40 358.13 37.71 o 12 7 0 434.16 348.53 96.96 o 13 7 0 159.95 120.09 62.91 o 0 8 0 227.11 211.46 15.37 o 1 8 0 38.09 64.57 10.53 o 2 8 0 1425.87 1409.73 75.41 o 3 8 0 4517.60 4521.58 191.72 o 4 8 0 0.26 -16.96 15.96 o 5 8 0 2666.35 2648.71 97.10 o 6 8 0 1384.70 1397.07 56.25 o 7 8 0 675.82 760.72 34.86 o 8 8 0 6.71 -6.01 12.81 o 9 8 0 153.64 170.20 26.95 o 10 8 0 277.18 272.97 32.43 o 11 8 0 41.39 -0.36 39.55 o 12 8 0 25.14 25.23 53.93 o 13 8 0 64.76 145.02 61.99 o 1 9 0 2056.91 1779.98 59.65 o 2 9 0 4847.85 4661.30 141.30 o 3 9 0 8973.95 8938.65 369.29 o 4 9 0 2253.11 1944.26 132.36 o 5 9 0 2187.94 2380.48 92.17 o 6 9 0 722.16 726.71 42.78 o 7 9 0 193.80 206.32 50.97 o 8 9 0 28.53 -4.89 19.72 o 9 9 0 257.41 277.03 31.33 o 10 9 0 871.99 1024.32 58.05 o 11 9 0 885.03 923.08 57.03 o 12 9 0 107.65 135.23 59.28 o 0 10 0 389.40 399.91 22.91 o 1 10 0 129.74 130.23 13.81 o 2 10 0 23.51 12.80 11.20 o 3 10 0 431.16 436.15 33.76 o 4 10 0 0.73 -3.02 16.53 o 5 10 0 10.33 4.57 29.44 o 6 10 0 1.89 -4.39 19.10 o 7 10 0 111.05 120.75 28.90 o 8 10 0 26.41 2.54 26.45 o 9 10 0 38.38 -6.23 22.22 o 10 10 0 6.75 18.67 28.12 o 11 10 0 44.73 65.12 37.43 o 12 10 0 28.81 36.29 60.81 o 1 11 0 268.28 284.84 19.20 o 2 11 0 421.41 416.31 30.95 o 3 11 0 2229.34 2203.22 85.54 o 4 11 0 5547.24 5514.20 216.99 o 5 11 0 428.02 482.68 34.56 o 6 11 0 64.99 52.22 21.45 o 7 11 0 101.80 121.48 48.36 o 8 11 0 437.20 508.41 48.53 o 9 11 0 148.39 174.91 29.69 o 10 11 0 282.93 323.58 35.90 o 11 11 0 365.21 336.45 73.84 o 12 11 0 333.92 327.48 77.19 o 0 12 0 501.32 426.65 60.28 o 1 12 0 24.32 22.26 18.78 o 2 12 0 13.90 -10.14 12.42 o 3 12 0 203.91 185.39 24.55 o 4 12 0 201.25 226.30 20.62 o 5 12 0 14.26 17.17 19.56 o 6 12 0 4.52 18.25 21.02 o 7 12 0 132.20 129.32 30.80 o 8 12 0 37.53 30.19 23.04 o 9 12 0 6.15 -23.90 22.86 o 10 12 0 39.60 18.06 34.10 o 11 12 0 16.69 12.06 61.94 o 1 13 0 70.66 91.97 23.03 o 2 13 0 195.69 192.44 42.81 o 3 13 0 265.70 268.90 21.81 o 4 13 0 794.89 780.50 98.10 o 5 13 0 188.24 209.12 26.09 o 6 13 0 38.81 24.56 21.92 o 7 13 0 2.21 -8.27 22.59 o 8 13 0 55.03 41.36 41.32 o 9 13 0 226.94 221.78 31.49 o 10 13 0 377.79 337.00 73.41 o 11 13 0 180.81 254.82 79.29 o 0 14 0 199.90 139.56 50.83 o 1 14 0 32.61 -12.85 20.50 o 2 14 0 0.55 -11.69 18.32 o 3 14 0 99.18 106.98 26.19 o 4 14 0 0.19 8.88 17.95 o 5 14 0 50.35 49.53 17.30 o 6 14 0 24.59 11.46 16.69 o 7 14 0 1.28 23.56 24.39 o 8 14 0 10.10 2.48 62.85 o 9 14 0 2.71 20.11 61.16 o 10 14 0 16.74 75.20 69.38 o 1 15 0 35.38 -23.76 32.97 o 2 15 0 151.16 147.75 26.74 o 3 15 0 372.46 342.34 51.75 o 4 15 0 253.38 201.17 55.88 o 5 15 0 368.99 349.87 44.38 o 6 15 0 13.75 11.52 26.60 o 7 15 0 0.04 -18.34 40.08 o 8 15 0 0.47 -83.25 57.24 o 9 15 0 167.05 109.01 70.88 o 0 16 0 29.43 -11.35 51.45 o 1 16 0 178.06 77.13 39.28 o 2 16 0 71.06 66.96 29.18 o 3 16 0 200.02 208.83 40.30 o 4 16 0 55.24 20.99 44.28 o 5 16 0 94.10 82.59 41.31 o 6 16 0 100.72 123.96 68.51 o 7 16 0 35.79 50.62 46.66 o 8 16 0 26.87 21.80 65.72 o 1 17 0 0.23 -44.59 38.71 o 2 17 0 53.24 53.06 27.03 o 3 17 0 120.55 122.28 101.68 o 4 17 0 59.65 22.63 35.49 o 5 17 0 113.89 107.46 45.01 o 6 17 0 10.68 -30.71 42.31 o 7 17 0 0.70 -8.40 45.07 o 0 18 0 83.83 -48.67 57.18 o 1 18 0 166.16 2.73 44.15 o 2 18 0 102.88 109.09 45.88 o 3 18 0 21.81 1.55 40.34 o 4 18 0 0.96 -18.31 59.81 o 5 18 0 11.99 13.55 44.27 o 6 18 0 62.33 78.14 47.63 o 1 19 0 2.81 39.54 46.93 o 2 19 0 25.97 -46.52 41.99 o 3 19 0 30.68 26.59 44.82 o 4 19 0 1.26 -14.09 30.28 o 5 19 0 1.85 -10.82 61.48 o 0 20 0 95.47 51.83 68.88 o 1 20 0 42.70 -5.17 47.23 o 2 20 0 54.94 -37.27 46.09 o -14 1 1 380.49 356.02 34.67 o -13 1 1 450.04 439.20 46.43 o -12 1 1 459.99 468.68 30.63 o -11 1 1 599.56 585.32 32.91 o -10 1 1 73.26 60.27 15.94 o -9 1 1 1.00 -3.60 14.38 o -8 1 1 5959.46 5734.35 201.21 o -7 1 1 9750.03 9684.41 332.00 o -6 1 1 7182.58 7038.38 205.73 o -5 1 1 1351.28 1152.38 38.69 o -4 1 1 1211.64 1083.45 41.10 o -3 1 1 8.46 17.26 5.62 o -2 1 1 10673.07 10863.73 312.11 o -1 1 1 965.17 735.06 41.13 o 0 1 1 26742.84 26580.06 676.33 o 1 1 1 23102.21 24048.22 913.50 o 2 1 1 9349.84 10094.68 341.80 o 3 1 1 2940.45 2927.13 87.33 o 4 1 1 1596.40 1627.94 52.30 o 5 1 1 2607.94 3175.48 96.87 o 6 1 1 2720.96 3040.13 94.73 o 7 1 1 2401.44 2457.97 80.08 o 8 1 1 2147.44 2137.89 72.65 o 9 1 1 360.32 410.14 28.02 o 10 1 1 205.48 201.20 25.53 o 11 1 1 114.79 98.69 21.42 o 12 1 1 21.50 -28.73 22.98 o 13 1 1 131.95 98.39 37.40 o -14 2 1 227.61 233.05 31.19 o -13 2 1 7.69 25.45 18.90 o -12 2 1 81.50 76.21 18.92 o -11 2 1 1.07 8.20 15.19 o -10 2 1 143.69 143.49 21.10 o -9 2 1 677.71 708.24 38.55 o -8 2 1 194.74 216.11 30.91 o -7 2 1 91.19 133.21 17.38 o -6 2 1 341.87 407.73 21.19 o -5 2 1 34.41 68.18 10.82 o -4 2 1 62.12 73.52 9.62 o -3 2 1 1382.99 1445.44 51.77 o -2 2 1 1338.48 1466.10 44.26 o -1 2 1 2169.88 2341.92 79.86 o 0 2 1 15.57 43.22 6.65 o 1 2 1 1.62 28.15 8.87 o 2 2 1 15231.32 16969.95 550.00 o 3 2 1 1051.97 1107.36 43.22 o 4 2 1 2662.22 2734.13 83.82 o 5 2 1 1305.85 1392.45 47.65 o 6 2 1 71.29 72.82 12.67 o 7 2 1 714.54 744.31 47.30 o 8 2 1 57.50 75.09 16.99 o 9 2 1 36.89 34.40 18.57 o 10 2 1 990.99 946.59 44.14 o 11 2 1 562.56 569.76 44.79 o 12 2 1 3.27 -22.59 23.76 o 13 2 1 17.88 1.81 26.48 o -14 3 1 516.99 506.27 41.07 o -13 3 1 789.01 813.44 49.98 o -12 3 1 1258.99 1184.12 50.10 o -11 3 1 421.00 451.16 29.08 o -10 3 1 573.84 580.73 36.00 o -9 3 1 3093.75 2849.01 136.36 o -8 3 1 1499.72 1528.46 73.65 o -7 3 1 1812.60 1677.88 56.32 o -6 3 1 733.71 679.03 27.89 o -5 3 1 2469.35 2339.68 72.37 o -4 3 1 3603.27 3235.13 101.11 o -3 3 1 5313.90 5505.63 159.96 o -2 3 1 6681.07 7807.40 264.23 o -1 3 1 13047.11 13134.59 375.99 o 0 3 1 6477.56 5969.55 142.02 o 1 3 1 1791.73 1629.38 57.91 o 2 3 1 2430.58 2400.59 72.45 o 3 3 1 1930.80 1974.89 102.18 o 4 3 1 529.33 471.03 25.37 o 5 3 1 4023.82 4311.21 129.86 o 6 3 1 466.76 527.55 26.73 o 7 3 1 3883.05 3880.01 120.32 o 8 3 1 3343.76 3391.99 118.38 o 9 3 1 1116.19 1032.74 44.36 o 10 3 1 322.45 346.49 34.46 o 11 3 1 79.33 92.40 26.80 o 12 3 1 15.53 10.00 25.35 o 13 3 1 1.14 -11.93 19.32 o -14 4 1 16.45 29.53 18.42 o -13 4 1 75.79 60.51 28.19 o -12 4 1 175.52 159.11 21.81 o -11 4 1 10.53 3.43 18.05 o -10 4 1 2.85 -2.19 15.11 o -9 4 1 609.14 707.39 38.68 o -8 4 1 6086.38 6309.10 188.73 o -7 4 1 2277.24 2306.39 74.16 o -6 4 1 15.91 42.73 9.81 o -5 4 1 231.90 215.39 17.22 o -4 4 1 3556.39 3444.73 116.09 o -3 4 1 664.51 815.15 32.19 o -2 4 1 4430.66 5329.92 181.90 o -1 4 1 411.90 516.29 16.88 o 0 4 1 45343.33 45026.89 1288.26 o 1 4 1 6908.87 7459.80 253.90 o 2 4 1 29.62 26.38 6.30 o 3 4 1 4341.89 4356.32 128.70 o 4 4 1 13741.05 14864.27 485.20 o 5 4 1 1798.69 1667.67 58.34 o 6 4 1 14.26 86.58 23.44 o 7 4 1 82.61 82.98 15.27 o 8 4 1 1232.48 1318.14 61.83 o 9 4 1 452.49 477.20 30.77 o 10 4 1 174.18 189.59 28.49 o 11 4 1 736.61 744.96 78.86 o 12 4 1 687.94 648.72 39.91 o 13 4 1 263.60 253.33 42.05 o -14 5 1 487.50 495.72 41.85 o -13 5 1 271.68 270.35 32.08 o -12 5 1 57.28 54.61 21.68 o -11 5 1 226.42 244.75 26.26 o -10 5 1 422.22 424.17 34.09 o -9 5 1 8.55 8.49 13.88 o -8 5 1 178.50 174.87 17.43 o -7 5 1 1962.16 1895.71 63.15 o -6 5 1 2911.22 2969.14 101.48 o -5 5 1 2221.20 2268.17 80.43 o -4 5 1 60.92 79.39 8.95 o -3 5 1 9.55 15.57 6.24 o -2 5 1 983.60 943.62 43.65 o -1 5 1 586.24 567.23 18.57 o 0 5 1 551.78 708.05 25.21 o 1 5 1 3867.55 3591.18 125.62 o 2 5 1 4281.04 3781.74 131.44 o 3 5 1 3311.75 3265.38 97.87 o 4 5 1 7.13 -3.49 8.88 o 5 5 1 621.70 673.23 29.32 o 6 5 1 2012.46 2018.00 66.94 o 7 5 1 1906.83 1951.77 66.82 o 8 5 1 97.59 110.93 18.10 o 9 5 1 1747.09 1736.09 79.45 o 10 5 1 336.32 392.68 42.60 o 11 5 1 481.17 433.19 31.51 o 12 5 1 62.77 67.64 21.91 o 13 5 1 408.99 412.34 43.46 o -14 6 1 4.54 20.29 34.81 o -13 6 1 0.47 -4.14 32.89 o -12 6 1 204.28 222.28 28.80 o -11 6 1 1189.07 1223.03 57.83 o -10 6 1 930.41 958.60 48.14 o -9 6 1 564.39 616.73 32.51 o -8 6 1 85.58 118.29 16.09 o -7 6 1 133.25 160.18 22.08 o -6 6 1 135.48 150.56 19.01 o -5 6 1 222.39 214.80 16.38 o -4 6 1 893.32 815.81 34.49 o -3 6 1 438.22 399.48 17.96 o -2 6 1 1467.97 1352.70 50.62 o -1 6 1 5529.97 5445.56 142.38 o 0 6 1 1876.38 1751.26 55.04 o 1 6 1 1594.12 1528.87 49.55 o 2 6 1 213.63 301.25 32.46 o 3 6 1 2758.99 2843.35 131.41 o 4 6 1 821.62 741.63 37.67 o 5 6 1 1067.28 1009.69 43.24 o 6 6 1 1662.46 1600.52 67.75 o 7 6 1 1269.55 1322.83 61.24 o 8 6 1 486.76 481.77 36.90 o 9 6 1 496.35 566.29 52.18 o 10 6 1 529.46 540.56 33.62 o 11 6 1 508.35 559.07 35.71 o 12 6 1 103.93 127.60 32.02 o 13 6 1 59.08 38.27 30.94 o -13 7 1 108.25 151.88 38.52 o -12 7 1 406.77 407.59 47.77 o -11 7 1 522.42 531.04 36.93 o -10 7 1 20.56 23.56 16.51 o -9 7 1 28.06 26.26 14.79 o -8 7 1 222.79 252.59 20.64 o -7 7 1 43.00 34.40 12.26 o -6 7 1 493.72 485.39 27.82 o -5 7 1 651.85 703.74 33.12 o -4 7 1 4019.48 4210.50 125.33 o -3 7 1 1935.02 1697.45 53.56 o -2 7 1 232.64 260.02 29.92 o -1 7 1 1251.96 1228.70 35.98 o 0 7 1 6661.32 6361.56 187.12 o 1 7 1 1431.54 1426.28 47.55 o 2 7 1 319.85 294.23 21.28 o 3 7 1 11.84 27.85 13.19 o 4 7 1 1194.68 1326.34 45.80 o 5 7 1 117.91 100.41 43.09 o 6 7 1 238.12 216.65 24.55 o 7 7 1 1132.16 1216.98 47.33 o 8 7 1 2630.36 2823.72 92.56 o 9 7 1 478.47 560.73 33.20 o 10 7 1 44.24 46.53 25.76 o 11 7 1 76.37 70.61 27.71 o 12 7 1 19.51 10.12 43.00 o 13 7 1 18.63 -2.77 29.73 o -13 8 1 87.22 165.56 42.59 o -12 8 1 92.30 108.79 37.06 o -11 8 1 407.77 468.40 72.72 o -10 8 1 635.63 731.98 56.96 o -9 8 1 478.47 559.24 35.04 o -8 8 1 192.80 239.14 20.06 o -7 8 1 507.78 552.78 48.84 o -6 8 1 23.56 19.21 11.86 o -5 8 1 6259.28 6446.66 190.21 o -4 8 1 2340.64 2509.48 77.73 o -3 8 1 2645.60 2420.13 87.83 o -2 8 1 4319.43 3971.16 120.64 o -1 8 1 3477.70 3423.57 101.10 o 0 8 1 403.92 460.90 20.00 o 1 8 1 3077.69 2890.21 89.70 o 2 8 1 16.41 15.61 9.44 o 3 8 1 7418.50 7605.83 263.31 o 4 8 1 3507.81 3674.91 130.25 o 5 8 1 1178.10 1263.00 45.64 o 6 8 1 794.10 889.50 41.58 o 7 8 1 484.54 471.28 35.80 o 8 8 1 15.39 21.98 21.50 o 9 8 1 19.16 43.93 23.83 o 10 8 1 156.74 183.46 30.26 o 11 8 1 590.42 580.62 56.73 o 12 8 1 637.56 607.31 80.48 o -13 9 1 16.75 -16.13 34.49 o -12 9 1 22.35 19.99 33.01 o -11 9 1 3.06 33.73 50.18 o -10 9 1 1.92 4.00 26.93 o -9 9 1 30.00 34.08 26.13 o -8 9 1 0.15 -1.20 18.45 o -7 9 1 87.70 120.11 27.66 o -6 9 1 386.86 405.16 42.49 o -5 9 1 619.84 662.55 29.39 o -4 9 1 417.02 422.26 43.16 o -3 9 1 57.23 48.46 23.93 o -2 9 1 552.23 569.78 24.53 o -1 9 1 20.53 10.13 6.66 o 0 9 1 1178.87 1104.74 35.55 o 1 9 1 195.58 214.64 31.96 o 2 9 1 126.77 184.08 15.54 o 3 9 1 225.48 191.08 21.29 o 4 9 1 17.96 69.75 45.76 o 5 9 1 45.87 43.89 16.48 o 6 9 1 21.73 27.98 22.95 o 7 9 1 1.47 -12.72 19.64 o 8 9 1 220.02 203.77 28.58 o 9 9 1 60.86 25.38 24.24 o 10 9 1 164.69 139.11 29.46 o 11 9 1 5.05 38.37 27.64 o 12 9 1 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