#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/82/2228249.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2228249_Fobs loop_ _publ_author_name 'Batrice, Rami J.' 'Nesterov, Vladimir N.' 'Smucker, Bradley W.' _publ_section_title ; Chlorido(4,4',4''-tri-tert-butyl-2,2':6',2''-terpyridine)platinum(II) chloride toluene monosolvate ; _journal_coeditor_code BV2164 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1704 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.948 _cell_angle_gamma 90.000 _cell_length_a 9.4418 _cell_length_b 20.0002 _cell_length_c 17.2321 _exptl_crystal_F_000 1520.00 _reflns_d_resolution_high 0.8000 _[local]_cod_data_source_file bv2164Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 169p21c in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 375.68 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 124308.53 99442.31 14599.98 o 2 0 0 116714.80 119221.67 2118.69 o 3 0 0 28.87 14.38 19.29 o 4 0 0 35810.85 34905.33 617.09 o 5 0 0 74489.59 74134.21 1270.20 o 6 0 0 36464.18 35966.52 581.68 o 7 0 0 13707.52 13871.89 267.91 o 8 0 0 5871.26 5742.71 263.01 o 9 0 0 494.79 515.53 76.25 o 10 0 0 4531.35 4630.37 283.52 o 11 0 0 9606.13 10474.16 264.19 o 1 1 0 2327.65 2132.89 22.87 o 2 1 0 15085.15 15390.69 145.27 o 3 1 0 10101.10 9781.15 106.46 o 4 1 0 323.24 428.96 23.28 o 5 1 0 4493.44 3972.04 84.41 o 6 1 0 132.71 271.96 32.88 o 7 1 0 1742.06 1636.62 54.65 o 8 1 0 567.33 669.38 49.75 o 9 1 0 7859.93 7393.06 139.20 o 10 1 0 220.51 275.78 48.31 o 11 1 0 37.47 79.65 52.53 o 0 2 0 70461.48 73491.28 1281.80 o 1 2 0 36977.89 42945.64 449.04 o 2 2 0 6888.17 7031.33 85.78 o 3 2 0 5794.88 5989.35 84.25 o 4 2 0 2992.95 3050.53 68.99 o 5 2 0 27731.99 27085.61 304.10 o 6 2 0 19666.61 19153.16 243.46 o 7 2 0 1255.60 1476.02 56.35 o 8 2 0 4199.97 3832.81 103.87 o 9 2 0 846.62 802.20 54.23 o 10 2 0 7698.94 7931.65 175.14 o 11 2 0 3061.90 2811.77 106.08 o 1 3 0 40177.59 42226.66 370.32 o 2 3 0 28779.74 31173.28 321.13 o 3 3 0 57964.76 54252.22 524.17 o 4 3 0 35541.84 34951.29 323.66 o 5 3 0 199.29 153.08 21.97 o 6 3 0 338.72 350.16 23.20 o 7 3 0 9238.53 8785.94 141.16 o 8 3 0 24300.72 23240.96 300.76 o 9 3 0 11870.25 11023.21 242.52 o 10 3 0 9109.43 9191.41 163.18 o 11 3 0 251.67 196.26 50.45 o 0 4 0 18600.36 21399.55 256.70 o 1 4 0 109740.20 122067.19 1832.18 o 2 4 0 1682.10 1757.71 57.25 o 3 4 0 6444.20 5925.07 78.00 o 4 4 0 3767.30 3933.12 55.23 o 5 4 0 1067.86 1257.77 28.36 o 6 4 0 6203.85 6187.14 94.19 o 7 4 0 325.31 401.81 36.97 o 8 4 0 103.77 198.73 43.94 o 9 4 0 222.86 289.63 44.52 o 10 4 0 11.00 84.46 42.49 o 11 4 0 191.62 177.48 50.40 o 1 5 0 45932.33 49085.79 523.59 o 2 5 0 106907.09 116475.48 1054.82 o 3 5 0 50807.11 49636.59 464.38 o 4 5 0 43185.24 44097.05 539.79 o 5 5 0 7023.91 6011.31 77.83 o 6 5 0 5428.68 4952.08 82.87 o 7 5 0 8054.47 7866.26 125.90 o 8 5 0 7667.21 7434.34 133.62 o 9 5 0 15237.09 15047.15 259.05 o 10 5 0 2939.85 2981.89 89.90 o 11 5 0 4.35 74.62 53.31 o 0 6 0 72404.99 75114.84 1033.60 o 1 6 0 64201.41 69067.44 681.53 o 2 6 0 26136.80 28374.15 265.33 o 3 6 0 2135.36 2779.08 39.70 o 4 6 0 23908.48 23262.85 235.10 o 5 6 0 16319.74 16499.38 181.66 o 6 6 0 24221.51 23373.91 264.28 o 7 6 0 26697.00 25815.34 316.80 o 8 6 0 215.22 288.22 38.89 o 9 6 0 1877.43 1890.34 70.98 o 10 6 0 2895.36 2640.96 87.13 o 11 6 0 11873.13 12008.71 221.53 o 1 7 0 4935.49 5706.45 73.49 o 2 7 0 91.58 162.55 13.44 o 3 7 0 5588.72 6092.62 81.18 o 4 7 0 1372.36 1685.58 35.07 o 5 7 0 149.14 166.35 22.11 o 6 7 0 14.02 127.86 21.65 o 7 7 0 77.20 142.60 32.91 o 8 7 0 301.08 328.40 40.07 o 9 7 0 72.49 80.75 38.46 o 10 7 0 135.85 122.59 50.18 o 11 7 0 42.21 291.69 59.51 o 0 8 0 41401.94 46419.71 610.45 o 1 8 0 25079.18 22383.70 284.93 o 2 8 0 19683.61 20818.29 212.94 o 3 8 0 2827.02 3186.77 52.61 o 4 8 0 4128.79 4072.81 61.00 o 5 8 0 17310.51 16495.98 179.12 o 6 8 0 35383.24 34137.35 346.80 o 7 8 0 8093.74 7150.00 122.17 o 8 8 0 1410.84 1685.64 63.38 o 9 8 0 1964.46 1892.34 70.69 o 10 8 0 5563.41 5641.39 154.57 o 11 8 0 8284.53 8368.80 203.65 o 1 9 0 10579.51 10173.30 119.12 o 2 9 0 24151.64 25424.25 274.69 o 3 9 0 40423.07 40159.46 391.99 o 4 9 0 8300.44 7439.89 94.00 o 5 9 0 159.86 332.28 34.16 o 6 9 0 32.22 30.00 21.24 o 7 9 0 8378.86 8045.53 132.18 o 8 9 0 10534.42 9759.94 262.31 o 9 9 0 4943.48 5274.27 178.99 o 10 9 0 3611.52 3166.83 118.29 o 11 9 0 713.61 763.73 144.21 o 0 10 0 6476.89 8599.13 150.62 o 1 10 0 9962.09 8403.80 112.18 o 2 10 0 1361.36 1684.88 39.54 o 3 10 0 617.81 723.83 38.91 o 4 10 0 2392.95 2378.71 55.47 o 5 10 0 866.61 731.72 38.27 o 6 10 0 734.33 774.04 34.51 o 7 10 0 2066.07 2054.12 58.37 o 8 10 0 265.66 367.69 46.93 o 9 10 0 75.61 139.55 52.43 o 10 10 0 146.54 224.30 82.29 o 1 11 0 3744.78 4117.51 73.56 o 2 11 0 77479.66 78101.78 797.96 o 3 11 0 51981.06 54781.90 529.96 o 4 11 0 16476.59 15925.41 200.59 o 5 11 0 7258.20 7408.15 100.68 o 6 11 0 150.36 181.31 27.49 o 7 11 0 8291.07 8411.10 139.19 o 8 11 0 15138.24 14819.70 236.33 o 9 11 0 8273.66 8416.26 284.30 o 10 11 0 4457.31 4388.49 141.40 o 0 12 0 30406.09 26471.77 437.53 o 1 12 0 10983.22 12470.33 150.87 o 2 12 0 59.47 95.33 22.52 o 3 12 0 3782.05 3948.51 67.70 o 4 12 0 3512.96 3233.39 64.43 o 5 12 0 6423.77 6890.25 104.24 o 6 12 0 5351.89 4821.01 88.31 o 7 12 0 4667.55 4908.54 101.36 o 8 12 0 739.46 889.87 68.23 o 9 12 0 113.09 137.52 55.03 o 10 12 0 1341.54 1349.59 114.54 o 1 13 0 3213.67 3612.30 63.79 o 2 13 0 4620.68 4343.41 71.06 o 3 13 0 11822.46 12298.47 154.66 o 4 13 0 7069.92 6792.26 105.75 o 5 13 0 593.41 516.80 35.39 o 6 13 0 566.77 690.83 42.04 o 7 13 0 4278.79 4834.42 101.65 o 8 13 0 6065.68 5641.81 154.60 o 9 13 0 858.92 1011.39 78.44 o 10 13 0 1414.54 1579.92 98.00 o 0 14 0 34511.20 33207.99 562.42 o 1 14 0 22743.08 22826.77 255.13 o 2 14 0 9195.10 8874.09 118.55 o 3 14 0 3161.84 2987.06 61.56 o 4 14 0 3809.82 3996.02 76.45 o 5 14 0 19503.19 18660.26 230.28 o 6 14 0 16434.55 16521.52 209.28 o 7 14 0 4391.00 4535.02 112.12 o 8 14 0 2150.82 2059.23 94.97 o 9 14 0 401.04 313.39 64.03 o 1 15 0 6323.12 6246.85 132.10 o 2 15 0 568.47 726.91 33.88 o 3 15 0 2044.67 2193.27 55.00 o 4 15 0 5356.42 5382.14 95.09 o 5 15 0 397.90 364.35 36.22 o 6 15 0 100.03 107.39 34.25 o 7 15 0 220.27 200.25 46.66 o 8 15 0 1423.68 1503.83 87.13 o 9 15 0 1665.62 1518.36 93.05 o 0 16 0 18609.45 19139.73 346.82 o 1 16 0 6927.31 6638.54 124.15 o 2 16 0 2877.02 2789.91 74.69 o 3 16 0 584.21 648.55 39.97 o 4 16 0 6332.92 6385.97 105.72 o 5 16 0 4040.45 4268.96 86.03 o 6 16 0 6392.42 6281.31 134.03 o 7 16 0 3466.08 3571.19 103.18 o 8 16 0 372.33 340.35 66.69 o 9 16 0 724.63 637.86 75.75 o 1 17 0 7974.27 8491.25 194.11 o 2 17 0 15949.61 15476.55 214.62 o 3 17 0 15286.21 15718.20 219.65 o 4 17 0 16254.29 16096.92 223.31 o 5 17 0 5298.09 4933.58 96.13 o 6 17 0 2331.91 2358.40 85.04 o 7 17 0 3598.28 3447.60 104.41 o 8 17 0 5657.00 5775.35 157.60 o 0 18 0 1302.36 1622.82 81.49 o 1 18 0 313.06 267.79 34.99 o 2 18 0 3.69 16.47 30.09 o 3 18 0 0.40 5.51 31.72 o 4 18 0 1102.83 1235.04 57.42 o 5 18 0 9.66 21.62 38.72 o 6 18 0 4.98 19.15 44.84 o 7 18 0 208.67 251.73 53.04 o 8 18 0 25.81 139.18 61.23 o 1 19 0 5749.18 5470.62 107.92 o 2 19 0 6299.55 6211.14 141.67 o 3 19 0 10750.65 10552.79 168.67 o 4 19 0 12043.53 11677.91 182.93 o 5 19 0 661.48 625.75 56.22 o 6 19 0 186.81 244.29 54.79 o 7 19 0 1977.25 1995.97 97.26 o 0 20 0 10629.35 9742.60 222.75 o 1 20 0 9367.58 9014.60 152.55 o 2 20 0 1433.60 1281.71 59.77 o 3 20 0 75.70 41.48 35.99 o 4 20 0 1261.94 1474.75 71.89 o 5 20 0 7904.19 7814.31 160.44 o 6 20 0 5558.18 5754.92 196.30 o 7 20 0 2904.77 2744.32 114.91 o 1 21 0 529.11 406.07 45.79 o 2 21 0 23.44 26.13 36.16 o 3 21 0 9.15 20.67 36.85 o 4 21 0 345.96 330.78 52.76 o 5 21 0 185.51 198.33 52.69 o 6 21 0 57.01 12.51 52.44 o 0 22 0 14466.93 13974.49 305.70 o 1 22 0 5257.76 5224.70 141.14 o 2 22 0 2063.73 1876.91 74.65 o 3 22 0 29.18 29.63 43.92 o 4 22 0 2863.10 3220.58 105.33 o 5 22 0 8581.95 8593.26 179.88 o 1 23 0 321.86 376.80 48.20 o 2 23 0 7166.09 7328.68 156.69 o 3 23 0 5869.47 6067.11 158.75 o 4 23 0 1840.41 1826.50 109.12 o 0 24 0 975.02 1143.59 88.81 o 1 24 0 1020.31 1042.40 64.67 o 2 24 0 121.85 151.68 52.76 o 3 24 0 0.44 37.92 54.64 o -11 1 1 5885.16 5752.42 144.57 o -10 1 1 7867.62 7782.22 145.13 o -9 1 1 195.47 288.96 42.90 o -8 1 1 2025.12 2186.84 75.25 o -7 1 1 10800.55 10551.00 231.79 o -6 1 1 15405.19 15920.58 187.97 o -5 1 1 87346.41 86943.48 821.93 o -4 1 1 8612.81 8700.93 99.92 o -3 1 1 4822.59 4925.68 79.75 o -2 1 1 23777.26 26192.11 270.86 o -1 1 1 71615.06 73891.36 1232.01 o 0 1 1 135604.80 85181.68 2346.20 o 1 1 1 51916.51 55277.08 518.42 o 2 1 1 2846.97 3615.86 42.77 o 3 1 1 7883.92 7754.41 91.28 o 4 1 1 34074.63 33976.21 413.03 o 5 1 1 47706.73 45608.17 515.01 o 6 1 1 36981.06 35541.75 416.25 o 7 1 1 9663.59 9243.67 158.89 o 8 1 1 4798.83 5006.95 150.16 o 9 1 1 1221.11 1300.04 69.67 o 10 1 1 11305.82 11003.58 181.79 o 11 1 1 8825.17 9044.11 198.15 o -11 2 1 41.61 115.88 49.13 o -10 2 1 1374.58 1380.62 67.94 o -9 2 1 11135.21 11201.56 176.84 o -8 2 1 12238.37 11120.44 171.00 o -7 2 1 10099.61 10543.35 181.47 o -6 2 1 1214.34 1135.29 36.49 o -5 2 1 5438.39 4908.55 65.37 o -4 2 1 14656.44 12583.92 138.07 o -3 2 1 56687.81 60619.49 665.96 o -2 2 1 25384.37 24384.29 232.05 o -1 2 1 3457.54 3879.90 43.93 o 0 2 1 64.12 30.19 3.40 o 1 2 1 8813.69 9876.51 97.00 o 2 2 1 23401.63 24562.85 255.16 o 3 2 1 33403.41 33580.84 372.89 o 4 2 1 15620.89 14310.13 160.65 o 5 2 1 9423.86 9751.46 159.89 o 6 2 1 305.19 340.69 31.06 o 7 2 1 8074.78 7177.57 134.24 o 8 2 1 20247.74 19168.90 254.40 o 9 2 1 17215.26 15953.80 326.49 o 10 2 1 4010.64 3949.89 102.40 o 11 2 1 37.70 36.59 46.11 o -11 3 1 300.41 209.65 50.15 o -10 3 1 1641.01 1495.46 70.67 o -9 3 1 20.13 71.54 39.09 o -8 3 1 485.90 580.01 45.49 o -7 3 1 1974.26 1923.36 58.78 o -6 3 1 204.63 187.18 23.24 o -5 3 1 9740.64 9813.43 124.07 o -4 3 1 31.75 104.79 22.04 o -3 3 1 3447.13 3739.24 53.72 o -2 3 1 19.78 163.96 14.97 o -1 3 1 2587.80 3260.40 39.27 o 0 3 1 754.69 1114.25 18.85 o 1 3 1 28847.10 28225.88 260.59 o 2 3 1 208.16 430.17 14.32 o 3 3 1 5108.46 5084.21 63.59 o 4 3 1 803.95 875.82 27.12 o 5 3 1 3565.81 3045.21 58.00 o 6 3 1 802.90 711.24 33.67 o 7 3 1 60.28 50.40 27.80 o 8 3 1 825.53 883.18 57.92 o 9 3 1 342.75 548.50 50.42 o 10 3 1 1334.15 1243.25 92.80 o 11 3 1 336.85 296.75 53.45 o -11 4 1 565.04 654.12 65.71 o -10 4 1 6854.53 6205.02 128.69 o -9 4 1 13483.01 14304.34 211.93 o -8 4 1 15232.31 13572.95 208.67 o -7 4 1 9907.62 9884.79 151.52 o -6 4 1 2859.18 2751.30 50.33 o -5 4 1 2234.07 2035.99 41.10 o -4 4 1 64520.89 64290.07 608.88 o -3 4 1 43079.84 44227.62 414.63 o -2 4 1 104504.71 107854.72 1010.50 o -1 4 1 102890.47 116598.85 1089.17 o 0 4 1 9545.64 9058.38 91.99 o 1 4 1 17629.48 18502.98 184.70 o 2 4 1 46475.80 45216.11 416.88 o 3 4 1 26972.75 28232.59 279.37 o 4 4 1 50377.48 47824.02 463.78 o 5 4 1 5087.76 5443.58 69.19 o 6 4 1 619.32 670.40 38.42 o 7 4 1 9215.81 8076.99 161.90 o 8 4 1 19864.84 18969.90 257.20 o 9 4 1 12698.22 12339.97 207.75 o 10 4 1 5718.58 5544.35 118.56 o 11 4 1 47.46 41.88 45.96 o -11 5 1 4430.73 4644.82 129.64 o -10 5 1 408.86 449.08 51.69 o -9 5 1 268.57 143.69 40.71 o -8 5 1 307.66 294.72 44.40 o -7 5 1 10061.23 10217.01 150.94 o -6 5 1 18921.15 19170.15 209.79 o -5 5 1 9232.06 8978.36 111.49 o -4 5 1 13469.75 13442.12 139.89 o -3 5 1 2062.45 1622.18 35.69 o -2 5 1 55187.61 57434.55 531.47 o -1 5 1 103616.98 115584.07 1088.10 o 0 5 1 14980.48 16105.14 168.99 o 1 5 1 32094.57 33525.79 308.45 o 2 5 1 4550.46 5021.48 60.49 o 3 5 1 5248.99 5979.93 68.30 o 4 5 1 10078.14 10442.63 128.40 o 5 5 1 7786.71 7680.09 95.09 o 6 5 1 13893.82 13164.65 158.27 o 7 5 1 8272.22 7822.18 145.39 o 8 5 1 174.10 272.44 41.48 o 9 5 1 1271.12 1393.75 64.26 o 10 5 1 1955.58 2158.41 135.81 o 11 5 1 5970.97 6007.09 132.84 o -11 6 1 213.86 255.53 62.19 o -10 6 1 1335.90 1286.48 74.73 o -9 6 1 5391.24 5497.96 113.63 o -8 6 1 2017.26 1875.19 66.81 o -7 6 1 2229.33 2368.59 98.51 o -6 6 1 1455.00 1410.34 37.36 o -5 6 1 1304.05 1393.60 43.59 o -4 6 1 5866.16 5733.56 74.87 o -3 6 1 28519.19 30124.47 303.16 o -2 6 1 30033.45 31273.10 295.29 o -1 6 1 49744.49 54261.66 539.01 o 0 6 1 7923.04 8677.21 96.58 o 1 6 1 7905.47 8623.52 91.38 o 2 6 1 7299.44 7811.66 91.70 o 3 6 1 19570.68 20693.33 210.64 o 4 6 1 8589.84 7823.58 91.02 o 5 6 1 1636.04 1678.85 39.56 o 6 6 1 1855.96 2153.87 52.21 o 7 6 1 758.70 784.73 44.66 o 8 6 1 1942.60 2108.04 65.81 o 9 6 1 3577.35 3336.36 89.98 o 10 6 1 287.26 420.00 51.96 o 11 6 1 17.98 185.89 52.45 o -11 7 1 8685.31 8753.05 225.90 o -10 7 1 4992.41 4650.02 140.67 o -9 7 1 1549.60 1512.40 65.63 o -8 7 1 997.80 966.47 51.71 o -7 7 1 20698.96 19766.84 264.10 o -6 7 1 28015.03 26394.13 270.40 o -5 7 1 29160.01 28850.32 291.24 o -4 7 1 17512.95 17415.50 189.75 o -3 7 1 3501.96 3513.97 49.62 o -2 7 1 36765.72 34957.27 344.92 o -1 7 1 57202.90 60225.80 593.81 o 0 7 1 48855.72 49014.41 493.65 o 1 7 1 32967.46 34913.06 347.22 o 2 7 1 16485.13 16257.42 163.30 o 3 7 1 3268.24 3083.03 53.05 o 4 7 1 26034.78 26434.08 258.90 o 5 7 1 20051.33 19400.60 204.83 o 6 7 1 39600.09 37783.03 413.08 o 7 7 1 16942.03 16420.78 217.87 o 8 7 1 206.42 167.22 41.14 o 9 7 1 1668.79 1590.58 65.55 o 10 7 1 7108.79 7252.04 142.05 o 11 7 1 9541.47 9683.95 237.83 o -11 8 1 848.89 932.47 85.68 o -10 8 1 1858.33 2157.42 89.20 o -9 8 1 872.46 682.40 57.19 o -8 8 1 1541.13 1675.51 63.65 o -7 8 1 2345.04 2214.78 73.35 o -6 8 1 107.40 167.88 24.31 o -5 8 1 1886.75 1654.41 38.54 o -4 8 1 1478.85 1964.89 40.34 o -3 8 1 17872.23 17242.66 185.75 o -2 8 1 12317.66 12613.09 129.19 o -1 8 1 9708.57 12310.73 148.00 o 0 8 1 1429.04 1433.70 34.16 o 1 8 1 2065.92 1816.79 35.16 o 2 8 1 4668.34 4018.34 57.85 o 3 8 1 3729.78 3793.24 52.45 o 4 8 1 1134.83 1155.00 30.79 o 5 8 1 1486.59 1424.37 38.84 o 6 8 1 5.32 189.47 25.95 o 7 8 1 775.60 813.59 46.14 o 8 8 1 2661.96 2582.09 73.53 o 9 8 1 778.38 820.19 53.43 o 10 8 1 375.96 564.97 56.50 o 11 8 1 122.73 222.83 68.26 o -11 9 1 5691.82 5333.73 160.69 o -10 9 1 1555.80 1545.14 89.35 o -9 9 1 440.26 579.10 57.59 o -8 9 1 21.37 100.09 36.66 o -7 9 1 4804.82 4666.58 84.34 o -6 9 1 11211.65 9953.08 127.54 o -5 9 1 7931.80 8588.82 109.05 o -4 9 1 8439.67 8065.75 96.21 o -3 9 1 3855.70 4661.25 65.59 o -2 9 1 355.46 279.74 23.40 o -1 9 1 2822.92 2975.97 51.56 o 0 9 1 13662.56 11743.08 133.96 o 1 9 1 19447.20 22497.95 232.57 o 2 9 1 6145.21 4875.59 64.97 o 3 9 1 1153.57 1665.19 37.12 o 4 9 1 5762.63 5449.05 78.06 o 5 9 1 8157.27 7713.92 104.59 o 6 9 1 16344.27 15551.00 186.24 o 7 9 1 5360.58 5309.94 102.64 o 8 9 1 486.63 537.78 52.55 o 9 9 1 891.27 747.89 54.79 o 10 9 1 972.12 944.48 82.06 o -10 10 1 4636.41 4747.96 146.04 o -9 10 1 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