#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/82/2228250.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2228250_Fobs loop_ _publ_author_name 'Loughrey, Bradley T.' 'Williams, Michael L.' 'Healy, Peter C.' _publ_section_title ; (\h^5^-Pentamethylcyclopentadienyl)(\h^6^-4-phenylbutan-2-one)ruthenium(II) tetraphenylborate ; _journal_coeditor_code BV2166 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1564 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.378 _cell_angle_gamma 90.000 _cell_length_a 13.1659 _cell_length_b 19.7064 _cell_length_c 14.3720 _exptl_crystal_F_000 1472.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file bv2166Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' xcalibur' _shelx_refln_list_code 4 _shelx_f_calc_maximum 280.50 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2203.77 2386.13 16.04 o 4 0 0 1814.41 1827.75 23.68 o 6 0 0 498.56 383.11 18.05 o 8 0 0 11878.43 11679.42 70.99 o 10 0 0 983.56 971.56 31.23 o 12 0 0 897.16 872.31 36.55 o 14 0 0 307.34 347.95 33.80 o 16 0 0 459.37 435.02 36.33 o 2 1 0 53012.41 49606.52 285.59 o 3 1 0 5301.15 5399.86 87.63 o 4 1 0 7172.28 6800.07 36.45 o 5 1 0 2467.53 2559.16 34.51 o 6 1 0 4135.90 4038.77 26.91 o 7 1 0 460.40 405.94 14.89 o 8 1 0 266.98 290.66 15.40 o 9 1 0 2252.54 2220.67 33.02 o 10 1 0 544.07 518.56 20.37 o 11 1 0 368.21 403.89 20.94 o 12 1 0 522.53 512.22 22.50 o 13 1 0 772.18 777.76 26.18 o 14 1 0 2432.85 2307.77 38.93 o 15 1 0 104.49 93.02 23.56 o 16 1 0 816.86 817.69 30.86 o 17 1 0 211.39 215.58 27.65 o 2 2 0 6494.81 7157.52 50.77 o 3 2 0 925.80 924.55 8.65 o 4 2 0 739.60 707.78 15.78 o 5 2 0 18386.39 17658.50 374.98 o 6 2 0 1627.64 1763.06 19.19 o 7 2 0 4741.68 4616.16 30.71 o 8 2 0 81.90 103.61 15.07 o 9 2 0 2.12 6.01 15.04 o 10 2 0 55.46 57.51 16.72 o 11 2 0 1345.15 1421.99 27.22 o 12 2 0 130.95 121.29 20.49 o 13 2 0 7061.95 6674.45 166.42 o 14 2 0 166.20 190.22 29.11 o 15 2 0 2091.60 1997.90 52.49 o 16 2 0 16.14 4.03 22.51 o 17 2 0 597.04 592.06 29.97 o 1 3 0 64476.60 57359.54 2430.58 o 2 3 0 12964.74 14070.72 100.41 o 3 3 0 4006.90 3986.29 15.54 o 4 3 0 16339.39 16269.13 173.91 o 5 3 0 17.47 23.04 8.54 o 6 3 0 1767.60 1801.41 38.22 o 7 3 0 9076.17 9441.89 42.00 o 8 3 0 405.66 390.35 16.57 o 9 3 0 7970.36 7608.66 44.06 o 10 3 0 0.95 -3.57 16.10 o 11 3 0 2850.21 2794.23 33.94 o 12 3 0 1095.54 1120.68 27.13 o 13 3 0 1335.79 1304.52 28.88 o 14 3 0 628.67 550.51 25.43 o 15 3 0 63.63 58.17 23.09 o 16 3 0 116.93 125.32 25.30 o 0 4 0 19602.99 20264.57 507.76 o 1 4 0 477.78 542.76 5.37 o 2 4 0 31589.13 31821.90 179.40 o 3 4 0 1094.62 1137.77 12.41 o 4 4 0 182.60 197.44 6.88 o 5 4 0 3946.77 3761.60 42.37 o 6 4 0 2060.11 1996.06 29.73 o 7 4 0 385.43 322.70 14.27 o 8 4 0 4898.83 4851.44 42.93 o 9 4 0 14.28 21.64 14.38 o 10 4 0 1561.75 1494.52 25.40 o 11 4 0 295.48 251.40 20.12 o 12 4 0 1181.47 1125.66 28.36 o 13 4 0 727.10 714.28 25.04 o 14 4 0 2.55 -1.00 20.88 o 15 4 0 1090.85 988.86 30.30 o 16 4 0 224.70 215.44 25.26 o 1 5 0 13633.40 14004.72 95.42 o 2 5 0 5987.57 6429.66 82.63 o 3 5 0 5377.99 5922.18 19.03 o 4 5 0 6942.59 7070.54 98.47 o 5 5 0 401.14 481.91 7.81 o 6 5 0 15021.68 14862.32 204.38 o 7 5 0 98.74 79.48 11.77 o 8 5 0 2863.97 2721.45 30.02 o 9 5 0 512.01 516.90 18.10 o 10 5 0 361.04 337.07 18.24 o 11 5 0 504.57 528.77 42.78 o 12 5 0 1194.83 1190.47 26.24 o 13 5 0 6.56 14.45 18.87 o 14 5 0 2225.90 2131.88 35.55 o 15 5 0 1.30 12.45 21.93 o 16 5 0 648.49 587.51 43.57 o 0 6 0 15008.84 15871.15 106.18 o 1 6 0 90.80 79.64 8.24 o 2 6 0 14207.94 14333.00 127.10 o 3 6 0 1622.95 1523.67 14.77 o 4 6 0 4818.40 5213.88 26.96 o 5 6 0 5238.89 4859.65 19.01 o 6 6 0 206.05 183.65 8.43 o 7 6 0 5302.53 5367.08 81.20 o 8 6 0 6507.23 6451.26 37.03 o 9 6 0 453.88 453.97 22.58 o 10 6 0 979.83 971.33 21.70 o 11 6 0 205.83 195.66 18.96 o 12 6 0 1016.65 1035.30 25.58 o 13 6 0 702.87 703.48 24.05 o 14 6 0 0.05 1.62 20.01 o 15 6 0 531.68 500.92 42.80 o 16 6 0 411.25 423.13 41.20 o 1 7 0 8269.37 7874.77 101.82 o 2 7 0 3483.78 3675.48 41.96 o 3 7 0 6119.09 6475.99 40.94 o 4 7 0 1.01 10.10 4.00 o 5 7 0 71.42 120.84 5.75 o 6 7 0 1528.82 1733.52 21.30 o 7 7 0 3895.64 3795.62 26.18 o 8 7 0 0.26 14.03 13.65 o 9 7 0 1891.49 1815.70 39.37 o 10 7 0 7.12 10.73 15.89 o 11 7 0 3160.87 3089.68 51.36 o 12 7 0 264.82 231.50 19.67 o 13 7 0 121.97 122.09 18.60 o 14 7 0 16.61 40.31 32.91 o 15 7 0 62.79 77.12 38.66 o 16 7 0 27.48 6.66 37.93 o 0 8 0 3569.02 3258.19 23.76 o 1 8 0 1630.78 1653.84 9.32 o 2 8 0 334.87 276.19 7.91 o 3 8 0 4768.63 4532.58 23.21 o 4 8 0 19.57 2.67 6.53 o 5 8 0 4791.09 4307.21 38.30 o 6 8 0 203.51 253.56 9.17 o 7 8 0 6915.64 6919.96 121.07 o 8 8 0 1792.40 1718.29 29.63 o 9 8 0 108.29 120.69 14.07 o 10 8 0 9.42 -1.85 15.45 o 11 8 0 5.60 8.74 16.47 o 12 8 0 445.31 403.10 36.26 o 13 8 0 1983.37 2006.66 53.70 o 14 8 0 162.99 165.83 32.08 o 15 8 0 1596.31 1696.19 56.11 o 16 8 0 177.66 200.88 43.58 o 1 9 0 5696.91 5758.68 31.51 o 2 9 0 5244.48 5261.00 21.87 o 3 9 0 1942.56 2094.47 37.43 o 4 9 0 3517.32 3247.85 18.54 o 5 9 0 98.73 99.99 3.97 o 6 9 0 2490.06 2108.72 31.55 o 7 9 0 1090.21 1006.09 18.65 o 8 9 0 598.27 638.10 14.93 o 9 9 0 357.85 391.92 15.17 o 10 9 0 0.67 5.59 14.20 o 11 9 0 1368.54 1374.96 44.64 o 12 9 0 635.67 659.73 39.84 o 13 9 0 0.62 -13.62 33.70 o 14 9 0 1080.25 1186.99 49.35 o 15 9 0 74.16 73.17 33.94 o 16 9 0 1315.71 1518.89 58.18 o 0 10 0 5870.33 5267.97 15.79 o 1 10 0 1317.04 1526.71 12.10 o 2 10 0 18989.93 18587.53 160.10 o 3 10 0 117.02 115.30 8.50 o 4 10 0 1108.85 1153.16 13.94 o 5 10 0 3.39 8.21 7.95 o 6 10 0 2453.59 2422.99 17.66 o 7 10 0 300.26 323.42 8.42 o 8 10 0 345.28 341.82 19.30 o 9 10 0 1198.95 1157.54 38.93 o 10 10 0 2582.35 2544.00 49.90 o 11 10 0 5.51 -13.27 31.64 o 12 10 0 603.24 624.94 39.98 o 13 10 0 22.92 26.15 33.43 o 14 10 0 12.45 30.15 35.64 o 15 10 0 215.51 204.25 42.06 o 1 11 0 9731.75 9590.21 50.87 o 2 11 0 1940.12 1851.52 14.56 o 3 11 0 1448.92 1410.03 13.59 o 4 11 0 6263.78 6344.17 71.28 o 5 11 0 0.41 -6.23 8.24 o 6 11 0 2404.37 2341.08 19.71 o 7 11 0 180.58 157.94 13.04 o 8 11 0 213.41 231.58 22.20 o 9 11 0 4274.20 4275.41 61.09 o 10 11 0 63.47 50.37 30.38 o 11 11 0 337.24 336.66 32.39 o 12 11 0 352.24 336.91 37.95 o 13 11 0 45.66 40.54 34.23 o 14 11 0 853.98 944.95 48.21 o 15 11 0 99.27 122.93 39.04 o 0 12 0 686.19 577.35 7.32 o 1 12 0 1878.79 1742.49 17.96 o 2 12 0 125.88 181.02 7.42 o 3 12 0 9137.53 9019.72 51.40 o 4 12 0 394.90 468.37 11.61 o 5 12 0 3034.32 2861.37 18.20 o 6 12 0 54.82 68.19 9.43 o 7 12 0 1695.36 1633.15 41.27 o 8 12 0 68.29 78.10 13.93 o 9 12 0 229.44 234.64 36.77 o 10 12 0 6.44 -23.95 31.42 o 11 12 0 1476.48 1487.96 46.81 o 12 12 0 7.87 32.62 29.69 o 13 12 0 1381.52 1458.97 51.88 o 14 12 0 46.56 62.11 37.03 o 15 12 0 1481.05 1562.46 57.92 o 1 13 0 5847.49 5671.94 48.01 o 2 13 0 3645.14 3610.84 25.20 o 3 13 0 3441.83 3332.95 19.62 o 4 13 0 445.73 440.23 11.70 o 5 13 0 938.61 945.32 14.95 o 6 13 0 519.89 471.85 14.88 o 7 13 0 1479.35 1531.37 20.54 o 8 13 0 82.21 93.23 13.71 o 9 13 0 1574.31 1614.53 31.83 o 10 13 0 182.44 217.23 34.03 o 11 13 0 669.93 665.38 40.24 o 12 13 0 299.54 300.18 36.11 o 13 13 0 175.33 153.22 33.22 o 14 13 0 1006.54 1062.20 53.08 o 0 14 0 14468.37 14580.68 131.99 o 1 14 0 11.39 22.19 3.39 o 2 14 0 5560.07 5456.39 32.31 o 3 14 0 606.93 612.77 13.48 o 4 14 0 694.75 657.40 12.83 o 5 14 0 1623.19 1636.79 15.43 o 6 14 0 178.36 189.06 13.23 o 7 14 0 404.85 391.43 15.84 o 8 14 0 2425.89 2468.64 41.61 o 9 14 0 252.41 213.80 30.98 o 10 14 0 2699.08 2743.34 56.81 o 11 14 0 130.99 133.96 34.57 o 12 14 0 524.97 526.45 40.62 o 13 14 0 140.22 127.23 34.95 o 14 14 0 195.31 210.41 40.27 o 1 15 0 453.52 473.01 10.22 o 2 15 0 492.36 465.19 13.18 o 3 15 0 163.72 190.33 14.67 o 4 15 0 5838.59 5588.56 40.37 o 5 15 0 176.76 177.51 13.04 o 6 15 0 2926.05 2791.60 24.97 o 7 15 0 416.09 396.81 16.10 o 8 15 0 3167.44 2970.44 67.59 o 9 15 0 693.46 736.70 28.02 o 10 15 0 0.11 15.36 23.21 o 11 15 0 111.67 102.29 34.54 o 12 15 0 1090.87 1262.72 49.74 o 13 15 0 3.54 34.09 36.98 o 0 16 0 619.58 605.77 21.99 o 1 16 0 2685.15 2641.87 23.69 o 2 16 0 1981.39 1885.68 20.04 o 3 16 0 684.70 688.92 15.76 o 4 16 0 785.13 717.45 21.46 o 5 16 0 2336.33 2275.31 30.82 o 6 16 0 46.43 35.72 12.85 o 7 16 0 2151.13 2099.42 44.52 o 8 16 0 2.94 12.11 23.93 o 9 16 0 0.19 0.93 21.23 o 10 16 0 692.59 708.48 29.55 o 11 16 0 396.86 385.87 39.18 o 12 16 0 225.71 180.15 39.08 o 13 16 0 947.52 1033.09 51.02 o 1 17 0 3465.18 3330.41 24.93 o 2 17 0 1196.31 1195.93 17.21 o 3 17 0 902.48 879.76 17.00 o 4 17 0 12.46 25.65 16.67 o 5 17 0 31.30 33.30 18.10 o 6 17 0 184.90 161.89 21.28 o 7 17 0 2690.76 2754.76 80.39 o 8 17 0 485.02 458.16 26.13 o 9 17 0 3026.67 3060.86 58.54 o 10 17 0 200.58 195.02 24.62 o 11 17 0 580.41 546.85 39.60 o 12 17 0 306.80 315.13 40.68 o 0 18 0 3253.38 3143.33 40.54 o 1 18 0 309.60 327.84 14.12 o 2 18 0 598.14 607.68 24.47 o 3 18 0 726.51 713.28 16.55 o 4 18 0 15.01 17.08 13.25 o 5 18 0 1951.99 1939.87 30.99 o 6 18 0 1695.16 1726.32 31.96 o 7 18 0 2736.90 2634.48 38.30 o 8 18 0 1973.31 1979.37 35.82 o 9 18 0 153.96 154.57 25.55 o 10 18 0 21.73 29.44 24.30 o 11 18 0 1215.52 1197.89 45.95 o 12 18 0 107.57 119.33 36.51 o 1 19 0 67.86 84.22 16.05 o 2 19 0 782.14 760.52 23.01 o 3 19 0 8.42 7.15 17.62 o 4 19 0 3130.08 3164.76 42.46 o 5 19 0 220.94 210.85 16.26 o 6 19 0 2527.67 2512.91 50.15 o 7 19 0 0.09 -0.82 20.77 o 8 19 0 59.21 49.31 23.11 o 9 19 0 351.51 316.96 26.63 o 10 19 0 45.79 54.64 25.69 o 11 19 0 64.50 71.75 36.31 o 0 20 0 1993.43 1879.61 51.79 o 1 20 0 1.05 13.99 17.88 o 2 20 0 3057.36 2948.25 35.03 o 3 20 0 437.99 453.59 22.92 o 4 20 0 71.47 59.63 19.43 o 5 20 0 59.25 69.27 20.89 o 6 20 0 389.03 352.82 22.84 o 7 20 0 29.69 26.33 22.14 o 8 20 0 730.59 727.85 42.87 o 9 20 0 57.78 59.77 24.97 o 10 20 0 508.85 521.52 31.13 o 1 21 0 2104.84 1966.59 54.07 o 2 21 0 196.50 212.04 20.49 o 3 21 0 723.05 691.35 23.88 o 4 21 0 762.38 783.78 26.33 o 5 21 0 48.31 62.76 21.76 o 6 21 0 1409.57 1322.36 31.66 o 7 21 0 447.14 430.31 46.44 o 8 21 0 251.99 214.95 25.75 o 9 21 0 89.28 78.62 25.52 o 0 22 0 239.45 228.30 39.81 o 1 22 0 1.09 -12.03 38.02 o 2 22 0 7.51 9.33 38.91 o 3 22 0 1223.00 1253.26 50.12 o 4 22 0 0.09 5.37 19.92 o 5 22 0 2047.31 1977.26 56.54 o 6 22 0 110.39 94.62 26.03 o 7 22 0 424.73 418.84 29.16 o 8 22 0 8.55 -5.86 43.30 o 1 23 0 989.56 971.76 54.78 o 2 23 0 290.81 282.84 42.98 o 3 23 0 155.91 171.40 41.12 o 4 23 0 90.93 143.22 41.14 o 5 23 0 34.46 62.01 42.96 o 6 23 0 138.82 144.48 25.42 o 7 23 0 162.05 184.11 26.83 o 0 24 0 1418.72 1356.35 50.39 o 1 24 0 40.02 30.33 30.21 o 2 24 0 878.48 862.95 48.87 o 3 24 0 444.21 448.91 40.95 o 4 24 0 3.00 18.90 36.95 o 5 24 0 171.97 149.77 42.27 o 1 25 0 198.62 220.37 44.10 o 2 25 0 373.46 384.43 30.98 o 3 25 0 10.51 47.24 41.25 o -17 0 1 148.47 142.86 36.52 o -15 0 1 2360.08 2168.81 51.81 o -13 0 1 3994.59 3747.85 59.27 o -11 0 1 2426.40 2288.78 43.23 o -9 0 1 111.35 75.02 23.20 o -7 0 1 4262.94 3932.02 40.28 o -5 0 1 16426.27 16044.86 249.31 o -3 0 1 13939.88 13351.61 176.91 o 3 0 1 20533.14 20122.68 231.29 o 5 0 1 49212.95 48531.77 459.28 o 7 0 1 4821.42 4988.88 46.14 o 9 0 1 296.97 268.26 23.67 o 11 0 1 148.88 138.37 27.99 o 13 0 1 4449.79 4202.33 61.18 o 15 0 1 2910.63 2635.43 57.86 o 17 0 1 27.88 25.32 35.53 o -17 1 1 357.55 297.21 27.03 o -16 1 1 228.41 235.98 24.83 o -15 1 1 448.43 423.68 25.90 o -14 1 1 2597.56 2439.54 37.98 o -13 1 1 244.52 241.78 22.48 o -12 1 1 798.47 760.58 24.80 o -11 1 1 366.11 295.55 19.88 o -10 1 1 92.34 72.75 16.69 o -9 1 1 5431.87 4938.06 37.13 o -8 1 1 1506.24 1588.38 22.57 o -7 1 1 3535.49 3504.44 37.47 o -6 1 1 6361.46 6426.87 37.51 o -5 1 1 9715.43 10182.96 139.75 o -4 1 1 7134.53 7130.87 104.39 o -3 1 1 17163.38 17223.93 253.69 o -2 1 1 19152.94 19368.38 543.36 o 2 1 1 8365.54 8898.38 74.04 o 3 1 1 9228.36 9688.43 91.99 o 4 1 1 3556.34 3464.99 21.79 o 5 1 1 1004.28 980.19 19.18 o 6 1 1 15053.07 16125.04 265.17 o 7 1 1 12616.56 13472.44 68.92 o 8 1 1 1039.17 1045.66 19.79 o 9 1 1 6129.75 6083.88 41.39 o 10 1 1 395.69 414.66 18.81 o 11 1 1 3642.98 3530.78 36.72 o 12 1 1 1003.65 906.01 26.65 o 13 1 1 2519.34 2520.66 36.96 o 14 1 1 1272.02 1285.12 31.42 o 15 1 1 80.37 82.13 21.75 o 16 1 1 421.90 367.92 25.76 o 17 1 1 178.92 133.40 25.89 o -17 2 1 2.57 5.05 22.80 o -16 2 1 279.28 236.01 25.75 o -15 2 1 34.75 30.40 23.31 o -14 2 1 43.71 44.65 20.54 o -13 2 1 156.04 94.24 23.08 o -12 2 1 2596.31 2650.49 63.79 o -11 2 1 1347.21 1261.53 25.91 o -10 2 1 4623.49 4420.55 70.76 o -9 2 1 294.19 297.65 17.21 o -8 2 1 4164.60 3766.71 36.00 o -7 2 1 45.13 38.30 14.48 o -6 2 1 8059.34 8311.42 65.30 o -5 2 1 7245.75 7848.72 39.68 o -4 2 1 540.17 533.04 11.61 o -3 2 1 85.24 71.18 7.24 o -2 2 1 5432.54 5726.60 120.97 o 2 2 1 38954.35 38828.05 351.05 o 3 2 1 3058.07 3280.37 14.86 o 4 2 1 3288.70 3490.67 49.47 o 5 2 1 688.77 749.49 21.06 o 6 2 1 2176.48 2165.27 17.99 o 7 2 1 3341.78 3555.82 23.32 o 8 2 1 9987.00 9729.37 128.77 o 9 2 1 1.43 25.12 16.55 o 10 2 1 6505.43 6467.79 44.44 o 11 2 1 86.83 87.13 17.68 o 12 2 1 1444.69 1399.76 50.87 o 13 2 1 274.99 276.92 24.25 o 14 2 1 48.07 65.26 23.12 o 15 2 1 204.40 184.28 24.25 o 16 2 1 413.64 378.37 26.84 o -16 3 1 42.93 15.35 22.42 o -15 3 1 3.69 2.13 22.34 o -14 3 1 3049.31 2861.34 50.95 o -13 3 1 51.72 37.38 20.32 o -12 3 1 2108.57 1951.28 31.83 o -11 3 1 1078.94 1122.78 25.25 o -10 3 1 3.23 2.38 15.42 o -9 3 1 110.20 106.36 16.15 o -8 3 1 4335.82 4168.05 31.68 o -7 3 1 512.30 441.97 14.67 o -6 3 1 11358.23 11747.23 163.75 o -5 3 1 1241.91 1402.92 16.09 o -4 3 1 18492.78 17465.31 160.11 o -3 3 1 93.20 90.71 7.38 o -2 3 1 7109.83 7354.87 113.97 o -1 3 1 16442.21 16215.63 156.86 o 0 3 1 2461.66 2660.97 11.20 o 1 3 1 1356.99 1418.61 14.09 o 2 3 1 3352.86 3432.26 15.42 o 3 3 1 1712.59 1811.64 14.37 o 4 3 1 5852.22 5755.52 30.19 o 5 3 1 53.32 62.07 10.50 o 6 3 1 9968.88 10292.12 72.10 o 7 3 1 130.90 143.12 15.23 o 8 3 1 2776.83 2818.40 34.90 o 9 3 1 2419.70 2370.36 28.45 o 10 3 1 109.60 132.90 17.91 o 11 3 1 24.51 24.61 18.09 o 12 3 1 500.68 441.70 22.23 o 13 3 1 408.10 370.51 22.99 o 14 3 1 2457.99 2271.69 47.96 o 15 3 1 0.37 19.36 22.34 o 16 3 1 489.30 412.48 26.89 o -16 4 1 439.12 422.92 27.45 o -15 4 1 820.67 746.19 27.07 o -14 4 1 51.88 30.03 22.11 o -13 4 1 2353.23 2239.24 33.65 o -12 4 1 1846.48 1668.13 37.40 o -11 4 1 979.19 940.13 23.52 o -10 4 1 1548.23 1555.94 25.45 o -9 4 1 185.66 219.76 16.59 o -8 4 1 4537.49 4723.71 37.13 o -7 4 1 7003.41 6878.70 35.95 o -6 4 1 424.46 456.55 13.42 o -5 4 1 14895.37 14369.71 161.48 o -4 4 1 447.20 544.58 21.84 o -3 4 1 7552.18 7772.87 88.06 o -2 4 1 301.93 328.17 8.17 o -1 4 1 14839.33 15482.20 163.52 o 0 4 1 5236.52 5765.26 50.95 o 1 4 1 15537.41 16101.45 116.90 o 2 4 1 5951.98 6263.41 30.92 o 3 4 1 32274.60 33550.37 325.61 o 4 4 1 439.23 521.07 18.74 o 5 4 1 8673.32 8551.49 59.69 o 6 4 1 1446.60 1663.56 15.92 o 7 4 1 11414.33 12007.08 76.46 o 8 4 1 2684.04 2739.29 25.08 o 9 4 1 513.61 550.23 25.86 o 10 4 1 1450.79 1397.61 28.06 o 11 4 1 917.61 920.11 24.15 o 12 4 1 2174.51 2040.46 31.62 o 13 4 1 718.64 700.30 26.81 o 14 4 1 318.42 339.24 22.90 o 15 4 1 1542.88 1554.07 33.09 o 16 4 1 413.14 424.80 34.92 o -16 5 1 73.71 70.26 39.49 o -15 5 1 125.83 141.96 22.30 o -14 5 1 4.13 4.91 20.57 o -13 5 1 230.60 249.85 20.84 o -12 5 1 98.47 83.26 19.59 o -11 5 1 4111.23 3989.78 45.27 o -10 5 1 605.78 582.07 19.78 o -9 5 1 4234.76 3985.32 72.45 o -8 5 1 238.04 275.57 15.41 o -7 5 1 12965.58 12906.72 72.62 o -6 5 1 568.41 723.25 14.21 o -5 5 1 48.72 35.06 7.75 o -4 5 1 204.29 237.34 7.70 o -3 5 1 397.01 589.47 9.82 o -2 5 1 786.67 939.77 17.95 o -1 5 1 4564.30 4595.09 55.83 o 0 5 1 4144.13 4446.65 43.29 o 1 5 1 20920.87 20919.63 141.38 o 2 5 1 1062.01 1030.95 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