#------------------------------------------------------------------------------ #$Date: 2011-03-09 10:38:09 +0200 (Wed, 09 Mar 2011) $ #$Revision: 14261 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2229066.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2229066_Fobs loop_ _publ_author_name 'Akkurt, Mehmet' 'Jarrahpour, Aliasghar' 'Sharghi, Hashem' 'Badrabady, Seid Ali Torabi' 'B\"uy\"ukg\"ung\"or, Orhan' _publ_section_title ; (3R*,4R*)-1-(4-Chlorophenyl)-4-[2-hydroxy-3-(morpholinomethyl)phenyl]-3-phenoxyazetidin-2-one ; _journal_coeditor_code HB5782 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o325 _journal_volume 67 _journal_year 2011 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 123.043 _cell_angle_gamma 90.000 _cell_length_a 29.6418 _cell_length_b 6.7166 _cell_length_c 28.5708 _exptl_crystal_F_000 1952.00 _reflns_d_resolution_high 0.8044 _[local]_cod_data_source_file hb5782Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' TB-35' _shelx_refln_list_code 4 _shelx_f_calc_maximum 614.96 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 32.95 94.60 326.54 o 4 0 0 25121.24 24598.70 405.58 o 6 0 0 378176.44 340969.63 8056.71 o 8 0 0 178080.05 168427.63 5445.04 o 10 0 0 9274.05 8897.33 226.88 o 12 0 0 13303.63 12861.21 192.79 o 14 0 0 932.69 656.59 326.94 o 16 0 0 3003.46 2905.12 180.99 o 18 0 0 148.70 173.76 144.09 o 20 0 0 641.49 252.17 195.15 o 22 0 0 153.48 556.61 397.07 o 24 0 0 39.36 208.13 120.52 o 26 0 0 227.04 436.93 119.33 o 28 0 0 95.78 139.12 239.71 o 30 0 0 0.01 -265.98 163.78 o 1 1 0 9778.59 9135.88 844.78 o 3 1 0 725.61 774.20 185.16 o 5 1 0 2666.14 3259.36 180.16 o 7 1 0 416.09 404.04 180.68 o 9 1 0 3797.49 3699.62 164.06 o 11 1 0 177.08 169.53 135.74 o 13 1 0 777.74 737.60 110.06 o 15 1 0 484.04 457.46 131.51 o 17 1 0 455.47 496.46 142.33 o 19 1 0 748.58 966.16 112.78 o 21 1 0 10.99 -31.91 107.19 o 23 1 0 102.51 228.35 107.71 o 25 1 0 9.14 47.23 96.31 o 27 1 0 4.59 301.23 137.29 o 29 1 0 0.51 69.60 88.64 o 0 2 0 10023.40 10503.14 392.18 o 2 2 0 1339.94 1276.14 154.84 o 4 2 0 113.57 182.64 123.78 o 6 2 0 3484.87 3762.57 146.71 o 8 2 0 725.09 754.26 119.17 o 10 2 0 1429.64 1460.11 126.43 o 12 2 0 1619.10 1609.12 97.99 o 14 2 0 22.43 -56.58 113.49 o 16 2 0 36.54 171.04 120.51 o 18 2 0 190.09 51.15 116.45 o 20 2 0 15.63 251.41 153.96 o 22 2 0 185.84 75.36 106.41 o 26 2 0 0.07 193.62 114.57 o 28 2 0 0.32 -136.25 142.22 o 1 3 0 1003.07 1085.18 105.26 o 3 3 0 6962.30 7323.58 148.97 o 5 3 0 451.84 348.13 115.48 o 7 3 0 1798.42 1957.99 99.27 o 9 3 0 10.05 -60.22 107.78 o 11 3 0 212.71 307.41 114.33 o 13 3 0 861.03 1044.27 117.35 o 15 3 0 460.78 403.28 95.40 o 17 3 0 1345.68 1336.90 96.59 o 19 3 0 13.50 130.93 123.51 o 21 3 0 244.91 85.85 129.98 o 23 3 0 23.16 42.03 103.49 o 25 3 0 108.80 -46.47 80.19 o 27 3 0 37.72 79.54 90.45 o 0 4 0 271.88 387.31 237.26 o 2 4 0 92.70 260.34 101.47 o 4 4 0 112.95 233.32 84.91 o 6 4 0 343.95 364.07 104.99 o 8 4 0 549.01 633.80 98.12 o 10 4 0 43.65 142.41 114.47 o 12 4 0 724.39 791.05 107.02 o 14 4 0 15.22 -6.52 111.05 o 16 4 0 843.23 654.80 97.31 o 18 4 0 1497.15 1456.85 169.97 o 20 4 0 20.02 -39.58 92.35 o 22 4 0 40.80 71.26 99.35 o 24 4 0 10.93 178.34 112.70 o 26 4 0 92.91 143.45 80.31 o 1 5 0 664.16 625.52 88.27 o 3 5 0 178.35 122.26 96.10 o 5 5 0 171.86 150.48 90.06 o 7 5 0 384.51 235.60 104.02 o 9 5 0 292.42 285.95 86.16 o 11 5 0 1.15 -67.67 89.73 o 13 5 0 38.56 178.37 103.52 o 15 5 0 344.24 307.63 92.24 o 17 5 0 5.96 190.41 84.08 o 19 5 0 19.47 -7.07 77.16 o 21 5 0 31.50 -165.97 90.34 o 23 5 0 28.32 90.14 125.75 o 0 6 0 85.97 317.36 132.59 o 2 6 0 447.02 407.49 93.59 o 4 6 0 5.29 -30.75 93.72 o 6 6 0 805.41 919.84 88.35 o 8 6 0 381.59 586.08 88.45 o 10 6 0 4.09 51.68 106.60 o 12 6 0 26.57 212.12 125.78 o 14 6 0 20.79 62.90 108.88 o 16 6 0 8.71 110.40 75.96 o 18 6 0 6.30 36.58 89.19 o 20 6 0 2.48 121.51 130.89 o 1 7 0 1.49 92.81 83.05 o 3 7 0 8.19 -28.99 92.00 o 5 7 0 71.64 -65.03 91.21 o 7 7 0 5.38 -35.39 137.97 o 9 7 0 77.73 19.97 85.64 o 11 7 0 18.27 288.98 95.11 o 13 7 0 4.78 -19.98 96.00 o 15 7 0 38.55 134.23 96.40 o 0 8 0 77.62 411.86 147.91 o 2 8 0 28.09 -30.16 93.42 o 4 8 0 5.37 -15.59 139.10 o 6 8 0 66.36 125.33 95.60 o 8 8 0 0.00 63.06 88.33 o -31 1 1 16.01 45.16 142.17 o -29 1 1 0.82 216.53 88.42 o -27 1 1 14.83 125.80 92.20 o -25 1 1 18.99 93.75 99.85 o -23 1 1 15.08 47.20 125.40 o -21 1 1 8.41 234.62 125.70 o -19 1 1 73.22 -96.83 138.04 o -17 1 1 14.35 92.50 116.74 o -15 1 1 76.28 466.18 129.65 o -13 1 1 44.34 -104.51 108.98 o -11 1 1 2288.28 2146.14 151.89 o -9 1 1 248.17 264.11 147.50 o -7 1 1 14186.37 14350.41 249.80 o -5 1 1 19257.85 19893.13 219.73 o -3 1 1 1454.16 1663.42 190.51 o -1 1 1 226.55 296.90 187.24 o 1 1 1 77675.79 82198.88 1638.52 o 3 1 1 73.27 160.84 170.25 o 5 1 1 2488.58 2412.35 170.24 o 7 1 1 836.76 791.56 148.04 o 9 1 1 77.84 -13.47 125.08 o 11 1 1 2367.27 2422.99 130.08 o 13 1 1 31.42 161.92 108.75 o 15 1 1 1130.65 1124.57 123.67 o 17 1 1 220.39 208.38 113.55 o 19 1 1 11.32 94.61 124.60 o 21 1 1 38.82 114.98 127.79 o 23 1 1 2.95 -195.07 99.84 o 25 1 1 24.78 94.67 121.71 o 27 1 1 48.18 15.80 187.50 o 29 1 1 39.68 -44.23 137.89 o -30 2 1 3.91 26.39 85.74 o -28 2 1 10.20 17.45 89.65 o -26 2 1 6.19 156.44 101.95 o -24 2 1 102.02 114.71 96.45 o -22 2 1 485.26 439.06 87.21 o -20 2 1 12.30 213.25 108.33 o -18 2 1 255.30 217.70 99.04 o -16 2 1 4.38 112.00 111.68 o -14 2 1 638.94 624.31 106.69 o -12 2 1 282.13 336.66 119.39 o -10 2 1 4001.80 3916.26 143.76 o -8 2 1 936.74 990.78 112.73 o -6 2 1 593.83 767.38 129.75 o -4 2 1 1022.26 907.35 135.27 o -2 2 1 13405.08 13406.13 236.10 o 0 2 1 1155.73 937.96 203.49 o 2 2 1 1.04 125.30 148.51 o 4 2 1 316.66 428.78 135.30 o 6 2 1 6231.07 6326.64 122.65 o 8 2 1 4376.56 4391.48 131.34 o 10 2 1 600.00 554.05 110.92 o 12 2 1 1254.90 1289.35 112.44 o 14 2 1 475.45 588.22 107.91 o 16 2 1 296.86 469.93 128.37 o 18 2 1 10.04 196.35 120.82 o 20 2 1 234.61 235.15 105.92 o 22 2 1 179.81 77.43 139.40 o 24 2 1 32.72 -12.45 89.26 o 26 2 1 0.00 23.36 104.50 o 28 2 1 12.69 126.91 120.26 o -29 3 1 0.02 -45.85 113.42 o -27 3 1 25.44 119.85 81.18 o -25 3 1 281.94 382.63 173.14 o -23 3 1 1.06 -46.37 173.36 o -21 3 1 0.18 18.17 104.03 o -19 3 1 52.86 185.43 102.35 o -17 3 1 1.84 6.87 126.51 o -15 3 1 30.03 137.03 89.84 o -13 3 1 592.16 729.57 115.13 o -11 3 1 4366.40 4299.22 194.25 o -9 3 1 611.44 522.98 92.24 o -7 3 1 2042.96 2057.66 105.49 o -5 3 1 12339.78 11514.59 1093.28 o -3 3 1 1739.30 1594.95 175.70 o -1 3 1 8613.95 8401.00 139.49 o 1 3 1 458.83 586.03 129.44 o 3 3 1 956.23 1143.60 110.19 o 5 3 1 290.60 263.02 102.64 o 7 3 1 2603.60 2598.53 107.93 o 9 3 1 14.91 92.34 112.50 o 11 3 1 1188.55 1410.26 166.30 o 13 3 1 905.59 857.41 112.42 o 15 3 1 97.81 212.67 87.41 o 17 3 1 1741.66 1787.78 105.53 o 19 3 1 180.06 231.83 89.90 o 21 3 1 78.02 154.34 148.01 o 23 3 1 379.20 166.09 82.77 o 25 3 1 0.41 109.75 115.21 o 27 3 1 7.53 88.83 87.17 o -26 4 1 32.66 81.20 117.04 o -24 4 1 2.83 24.63 79.76 o -22 4 1 74.00 187.86 82.15 o -20 4 1 10.40 251.47 81.52 o -18 4 1 351.53 564.89 95.89 o -16 4 1 654.95 482.50 98.95 o -14 4 1 1143.48 1267.77 109.06 o -12 4 1 0.14 61.18 96.84 o -10 4 1 66.63 58.93 98.95 o -8 4 1 311.51 193.53 91.57 o -6 4 1 709.42 644.54 98.70 o -4 4 1 2416.40 2562.83 319.09 o -2 4 1 1010.27 917.05 239.54 o 0 4 1 2999.63 2921.69 499.53 o 2 4 1 70.35 92.29 101.46 o 4 4 1 2414.31 2298.40 107.07 o 6 4 1 439.07 614.80 107.19 o 8 4 1 871.00 866.11 118.96 o 10 4 1 1739.86 1607.51 139.20 o 12 4 1 420.62 335.18 89.64 o 14 4 1 737.77 662.03 92.27 o 16 4 1 1397.24 1350.14 119.34 o 18 4 1 474.26 594.78 95.76 o 20 4 1 317.46 182.39 93.40 o 22 4 1 19.52 146.88 83.68 o 24 4 1 68.97 159.65 148.92 o 26 4 1 111.79 221.75 101.70 o -25 5 1 13.80 71.11 94.28 o -23 5 1 2.24 228.14 111.80 o -21 5 1 6.39 -75.79 78.79 o -19 5 1 193.88 295.89 123.79 o -17 5 1 93.86 165.35 91.74 o -15 5 1 362.82 338.21 86.81 o -13 5 1 737.08 728.05 86.76 o -11 5 1 286.98 286.58 93.44 o -9 5 1 27.59 208.69 129.93 o -7 5 1 1581.06 1639.51 113.54 o -5 5 1 293.95 288.03 82.27 o -3 5 1 42.70 -58.23 128.08 o -1 5 1 9.24 99.97 83.20 o 1 5 1 68.98 203.37 88.15 o 3 5 1 556.13 514.70 84.26 o 5 5 1 67.97 97.48 117.20 o 7 5 1 71.67 256.15 98.67 o 9 5 1 317.63 439.42 83.23 o 11 5 1 79.38 41.07 91.31 o 13 5 1 526.78 572.13 83.73 o 15 5 1 40.80 -24.64 91.09 o 17 5 1 106.94 108.03 88.27 o 19 5 1 193.62 207.77 89.29 o 21 5 1 2.82 107.85 127.07 o 23 5 1 1.12 -2.74 79.19 o -22 6 1 0.98 143.41 232.38 o -20 6 1 55.14 165.18 127.32 o -18 6 1 39.29 121.75 97.08 o -16 6 1 16.11 97.82 96.04 o -14 6 1 70.87 426.55 137.34 o -12 6 1 159.87 412.89 120.84 o -10 6 1 6.94 91.22 95.89 o -8 6 1 202.56 133.34 87.95 o -6 6 1 549.66 505.82 85.43 o -4 6 1 95.56 266.03 104.39 o -2 6 1 44.74 -53.80 121.67 o 0 6 1 163.55 263.88 103.79 o 2 6 1 86.56 104.59 77.80 o 4 6 1 76.97 225.93 120.46 o 6 6 1 1159.80 1287.12 87.49 o 8 6 1 0.70 102.75 93.10 o 10 6 1 27.26 123.57 94.13 o 12 6 1 158.70 93.85 81.63 o 14 6 1 141.17 -22.35 99.56 o 16 6 1 62.34 53.15 108.19 o 18 6 1 1.69 1.25 89.24 o 20 6 1 30.27 57.84 85.64 o -17 7 1 40.94 244.38 102.34 o -15 7 1 2.32 176.07 88.79 o -13 7 1 10.63 27.92 79.62 o -11 7 1 0.92 -34.64 109.21 o -9 7 1 148.46 -59.81 85.08 o -7 7 1 5.39 -68.64 94.68 o -5 7 1 24.37 111.89 122.08 o -3 7 1 16.15 103.96 89.95 o -1 7 1 29.82 8.41 95.23 o 1 7 1 13.84 140.08 74.88 o 3 7 1 29.59 83.71 97.16 o 5 7 1 38.61 -20.70 93.07 o 7 7 1 65.37 -31.93 104.11 o 9 7 1 3.68 215.72 84.90 o 11 7 1 53.39 -8.42 80.31 o 13 7 1 51.51 72.86 79.99 o 15 7 1 37.33 115.14 90.41 o -8 8 1 76.30 47.61 87.84 o -6 8 1 93.81 -31.02 76.80 o -4 8 1 1.85 168.51 119.96 o -2 8 1 6.71 197.78 107.91 o 0 8 1 113.84 75.70 116.69 o 2 8 1 24.64 29.07 78.48 o 4 8 1 11.89 76.67 79.05 o 6 8 1 3.28 36.81 137.49 o 8 8 1 6.18 -106.42 152.13 o -30 0 2 46.76 140.90 157.63 o -28 0 2 10.89 -16.88 267.27 o -26 0 2 160.68 363.39 114.09 o -24 0 2 596.01 579.01 141.75 o -22 0 2 38.20 119.03 265.35 o -20 0 2 163.33 636.12 157.88 o -18 0 2 5604.43 6038.82 216.81 o -16 0 2 33.22 77.12 171.31 o -14 0 2 940.08 1184.58 209.51 o -12 0 2 2408.59 2184.79 230.31 o -10 0 2 39776.16 38754.71 365.96 o -8 0 2 6442.92 5679.50 290.68 o -6 0 2 926.27 887.34 268.65 o -4 0 2 4189.84 4421.77 356.46 o -2 0 2 50958.41 55179.54 798.04 o 0 0 2 501.07 445.27 343.97 o 2 0 2 25094.70 25810.78 460.01 o 4 0 2 56818.46 56068.20 749.30 o 6 0 2 18203.28 17242.15 320.08 o 8 0 2 20.18 25.90 199.72 o 10 0 2 46.36 235.13 161.71 o 12 0 2 27144.03 25256.20 552.51 o 14 0 2 463.59 638.83 170.07 o 16 0 2 43.64 138.61 148.81 o 18 0 2 10.23 183.62 163.82 o 20 0 2 87.23 -36.74 268.67 o 22 0 2 49.45 129.57 339.15 o 24 0 2 421.79 381.17 176.65 o 26 0 2 0.13 -152.83 165.91 o 28 0 2 22.62 -149.41 117.93 o -31 1 2 1.82 100.05 121.88 o -29 1 2 1.95 105.92 115.13 o -27 1 2 103.32 74.65 151.04 o -25 1 2 10.96 76.40 90.35 o -23 1 2 258.77 206.09 102.01 o -21 1 2 63.55 336.83 110.70 o -19 1 2 340.63 304.57 112.17 o -17 1 2 949.80 1077.49 134.29 o -15 1 2 7450.78 7064.81 152.95 o -13 1 2 22273.03 22519.35 633.60 o -11 1 2 415.59 392.32 115.38 o -9 1 2 28208.17 28625.23 485.19 o -7 1 2 88313.70 91418.37 1023.00 o -5 1 2 127686.40 135719.98 2618.98 o -3 1 2 12586.69 13005.87 226.70 o -1 1 2 38267.01 40950.68 659.44 o 1 1 2 23208.49 23809.78 259.41 o 3 1 2 18887.94 19785.79 301.58 o 5 1 2 1675.38 1577.94 174.19 o 7 1 2 147.26 178.87 151.77 o 9 1 2 186.11 272.43 116.06 o 11 1 2 45.00 173.34 121.49 o 13 1 2 447.26 354.46 110.62 o 15 1 2 23.02 -48.58 117.75 o 17 1 2 414.74 291.28 108.58 o 19 1 2 459.27 576.04 149.88 o 21 1 2 187.42 257.88 112.82 o 23 1 2 160.92 68.48 127.21 o 25 1 2 52.37 157.99 97.86 o 27 1 2 6.78 186.83 151.43 o 29 1 2 0.05 231.50 105.30 o -30 2 2 28.24 196.21 102.00 o -28 2 2 11.84 -103.16 109.62 o -26 2 2 41.10 -24.19 80.93 o -24 2 2 277.58 98.40 98.80 o -22 2 2 146.08 23.12 100.93 o -20 2 2 0.16 49.96 111.07 o -18 2 2 719.13 717.32 115.92 o -16 2 2 7.56 175.93 97.94 o -14 2 2 455.28 434.00 112.93 o -12 2 2 665.37 629.52 96.71 o -10 2 2 5108.64 5043.91 121.24 o -8 2 2 1201.48 1327.91 127.16 o -6 2 2 12115.61 11797.36 209.03 o -4 2 2 30.23 18.78 123.35 o -2 2 2 5850.13 5726.80 142.08 o 0 2 2 11658.42 10910.65 1301.06 o 2 2 2 2398.18 2385.82 198.10 o 4 2 2 5.22 148.30 158.48 o 6 2 2 216.26 336.73 122.90 o 8 2 2 6618.19 6862.22 181.97 o 10 2 2 62.90 138.01 113.55 o 12 2 2 0.03 40.96 112.32 o 14 2 2 135.10 321.74 111.62 o 16 2 2 79.02 308.06 120.21 o 18 2 2 18.86 33.63 117.90 o 20 2 2 92.54 160.70 99.01 o 22 2 2 103.85 202.19 108.99 o 24 2 2 12.78 200.78 132.56 o 26 2 2 5.06 24.63 176.56 o 28 2 2 0.31 -12.19 130.19 o -29 3 2 2.66 57.23 106.13 o -27 3 2 124.43 -81.67 121.98 o -25 3 2 0.38 144.50 102.70 o -23 3 2 188.02 139.29 95.10 o -21 3 2 347.05 279.99 91.54 o -19 3 2 136.44 117.25 185.23 o -17 3 2 8.56 235.32 96.49 o -15 3 2 702.42 885.20 96.04 o -13 3 2 231.41 242.19 95.69 o -11 3 2 275.04 419.88 112.44 o -9 3 2 2868.22 2817.05 117.02 o -7 3 2 2481.42 2274.24 116.38 o -5 3 2 186.66 149.19 103.47 o -3 3 2 499.91 500.48 126.04 o -1 3 2 3748.12 3251.55 489.17 o 1 3 2 6649.17 6554.43 131.95 o 3 3 2 170.13 259.89 96.54 o 5 3 2 4191.71 4221.03 119.99 o 7 3 2 1228.05 1343.00 123.19 o 9 3 2 577.35 670.28 90.12 o 11 3 2 2063.82 2074.23 110.17 o 13 3 2 2880.95 2901.31 189.21 o 15 3 2 1147.50 1172.91 157.58 o 17 3 2 127.72 169.61 115.08 o 19 3 2 92.54 62.10 104.42 o 21 3 2 5.44 79.28 103.01 o 23 3 2 29.63 238.91 134.01 o 25 3 2 137.90 -91.66 87.50 o 27 3 2 14.60 31.72 107.32 o -28 4 2 36.00 236.03 195.69 o -26 4 2 6.19 237.90 215.40 o -24 4 2 45.42 237.96 100.94 o -22 4 2 59.59 -86.61 101.30 o -20 4 2 103.88 21.97 110.85 o -18 4 2 131.79 259.94 115.33 o -16 4 2 1579.95 1655.36 111.30 o -14 4 2 56.35 68.07 93.37 o -12 4 2 1159.02 1221.14 138.45 o -10 4 2 438.05 568.43 85.42 o -8 4 2 2002.67 1860.12 102.57 o -6 4 2 212.84 267.16 106.49 o -4 4 2 2740.84 2689.42 116.69 o -2 4 2 301.07 409.13 85.49 o 0 4 2 1164.86 717.17 211.33 o 2 4 2 610.87 711.84 92.65 o 4 4 2 100.75 208.87 86.92 o 6 4 2 855.21 885.61 97.78 o 8 4 2 649.41 648.04 119.92 o 10 4 2 315.14 421.95 84.08 o 12 4 2 1378.52 1309.22 136.23 o 14 4 2 0.86 124.07 94.29 o 16 4 2 835.79 969.02 103.74 o 18 4 2 262.21 389.83 79.82 o 20 4 2 61.57 240.49 97.90 o 22 4 2 7.70 -12.43 116.89 o 24 4 2 33.92 -50.37 88.28 o -25 5 2 2.69 -79.22 103.02 o -23 5 2 2.40 98.58 152.80 o -21 5 2 0.23 33.01 91.71 o -19 5 2 130.25 65.44 90.43 o -17 5 2 1.06 178.80 95.99 o -15 5 2 81.62 128.88 95.92 o -13 5 2 306.81 296.80 102.67 o -11 5 2 275.44 402.76 96.86 o -9 5 2 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118.10 o -29 1 28 9.80 27.83 114.17 o -27 1 28 43.29 164.07 116.23 o -25 1 28 220.00 159.37 143.10 o -23 1 28 24.14 105.33 135.09 o -21 1 28 0.15 48.92 158.73 o -19 1 28 5.45 73.20 195.65 o -17 1 28 9.63 33.23 198.74 o -15 1 28 1.01 -10.50 209.79 o -13 1 28 19.44 88.16 210.30 o -11 1 28 64.69 92.48 198.36 o -9 1 28 1.53 66.27 196.43 o -7 1 28 41.89 65.31 178.59 o -5 1 28 67.21 -136.53 180.09 o -3 1 28 0.01 131.95 196.93 o -1 1 28 14.54 11.91 122.86 o 1 1 28 1.58 86.48 118.08 o -32 2 28 3.49 -30.86 105.08 o -30 2 28 4.20 -17.53 112.68 o -28 2 28 48.48 133.79 116.33 o -26 2 28 20.95 0.52 121.47 o -24 2 28 0.45 88.75 137.10 o -22 2 28 38.94 5.38 194.87 o -20 2 28 139.90 206.80 185.45 o -18 2 28 6.08 122.35 156.09 o -16 2 28 11.87 120.88 159.33 o -14 2 28 432.62 517.50 163.08 o -12 2 28 3.27 91.35 158.34 o -10 2 28 120.85 226.28 156.73 o -8 2 28 20.93 -36.65 156.00 o -6 2 28 7.98 55.71 155.24 o -4 2 28 60.05 175.51 239.36 o -2 2 28 37.84 -67.66 115.51 o 0 2 28 36.61 78.21 128.78 o -31 3 28 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