#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/22/2232295.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232295_Fobs loop_ _publ_author_name 'Yin, Bang-Shao' 'Li, Tian-Bao' 'Yang, Ming-Sheng' _publ_section_title ; [N,N-Bis(diphenylphosphanyl)propanamine-\k^2^P,P']dichloridonickel(II) ; _journal_coeditor_code HB6453 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1572 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 122.669 _cell_angle_gamma 90.000 _cell_length_a 10.2100 _cell_length_b 19.3080 _cell_length_c 15.5380 _exptl_crystal_F_000 1152.00 _reflns_d_resolution_high 0.8403 _[local]_cod_data_source_file hb6453Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' shelx in P2(1)/n New: P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 274.33 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 79.97 405.65 42.42 o 2 0 0 4167.36 3473.91 84.59 o 3 0 0 18587.38 17571.16 215.94 o 4 0 0 1588.43 2821.78 170.61 o 5 0 0 4101.71 3811.54 182.73 o 6 0 0 226.56 314.79 92.85 o 7 0 0 42.96 85.68 43.27 o 8 0 0 14402.35 15043.88 769.97 o 9 0 0 1.33 137.30 79.70 o 10 0 0 169.49 227.10 112.52 o 1 1 0 26456.16 22575.17 188.11 o 2 1 0 40012.80 40174.14 273.39 o 3 1 0 3323.40 3551.93 46.08 o 4 1 0 28295.83 27810.50 401.65 o 5 1 0 269.18 282.25 45.10 o 6 1 0 907.64 1091.23 121.33 o 7 1 0 202.29 211.16 55.53 o 8 1 0 22.48 214.37 51.95 o 9 1 0 424.19 351.95 63.86 o 10 1 0 61.64 20.49 41.01 o 0 2 0 49060.02 46010.74 484.73 o 1 2 0 923.76 861.70 28.28 o 2 2 0 2.39 28.37 11.43 o 3 2 0 2274.43 2191.50 34.04 o 4 2 0 1083.58 1198.37 67.61 o 5 2 0 2933.67 2824.47 110.07 o 6 2 0 2924.32 2799.51 123.56 o 7 2 0 96.44 128.26 35.69 o 8 2 0 2088.91 2148.92 177.64 o 9 2 0 1.17 44.04 40.56 o 10 2 0 530.05 459.27 108.26 o 1 3 0 761.39 668.22 28.13 o 2 3 0 26359.16 26054.89 360.73 o 3 3 0 4005.85 3688.05 41.93 o 4 3 0 1610.54 1645.44 77.23 o 5 3 0 706.16 744.21 74.17 o 6 3 0 1728.47 1729.10 142.90 o 7 3 0 173.60 142.64 39.07 o 8 3 0 250.64 284.81 54.61 o 9 3 0 67.17 52.43 41.69 o 10 3 0 647.45 455.31 74.29 o 0 4 0 57510.35 55524.29 797.96 o 1 4 0 700.18 627.30 33.62 o 2 4 0 11.03 45.05 11.77 o 3 4 0 720.42 686.57 37.25 o 4 4 0 819.68 845.64 67.64 o 5 4 0 36.59 78.02 27.43 o 6 4 0 909.01 886.08 86.79 o 7 4 0 79.46 87.86 38.37 o 8 4 0 663.64 738.39 79.40 o 9 4 0 6.07 71.09 41.38 o 10 4 0 140.29 151.03 43.54 o 1 5 0 161.65 194.10 17.85 o 2 5 0 15.02 63.41 9.68 o 3 5 0 335.76 555.17 36.53 o 4 5 0 26.91 58.28 10.98 o 5 5 0 61.27 139.28 27.31 o 6 5 0 1159.78 1240.86 139.37 o 7 5 0 493.95 477.06 99.86 o 8 5 0 71.66 72.64 39.23 o 9 5 0 765.33 610.93 80.71 o 0 6 0 2825.80 2686.94 59.74 o 1 6 0 1025.90 1110.49 46.50 o 2 6 0 2068.07 2029.78 33.86 o 3 6 0 1263.29 1244.82 53.58 o 4 6 0 221.16 248.98 22.79 o 5 6 0 1786.54 1664.02 185.71 o 6 6 0 2.09 71.85 61.95 o 7 6 0 167.57 174.88 63.35 o 8 6 0 2902.80 3164.56 189.67 o 9 6 0 1.32 33.58 43.30 o 1 7 0 5213.25 4273.42 151.21 o 2 7 0 2378.86 2443.64 51.64 o 3 7 0 2338.44 2645.72 86.56 o 4 7 0 14769.26 14146.47 203.47 o 5 7 0 538.58 660.49 75.70 o 6 7 0 318.10 346.54 64.38 o 7 7 0 835.46 905.70 93.63 o 8 7 0 1.27 115.97 44.33 o 9 7 0 1302.51 1270.64 153.90 o 0 8 0 60952.44 64635.05 991.16 o 1 8 0 2275.31 1948.49 54.73 o 2 8 0 3378.04 3068.96 55.35 o 3 8 0 7341.55 7177.48 85.66 o 4 8 0 1054.58 1603.14 150.80 o 5 8 0 5449.16 5613.96 154.46 o 6 8 0 339.73 191.37 49.20 o 7 8 0 30.88 60.38 34.12 o 8 8 0 5582.07 5759.37 737.17 o 9 8 0 29.19 85.72 32.48 o 1 9 0 7010.52 6401.80 151.10 o 2 9 0 5582.55 6204.71 104.03 o 3 9 0 1310.47 1246.78 75.21 o 4 9 0 12361.96 12448.12 280.75 o 5 9 0 611.25 574.19 77.73 o 6 9 0 2.60 30.53 16.74 o 7 9 0 233.28 198.88 63.52 o 8 9 0 200.63 406.28 94.54 o 9 9 0 110.59 191.02 50.47 o 0 10 0 16170.23 16879.52 394.43 o 1 10 0 191.33 209.35 26.53 o 2 10 0 1610.74 1489.75 85.18 o 3 10 0 66.54 56.90 29.50 o 4 10 0 129.55 65.71 22.94 o 5 10 0 506.94 601.17 74.70 o 6 10 0 1915.76 1877.75 168.05 o 7 10 0 3.18 34.25 34.16 o 8 10 0 310.51 369.83 56.75 o 9 10 0 63.42 74.33 36.22 o 1 11 0 43.27 56.34 14.72 o 2 11 0 4373.13 4703.57 171.31 o 3 11 0 238.67 289.19 47.67 o 4 11 0 225.28 245.28 40.69 o 5 11 0 1618.69 1866.90 162.36 o 6 11 0 1316.51 1456.49 130.35 o 7 11 0 957.72 904.13 99.02 o 8 11 0 445.97 446.28 72.38 o 0 12 0 489.43 957.68 139.60 o 1 12 0 0.37 66.47 31.38 o 2 12 0 446.86 323.72 59.69 o 3 12 0 2733.49 3193.62 169.57 o 4 12 0 628.92 700.92 86.70 o 5 12 0 645.17 740.25 117.24 o 6 12 0 3449.05 3730.82 172.26 o 7 12 0 250.42 375.74 69.47 o 8 12 0 725.61 746.07 74.17 o 1 13 0 30.45 81.91 29.58 o 2 13 0 2373.37 2781.51 164.20 o 3 13 0 114.97 99.18 39.65 o 4 13 0 112.03 137.07 35.38 o 5 13 0 979.01 1083.71 106.16 o 6 13 0 1606.14 1674.31 158.07 o 7 13 0 943.97 1112.14 146.93 o 8 13 0 21.24 51.28 37.90 o 0 14 0 279.08 470.94 116.14 o 1 14 0 693.63 743.98 99.22 o 2 14 0 48.56 78.59 36.81 o 3 14 0 467.66 614.76 96.42 o 4 14 0 48.65 58.52 67.97 o 5 14 0 269.36 303.59 60.08 o 6 14 0 674.00 693.52 78.02 o 7 14 0 13.12 100.71 38.53 o 8 14 0 1419.49 1398.24 169.70 o 1 15 0 193.50 158.53 39.63 o 2 15 0 451.38 571.98 87.00 o 3 15 0 564.49 593.60 91.37 o 4 15 0 3133.55 3357.34 267.68 o 5 15 0 145.24 225.61 60.00 o 6 15 0 580.68 563.18 94.12 o 7 15 0 730.05 667.72 99.98 o 0 16 0 1944.97 2438.42 175.08 o 1 16 0 122.27 121.16 36.61 o 2 16 0 294.24 291.86 73.75 o 3 16 0 465.48 561.12 68.00 o 4 16 0 505.91 552.36 90.44 o 5 16 0 821.34 862.53 112.38 o 6 16 0 619.54 523.92 78.94 o 7 16 0 52.21 117.84 42.77 o 1 17 0 740.41 852.60 82.90 o 2 17 0 1.43 48.05 40.97 o 3 17 0 483.69 444.80 85.03 o 4 17 0 2925.51 2659.36 326.89 o 5 17 0 14.54 101.26 44.98 o 6 17 0 229.23 140.09 47.77 o 0 18 0 89.09 155.93 83.32 o 1 18 0 231.08 294.40 64.05 o 2 18 0 945.02 1085.50 156.59 o 3 18 0 0.29 60.36 42.26 o 4 18 0 202.89 174.01 51.76 o 5 18 0 375.55 338.65 73.24 o 6 18 0 162.83 210.02 67.05 o 1 19 0 518.45 536.52 91.14 o 2 19 0 1427.56 1615.34 222.88 o 3 19 0 1.11 55.53 42.97 o 4 19 0 477.62 469.02 82.48 o 5 19 0 137.85 157.28 45.86 o 0 20 0 127.09 166.08 78.36 o 1 20 0 80.66 6.23 150.63 o 2 20 0 681.69 660.09 97.00 o 3 20 0 467.78 518.18 136.22 o 4 20 0 44.48 106.80 37.74 o 5 20 0 497.36 316.74 91.81 o 1 21 0 483.78 608.75 129.26 o 2 21 0 60.32 111.71 45.36 o 3 21 0 349.24 315.65 68.17 o 4 21 0 117.14 141.43 53.22 o 0 22 0 229.13 270.37 111.17 o 1 22 0 41.60 31.83 62.63 o 2 22 0 66.39 60.96 32.90 o -10 1 1 135.10 131.75 47.61 o -9 1 1 1850.20 2068.23 185.26 o -8 1 1 54.01 98.72 48.33 o -7 1 1 461.87 516.99 94.41 o -6 1 1 388.47 343.09 46.83 o -5 1 1 1959.74 2058.44 100.82 o -4 1 1 7107.88 6758.72 95.69 o -3 1 1 6251.02 6086.76 106.22 o -2 1 1 2.76 6.28 10.99 o -1 1 1 2303.34 2149.25 37.26 o 0 1 1 102.70 127.88 15.19 o 1 1 1 497.35 483.99 22.54 o 2 1 1 1012.37 945.52 30.00 o 3 1 1 807.24 819.45 28.78 o 4 1 1 3094.94 2553.88 88.00 o 5 1 1 59.39 81.42 23.80 o 6 1 1 15.10 100.19 59.15 o 7 1 1 2587.53 2754.46 146.03 o 8 1 1 299.88 395.16 64.80 o 9 1 1 286.43 302.50 50.60 o -10 2 1 235.95 212.77 56.41 o -9 2 1 142.64 84.09 30.66 o -8 2 1 3079.00 1808.44 528.30 o -7 2 1 334.37 306.78 43.06 o -6 2 1 1846.13 1984.22 139.98 o -5 2 1 10231.04 10294.50 158.13 o -4 2 1 2021.57 2059.16 57.08 o -3 2 1 13442.98 12189.69 218.78 o -2 2 1 170.10 256.83 20.29 o -1 2 1 1341.02 1103.17 32.02 o 0 2 1 7322.18 7111.66 72.15 o 1 2 1 530.92 443.98 39.73 o 2 2 1 16.22 28.24 10.58 o 3 2 1 3364.64 3185.25 46.81 o 4 2 1 460.15 393.26 38.30 o 5 2 1 350.66 259.65 36.48 o 6 2 1 664.46 566.08 74.84 o 7 2 1 301.97 291.12 76.28 o 8 2 1 3009.97 3367.53 211.19 o 9 2 1 118.31 192.69 44.54 o -10 3 1 17.51 81.15 55.18 o -9 3 1 3768.78 4192.85 260.21 o -8 3 1 116.93 126.30 43.70 o -7 3 1 8.28 28.27 25.08 o -6 3 1 173.02 188.76 40.75 o -5 3 1 1384.00 1402.54 150.61 o -4 3 1 16968.35 16209.46 235.92 o -3 3 1 28.25 71.73 8.57 o -2 3 1 475.00 490.66 35.55 o -1 3 1 988.23 918.17 30.69 o 0 3 1 44.41 59.94 10.21 o 1 3 1 10885.54 10680.52 96.16 o 2 3 1 5609.80 5507.40 59.31 o 3 3 1 1938.40 2000.01 27.55 o 4 3 1 6499.57 5519.61 96.18 o 5 3 1 810.42 866.97 65.07 o 6 3 1 17.29 29.97 15.83 o 7 3 1 3737.09 4329.07 219.93 o 8 3 1 200.53 131.91 47.24 o 9 3 1 670.61 521.32 80.38 o -10 4 1 89.44 105.49 47.50 o -9 4 1 5.41 136.47 54.24 o -8 4 1 3160.71 3291.48 243.54 o -7 4 1 69.44 95.39 23.28 o -6 4 1 1067.65 1051.97 97.44 o -5 4 1 1819.00 1608.41 106.16 o -4 4 1 728.31 644.46 44.40 o -3 4 1 82.24 102.61 11.47 o -2 4 1 1178.91 1129.82 33.79 o -1 4 1 3.40 57.93 16.20 o 0 4 1 5371.04 4968.70 85.22 o 1 4 1 11.44 397.64 37.17 o 2 4 1 850.91 783.46 46.70 o 3 4 1 2642.16 2318.35 36.79 o 4 4 1 264.78 236.56 29.88 o 5 4 1 114.64 179.31 28.30 o 6 4 1 19.90 77.16 41.12 o 7 4 1 94.12 266.05 68.29 o 8 4 1 4676.31 5501.42 284.98 o 9 4 1 2.03 41.12 51.83 o -10 5 1 3.14 67.54 38.23 o -9 5 1 3792.26 4109.70 278.47 o -8 5 1 4.18 104.33 39.79 o -7 5 1 522.98 602.23 87.43 o -6 5 1 10.07 26.28 23.54 o -5 5 1 1547.93 1550.45 82.92 o -4 5 1 5896.80 5219.29 78.74 o -3 5 1 2577.63 2251.01 39.20 o -2 5 1 41.52 40.46 12.85 o -1 5 1 14296.79 12306.30 368.37 o 0 5 1 2064.76 2062.66 35.32 o 1 5 1 17182.68 15780.03 124.53 o 2 5 1 870.12 955.08 51.91 o 3 5 1 74.69 146.58 16.68 o 4 5 1 4964.60 4394.25 71.57 o 5 5 1 2414.27 2516.03 186.28 o 6 5 1 484.40 408.05 68.25 o 7 5 1 2595.59 2919.32 224.22 o 8 5 1 51.23 146.55 47.00 o 9 5 1 514.58 391.31 61.28 o -10 6 1 46.12 91.39 35.61 o -9 6 1 1918.29 1903.77 240.65 o -8 6 1 4799.33 5176.87 208.94 o -7 6 1 4.32 72.77 59.28 o -6 6 1 1527.25 1446.10 169.93 o -5 6 1 7026.12 7128.40 165.06 o -4 6 1 24.40 42.23 16.83 o -3 6 1 374.32 362.94 25.71 o -2 6 1 886.05 914.52 41.41 o -1 6 1 1267.16 1338.23 83.94 o 0 6 1 474.99 512.42 42.49 o 1 6 1 11326.45 11085.54 99.41 o 2 6 1 368.94 362.10 23.86 o 3 6 1 4098.58 3794.33 60.12 o 4 6 1 1759.89 1720.94 98.43 o 5 6 1 149.42 86.48 36.42 o 6 6 1 626.30 561.31 101.72 o 7 6 1 213.13 138.34 38.39 o 8 6 1 5167.26 5889.74 250.10 o 9 6 1 653.97 495.58 66.64 o -10 7 1 809.93 711.03 111.80 o -9 7 1 2661.21 2646.38 246.01 o -8 7 1 170.11 322.36 79.85 o -7 7 1 1494.16 1721.96 118.29 o -6 7 1 5.63 31.29 19.74 o -5 7 1 4784.90 4788.79 136.49 o -4 7 1 708.41 608.85 48.73 o -3 7 1 1114.22 1125.70 55.33 o -2 7 1 44.95 62.69 18.17 o -1 7 1 8098.64 6531.92 581.73 o 0 7 1 2306.92 2197.83 42.76 o 1 7 1 75.61 86.42 13.74 o 2 7 1 88.20 135.89 15.22 o 3 7 1 26.74 80.38 18.69 o 4 7 1 3453.54 3054.72 99.74 o 5 7 1 626.44 515.07 59.96 o 6 7 1 0.02 74.11 37.70 o 7 7 1 3212.77 3701.97 234.24 o 8 7 1 722.53 663.85 89.89 o 9 7 1 65.91 81.22 44.39 o -9 8 1 141.35 145.55 54.91 o -8 8 1 1478.95 1516.56 138.05 o -7 8 1 170.02 223.65 48.54 o -6 8 1 650.82 621.54 84.63 o -5 8 1 70.94 88.42 34.11 o -4 8 1 558.00 464.78 44.79 o -3 8 1 2376.29 2206.57 88.76 o -2 8 1 4156.31 3969.75 63.62 o -1 8 1 572.47 570.34 39.20 o 0 8 1 3714.33 3847.72 65.36 o 1 8 1 1330.64 1552.43 62.29 o 2 8 1 299.59 212.79 24.34 o 3 8 1 271.44 298.36 28.78 o 4 8 1 3172.76 3165.35 142.48 o 5 8 1 835.60 887.16 90.14 o 6 8 1 243.04 181.47 42.36 o 7 8 1 216.13 158.18 41.81 o 8 8 1 0.24 43.12 37.79 o 9 8 1 818.04 729.58 88.35 o -9 9 1 672.44 667.37 79.37 o -8 9 1 264.34 246.90 48.11 o -7 9 1 774.36 1035.61 96.35 o -6 9 1 1502.40 1616.44 156.69 o -5 9 1 650.71 720.16 78.79 o -4 9 1 2734.32 2638.66 100.43 o -3 9 1 391.57 328.55 45.32 o -2 9 1 53.90 42.25 11.35 o -1 9 1 14792.35 13718.58 246.03 o 0 9 1 573.32 658.94 51.14 o 1 9 1 2756.87 2278.16 102.67 o 2 9 1 4630.09 4204.56 90.88 o 3 9 1 279.36 290.04 27.98 o 4 9 1 2498.81 2529.58 184.18 o 5 9 1 262.73 311.40 43.08 o 6 9 1 2418.67 1435.41 494.24 o 7 9 1 226.30 300.83 54.87 o 8 9 1 194.43 194.59 41.48 o 9 9 1 120.25 208.76 87.81 o -9 10 1 0.57 210.65 61.83 o -8 10 1 886.54 766.19 101.57 o -7 10 1 289.93 328.05 55.10 o -6 10 1 61.34 61.39 21.63 o -5 10 1 5977.67 6061.58 186.51 o -4 10 1 141.68 119.28 20.58 o -3 10 1 5682.94 5464.64 110.06 o -2 10 1 5173.78 4515.67 89.29 o -1 10 1 122.29 187.66 34.09 o 0 10 1 13411.99 13233.38 237.41 o 1 10 1 2149.54 1911.99 184.99 o 2 10 1 1083.21 880.17 95.74 o 3 10 1 8259.70 8311.00 195.10 o 4 10 1 1081.92 1097.84 91.40 o 5 10 1 3126.43 3307.31 145.73 o 6 10 1 847.88 847.33 123.70 o 7 10 1 48.30 76.51 35.48 o 8 10 1 1527.46 1539.34 179.78 o -9 11 1 1604.27 1436.26 152.93 o -8 11 1 193.24 140.49 43.73 o -7 11 1 8.54 133.93 37.51 o -6 11 1 440.66 456.97 61.63 o -5 11 1 554.35 508.57 100.96 o -4 11 1 6247.18 6386.62 186.33 o -3 11 1 857.49 895.34 82.96 o -2 11 1 15.79 56.71 25.84 o -1 11 1 12013.02 11001.86 722.54 o 0 11 1 12.03 55.33 21.17 o 1 11 1 3549.03 2798.37 226.63 o 2 11 1 429.72 429.92 61.92 o 3 11 1 101.94 164.45 45.32 o 4 11 1 7267.81 7185.10 283.57 o 5 11 1 217.48 209.82 36.25 o 6 11 1 93.17 150.82 47.85 o 7 11 1 1895.78 2002.64 212.03 o 8 11 1 2.75 31.18 25.18 o -9 12 1 464.17 397.55 66.51 o -8 12 1 1839.14 1717.71 172.71 o -7 12 1 26.44 87.36 35.43 o -6 12 1 133.12 169.66 126.78 o -5 12 1 2370.58 2299.73 146.97 o -4 12 1 53.46 122.71 31.96 o -3 12 1 191.87 163.43 35.00 o -2 12 1 573.00 558.29 65.45 o -1 12 1 239.63 274.78 51.97 o 0 12 1 3618.55 3329.47 191.20 o 1 12 1 2.58 14.47 21.90 o 2 12 1 83.09 118.90 30.53 o 3 12 1 3000.14 3491.02 303.82 o 4 12 1 244.50 292.85 51.27 o 5 12 1 37.58 81.29 24.94 o 6 12 1 39.25 7.80 38.10 o 7 12 1 26.95 64.21 39.25 o 8 12 1 519.05 599.20 110.40 o -8 13 1 304.92 204.63 54.01 o -7 13 1 69.96 115.74 32.16 o -6 13 1 73.68 96.23 35.92 o -5 13 1 235.11 315.15 52.08 o -4 13 1 5090.42 5423.71 239.71 o -3 13 1 106.11 90.64 35.66 o -2 13 1 234.94 310.80 68.46 o -1 13 1 3414.71 2960.34 141.81 o 0 13 1 892.98 1042.04 133.80 o 1 13 1 609.89 679.45 98.81 o 2 13 1 1416.17 1806.90 164.28 o 3 13 1 74.94 59.15 51.20 o 4 13 1 4487.40 4597.90 245.96 o 5 13 1 915.49 954.40 93.88 o 6 13 1 608.41 542.48 63.18 o 7 13 1 759.98 630.23 81.39 o 8 13 1 10.78 52.81 43.94 o -8 14 1 1511.00 1497.15 131.82 o -7 14 1 282.02 318.15 78.49 o -6 14 1 170.51 229.44 47.11 o -5 14 1 3708.35 4569.11 258.03 o -4 14 1 21.41 33.48 28.37 o -3 14 1 102.92 58.35 48.15 o -2 14 1 8.50 -27.09 37.16 o -1 14 1 41.48 34.22 43.44 o 0 14 1 2322.42 2292.25 175.58 o 1 14 1 32.08 54.57 21.72 o 2 14 1 140.17 171.59 51.88 o 3 14 1 1986.58 2273.39 164.54 o 4 14 1 364.77 329.12 60.33 o 5 14 1 0.21 40.54 24.56 o 6 14 1 16.51 66.37 29.98 o 7 14 1 31.99 127.56 37.21 o -8 15 1 6.31 36.62 112.18 o -7 15 1 967.11 892.97 122.54 o -6 15 1 162.32 134.02 35.30 o -5 15 1 1026.53 1024.25 108.88 o -4 15 1 1607.62 1593.03 124.11 o -3 15 1 353.99 274.06 61.28 o -2 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