#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/29/2232985.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232985_Fobs loop_ _publ_author_name 'Yang, Yongbo W.' 'Stevenson, Ryan A.' 'Siegel, Alesha M.' 'Downs, Gordon W.' _publ_section_title ; Redetermination of eveite, Mn~2~AsO~4~(OH), based on single-crystal X-ray diffraction data ; _journal_coeditor_code WM2546 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first i68 _journal_volume 67 _journal_year 2011 _space_group_IT_number 58 _symmetry_space_group_name_Hall '-P 2 2n' _symmetry_space_group_name_H-M 'P n n m' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.5478 _cell_length_b 8.7207 _cell_length_c 6.2961 _exptl_crystal_F_000 496.00 _reflns_d_resolution_high 0.6606 _[local]_cod_data_source_file wm2546Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' eveite in Pnnm' _shelx_refln_list_code 4 _shelx_f_calc_maximum 258.18 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' '-x+1/2, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x, y, -z' 'x-1/2, -y-1/2, z-1/2' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 7435.21 7910.66 110.55 o 6 0 0 1189.40 1294.29 24.27 o 8 0 0 18201.31 18982.89 267.62 o 10 0 0 757.34 800.17 24.94 o 12 0 0 2086.37 2039.85 46.51 o 2 1 0 3735.91 3705.42 58.98 o 3 1 0 11353.72 12088.88 266.95 o 4 1 0 541.91 679.79 12.81 o 5 1 0 5891.87 6373.69 91.68 o 6 1 0 4943.68 5446.33 83.25 o 7 1 0 3.80 11.99 5.39 o 8 1 0 2378.76 2422.87 30.97 o 9 1 0 1868.47 1989.14 28.36 o 10 1 0 365.99 377.58 16.18 o 11 1 0 1285.00 1303.73 34.38 o 12 1 0 61.95 60.40 8.81 o 0 2 0 2880.81 2583.64 50.22 o 1 2 0 3490.45 3272.51 34.80 o 2 2 0 39573.37 40318.05 389.19 o 4 2 0 684.00 720.71 11.19 o 5 2 0 1855.35 1852.60 23.11 o 6 2 0 15418.29 16233.79 161.59 o 7 2 0 445.59 404.46 14.83 o 8 2 0 512.86 551.54 12.62 o 9 2 0 1494.04 1462.05 23.59 o 10 2 0 5385.33 5313.12 62.91 o 11 2 0 104.49 85.28 8.58 o 12 2 0 134.80 152.60 15.50 o 1 3 0 7754.65 7328.59 53.08 o 2 3 0 2365.66 2206.01 26.45 o 3 3 0 1433.95 1547.50 25.62 o 4 3 0 499.93 607.97 11.19 o 5 3 0 1682.49 1829.18 30.67 o 6 3 0 163.32 180.04 7.58 o 7 3 0 8247.63 8464.88 90.09 o 8 3 0 4.07 17.53 7.42 o 9 3 0 257.74 270.77 10.72 o 10 3 0 480.23 469.11 14.53 o 11 3 0 32.75 28.65 7.63 o 12 3 0 760.62 727.83 19.78 o 1 4 0 146.44 188.95 4.63 o 2 4 0 32.95 40.39 3.00 o 3 4 0 34.47 48.39 4.29 o 4 4 0 39236.50 39848.38 431.43 o 5 4 0 457.81 412.34 10.72 o 6 4 0 419.97 447.84 19.21 o 7 4 0 28.94 38.70 5.47 o 8 4 0 2936.63 2857.45 38.60 o 9 4 0 0.62 4.54 5.47 o 10 4 0 34.73 31.87 6.90 o 11 4 0 56.74 65.02 8.54 o 12 4 0 3236.05 2964.34 44.55 o 1 5 0 6500.50 6498.91 72.97 o 2 5 0 4726.52 4561.41 36.65 o 3 5 0 1286.06 1301.89 16.73 o 4 5 0 24.30 22.94 4.29 o 5 5 0 927.46 930.54 18.09 o 6 5 0 997.71 959.81 18.57 o 7 5 0 3416.71 3358.62 44.32 o 8 5 0 88.47 82.58 7.85 o 9 5 0 339.82 317.51 18.88 o 10 5 0 362.55 322.53 13.80 o 11 5 0 361.12 340.87 15.01 o 0 6 0 119.70 121.95 7.38 o 1 6 0 3390.55 3309.04 29.32 o 2 6 0 12687.37 12413.69 91.25 o 3 6 0 1463.43 1452.80 19.19 o 4 6 0 732.79 772.22 22.58 o 5 6 0 153.33 136.98 13.15 o 6 6 0 8908.30 9023.20 100.34 o 7 6 0 24.72 30.09 7.42 o 8 6 0 205.96 196.13 11.41 o 9 6 0 1622.65 1545.73 41.79 o 10 6 0 2763.19 2518.55 40.01 o 11 6 0 460.99 430.16 19.55 o 1 7 0 1434.93 1403.53 16.93 o 2 7 0 86.76 98.99 5.18 o 3 7 0 3786.71 3861.08 40.33 o 4 7 0 1.39 14.01 12.47 o 5 7 0 2353.52 2225.50 63.37 o 6 7 0 446.17 439.74 16.18 o 7 7 0 336.54 329.55 14.06 o 8 7 0 709.41 668.87 19.27 o 9 7 0 2154.58 2029.87 35.74 o 10 7 0 43.42 54.60 9.50 o 0 8 0 28517.18 27400.91 275.99 o 1 8 0 2299.56 2203.84 23.92 o 2 8 0 1129.60 1153.02 18.80 o 3 8 0 541.98 509.43 15.73 o 4 8 0 2818.63 2851.94 42.42 o 5 8 0 65.46 78.96 8.58 o 6 8 0 220.19 220.37 12.62 o 7 8 0 304.97 302.71 14.78 o 8 8 0 7377.22 7074.29 87.94 o 9 8 0 601.15 519.87 18.82 o 10 8 0 426.18 411.91 17.39 o 1 9 0 462.56 465.35 12.83 o 2 9 0 1316.14 1294.02 60.67 o 3 9 0 2151.06 2133.59 36.46 o 4 9 0 61.93 65.06 8.81 o 5 9 0 725.74 696.71 20.50 o 6 9 0 2175.17 2066.48 37.66 o 7 9 0 836.21 824.76 33.37 o 8 9 0 733.93 690.61 21.91 o 9 9 0 150.39 146.60 15.17 o 0 10 0 1996.26 2042.19 41.46 o 1 10 0 8.11 8.09 5.45 o 2 10 0 7564.06 7580.58 92.70 o 3 10 0 353.00 353.79 20.22 o 4 10 0 109.61 99.83 11.19 o 5 10 0 1074.96 1004.89 25.98 o 6 10 0 3441.98 3374.38 53.86 o 7 10 0 446.01 381.76 17.87 o 8 10 0 278.65 272.70 43.48 o 1 11 0 1184.42 1257.31 28.59 o 2 11 0 28.36 24.75 8.33 o 3 11 0 36.95 44.73 9.50 o 4 11 0 259.77 293.63 16.88 o 5 11 0 632.25 646.58 22.64 o 6 11 0 45.49 43.84 10.96 o 7 11 0 1699.38 1749.32 38.13 o 1 12 0 4.43 5.39 12.81 o 2 12 0 70.19 76.85 16.85 o 3 12 0 303.39 317.19 18.31 o 4 12 0 5485.34 5684.17 80.79 o 5 12 0 770.93 812.27 26.93 o 2 13 0 918.55 968.02 41.79 o 1 0 1 7517.91 7196.78 101.79 o 3 0 1 10784.19 12064.52 169.20 o 5 0 1 41.90 53.25 6.74 o 7 0 1 909.04 941.61 21.00 o 9 0 1 951.31 1013.37 34.38 o 11 0 1 2047.47 1959.66 56.63 o 0 1 1 5482.34 4962.68 50.29 o 1 1 1 6949.28 7082.26 70.98 o 2 1 1 0.71 -2.38 2.38 o 3 1 1 13454.13 14414.85 142.52 o 4 1 1 2361.82 2546.64 30.27 o 5 1 1 18815.00 20291.97 209.65 o 6 1 1 57.81 66.84 3.13 o 7 1 1 4850.39 5213.25 76.96 o 8 1 1 218.69 229.03 12.51 o 9 1 1 377.23 387.77 8.01 o 10 1 1 222.29 214.72 7.16 o 11 1 1 1164.02 1103.47 15.37 o 12 1 1 2.33 5.12 5.09 o 1 2 1 0.24 -2.61 2.61 o 2 2 1 2688.75 2731.91 38.00 o 3 2 1 393.53 362.85 5.81 o 4 2 1 746.01 778.04 12.65 o 5 2 1 435.10 467.79 7.55 o 6 2 1 484.57 511.42 7.01 o 7 2 1 191.20 218.64 5.54 o 8 2 1 987.15 1040.10 12.53 o 9 2 1 332.71 346.71 11.09 o 10 2 1 19.81 23.87 4.77 o 11 2 1 553.70 553.88 11.19 o 12 2 1 738.56 736.72 15.31 o 0 3 1 6629.19 6535.29 65.58 o 1 3 1 16337.18 16048.95 84.73 o 2 3 1 42.23 19.93 2.82 o 3 3 1 7022.70 7005.87 46.17 o 4 3 1 1591.65 1549.22 20.37 o 5 3 1 1793.91 1922.15 20.14 o 6 3 1 47.94 47.46 3.32 o 7 3 1 3412.09 3412.37 29.32 o 8 3 1 412.11 380.22 8.05 o 9 3 1 5086.45 4968.25 41.63 o 10 3 1 454.34 437.19 9.89 o 11 3 1 1703.97 1692.07 20.58 o 12 3 1 27.38 34.78 5.86 o 1 4 1 2673.45 2665.04 16.08 o 2 4 1 691.16 655.04 10.10 o 3 4 1 3388.84 3343.56 22.83 o 4 4 1 21.90 16.53 2.93 o 5 4 1 1383.12 1385.05 17.03 o 6 4 1 149.05 161.26 6.52 o 7 4 1 3377.85 3362.81 30.03 o 8 4 1 9.18 18.99 8.11 o 9 4 1 117.57 120.18 6.16 o 10 4 1 4.65 -0.39 6.90 o 11 4 1 49.02 69.35 6.39 o 12 4 1 0.14 7.20 5.42 o 0 5 1 287.92 277.20 6.31 o 1 5 1 13895.60 13598.80 69.23 o 2 5 1 307.13 293.55 6.11 o 3 5 1 3544.78 3610.51 25.22 o 4 5 1 1761.26 1702.06 17.86 o 5 5 1 407.81 389.43 11.77 o 6 5 1 452.84 451.16 9.07 o 7 5 1 3098.18 3124.59 54.48 o 8 5 1 0.38 12.19 3.90 o 9 5 1 5534.55 5284.50 46.21 o 10 5 1 1.18 1.13 4.45 o 11 5 1 1284.25 1205.29 18.21 o 1 6 1 11.43 13.07 2.05 o 2 6 1 1342.50 1313.05 10.77 o 3 6 1 10.89 8.48 2.37 o 4 6 1 594.03 621.37 12.75 o 5 6 1 23.25 47.34 7.63 o 6 6 1 133.83 143.00 6.57 o 7 6 1 871.62 837.20 21.62 o 8 6 1 312.16 320.92 9.32 o 9 6 1 307.06 291.89 9.48 o 10 6 1 131.48 127.23 7.75 o 11 6 1 18.37 13.91 5.86 o 0 7 1 352.03 354.69 8.32 o 1 7 1 3121.06 3126.66 20.73 o 2 7 1 317.74 339.71 6.69 o 3 7 1 4758.60 4686.41 36.78 o 4 7 1 2801.27 2576.80 26.79 o 5 7 1 4952.20 4878.75 43.56 o 6 7 1 888.74 805.71 14.06 o 7 7 1 2428.97 2356.48 38.82 o 8 7 1 3.90 1.84 5.15 o 9 7 1 696.64 671.18 14.13 o 10 7 1 68.98 71.14 7.03 o 1 8 1 1155.50 1154.64 18.93 o 2 8 1 910.05 919.74 11.78 o 3 8 1 1817.79 1741.90 19.11 o 4 8 1 16.42 22.92 4.52 o 5 8 1 11.45 15.80 4.63 o 6 8 1 37.32 39.87 5.47 o 7 8 1 209.33 204.14 9.26 o 8 8 1 40.50 39.43 6.87 o 9 8 1 302.14 303.63 11.44 o 10 8 1 86.72 93.88 10.41 o 0 9 1 1004.63 999.75 20.53 o 1 9 1 830.78 821.11 10.84 o 2 9 1 570.82 560.05 11.07 o 3 9 1 4520.06 4521.19 43.14 o 4 9 1 86.52 85.33 6.73 o 5 9 1 6033.18 5998.85 54.60 o 6 9 1 152.53 153.43 8.84 o 7 9 1 1244.27 1207.60 19.95 o 8 9 1 323.78 318.62 19.01 o 9 9 1 62.71 55.37 7.42 o 1 10 1 12.19 11.86 4.37 o 2 10 1 245.86 252.03 9.85 o 3 10 1 337.05 341.72 11.20 o 4 10 1 70.70 81.34 8.08 o 5 10 1 168.29 172.12 9.59 o 6 10 1 279.24 295.01 11.77 o 7 10 1 22.62 32.56 8.04 o 8 10 1 492.32 482.69 14.66 o 0 11 1 1829.84 1852.45 51.23 o 1 11 1 2110.14 2079.43 27.30 o 2 11 1 515.56 523.44 18.97 o 3 11 1 1331.48 1341.31 21.99 o 4 11 1 3.12 9.37 6.23 o 5 11 1 1008.29 1033.67 20.14 o 6 11 1 5.50 3.27 6.30 o 7 11 1 868.48 869.61 24.47 o 1 12 1 228.82 255.49 24.94 o 2 12 1 386.78 456.26 16.71 o 3 12 1 235.10 266.37 14.48 o 4 12 1 7.27 11.53 6.99 o 5 12 1 231.14 241.35 12.87 o 0 0 2 19632.90 20035.17 277.06 o 2 0 2 19201.61 18482.86 281.78 o 4 0 2 8230.93 9130.80 132.80 o 6 0 2 11094.65 11638.48 172.57 o 8 0 2 2434.53 2478.70 51.23 o 10 0 2 6699.55 6883.32 117.29 o 12 0 2 113.08 115.48 9.59 o 1 1 2 10992.99 11486.02 67.43 o 2 1 2 5469.08 5779.66 34.54 o 3 1 2 401.21 420.08 5.70 o 4 1 2 85.91 90.65 3.87 o 5 1 2 3836.02 4018.74 47.90 o 6 1 2 1348.12 1390.46 43.14 o 7 1 2 3702.90 4003.90 50.29 o 8 1 2 623.11 598.63 16.21 o 9 1 2 1184.03 1192.18 16.93 o 10 1 2 8.59 21.44 4.42 o 11 1 2 1.70 5.11 4.04 o 12 1 2 6.53 7.12 7.67 o 0 2 2 32097.58 31022.59 245.58 o 2 2 2 356.14 333.96 5.27 o 3 2 2 306.09 250.71 6.37 o 4 2 2 17783.77 18288.72 96.20 o 5 2 2 5066.87 5056.36 60.71 o 6 2 2 426.41 443.73 7.39 o 7 2 2 880.05 880.98 13.08 o 8 2 2 8162.01 8464.74 71.90 o 9 2 2 1157.66 1133.48 13.62 o 10 2 2 388.32 383.54 10.87 o 11 2 2 227.68 217.84 8.47 o 12 2 2 2720.42 2617.24 30.49 o 1 3 2 2198.54 2293.57 16.37 o 2 3 2 2824.30 2729.92 18.93 o 3 3 2 13262.38 13782.03 80.16 o 4 3 2 995.79 1064.08 10.15 o 5 3 2 964.00 978.53 10.42 o 6 3 2 4.85 18.54 2.72 o 7 3 2 303.83 293.97 6.69 o 8 3 2 59.64 70.76 5.15 o 9 3 2 525.11 541.34 9.84 o 10 3 2 916.57 872.19 13.23 o 11 3 2 2696.18 2633.77 27.74 o 12 3 2 939.45 863.35 14.63 o 0 4 2 3115.45 3053.04 26.03 o 1 4 2 289.03 335.77 4.82 o 2 4 2 27767.98 27572.08 190.48 o 3 4 2 704.06 745.69 8.32 o 4 4 2 12382.02 12570.40 77.78 o 5 4 2 791.29 752.42 10.63 o 6 4 2 13833.59 14092.70 102.83 o 7 4 2 104.52 110.53 5.37 o 8 4 2 45.35 66.56 4.84 o 9 4 2 7.78 7.11 3.88 o 10 4 2 2715.47 2568.42 26.91 o 11 4 2 29.92 42.11 7.14 o 12 4 2 176.22 171.24 8.63 o 1 5 2 1381.53 1359.28 11.30 o 2 5 2 5903.07 5675.38 43.17 o 3 5 2 4911.73 4917.35 36.11 o 4 5 2 952.66 887.65 12.14 o 5 5 2 2629.09 2713.85 26.15 o 6 5 2 42.60 49.00 4.28 o 7 5 2 244.98 240.33 7.79 o 8 5 2 219.51 231.12 8.17 o 9 5 2 947.46 887.59 14.42 o 10 5 2 1021.15 959.62 15.70 o 11 5 2 648.77 610.57 13.14 o 0 6 2 14038.70 13833.98 117.14 o 1 6 2 552.08 545.15 7.19 o 2 6 2 1185.64 1140.79 10.96 o 3 6 2 61.37 57.31 3.78 o 4 6 2 15503.78 15538.75 114.17 o 5 6 2 634.93 587.73 11.08 o 6 6 2 767.50 778.73 13.09 o 7 6 2 35.81 37.47 4.93 o 8 6 2 4763.95 4570.79 42.27 o 9 6 2 1499.95 1388.52 26.66 o 10 6 2 25.30 29.61 5.82 o 11 6 2 388.60 354.54 12.45 o 1 7 2 3204.05 3156.35 27.63 o 2 7 2 40.72 56.13 3.82 o 3 7 2 44.26 38.06 3.57 o 4 7 2 0.55 5.50 4.14 o 5 7 2 1732.40 1721.05 21.30 o 6 7 2 604.84 576.62 12.21 o 7 7 2 2958.49 2960.14 35.12 o 8 7 2 549.47 523.50 12.60 o 9 7 2 289.09 308.95 10.47 o 10 7 2 82.39 83.44 7.88 o 0 8 2 4229.37 4000.53 36.97 o 1 8 2 476.85 463.92 8.57 o 2 8 2 7922.35 7772.31 51.92 o 3 8 2 39.49 48.60 7.54 o 4 8 2 754.47 757.16 16.21 o 5 8 2 31.41 41.38 5.93 o 6 8 2 3833.24 3683.21 37.48 o 7 8 2 233.13 224.28 9.65 o 8 8 2 1000.10 984.78 21.11 o 9 8 2 472.40 435.84 14.59 o 1 9 2 1867.75 1808.19 18.70 o 2 9 2 1789.49 1722.11 20.20 o 3 9 2 465.20 471.08 14.63 o 4 9 2 7.84 13.81 5.64 o 5 9 2 566.20 563.87 16.12 o 6 9 2 745.24 750.58 15.75 o 7 9 2 552.04 536.90 13.97 o 8 9 2 227.41 226.70 15.67 o 9 9 2 518.83 533.76 14.80 o 0 10 2 6662.09 6739.53 84.37 o 1 10 2 122.25 125.35 7.11 o 2 10 2 106.82 128.87 11.13 o 3 10 2 555.40 574.25 30.01 o 4 10 2 2374.33 2269.51 33.34 o 5 10 2 1565.05 1534.90 24.03 o 6 10 2 25.35 31.76 6.54 o 7 10 2 468.54 476.86 14.37 o 8 10 2 2790.96 2768.58 34.86 o 1 11 2 224.11 241.03 12.71 o 2 11 2 8.49 11.17 8.33 o 3 11 2 2337.23 2410.88 44.09 o 4 11 2 55.69 64.65 7.66 o 5 11 2 100.69 122.34 9.52 o 6 11 2 5.87 1.26 6.62 o 0 12 2 140.56 150.33 20.90 o 1 12 2 206.13 238.11 17.14 o 2 12 2 2888.23 3057.80 52.91 o 3 12 2 899.93 918.39 22.82 o 4 12 2 1115.16 1148.54 25.81 o 1 0 3 2603.83 2339.62 36.12 o 3 0 3 5213.35 5244.82 46.42 o 5 0 3 381.25 400.18 11.89 o 7 0 3 1169.54 1213.39 33.71 o 9 0 3 256.09 275.04 20.22 o 11 0 3 1329.84 1220.14 41.12 o 0 1 3 5911.22 5662.19 49.29 o 1 1 3 1853.87 1773.87 13.38 o 2 1 3 194.89 248.43 4.27 o 3 1 3 6748.58 7026.00 46.70 o 4 1 3 539.42 553.44 5.31 o 5 1 3 11504.57 12069.93 102.60 o 6 1 3 23.06 27.04 5.72 o 7 1 3 3286.05 3492.14 51.91 o 8 1 3 293.01 290.32 13.82 o 9 1 3 304.42 309.43 14.78 o 10 1 3 141.78 128.96 7.05 o 11 1 3 1059.78 990.86 35.05 o 12 1 3 2.34 22.10 9.76 o 1 2 3 22.83 28.58 2.91 o 2 2 3 1348.06 1383.66 11.59 o 3 2 3 101.71 98.08 3.52 o 4 2 3 103.12 111.21 5.58 o 5 2 3 324.14 331.82 7.05 o 6 2 3 993.30 1035.00 14.64 o 7 2 3 56.11 73.08 4.86 o 8 2 3 1343.07 1411.18 19.30 o 9 2 3 277.64 301.49 10.61 o 10 2 3 12.43 21.04 5.18 o 11 2 3 347.75 356.98 19.30 o 12 2 3 379.62 407.43 19.55 o 0 3 3 6695.70 6704.93 50.72 o 1 3 3 13856.28 13936.75 85.64 o 2 3 3 947.48 933.57 9.51 o 3 3 3 6216.45 6143.66 39.05 o 4 3 3 503.08 471.02 7.29 o 5 3 3 1927.93 2029.96 17.85 o 6 3 3 10.30 17.57 2.98 o 7 3 3 3078.65 3118.94 28.15 o 8 3 3 321.38 302.51 13.04 o 9 3 3 4230.80 4188.29 36.73 o 10 3 3 423.38 404.52 9.16 o 11 3 3 1393.11 1400.30 22.96 o 1 4 3 1633.19 1564.50 13.02 o 2 4 3 283.97 260.91 5.24 o 3 4 3 1231.12 1186.63 11.66 o 4 4 3 66.47 55.84 3.29 o 5 4 3 1389.19 1378.96 16.13 o 6 4 3 225.02 249.69 9.24 o 7 4 3 3879.64 3869.58 34.73 o 8 4 3 47.55 57.36 4.84 o 9 4 3 243.41 229.07 8.09 o 10 4 3 23.67 27.16 4.72 o 11 4 3 1.06 15.42 5.03 o 0 5 3 171.86 158.46 5.68 o 1 5 3 14130.41 13688.55 75.59 o 2 5 3 51.43 53.03 3.47 o 3 5 3 4372.67 4331.79 30.54 o 4 5 3 1228.22 1211.67 12.67 o 5 5 3 767.80 758.49 12.27 o 6 5 3 215.36 220.99 7.43 o 7 5 3 2919.54 2929.03 29.30 o 8 5 3 0.74 2.25 4.04 o 9 5 3 4611.42 4581.45 42.23 o 10 5 3 2.72 6.03 4.99 o 11 5 3 995.05 971.68 16.59 o 1 6 3 45.56 45.02 3.05 o 2 6 3 840.37 828.40 13.06 o 3 6 3 2.01 10.22 2.81 o 4 6 3 226.97 246.05 7.10 o 5 6 3 162.57 168.50 7.36 o 6 6 3 280.56 292.11 10.99 o 7 6 3 872.77 846.67 14.72 o 8 6 3 463.85 470.59 11.56 o 9 6 3 468.40 450.71 18.78 o 10 6 3 32.42 28.43 5.99 o 0 7 3 980.12 907.91 16.34 o 1 7 3 2420.15 2349.78 20.40 o 2 7 3 47.13 59.36 4.02 o 3 7 3 3775.82 3687.73 28.75 o 4 7 3 1270.70 1245.46 15.85 o 5 7 3 3878.63 3827.05 37.30 o 6 7 3 564.95 545.99 12.58 o 7 7 3 1856.70 1830.49 23.80 o 8 7 3 3.48 2.55 4.97 o 9 7 3 546.68 534.56 13.42 o 10 7 3 35.73 39.64 6.68 o 1 8 3 666.43 671.44 11.56 o 2 8 3 529.05 550.03 9.72 o 3 8 3 1373.02 1307.75 16.82 o 4 8 3 1.44 -2.85 4.02 o 5 8 3 66.80 86.30 6.81 o 6 8 3 114.11 134.93 15.86 o 7 8 3 237.75 243.28 10.64 o 8 8 3 0.48 10.29 5.93 o 9 8 3 112.23 115.82 8.80 o 0 9 3 804.77 814.00 39.10 o 1 9 3 308.62 305.32 9.04 o 2 9 3 328.89 327.70 11.99 o 3 9 3 2801.26 2776.65 30.34 o 4 9 3 101.75 102.18 7.57 o 5 9 3 4212.11 4345.56 43.98 o 6 9 3 87.03 103.91 8.16 o 7 9 3 874.00 860.95 25.46 o 8 9 3 342.23 356.22 12.85 o 1 10 3 17.29 17.10 5.47 o 2 10 3 180.45 192.86 9.73 o 3 10 3 135.41 134.83 10.24 o 4 10 3 36.06 29.75 6.48 o 5 10 3 73.14 72.64 7.73 o 6 10 3 305.48 312.28 12.88 o 7 10 3 113.86 113.28 16.35 o 0 11 3 1914.91 1931.27 38.85 o 1 11 3 1561.16 1577.78 28.28 o 2 11 3 797.08 822.96 25.26 o 3 11 3 957.41 1040.84 41.32 o 4 11 3 3.86 4.65 7.50 o 5 11 3 792.43 856.06 22.04 o 1 12 3 231.24 258.40 18.09 o 2 12 3 252.68 254.39 25.95 o 3 12 3 152.84 170.89 32.36 o 0 0 4 66657.42 66996.06 646.36 o 2 0 4 1721.27 1677.21 19.79 o 4 0 4 4063.14 4081.49 39.34 o 6 0 4 447.93 445.67 10.12 o 8 0 4 11033.96 10805.28 173.92 o 10 0 4 523.11 620.85 31.01 o 1 1 4 1835.11 1736.44 14.21 o 2 1 4 1523.66 1445.49 12.71 o 3 1 4 5605.66 5603.60 36.41 o 4 1 4 125.66 121.14 4.15 o 5 1 4 2525.67 2663.83 20.05 o 6 1 4 2322.51 2422.11 40.96 o 7 1 4 30.31 34.52 4.35 o 8 1 4 1212.08 1245.06 17.64 o 9 1 4 1129.07 1166.54 27.65 o 10 1 4 181.70 173.87 14.28 o 11 1 4 1055.98 1083.08 29.31 o 0 2 4 1297.74 1238.47 13.62 o 1 2 4 844.54 748.46 8.47 o 2 2 4 17836.90 17927.19 104.57 o 3 2 4 166.39 204.29 4.98 o 4 2 4 448.57 442.34 8.39 o 5 2 4 1349.89 1340.13 12.73 o 6 2 4 9117.37 9641.32 72.83 o 7 2 4 272.11 296.38 13.72 o 8 2 4 341.77 365.88 11.40 o 9 2 4 887.17 882.14 16.14 o 10 2 4 3734.77 3708.15 41.53 o 11 2 4 68.69 83.84 19.89 o 1 3 4 3980.43 3946.43 32.64 o 2 3 4 1236.47 1145.36 11.49 o 3 3 4 476.91 488.34 7.45 o 4 3 4 321.82 355.26 8.24 o 5 3 4 1246.12 1306.86 14.17 o 6 3 4 54.70 71.27 6.81 o 7 3 4 4395.38 4604.98 63.00 o 8 3 4 4.15 3.42 3.64 o 9 3 4 265.62 257.15 7.95 o 10 3 4 382.37 400.50 12.56 o 11 3 4 9.19 21.64 6.66 o 0 4 4 1127.98 1092.05 13.53 o 1 4 4 3.35 3.82 2.20 o 2 4 4 119.79 122.94 5.83 o 3 4 4 64.04 75.57 3.91 o 4 4 4 22496.59 22744.46 132.86 o 5 4 4 313.85 303.66 11.16 o 6 4 4 473.40 509.72 10.28 o 7 4 4 29.66 33.31 4.44 o 8 4 4 2174.14 2216.88 24.32 o 9 4 4 0.44 -0.34 4.53 o 10 4 4 17.10 16.85 4.97 o 11 4 4 33.54 27.31 7.51 o 1 5 4 3190.30 3154.96 24.25 o 2 5 4 2505.43 2384.25 20.03 o 3 5 4 715.40 747.62 12.91 o 4 5 4 68.77 65.81 4.22 o 5 5 4 669.23 670.64 12.55 o 6 5 4 400.72 407.69 10.10 o 7 5 4 2133.59 2130.71 24.40 o 8 5 4 17.00 18.43 6.71 o 9 5 4 252.49 275.89 10.31 o 10 5 4 335.44 324.36 10.59 o 0 6 4 13.43 45.75 28.31 o 1 6 4 1578.27 1550.96 17.12 o 2 6 4 8283.86 8053.08 68.53 o 3 6 4 505.29 503.50 8.93 o 4 6 4 633.74 648.48 13.21 o 5 6 4 142.22 131.24 7.12 o 6 6 4 5928.48 6048.46 53.15 o 7 6 4 13.10 18.05 5.13 o 8 6 4 133.61 122.04 7.77 o 9 6 4 1059.19 1064.00 27.15 o 10 6 4 2023.89 1961.94 25.78 o 1 7 4 780.73 783.63 12.41 o 2 7 4 62.99 59.87 4.47 o 3 7 4 2507.84 2468.86 22.37 o 4 7 4 0.68 4.78 3.84 o 5 7 4 1328.46 1311.07 19.39 o 6 7 4 312.08 309.83 10.62 o 7 7 4 132.44 155.52 8.79 o 8 7 4 455.24 464.45 12.99 o 9 7 4 1378.11 1356.17 21.54 o 0 8 4 16530.51 15790.36 170.17 o 1 8 4 1152.96 1089.35 17.44 o 2 8 4 595.49 614.40 11.88 o 3 8 4 285.23 297.40 9.09 o 4 8 4 1811.44 1786.41 23.75 o 5 8 4 28.78 37.55 5.96 o 6 8 4 100.37 104.38 8.05 o 7 8 4 173.29 180.49 13.23 o 8 8 4 5107.31 5229.45 51.52 o 1 9 4 352.50 349.96 11.37 o 2 9 4 873.98 853.14 19.65 o 3 9 4 1400.24 1355.73 21.23 o 4 9 4 21.11 22.31 6.74 o 5 9 4 501.10 530.57 24.91 o 6 9 4 1327.33 1326.68 21.93 o 7 9 4 594.24 618.09 15.84 o 0 10 4 1175.46 1217.07 29.55 o 1 10 4 15.28 11.71 6.74 o 2 10 4 4846.00 4962.61 57.60 o 3 10 4 302.45 311.90 16.88 o 4 10 4 36.63 45.61 11.18 o 5 10 4 812.38 785.74 20.72 o 6 10 4 2434.07 2421.97 32.34 o 1 11 4 887.31 916.99 22.05 o 2 11 4 21.83 15.57 12.13 o 3 11 4 21.59 13.02 15.50 o 4 11 4 160.49 168.26 15.49 o 1 0 5 1948.07 1758.17 21.77 o 3 0 5 3215.80 3190.54 34.16 o 5 0 5 101.81 114.14 6.88 o 7 0 5 202.60 233.50 17.86 o 9 0 5 862.03 827.13 35.05 o 11 0 5 1496.17 1418.32 49.88 o 0 1 5 522.95 471.20 12.87 o 1 1 5 3628.39 3456.41 25.12 o 2 1 5 1.40 7.90 2.49 o 3 1 5 7161.13 7152.30 46.38 o 4 1 5 1139.49 1128.39 12.41 o 5 1 5 8922.69 9344.39 59.23 o 6 1 5 45.28 52.71 4.44 o 7 1 5 2614.60 2789.27 26.88 o 8 1 5 47.64 50.72 6.32 o 9 1 5 248.48 261.75 9.81 o 10 1 5 184.16 198.94 16.21 o 1 2 5 0.65 7.41 2.40 o 2 2 5 1424.35 1426.75 13.86 o 3 2 5 290.55 275.55 6.37 o 4 2 5 453.06 469.41 7.99 o 5 2 5 154.91 152.46 5.42 o 6 2 5 90.62 100.64 8.13 o 7 2 5 198.63 216.97 7.42 o 8 2 5 210.83 246.97 8.76 o 9 2 5 182.32 172.71 7.17 o 10 2 5 74.83 57.58 11.89 o 0 3 5 1356.88 1282.74 23.36 o 1 3 5 5858.41 5778.42 42.68 o 2 3 5 34.70 33.71 3.29 o 3 3 5 2474.40 2394.86 22.26 o 4 3 5 697.90 670.54 9.70 o 5 3 5 854.63 881.50 12.29 o 6 3 5 122.28 120.86 6.38 o 7 3 5 1785.43 1788.31 36.84 o 8 3 5 224.87 231.48 8.50 o 9 3 5 2713.57 2789.42 31.97 o 10 3 5 242.73 229.98 11.57 o 1 4 5 625.19 617.81 10.12 o 2 4 5 215.46 215.74 6.18 o 3 4 5 1530.01 1489.43 15.19 o 4 4 5 0.15 0.21 3.03 o 5 4 5 399.22 396.66 9.85 o 6 4 5 25.38 26.94 4.79 o 7 4 5 1131.68 1153.31 17.18 o 8 4 5 0.56 5.79 4.57 o 9 4 5 35.42 50.75 7.74 o 10 4 5 0.17 1.19 5.14 o 0 5 5 55.79 57.39 7.38 o 1 5 5 4839.06 4708.78 50.11 o 2 5 5 248.86 258.19 8.63 o 3 5 5 1192.48 1196.03 13.92 o 4 5 5 665.97 679.57 10.64 o 5 5 5 155.03 160.49 7.83 o 6 5 5 379.50 380.64 10.65 o 7 5 5 1505.23 1575.43 21.45 o 8 5 5 0.30 5.78 5.19 o 9 5 5 3132.30 3250.92 34.96 o 1 6 5 7.64 7.67 4.27 o 2 6 5 777.01 716.53 12.05 o 3 6 5 6.47 10.15 4.17 o 4 6 5 375.71 390.20 9.73 o 5 6 5 2.58 0.46 4.61 o 6 6 5 22.65 24.25 5.59 o 7 6 5 388.73 403.55 12.00 o 8 6 5 65.94 81.56 7.61 o 9 6 5 70.11 78.59 7.84 o 0 7 5 1.47 1.01 6.20 o 1 7 5 1592.86 1574.42 21.49 o 2 7 5 314.79 330.74 10.35 o 3 7 5 2637.40 2582.58 26.40 o 4 7 5 2015.45 1946.31 22.47 o 5 7 5 2696.69 2772.48 31.71 o 6 7 5 550.24 545.34 15.57 o 7 7 5 1353.03 1414.65 24.52 o 8 7 5 18.47 28.87 6.97 o 1 8 5 642.35 614.59 14.06 o 2 8 5 478.38 462.43 12.63 o 3 8 5 879.34 879.23 21.72 o 4 8 5 43.55 54.59 7.76 o 5 8 5 8.01 4.37 6.39 o 6 8 5 0.00 10.29 6.05 o 7 8 5 97.04 100.62 8.98 o 0 9 5 466.94 474.93 19.27 o 1 9 5 788.09 791.15 18.97 o 2 9 5 441.37 423.71 14.68 o 3 9 5 2993.68 3022.59 40.99 o 4 9 5 49.35 63.67 10.72 o 5 9 5 3873.91 4001.07 65.68 o 6 9 5 105.76 117.51 10.90 o 1 10 5 6.34 -2.45 6.20 o 2 10 5 162.26 174.81 12.32 o 3 10 5 330.04 336.91 24.27 o 4 10 5 50.28 57.92 11.41 o 5 10 5 125.20 140.98 14.30 o 0 11 5 909.84 958.27 32.02 o 1 11 5 1423.53 1445.28 29.05 o 2 11 5 138.79 136.19 15.01 o 0 0 6 5627.42 5518.92 94.38 o 2 0 6 8926.24 8807.14 101.45 o 4 0 6 798.21 846.54 16.16 o 6 0 6 4807.93 4786.20 60.64 o 8 0 6 1077.82 1134.16 30.00 o 10 0 6 3503.53 3769.61 88.98 o 1 1 6 2540.48 2505.08 33.47 o 2 1 6 921.20 864.18 13.79 o 3 1 6 252.45 251.07 6.65 o 4 1 6 2.36 1.52 3.28 o 5 1 6 1109.74 1148.78 13.74 o 6 1 6 785.51 788.20 13.62 o 7 1 6 1810.68 1903.70 22.53 o 8 1 6 403.38 405.42 17.51 o 9 1 6 417.38 420.72 11.36 o 10 1 6 27.21 39.50 12.81 o 0 2 6 10254.12 9820.83 109.16 o 1 2 6 40.91 27.27 4.44 o 2 2 6 352.81 356.06 9.41 o 3 2 6 33.35 34.40 4.07 o 4 2 6 6642.74 6648.99 45.72 o 5 2 6 1183.68 1202.82 15.44 o 6 2 6 232.64 250.12 8.90 o 7 2 6 184.14 189.97 8.41 o 8 2 6 3786.73 3936.95 38.01 o 9 2 6 539.71 556.93 12.15 o 1 3 6 681.79 652.38 12.55 o 2 3 6 757.00 752.65 17.22 o 3 3 6 3461.69 3496.62 30.71 o 4 3 6 223.43 238.10 8.79 o 5 3 6 608.64 624.75 11.51 o 6 3 6 2.39 7.54 4.74 o 7 3 6 58.22 62.38 6.25 o 8 3 6 17.54 25.08 5.72 o 9 3 6 457.89 488.10 16.83 o 0 4 6 755.35 733.45 19.07 o 1 4 6 40.79 43.54 5.20 o 2 4 6 7674.10 7492.64 62.76 o 3 4 6 140.29 148.85 7.65 o 4 4 6 3243.83 3278.30 29.98 o 5 4 6 228.91 247.22 12.36 o 6 4 6 5525.90 5767.58 58.68 o 7 4 6 45.21 60.96 6.61 o 8 4 6 39.44 55.27 8.95 o 9 4 6 4.57 8.64 6.11 o 1 5 6 588.45 579.91 12.89 o 2 5 6 1580.13 1504.10 21.70 o 3 5 6 1650.01 1615.31 21.71 o 4 5 6 215.10 209.93 8.26 o 5 5 6 1054.61 1074.81 17.59 o 6 5 6 72.79 76.31 7.49 o 7 5 6 105.87 112.88 8.18 o 8 5 6 38.98 48.11 7.39 o 0 6 6 4743.72 4591.23 62.68 o 1 6 6 531.75 526.05 12.80 o 2 6 6 338.40 332.31 10.78 o 3 6 6 78.80 79.83 6.94 o 4 6 6 6176.17 6203.00 64.32 o 5 6 6 138.25 128.31 9.64 o 6 6 6 251.54 286.15 11.45 o 7 6 6 2.35 -4.31 6.02 o 8 6 6 2349.69 2496.98 81.85 o 1 7 6 1246.75 1219.73 19.97 o 2 7 6 27.02 33.01 6.30 o 3 7 6 73.92 65.92 6.95 o 4 7 6 0.90 12.28 7.85 o 5 7 6 611.87 639.06 20.96 o 6 7 6 311.15 319.74 13.82 o 7 7 6 1835.24 1895.64 64.84 o 0 8 6 1971.05 1900.28 37.66 o 1 8 6 320.99 297.17 11.71 o 2 8 6 4131.57 4166.12 69.28 o 3 8 6 78.66 84.63 9.47 o 4 8 6 225.29 237.09 17.86 o 5 8 6 2.68 25.96 13.48 o 6 8 6 2107.22 2087.40 39.75 o 1 9 6 860.63 897.83 18.79 o 2 9 6 705.21 711.44 17.01 o 3 9 6 248.66 268.58 17.39 o 4 9 6 0.67 1.43 9.29 o 0 10 6 3926.32 4023.54 146.28 o 1 10 6 26.22 32.13 7.98 o 2 10 6 86.84 94.68 11.29 o 1 0 7 288.18 259.42 12.84 o 3 0 7 1119.98 1081.48 24.46 o 5 0 7 142.28 165.16 15.50 o 7 0 7 434.51 461.29 17.08 o 0 1 7 1338.16 1223.76 25.98 o 1 1 7 598.50 562.20 12.38 o 2 1 7 54.71 60.33 6.05 o 3 1 7 2085.96 2041.52 24.73 o 4 1 7 35.15 28.20 5.43 o 5 1 7 3380.57 3441.29 68.08 o 6 1 7 19.10 21.84 5.77 o 7 1 7 1098.07 1163.42 28.31 o 8 1 7 139.61 154.66 8.58 o 1 2 7 32.11 30.78 5.22 o 2 2 7 379.63 409.99 11.33 o 3 2 7 10.22 13.80 5.03 o 4 2 7 4.35 10.36 4.97 o 5 2 7 123.79 100.73 9.76 o 6 2 7 477.67 505.59 14.13 o 7 2 7 6.31 10.61 5.75 o 8 2 7 580.40 630.91 14.30 o 0 3 7 1502.16 1420.69 29.08 o 1 3 7 4207.87 4083.55 40.44 o 2 3 7 470.04 452.80 11.83 o 3 3 7 1921.41 1865.17 24.07 o 4 3 7 98.65 99.52 7.46 o 5 3 7 785.11 800.39 20.50 o 6 3 7 23.95 31.80 7.03 o 7 3 7 1286.65 1325.23 35.49 o 8 3 7 93.25 97.11 8.15 o 1 4 7 371.71 336.90 10.95 o 2 4 7 40.94 35.92 5.86 o 3 4 7 159.47 168.27 9.01 o 4 4 7 27.57 13.89 5.79 o 5 4 7 403.61 406.59 31.01 o 6 4 7 96.54 105.46 10.72 o 7 4 7 1798.28 1831.32 28.35 o 0 5 7 7.02 13.30 7.85 o 1 5 7 4851.46 4800.67 46.93 o 2 5 7 2.21 -3.24 7.10 o 3 5 7 1732.22 1721.14 24.23 o 4 5 7 397.14 394.63 14.12 o 5 5 7 403.38 401.46 16.66 o 6 5 7 60.79 62.27 16.18 o 7 5 7 1239.45 1234.01 49.88 o 1 6 7 26.78 25.63 6.29 o 2 6 7 283.19 302.64 11.36 o 3 6 7 2.19 5.60 6.08 o 4 6 7 42.54 50.60 9.98 o 5 6 7 148.17 155.32 13.35 o 6 6 7 163.81 176.41 13.80 o 0 7 7 508.83 526.50 20.50 o 1 7 7 880.55 882.18 18.19 o 2 7 7 10.51 20.60 6.85 o 3 7 7 1525.71 1469.61 27.49 o 4 7 7 306.99 325.34 17.87 o 5 7 7 1528.12 1496.24 33.11 o 1 8 7 161.06 163.23 10.92 o 2 8 7 140.99 144.18 10.34 o 3 8 7 539.63 558.10 20.03 o 0 0 8 11372.27 11213.79 182.68 o 2 0 8 197.59 202.61 14.28 o 4 0 8 1059.08 1029.75 25.82 o 6 0 8 38.35 47.86 12.81 o 1 1 8 442.99 407.85 12.11 o 2 1 8 384.70 377.59 12.29 o 3 1 8 1538.45 1475.70 30.04 o 4 1 8 7.68 10.15 6.06 o 5 1 8 530.60 546.68 18.59 o 6 1 8 496.40 461.76 17.14 o 0 2 8 309.92 287.10 15.49 o 1 2 8 43.15 50.78 9.54 o 2 2 8 4445.33 4328.21 44.22 o 3 2 8 17.41 25.18 6.64 o 4 2 8 103.62 102.53 9.55 o 5 2 8 567.69 567.29 19.05 o 6 2 8 2910.92 2882.42 45.04 o 1 3 8 1078.56 1063.04 19.13 o 2 3 8 364.84 373.00 15.18 o 3 3 8 91.72 85.30 8.16 o 4 3 8 109.56 109.75 8.80 o 5 3 8 643.26 674.43 21.45 o 6 3 8 6.44 9.62 8.81 o 0 4 8 1031.24 1004.34 26.93 o 1 4 8 12.31 8.35 6.17 o 2 4 8 155.72 148.72 9.66 o 3 4 8 41.32 45.99 7.32 o 4 4 8 7243.40 7240.16 75.58 o 5 4 8 127.04 124.13 12.39 o 1 5 8 868.22 873.60 18.20 o 2 5 8 776.01 745.17 17.09 o 3 5 8 251.07 231.29 11.59 o 4 5 8 65.37 64.89 11.44 o 5 5 8 334.57 360.33 18.11 o 0 6 8 13.86 17.17 10.79 o 1 6 8 286.35 290.73 18.58 o 2 6 8 3088.26 3146.08 43.98 o 3 6 8 47.69 54.75 8.32 o 1 7 8 268.37 269.17 13.14 o 1 0 9 406.09 427.21 28.31 o 3 0 9 586.29 572.85 22.07 o 0 1 9 51.87 58.67 11.80 o 1 1 9 882.45 854.77 18.36 o 2 1 9 4.41 7.82 6.65 o 3 1 9 1822.65 1792.83 38.05 o 4 1 9 288.53 278.59 24.94 o 1 2 9 3.00 8.89 6.70 o 2 2 9 369.28 398.39 13.79 o 3 2 9 107.42 102.50 9.39 o 0 3 9 326.75 389.63 27.64 o 1 3 9 1484.79 1490.57 28.78 o 2 3 9 20.79 9.48 7.24 o 3 3 9 603.44 607.53 19.31 o 1 4 9 81.21 64.84 11.62 o