#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:33:07 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181251 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/29/2232986.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232986_Fobs loop_ _publ_author_name 'Warsink, Stefan' 'Roodt, Andreas' _publ_section_title ; trans-Carbonylchloridobis[tris(4-methoxyphenyl)phosphane-\kP]rhodium(I) ; _journal_coeditor_code WM2548 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1695 _journal_page_last m1696 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 90.995 _cell_angle_beta 99.591 _cell_angle_gamma 101.220 _cell_length_a 7.8350 _cell_length_b 12.3150 _cell_length_c 21.0590 _exptl_crystal_F_000 896.00 _reflns_d_resolution_high 0.7569 _cod_data_source_file wm2548Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 11Ssw2_0m in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 200.69 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 13564.61 15439.42 1162.92 o 3 0 0 1094.36 1134.74 83.25 o 4 0 0 1478.08 1207.17 63.65 o 5 0 0 3981.10 3321.75 212.76 o 6 0 0 1337.54 1185.30 98.88 o 7 0 0 28.69 28.04 24.21 o 8 0 0 6.03 -9.69 19.37 o 9 0 0 15.24 -1.37 28.45 o -10 1 0 6.45 -15.13 24.21 o -9 1 0 23.25 14.26 16.72 o -8 1 0 178.64 161.47 21.79 o -7 1 0 11.83 2.02 10.71 o -6 1 0 164.76 162.01 16.12 o -5 1 0 88.34 40.46 41.36 o -2 1 0 1248.26 1102.99 87.17 o -1 1 0 539.22 640.62 22.58 o 1 1 0 18534.32 16255.99 458.50 o 2 1 0 134.24 98.47 32.31 o 3 1 0 106.75 86.60 17.66 o 4 1 0 3142.68 2874.46 118.18 o 5 1 0 17.20 6.74 23.83 o 6 1 0 32.29 26.75 13.90 o 7 1 0 279.02 260.38 40.26 o 8 1 0 130.83 111.39 27.85 o 9 1 0 264.10 275.44 41.77 o -10 2 0 463.26 446.16 50.85 o -9 2 0 260.97 304.50 37.53 o -8 2 0 183.70 186.90 22.17 o -7 2 0 1711.84 1604.69 62.61 o -6 2 0 4295.68 4021.01 148.62 o -5 2 0 8256.88 8095.90 290.60 o -4 2 0 1249.78 877.18 79.91 o -3 2 0 2580.18 2420.81 88.97 o -2 2 0 12622.25 14750.23 473.69 o -1 2 0 35871.43 43900.91 1121.99 o 0 2 0 2550.77 2195.55 59.66 o 1 2 0 180.60 128.14 19.30 o 2 2 0 2013.19 1624.71 48.15 o 3 2 0 1563.21 1252.73 40.00 o 4 2 0 6717.61 5746.37 220.27 o 5 2 0 297.85 231.43 23.23 o 6 2 0 1726.72 1575.42 151.59 o 7 2 0 356.30 360.80 41.17 o 8 2 0 630.29 592.05 59.33 o 9 2 0 654.95 799.09 72.64 o -10 3 0 841.15 852.36 73.86 o -9 3 0 0.30 18.77 19.98 o -8 3 0 178.28 224.93 35.72 o -7 3 0 1015.12 956.49 44.51 o -6 3 0 375.04 348.33 22.08 o -5 3 0 317.77 274.63 20.74 o -4 3 0 162.49 165.90 12.72 o -3 3 0 2602.74 2849.89 96.65 o -2 3 0 25259.02 31830.27 744.84 o -1 3 0 25.94 34.62 13.94 o 0 3 0 585.10 424.97 33.30 o 1 3 0 4757.79 4055.13 136.14 o 2 3 0 1687.49 1546.65 54.46 o 3 3 0 657.36 575.03 28.84 o 4 3 0 62.95 1.91 32.42 o 5 3 0 2438.10 2180.38 107.40 o 6 3 0 610.40 496.33 40.37 o 7 3 0 16.91 -12.71 16.95 o 8 3 0 70.40 79.91 28.45 o 9 3 0 91.97 99.89 32.08 o -10 4 0 910.21 1079.38 87.17 o -9 4 0 1205.77 1271.28 93.83 o -8 4 0 1304.27 1311.02 77.42 o -7 4 0 2.90 -18.22 9.11 o -6 4 0 713.35 753.46 46.29 o -5 4 0 3753.85 3987.96 132.07 o -4 4 0 391.19 256.24 19.78 o -3 4 0 20691.85 24107.87 623.79 o -2 4 0 52.19 29.64 12.15 o -1 4 0 4672.26 4784.48 118.06 o 0 4 0 1035.18 957.79 57.59 o 1 4 0 14572.21 12102.01 305.93 o 2 4 0 10879.30 8945.45 318.22 o 3 4 0 1881.29 1453.10 57.04 o 4 4 0 770.79 641.79 46.82 o 5 4 0 218.55 190.32 25.22 o 6 4 0 4640.55 4301.17 265.76 o 7 4 0 1061.11 1174.42 90.20 o 8 4 0 1300.43 1542.49 114.42 o 9 4 0 282.30 280.89 47.82 o -10 5 0 0.01 -27.24 25.43 o -9 5 0 0.11 10.80 24.18 o -8 5 0 743.49 728.36 57.46 o -7 5 0 738.05 689.83 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577.82 590.61 82.40 o -6 11 0 0.91 6.84 45.51 o -5 11 0 73.50 29.56 47.42 o -4 11 0 378.66 285.38 68.10 o -3 11 0 1.79 144.72 62.86 o -2 11 0 790.55 951.90 134.56 o -1 11 0 892.47 967.12 50.56 o 0 11 0 1.12 4.08 173.18 o 1 11 0 743.06 768.35 123.50 o 2 11 0 14.89 -20.16 222.41 o 3 11 0 4.58 41.21 58.72 o 4 11 0 234.67 225.80 45.40 o 5 11 0 192.30 183.43 44.80 o -8 12 0 558.95 519.74 178.89 o -7 12 0 428.42 407.62 80.66 o -6 12 0 358.78 308.05 75.34 o -5 12 0 885.93 845.56 177.37 o -4 12 0 3399.36 3698.91 581.76 o -3 12 0 2959.29 1594.56 292.09 o -2 12 0 1822.79 1895.56 223.55 o -1 12 0 1147.11 1227.03 98.90 o 0 12 0 434.14 354.08 244.27 o 1 12 0 1538.72 1515.56 183.67 o 2 12 0 337.88 329.39 199.35 o 3 12 0 1151.10 1312.70 105.03 o 4 12 0 211.11 219.75 49.64 o 5 12 0 292.11 400.76 67.80 o -7 13 0 29.61 -55.93 84.75 o -6 13 0 68.01 94.69 86.57 o -5 13 0 334.50 394.12 85.29 o -4 13 0 36.67 8.48 73.49 o -3 13 0 353.93 405.08 154.94 o -2 13 0 104.12 -22.61 172.17 o -1 13 0 0.21 -47.52 51.90 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