#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:34:53 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181256 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/34/2233437.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233437_Fobs loop_ _publ_author_name 'Nichol, Gary S.' 'Walton, David P.' 'Anna, Laura J.' 'Rajaseelan, Edward' _publ_section_title ; [2-Butyl-4-(4-tert-butylbenzyl)-1,2,4-triazol-3-ylidene]chlorido[(1,2,5,6-\h)-cycloocta-1,5-diene]iridium(I) ; _journal_coeditor_code FJ2494 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m158 _journal_page_last m159 _journal_volume 68 _journal_year 2012 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 65.213 _cell_angle_beta 75.170 _cell_angle_gamma 76.052 _cell_length_a 10.2485 _cell_length_b 11.2843 _cell_length_c 11.9237 _exptl_crystal_F_000 604.00 _reflns_d_resolution_high 0.7101 _cod_data_source_file fj2494Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' exer115 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 197.30 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2253.09 2350.40 57.06 o 2 0 0 23332.70 26813.23 530.45 o 3 0 0 319.08 367.22 22.01 o 4 0 0 17210.57 19096.84 306.06 o 5 0 0 988.95 1020.42 38.84 o 6 0 0 10485.09 10914.94 186.64 o 7 0 0 808.41 826.07 39.23 o 8 0 0 2833.86 2741.19 73.20 o 9 0 0 2495.20 2483.84 72.46 o 10 0 0 2944.69 2848.61 81.74 o 11 0 0 3477.14 3352.80 92.85 o 12 0 0 940.11 933.24 56.33 o 13 0 0 1911.83 1687.97 113.74 o -13 1 0 541.96 528.08 66.61 o -12 1 0 2572.14 2347.38 104.12 o -11 1 0 2438.99 2459.16 102.80 o -10 1 0 2204.14 2285.87 75.72 o -9 1 0 1477.70 1568.70 57.82 o -8 1 0 3061.33 3211.30 80.34 o -7 1 0 4214.15 3873.85 85.74 o -6 1 0 1293.53 1188.85 51.66 o -5 1 0 7350.75 7186.44 153.51 o -4 1 0 3202.48 3552.03 112.52 o -3 1 0 7848.90 7620.00 152.72 o -2 1 0 301.34 468.56 23.92 o -1 1 0 16875.59 16201.95 291.50 o 0 1 0 50.81 60.36 8.04 o 1 1 0 19979.82 20296.02 1015.11 o 2 1 0 689.13 727.48 20.21 o 3 1 0 32204.28 35838.73 735.24 o 4 1 0 4960.63 5724.44 120.96 o 5 1 0 21777.45 24361.68 471.31 o 6 1 0 2384.76 2458.47 60.46 o 7 1 0 8362.94 8453.34 153.57 o 8 1 0 1418.26 1422.44 60.75 o 9 1 0 3370.24 3419.79 87.23 o 10 1 0 689.65 747.66 51.19 o 11 1 0 995.68 1026.05 55.50 o 12 1 0 1107.73 1242.55 62.53 o 13 1 0 765.03 733.73 119.84 o -13 2 0 1997.20 1989.14 104.10 o -12 2 0 1644.17 1707.63 131.83 o -11 2 0 3270.29 3164.94 116.52 o -10 2 0 3456.20 3498.51 153.16 o -9 2 0 3719.42 3706.59 117.51 o -8 2 0 4040.69 4231.58 95.11 o -7 2 0 2052.18 2078.98 47.03 o -6 2 0 6663.06 6703.11 151.36 o -5 2 0 8036.58 8363.22 177.42 o -4 2 0 12483.40 13011.92 251.07 o -3 2 0 2481.48 2569.83 76.85 o -2 2 0 7442.58 6373.74 162.60 o -1 2 0 8529.92 7913.84 180.84 o 0 2 0 38925.82 35831.43 881.28 o 1 2 0 3332.19 3179.59 64.43 o 2 2 0 31077.48 32835.02 569.43 o 3 2 0 5185.34 5782.63 145.87 o 4 2 0 13446.15 14479.10 462.34 o 5 2 0 998.96 948.21 34.87 o 6 2 0 16856.53 18168.95 391.75 o 7 2 0 1361.26 1366.18 48.32 o 8 2 0 7848.81 8243.92 155.48 o 9 2 0 1070.66 1162.75 52.09 o 10 2 0 4445.01 4253.09 104.11 o 11 2 0 1642.27 1516.96 78.01 o 12 2 0 2015.53 1871.15 90.36 o 13 2 0 680.95 732.40 65.95 o -13 3 0 404.63 307.14 63.00 o -12 3 0 1077.94 1063.83 79.58 o -11 3 0 1940.58 2126.29 98.98 o -10 3 0 2424.81 2270.04 137.27 o -9 3 0 4676.66 4834.68 169.97 o -8 3 0 2429.57 2411.19 120.30 o -7 3 0 11156.11 11135.56 195.61 o -6 3 0 2724.19 2733.59 66.71 o -5 3 0 8888.19 8900.37 217.82 o -4 3 0 2550.67 2505.62 81.54 o -3 3 0 4570.79 4004.93 125.25 o -2 3 0 103.02 96.33 12.35 o -1 3 0 15954.97 14422.71 323.57 o 0 3 0 93.69 79.35 11.96 o 1 3 0 13719.45 13397.53 241.50 o 2 3 0 64.08 60.48 19.74 o 3 3 0 10587.70 10662.19 246.96 o 4 3 0 1355.19 1419.29 51.06 o 5 3 0 15553.58 16533.62 258.11 o 6 3 0 3858.74 4293.46 82.87 o 7 3 0 6350.42 6941.44 152.93 o 8 3 0 1335.33 1393.23 63.25 o 9 3 0 5120.75 5344.57 137.63 o 10 3 0 3808.83 3601.35 112.69 o 11 3 0 1946.66 2028.16 149.63 o 12 3 0 1127.77 1183.29 76.33 o 13 3 0 2171.23 2182.08 106.51 o -12 4 0 247.25 214.12 55.69 o -11 4 0 1882.75 1927.39 98.27 o -10 4 0 1659.93 1639.01 105.37 o -9 4 0 1521.50 1676.26 102.83 o -8 4 0 2369.17 2414.20 68.40 o -7 4 0 2134.98 2164.35 62.99 o -6 4 0 7460.64 7135.18 135.38 o -5 4 0 2509.05 2547.15 69.42 o -4 4 0 14788.75 14437.31 339.58 o -3 4 0 4821.28 4702.28 125.40 o -2 4 0 17068.04 16251.24 369.19 o -1 4 0 1156.81 1137.44 35.73 o 0 4 0 12065.23 10993.47 248.39 o 1 4 0 4164.66 4464.20 70.33 o 2 4 0 12991.96 12498.71 197.26 o 3 4 0 385.16 497.78 23.86 o 4 4 0 4047.35 3728.11 63.87 o 5 4 0 1219.33 1228.66 38.49 o 6 4 0 6848.92 7048.75 125.05 o 7 4 0 2954.31 3031.46 103.41 o 8 4 0 3077.26 3296.44 105.25 o 9 4 0 1885.43 1803.49 77.85 o 10 4 0 3276.37 3300.19 109.91 o 11 4 0 2332.66 2305.84 112.03 o 12 4 0 2001.72 1915.80 94.13 o 13 4 0 1515.19 1223.14 103.12 o -12 5 0 1334.62 1162.32 85.63 o -11 5 0 239.22 188.38 53.97 o -10 5 0 2733.69 2563.99 295.62 o -9 5 0 1009.81 1091.19 105.22 o -8 5 0 2332.46 2186.67 122.47 o -7 5 0 3489.39 3351.86 84.28 o -6 5 0 1296.60 1227.84 49.91 o -5 5 0 9200.72 9134.34 185.91 o -4 5 0 368.60 333.63 32.89 o -3 5 0 8467.36 7939.10 174.43 o -2 5 0 574.88 545.61 29.65 o -1 5 0 23958.30 22658.95 348.98 o 0 5 0 1143.29 1128.56 45.97 o 1 5 0 23072.36 23673.31 361.37 o 2 5 0 0.48 8.07 16.22 o 3 5 0 8534.45 8139.86 121.41 o 4 5 0 3.37 -16.59 16.73 o 5 5 0 12556.80 12659.42 182.77 o 6 5 0 43.84 40.91 19.97 o 7 5 0 4726.98 4845.93 98.30 o 8 5 0 911.26 906.36 40.05 o 9 5 0 2567.10 2604.08 93.01 o 10 5 0 2310.13 2232.80 92.07 o 11 5 0 1397.60 1351.38 79.73 o 12 5 0 2535.82 2440.08 145.10 o 13 5 0 511.38 464.48 63.91 o -11 6 0 1736.83 1542.14 113.29 o -10 6 0 718.47 852.68 129.89 o -9 6 0 1770.07 1867.66 118.99 o -8 6 0 710.58 818.86 65.25 o -7 6 0 1740.91 1751.74 61.55 o -6 6 0 2054.43 1987.93 70.47 o -5 6 0 2688.88 2489.46 74.62 o -4 6 0 4902.44 4565.75 153.09 o -3 6 0 870.38 798.00 39.02 o -2 6 0 6131.62 5711.40 121.75 o -1 6 0 127.38 103.84 18.12 o 0 6 0 11885.24 11306.08 213.51 o 1 6 0 60.89 69.94 16.39 o 2 6 0 12099.34 11723.57 154.01 o 3 6 0 396.78 449.12 24.27 o 4 6 0 11784.77 12161.13 177.35 o 5 6 0 32.77 20.98 17.89 o 6 6 0 11255.48 11620.36 174.16 o 7 6 0 592.01 642.99 43.16 o 8 6 0 4284.29 4412.92 97.43 o 9 6 0 165.83 158.49 40.93 o 10 6 0 2165.61 2214.68 92.43 o 11 6 0 966.93 989.51 106.10 o 12 6 0 1060.78 1049.38 156.49 o 13 6 0 1887.36 1501.55 93.25 o -11 7 0 878.02 1000.58 144.01 o -10 7 0 1990.50 1986.06 232.57 o -9 7 0 907.46 951.25 99.57 o -8 7 0 2202.95 2239.93 76.12 o -7 7 0 1199.97 1184.36 56.64 o -6 7 0 3235.89 3111.20 111.66 o -5 7 0 3389.14 3293.73 92.11 o -4 7 0 1838.95 1813.92 73.02 o -3 7 0 2602.51 2358.18 69.42 o -2 7 0 408.42 377.69 31.30 o -1 7 0 7081.08 6571.42 119.22 o 0 7 0 18.61 8.65 19.26 o 1 7 0 7894.51 7282.80 122.53 o 2 7 0 39.48 23.34 14.63 o 3 7 0 9231.64 9344.12 129.09 o 4 7 0 280.86 340.82 26.53 o 5 7 0 6329.83 6490.11 108.80 o 6 7 0 62.09 80.10 22.86 o 7 7 0 7597.75 7805.74 148.00 o 8 7 0 772.17 795.96 60.93 o 9 7 0 4510.44 4594.56 132.28 o 10 7 0 629.11 573.18 60.39 o 11 7 0 2197.19 2133.74 275.85 o 12 7 0 1102.99 955.43 79.22 o 13 7 0 1095.65 1092.77 113.34 o -10 8 0 756.29 709.90 75.12 o -9 8 0 1743.34 1820.16 103.55 o -8 8 0 2363.37 2346.43 107.24 o -7 8 0 1361.90 1437.81 71.00 o -6 8 0 1768.17 1738.58 63.69 o -5 8 0 2399.97 2310.93 68.67 o -4 8 0 2958.15 2840.99 73.53 o -3 8 0 1005.41 1005.40 42.88 o -2 8 0 4462.16 4215.62 97.15 o -1 8 0 2111.96 1909.91 53.03 o 0 8 0 4621.38 4610.94 87.96 o 1 8 0 106.52 82.79 19.17 o 2 8 0 6458.23 6321.92 102.70 o 3 8 0 655.82 738.27 32.23 o 4 8 0 4935.21 4858.23 79.55 o 5 8 0 589.69 686.96 35.16 o 6 8 0 3569.53 3586.90 108.60 o 7 8 0 808.70 863.30 42.80 o 8 8 0 5090.25 5363.68 118.01 o 9 8 0 480.62 459.40 55.16 o 10 8 0 3523.50 3434.45 151.86 o 11 8 0 747.21 631.24 68.13 o 12 8 0 2704.40 2550.72 228.06 o -9 9 0 793.90 780.84 103.44 o -8 9 0 645.22 629.48 58.06 o -7 9 0 1357.03 1407.03 64.56 o -6 9 0 1611.44 1623.95 67.81 o -5 9 0 3702.84 3662.59 120.48 o -4 9 0 1226.67 1227.92 51.89 o -3 9 0 5045.28 4856.51 118.02 o -2 9 0 1562.57 1554.52 66.93 o -1 9 0 5476.28 4961.90 101.42 o 0 9 0 666.15 723.12 49.45 o 1 9 0 4619.96 4557.57 95.33 o 2 9 0 207.32 268.15 34.00 o 3 9 0 3308.00 3294.78 79.12 o 4 9 0 30.20 11.26 23.90 o 5 9 0 3992.81 4021.82 73.30 o 6 9 0 1254.46 1328.94 76.37 o 7 9 0 3077.98 3153.94 74.84 o 8 9 0 660.62 628.50 46.27 o 9 9 0 2151.76 2000.20 104.46 o 10 9 0 1000.05 949.40 74.11 o 11 9 0 1987.20 1863.96 100.64 o 12 9 0 1130.93 1127.42 129.97 o -8 10 0 847.25 937.26 68.12 o -7 10 0 603.01 725.78 69.50 o -6 10 0 1199.42 1302.85 103.13 o -5 10 0 707.68 698.67 62.27 o -4 10 0 2511.70 2395.55 92.12 o -3 10 0 785.13 835.21 60.16 o -2 10 0 3631.95 3457.95 105.59 o -1 10 0 1428.09 1519.23 70.25 o 0 10 0 5634.37 5577.76 148.15 o 1 10 0 393.70 441.98 37.00 o 2 10 0 6968.53 6937.08 134.12 o 3 10 0 45.30 34.61 28.31 o 4 10 0 5406.17 5236.49 111.45 o 5 10 0 15.95 -1.06 28.91 o 6 10 0 2357.75 2355.23 96.57 o 7 10 0 111.68 73.24 32.99 o 8 10 0 1735.22 1876.40 93.43 o 9 10 0 452.58 299.31 55.22 o 10 10 0 1282.75 1187.80 83.70 o 11 10 0 711.71 708.32 76.31 o -7 11 0 357.71 477.45 66.75 o -6 11 0 865.35 940.46 75.59 o -5 11 0 882.48 945.80 71.46 o -4 11 0 371.12 401.33 55.07 o -3 11 0 2490.73 2631.16 99.65 o -2 11 0 147.48 146.04 44.21 o -1 11 0 2410.25 2480.92 92.19 o 0 11 0 591.71 628.39 55.09 o 1 11 0 5676.20 5606.70 118.46 o 2 11 0 48.33 14.29 32.02 o 3 11 0 5496.69 5404.48 130.20 o 4 11 0 298.92 357.11 43.46 o 5 11 0 5636.02 5548.78 149.37 o 6 11 0 4.77 -17.17 29.40 o 7 11 0 2870.79 2856.79 77.92 o 8 11 0 247.83 219.37 42.31 o 9 11 0 1635.71 1377.64 104.05 o 10 11 0 182.89 164.40 58.19 o -5 12 0 730.51 741.81 148.81 o -4 12 0 604.68 611.20 65.91 o -3 12 0 385.06 370.48 56.63 o -2 12 0 1651.85 1752.38 87.28 o -1 12 0 324.92 501.42 56.88 o 0 12 0 1960.31 1967.11 87.01 o 1 12 0 234.28 259.30 49.88 o 2 12 0 3057.37 2952.07 84.33 o 3 12 0 14.25 -24.89 32.67 o 4 12 0 3805.84 4048.32 113.17 o 5 12 0 1.78 12.77 35.05 o 6 12 0 3779.48 3701.23 108.87 o 7 12 0 96.14 112.67 41.91 o 8 12 0 3506.90 3352.15 103.15 o 9 12 0 121.22 102.98 56.28 o -4 13 0 567.88 619.10 70.84 o -3 13 0 1479.07 1588.15 91.21 o -2 13 0 449.07 479.38 82.18 o -1 13 0 712.48 739.09 90.59 o 0 13 0 509.59 494.57 58.80 o 1 13 0 1055.65 1134.75 74.86 o 2 13 0 20.57 -61.07 73.87 o 3 13 0 2426.19 2434.14 97.79 o 4 13 0 33.61 27.33 37.20 o 5 13 0 2136.45 2127.32 107.01 o 6 13 0 116.79 61.21 40.75 o 7 13 0 2290.06 2270.93 126.82 o -1 14 0 585.03 525.08 66.43 o 0 14 0 867.32 704.88 69.63 o 1 14 0 212.64 135.58 53.88 o 2 14 0 1673.75 1539.33 86.39 o 3 14 0 26.42 8.17 48.50 o 4 14 0 1522.25 1451.27 72.13 o 5 14 0 42.33 -13.08 39.88 o -2 -14 1 1152.92 1097.27 79.19 o -6 -13 1 15.26 -40.65 40.65 o -5 -13 1 2268.34 2242.64 79.64 o -4 -13 1 85.92 16.43 38.72 o -3 -13 1 1912.80 1904.90 74.76 o -2 -13 1 97.58 25.86 55.63 o -1 -13 1 813.60 813.68 68.24 o 0 -13 1 563.74 505.79 60.85 o 1 -13 1 643.45 752.39 84.70 o 2 -13 1 674.64 702.15 73.36 o 3 -13 1 591.45 630.30 71.89 o -8 -12 1 3046.79 2810.10 118.10 o -7 -12 1 1.76 20.00 40.65 o -6 -12 1 2699.85 2644.05 135.37 o -5 -12 1 174.06 149.12 40.22 o -4 -12 1 2764.55 2833.52 101.20 o -3 -12 1 219.29 179.92 40.11 o -2 -12 1 2553.31 2688.03 81.67 o -1 -12 1 308.96 340.90 52.54 o 0 -12 1 1111.15 1097.22 71.58 o 1 -12 1 558.16 652.14 61.78 o 2 -12 1 1564.71 1655.28 86.72 o 3 -12 1 962.04 1132.44 77.96 o 4 -12 1 290.60 266.66 58.81 o 5 -12 1 717.18 784.67 75.47 o -9 -11 1 1663.81 1615.93 94.32 o -8 -11 1 1.12 3.22 39.23 o -7 -11 1 2526.81 2619.06 88.35 o -6 -11 1 241.96 217.23 41.90 o -5 -11 1 3352.08 3464.29 92.43 o -4 -11 1 710.21 752.86 53.90 o -3 -11 1 3713.08 3656.81 142.25 o -2 -11 1 570.44 510.03 43.98 o -1 -11 1 4285.90 4192.31 110.29 o 0 -11 1 1657.85 1627.05 76.87 o 1 -11 1 2100.51 2048.38 86.01 o 2 -11 1 279.76 256.29 49.24 o 3 -11 1 1476.40 1421.24 79.50 o 4 -11 1 738.25 791.60 71.85 o 5 -11 1 393.53 347.02 65.59 o 6 -11 1 1041.46 1155.38 83.33 o -10 -10 1 1310.47 1373.83 89.13 o -9 -10 1 300.29 321.35 57.45 o -8 -10 1 2429.75 2305.43 80.78 o -7 -10 1 5.30 -20.38 33.59 o -6 -10 1 2198.10 2182.50 65.48 o -5 -10 1 232.88 256.50 33.66 o -4 -10 1 2570.44 2688.94 76.17 o -3 -10 1 496.94 504.16 40.74 o -2 -10 1 4051.89 4061.09 93.94 o -1 -10 1 1647.43 1739.31 60.45 o 0 -10 1 3109.16 3053.73 96.57 o 1 -10 1 1708.20 1680.64 73.78 o 2 -10 1 3411.90 3408.48 107.28 o 3 -10 1 2366.88 2376.96 99.95 o 4 -10 1 1720.50 1703.02 82.05 o 5 -10 1 1691.93 1867.49 126.37 o 6 -10 1 476.52 434.77 60.74 o 7 -10 1 1014.84 1043.64 80.10 o 8 -10 1 300.41 298.17 55.19 o -11 -9 1 2135.41 1974.59 104.00 o -10 -9 1 156.99 139.73 69.84 o -9 -9 1 2617.96 2433.58 103.38 o -8 -9 1 192.36 186.07 38.12 o -7 -9 1 3754.87 3901.38 99.13 o -6 -9 1 299.76 276.53 32.54 o -5 -9 1 5613.57 5572.26 96.21 o -4 -9 1 726.14 717.72 32.27 o -3 -9 1 2185.03 2081.67 52.87 o -2 -9 1 91.68 55.19 21.51 o -1 -9 1 3096.17 3036.82 64.91 o 0 -9 1 1199.09 1210.61 40.85 o 1 -9 1 2139.61 1988.69 83.35 o 2 -9 1 2454.06 2341.69 67.17 o 3 -9 1 2912.19 2709.17 94.53 o 4 -9 1 2096.35 2251.57 71.62 o 5 -9 1 2070.79 2213.75 94.10 o 6 -9 1 2613.44 2752.30 84.95 o 7 -9 1 1036.54 1148.19 63.75 o 8 -9 1 1221.70 1435.85 66.19 o 9 -9 1 497.58 576.33 75.94 o -12 -8 1 3331.41 3087.48 128.17 o -11 -8 1 205.49 262.46 58.41 o -10 -8 1 3624.47 3320.45 119.99 o -9 -8 1 8.64 5.92 42.05 o -8 -8 1 5924.18 5846.90 126.36 o -7 -8 1 14.83 50.41 30.56 o -6 -8 1 5178.17 5232.00 97.85 o -5 -8 1 10.79 -16.17 22.02 o -4 -8 1 2872.42 2883.60 57.53 o -3 -8 1 135.60 113.13 19.33 o -2 -8 1 5463.96 5391.15 92.68 o -1 -8 1 1451.47 1407.62 40.96 o 0 -8 1 4731.03 4492.34 80.49 o 1 -8 1 2255.97 2089.33 58.39 o 2 -8 1 2834.10 2707.40 69.09 o 3 -8 1 2070.88 2100.67 100.48 o 4 -8 1 2346.21 2312.43 68.17 o 5 -8 1 3655.36 3492.67 88.98 o 6 -8 1 1102.24 1149.36 65.23 o 7 -8 1 2239.29 2462.45 91.86 o 8 -8 1 1080.42 1040.56 61.95 o 9 -8 1 2840.29 2984.84 118.41 o 10 -8 1 177.89 287.57 75.75 o -12 -7 1 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83.71 o 2 8 16 1087.01 999.94 120.59 o 3 8 16 3.40 13.03 45.53 o 4 8 16 1299.96 1239.16 80.48 o 5 8 16 125.07 133.95 50.06 o 6 8 16 1028.35 989.70 74.58 o 7 8 16 180.09 112.28 45.65 o 1 9 16 858.13 869.21 69.55 o 2 9 16 5.25 -8.01 51.19 o 3 9 16 1124.31 909.49 71.16 o 4 9 16 408.67 297.76 56.57 o 5 9 16 809.71 872.86 72.17 o 6 9 16 133.05 121.23 44.81 o 7 9 16 1325.53 1396.56 123.72 o 2 10 16 752.61 816.16 87.73 o 3 10 16 33.89 56.39 65.37 o 4 10 16 740.78 687.79 70.19 o 5 10 16 175.21 98.69 54.13 o 6 10 16 700.08 763.64 142.32 o