#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:34:53 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181256 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/34/2233463.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233463_Fobs loop_ _publ_author_name 'Salehzadeh, Sadegh' 'Mahdavian, Mahsa' 'Khalaj, Mehdi' _publ_section_title ; Aqua[tris(2-{5-[(4-methylphenyl)diazenyl]-2-oxidobenzylideneamino}ethyl)amine]samarium(III) acetonitrile monosolvate ; _journal_coeditor_code HB6567 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m96 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.375 _cell_angle_gamma 90.000 _cell_length_a 19.9785 _cell_length_b 20.4849 _cell_length_c 11.4683 _exptl_crystal_F_000 2084.00 _reflns_d_resolution_high 0.7701 _cod_data_source_file hb6567Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' k10261a in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 408.31 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 13330.12 13336.51 419.97 o 4 0 0 5779.63 5312.06 240.73 o 5 0 0 4769.75 4539.47 222.30 o 6 0 0 3445.32 3700.93 348.82 o 7 0 0 2782.18 3348.34 238.71 o 8 0 0 4154.41 4632.41 629.85 o 9 0 0 103.38 0.34 105.58 o 10 0 0 331.97 -112.54 175.75 o 11 0 0 4103.22 3494.76 306.95 o 12 0 0 16830.61 17754.07 711.47 o 13 0 0 23995.89 25322.64 831.21 o 14 0 0 18164.80 18646.69 819.55 o 15 0 0 19952.04 23021.48 975.51 o 16 0 0 10268.14 11206.72 1206.63 o 17 0 0 136.28 179.46 256.30 o 18 0 0 2191.42 1790.30 430.38 o 19 0 0 3954.54 4637.87 736.95 o 20 0 0 2779.72 3529.50 638.69 o 21 0 0 703.34 660.31 542.40 o 22 0 0 324.61 375.35 705.51 o 23 0 0 659.87 444.14 562.05 o 24 0 0 1480.15 1212.53 676.03 o 25 0 0 1568.51 697.65 884.34 o 3 1 0 8869.72 8925.96 213.69 o 4 1 0 9768.76 9334.31 238.27 o 5 1 0 16731.26 16222.23 380.16 o 6 1 0 17855.13 17081.16 408.53 o 7 1 0 20043.05 20026.46 662.02 o 8 1 0 19924.79 19861.31 493.57 o 9 1 0 9300.32 8984.80 290.53 o 10 1 0 16304.45 16930.14 445.76 o 11 1 0 1769.51 1587.94 89.98 o 12 1 0 3689.97 3705.82 236.27 o 13 1 0 1013.29 785.37 125.45 o 14 1 0 714.43 589.61 98.46 o 15 1 0 945.82 991.00 178.13 o 16 1 0 6909.12 6916.04 562.48 o 17 1 0 4836.78 4883.56 362.76 o 18 1 0 2847.41 3615.78 427.78 o 19 1 0 1754.03 1256.79 344.32 o 20 1 0 1758.50 1761.10 424.41 o 21 1 0 491.94 747.46 373.84 o 22 1 0 1923.69 1416.33 422.52 o 23 1 0 1423.65 1656.72 523.24 o 24 1 0 1635.85 1667.47 494.70 o 25 1 0 421.47 -581.70 581.70 o 2 2 0 4238.58 4311.85 89.14 o 3 2 0 22610.71 21259.58 364.30 o 4 2 0 1984.74 1691.38 71.24 o 5 2 0 644.01 622.59 41.15 o 6 2 0 3088.89 2551.16 120.11 o 7 2 0 20.07 69.28 39.33 o 8 2 0 4.23 16.48 51.22 o 9 2 0 4363.20 4290.09 163.05 o 10 2 0 779.94 823.63 65.36 o 11 2 0 119.67 89.68 59.18 o 12 2 0 14.04 -0.43 66.79 o 13 2 0 314.27 149.61 87.12 o 14 2 0 3213.06 2575.45 238.66 o 15 2 0 326.46 254.65 84.56 o 16 2 0 892.10 580.78 221.18 o 17 2 0 3314.60 3493.81 330.19 o 18 2 0 724.25 406.83 313.01 o 19 2 0 229.82 -178.54 252.21 o 20 2 0 272.90 -332.12 332.12 o 21 2 0 378.84 -1.68 331.52 o 22 2 0 311.89 801.90 371.30 o 23 2 0 80.23 406.17 379.66 o 24 2 0 8.92 -32.12 1002.25 o 25 2 0 13.72 -372.26 534.53 o 1 3 0 436.63 389.84 35.77 o 2 3 0 532.89 408.69 28.41 o 3 3 0 20028.40 19717.11 333.09 o 4 3 0 1172.54 1141.18 54.60 o 5 3 0 2217.64 2024.57 87.10 o 6 3 0 10430.10 9313.61 248.35 o 7 3 0 7007.06 5996.75 177.83 o 8 3 0 13788.42 12798.84 312.72 o 9 3 0 3072.98 2422.93 120.65 o 10 3 0 26383.24 28451.64 565.18 o 11 3 0 1118.10 1098.85 137.00 o 12 3 0 6149.16 5642.90 175.98 o 13 3 0 750.09 391.28 234.82 o 14 3 0 513.70 556.48 99.67 o 15 3 0 917.13 782.85 111.50 o 16 3 0 4617.81 4914.20 245.25 o 17 3 0 2902.07 3461.84 196.83 o 18 3 0 14153.18 17296.47 927.88 o 19 3 0 4840.37 5065.54 517.64 o 20 3 0 3519.37 3763.95 645.57 o 21 3 0 2229.65 3011.40 466.21 o 22 3 0 1683.32 1967.16 450.93 o 23 3 0 1228.79 760.73 958.04 o 24 3 0 1241.71 1350.09 721.23 o 25 3 0 442.91 -82.88 453.81 o 0 4 0 78949.63 81493.23 2940.34 o 1 4 0 26759.99 28459.03 655.07 o 2 4 0 166716.52 161139.83 2780.52 o 3 4 0 2079.00 2001.18 67.24 o 4 4 0 6689.03 5801.48 142.82 o 5 4 0 115.06 26.68 39.02 o 6 4 0 45.68 129.33 49.45 o 7 4 0 94.74 101.47 66.46 o 8 4 0 465.30 427.60 75.17 o 9 4 0 46.05 194.62 61.28 o 10 4 0 9635.17 9565.95 293.59 o 11 4 0 27227.50 28755.46 538.08 o 12 4 0 11252.69 10489.26 261.88 o 13 4 0 19132.02 19923.81 502.33 o 14 4 0 14323.57 13985.17 407.30 o 15 4 0 7973.40 8409.49 322.22 o 16 4 0 10178.50 11479.04 695.32 o 17 4 0 5237.73 5778.00 296.12 o 18 4 0 3670.69 3660.15 271.75 o 19 4 0 5873.06 5860.17 988.50 o 20 4 0 1400.04 1769.32 366.51 o 21 4 0 2.05 100.44 374.47 o 22 4 0 768.21 173.93 346.80 o 23 4 0 974.72 625.54 475.41 o 24 4 0 1460.45 986.43 473.70 o 25 4 0 1322.36 353.24 591.53 o 1 5 0 5006.02 4898.81 195.67 o 2 5 0 86611.02 87250.52 1959.45 o 3 5 0 32791.72 31696.19 524.27 o 4 5 0 19604.20 18943.60 328.35 o 5 5 0 14927.44 14152.86 427.60 o 6 5 0 34117.70 32646.10 607.30 o 7 5 0 14651.21 13660.37 330.42 o 8 5 0 16808.23 16467.02 432.84 o 9 5 0 21101.08 20739.69 408.17 o 10 5 0 12734.31 12687.11 381.69 o 11 5 0 4988.81 4762.18 368.03 o 12 5 0 1534.08 1117.94 154.09 o 13 5 0 2.18 140.04 93.40 o 14 5 0 395.10 -18.56 132.37 o 15 5 0 614.06 299.86 230.83 o 16 5 0 82.81 174.39 112.08 o 17 5 0 853.30 759.01 147.80 o 18 5 0 7191.82 8350.37 441.53 o 19 5 0 6471.14 7150.17 422.99 o 20 5 0 976.98 852.90 473.61 o 21 5 0 1374.04 1539.64 374.17 o 22 5 0 2906.77 2342.84 511.69 o 23 5 0 1443.19 1927.35 533.04 o 24 5 0 2287.88 2308.23 534.73 o 25 5 0 1443.60 865.94 495.69 o 0 6 0 4179.42 3712.32 232.31 o 1 6 0 5692.98 5322.81 173.46 o 2 6 0 58184.26 60390.61 1204.81 o 3 6 0 4392.73 4554.85 114.47 o 4 6 0 168.14 130.51 36.65 o 5 6 0 10.03 -39.21 56.85 o 6 6 0 39.69 65.84 78.45 o 7 6 0 229.75 -13.91 80.25 o 8 6 0 832.00 594.50 101.21 o 9 6 0 4204.59 3973.78 246.35 o 10 6 0 0.25 74.64 59.32 o 11 6 0 138.58 96.39 92.13 o 12 6 0 319.77 276.45 79.81 o 13 6 0 353.03 325.26 116.78 o 14 6 0 0.71 -115.81 148.56 o 15 6 0 2.00 -53.14 241.39 o 16 6 0 742.98 630.69 147.92 o 17 6 0 0.15 -76.94 238.84 o 18 6 0 32.48 -3.93 136.18 o 19 6 0 207.89 -221.02 229.04 o 20 6 0 15.74 94.33 446.10 o 21 6 0 411.17 -192.79 343.69 o 22 6 0 57.00 -16.64 339.28 o 23 6 0 163.05 180.94 548.29 o 24 6 0 86.95 -579.73 579.73 o 25 6 0 16.27 -176.16 416.50 o 1 7 0 3984.78 4129.57 125.20 o 2 7 0 594.70 685.17 54.97 o 3 7 0 4868.30 4466.87 113.09 o 4 7 0 20074.67 19411.04 337.86 o 5 7 0 28885.40 28013.31 623.79 o 6 7 0 20860.65 19299.72 355.76 o 7 7 0 10530.51 9807.53 234.40 o 8 7 0 54929.99 56766.75 1312.88 o 9 7 0 3981.02 3760.16 148.75 o 10 7 0 13528.37 13917.12 733.85 o 11 7 0 5476.89 5370.70 193.81 o 12 7 0 3492.48 3301.36 172.58 o 13 7 0 21.22 17.38 93.97 o 14 7 0 97.05 286.99 138.76 o 15 7 0 59.37 194.33 179.66 o 16 7 0 557.75 290.76 219.72 o 17 7 0 2402.06 2462.90 208.25 o 18 7 0 1350.73 1648.73 227.61 o 19 7 0 2106.79 2556.11 382.00 o 20 7 0 4985.49 6178.34 592.31 o 21 7 0 2153.85 2963.31 478.15 o 22 7 0 1846.94 1412.75 444.33 o 23 7 0 751.57 190.07 411.34 o 24 7 0 390.87 -79.65 489.57 o 0 8 0 72195.50 76120.19 2402.19 o 1 8 0 50637.04 51351.96 1059.29 o 2 8 0 48982.27 48848.59 964.21 o 3 8 0 23269.53 22446.99 627.22 o 4 8 0 20923.38 20122.94 507.12 o 5 8 0 7030.51 7000.43 265.88 o 6 8 0 368.21 391.47 54.47 o 7 8 0 1705.55 1705.55 94.74 o 8 8 0 9632.74 10002.49 328.90 o 9 8 0 5875.19 5922.78 423.53 o 10 8 0 4235.54 3783.91 158.41 o 11 8 0 10109.76 10234.22 359.91 o 12 8 0 10102.37 9613.33 432.58 o 13 8 0 13486.91 12826.83 411.82 o 14 8 0 9999.94 10075.17 607.99 o 15 8 0 10137.31 10434.69 394.21 o 16 8 0 3487.54 3433.05 235.04 o 17 8 0 7010.29 7866.85 475.36 o 18 8 0 3444.38 3241.35 374.44 o 19 8 0 478.32 349.35 255.58 o 20 8 0 123.02 92.26 350.06 o 21 8 0 18.18 560.08 512.92 o 22 8 0 159.87 149.42 945.26 o 23 8 0 570.83 202.08 386.16 o 24 8 0 1184.51 1053.77 535.04 o 1 9 0 65.91 52.02 40.71 o 2 9 0 5752.16 5404.22 158.28 o 3 9 0 20351.54 19879.91 570.66 o 4 9 0 6011.64 5413.38 140.95 o 5 9 0 14440.99 14398.22 284.96 o 6 9 0 4110.40 3904.24 176.41 o 7 9 0 15065.40 14808.78 298.93 o 8 9 0 5487.37 4835.89 181.38 o 9 9 0 4923.78 4568.41 326.75 o 10 9 0 2292.94 1920.06 187.04 o 11 9 0 1903.00 2036.88 184.04 o 12 9 0 766.02 601.33 140.71 o 13 9 0 1308.91 1081.16 152.05 o 14 9 0 846.14 352.67 152.98 o 15 9 0 253.53 -101.12 149.48 o 16 9 0 70.06 -69.51 150.71 o 17 9 0 4236.29 3363.09 277.77 o 18 9 0 1734.77 1803.25 404.10 o 19 9 0 1126.21 1074.46 245.37 o 20 9 0 1156.21 1241.22 372.64 o 21 9 0 284.13 813.59 487.37 o 22 9 0 423.33 1150.55 480.49 o 23 9 0 1386.71 1785.99 488.73 o 24 9 0 950.37 562.16 451.74 o 0 10 0 5966.20 6308.58 260.71 o 1 10 0 53.08 82.72 41.33 o 2 10 0 1102.62 1020.93 98.58 o 3 10 0 52.29 67.80 53.76 o 4 10 0 3635.98 3739.81 143.55 o 5 10 0 14.34 76.21 51.92 o 6 10 0 228.02 209.18 55.04 o 7 10 0 12.94 -23.13 54.96 o 8 10 0 0.11 -17.88 64.96 o 9 10 0 1.56 -73.66 73.66 o 10 10 0 539.97 520.82 101.86 o 11 10 0 874.85 954.05 154.18 o 12 10 0 55.64 139.28 115.16 o 13 10 0 1286.27 883.43 253.03 o 14 10 0 15.74 99.75 134.93 o 15 10 0 6.77 -78.17 139.40 o 16 10 0 153.58 60.87 139.77 o 17 10 0 507.24 71.69 181.65 o 18 10 0 3.29 -207.57 455.15 o 19 10 0 65.12 -225.69 225.69 o 20 10 0 4.38 21.15 311.92 o 21 10 0 215.09 286.37 405.56 o 22 10 0 172.27 -355.67 355.67 o 23 10 0 223.43 1214.08 610.53 o 1 11 0 13279.26 14185.83 595.95 o 2 11 0 6723.81 6480.45 146.79 o 3 11 0 5902.74 6292.98 171.15 o 4 11 0 3174.02 2934.47 113.95 o 5 11 0 8349.71 8186.39 374.15 o 6 11 0 14099.45 14454.04 317.80 o 7 11 0 4093.89 4049.48 181.22 o 8 11 0 6786.28 6610.43 237.29 o 9 11 0 5688.45 5713.10 224.72 o 10 11 0 6717.04 7244.61 263.24 o 11 11 0 3022.48 3229.99 251.07 o 12 11 0 1365.07 1173.96 225.48 o 13 11 0 245.68 504.32 152.17 o 14 11 0 2479.53 2064.35 217.24 o 15 11 0 213.08 72.42 143.82 o 16 11 0 2080.39 2136.13 310.10 o 17 11 0 2731.47 2558.28 315.67 o 18 11 0 2195.37 2110.23 268.00 o 19 11 0 3505.43 3400.70 334.69 o 20 11 0 4040.17 4621.38 591.28 o 21 11 0 2756.38 2360.21 878.44 o 22 11 0 895.61 275.33 707.47 o 23 11 0 245.34 -404.35 404.35 o 0 12 0 11566.44 11447.74 287.26 o 1 12 0 10901.78 10931.56 687.57 o 2 12 0 20110.63 20107.36 428.01 o 3 12 0 14681.03 14541.94 605.42 o 4 12 0 8720.94 8967.11 274.33 o 5 12 0 6962.17 7204.17 357.50 o 6 12 0 49.04 31.06 54.64 o 7 12 0 30.16 -81.64 96.38 o 8 12 0 1907.32 1618.65 126.40 o 9 12 0 3559.76 3650.50 191.39 o 10 12 0 5135.24 5061.63 239.19 o 11 12 0 7044.85 7161.05 285.73 o 12 12 0 7630.02 8056.18 327.64 o 13 12 0 9795.06 10550.81 390.62 o 14 12 0 11678.19 12724.99 455.23 o 15 12 0 11789.08 13613.91 700.59 o 16 12 0 9414.47 10898.30 782.98 o 17 12 0 4594.68 4455.59 400.70 o 18 12 0 2685.83 2708.53 396.39 o 19 12 0 344.39 320.29 277.07 o 20 12 0 1.43 234.56 352.59 o 21 12 0 15.87 -67.26 419.92 o 22 12 0 100.67 -104.51 442.34 o 23 12 0 400.22 331.87 623.95 o 1 13 0 2465.32 2512.80 101.92 o 2 13 0 39.18 -14.28 62.97 o 3 13 0 1931.83 1940.09 127.25 o 4 13 0 8086.39 8561.28 387.12 o 5 13 0 11964.58 12310.37 279.75 o 6 13 0 5892.53 5598.95 300.13 o 7 13 0 10787.70 10778.41 299.25 o 8 13 0 8411.24 8142.47 254.28 o 9 13 0 5214.85 5153.72 204.11 o 10 13 0 4246.24 4010.90 215.00 o 11 13 0 3547.46 3365.59 197.85 o 12 13 0 627.31 377.22 144.79 o 13 13 0 365.61 277.12 136.34 o 14 13 0 135.19 327.21 172.45 o 15 13 0 150.16 49.02 220.52 o 16 13 0 99.10 116.21 204.22 o 17 13 0 458.01 35.41 305.72 o 18 13 0 463.56 94.29 302.59 o 19 13 0 1064.71 723.66 455.93 o 20 13 0 1558.74 1174.66 503.09 o 21 13 0 1130.00 816.11 544.22 o 22 13 0 677.56 1245.32 462.33 o 0 14 0 3516.08 2554.76 438.24 o 1 14 0 4059.09 3924.02 143.67 o 2 14 0 992.42 964.85 74.12 o 3 14 0 492.30 288.23 92.94 o 4 14 0 14.48 5.55 33.92 o 5 14 0 429.08 294.56 97.00 o 6 14 0 25.16 84.74 105.50 o 7 14 0 5.87 57.31 68.70 o 8 14 0 180.69 96.54 79.08 o 9 14 0 4.23 -68.84 88.95 o 10 14 0 68.38 -24.67 98.84 o 11 14 0 16.43 139.41 254.51 o 12 14 0 757.25 842.58 159.92 o 13 14 0 915.49 824.22 177.81 o 14 14 0 259.01 144.89 176.73 o 15 14 0 469.93 492.96 197.28 o 16 14 0 8.05 234.30 190.04 o 17 14 0 204.10 -33.77 375.74 o 18 14 0 6.58 163.23 237.65 o 19 14 0 14.06 -305.37 338.88 o 20 14 0 8.45 -27.86 509.97 o 21 14 0 80.01 518.64 428.83 o 1 15 0 310.03 156.66 256.46 o 2 15 0 7694.43 8945.42 580.35 o 3 15 0 6755.32 6382.66 226.17 o 4 15 0 3593.61 3685.80 186.01 o 5 15 0 13100.06 14595.88 343.83 o 6 15 0 11110.67 12028.27 286.23 o 7 15 0 9984.75 10459.71 308.03 o 8 15 0 8788.71 8904.03 419.32 o 9 15 0 2703.43 2844.64 256.92 o 10 15 0 3976.69 3991.33 260.98 o 11 15 0 1657.32 1745.96 341.44 o 12 15 0 894.73 554.83 144.32 o 13 15 0 731.67 471.76 166.64 o 14 15 0 179.57 120.45 158.21 o 15 15 0 216.27 215.70 262.28 o 16 15 0 392.00 289.85 249.20 o 17 15 0 725.94 824.00 461.82 o 18 15 0 699.82 541.27 255.57 o 19 15 0 2191.28 1590.92 365.83 o 20 15 0 2029.01 2736.97 1383.50 o 21 15 0 1946.37 2218.18 519.86 o 0 16 0 1819.87 1285.24 436.27 o 1 16 0 2675.54 2439.68 453.96 o 2 16 0 8749.57 9443.71 642.86 o 3 16 0 7576.77 8236.26 463.80 o 4 16 0 3091.57 3254.90 215.01 o 5 16 0 5160.67 5055.84 222.35 o 6 16 0 215.40 220.88 74.00 o 7 16 0 419.20 161.02 138.36 o 8 16 0 2432.51 2408.36 196.13 o 9 16 0 6030.60 6138.57 477.22 o 10 16 0 7297.92 7596.09 377.97 o 11 16 0 4296.82 4416.98 317.50 o 12 16 0 4719.99 5740.51 476.21 o 13 16 0 6341.67 7115.65 442.74 o 14 16 0 7635.57 8968.47 596.24 o 15 16 0 3552.94 3985.84 337.62 o 16 16 0 3769.66 3986.79 492.71 o 17 16 0 2642.30 2141.63 1370.73 o 18 16 0 624.40 317.48 291.51 o 19 16 0 95.83 -554.67 554.67 o 20 16 0 95.78 257.14 368.48 o 1 17 0 1046.56 758.72 262.24 o 2 17 0 1826.88 1414.79 305.82 o 3 17 0 2356.23 2093.65 176.64 o 4 17 0 785.89 573.30 213.59 o 5 17 0 3921.05 3810.27 217.13 o 6 17 0 6830.92 7304.09 553.53 o 7 17 0 3618.33 3536.30 169.18 o 8 17 0 5006.86 5097.74 292.08 o 9 17 0 2076.61 2005.98 188.00 o 10 17 0 1530.70 1488.08 247.54 o 11 17 0 82.27 -8.93 135.01 o 12 17 0 257.63 427.59 149.92 o 13 17 0 394.20 438.12 153.76 o 14 17 0 155.03 -5.95 307.58 o 15 17 0 19.46 131.92 237.61 o 16 17 0 451.25 265.22 1242.99 o 17 17 0 137.19 33.19 260.87 o 18 17 0 405.41 150.35 250.72 o 19 17 0 693.04 -261.92 316.38 o 0 18 0 127.51 587.60 536.50 o 1 18 0 482.04 213.15 250.67 o 2 18 0 380.11 613.56 359.54 o 3 18 0 501.06 481.74 260.33 o 4 18 0 352.87 232.25 115.63 o 5 18 0 14.84 118.10 100.98 o 6 18 0 31.03 84.70 121.40 o 7 18 0 298.82 226.65 86.86 o 8 18 0 446.39 380.25 91.54 o 9 18 0 23.12 6.30 93.32 o 10 18 0 39.98 62.45 111.39 o 11 18 0 5.38 -5.09 98.44 o 12 18 0 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