#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/38/2233890.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233890_Fobs loop_ _publ_author_name 'Wen, Hua-Wen' 'Fan, Li-Xia' 'Liu, Li' 'Li, Ao' 'Fang, Qi' _publ_section_title ; 5-Sulfanylidene-2H,5H-1,3-dithiolo[4,5-d][1,3]dithiol-2-one ; _journal_coeditor_code IS5027 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o721 _journal_volume 68 _journal_year 2012 _space_group_IT_number 7 _symmetry_space_group_name_Hall 'P -2yac' _symmetry_space_group_name_H-M 'P 1 n 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.344 _cell_angle_gamma 90.000 _cell_length_a 3.9638 _cell_length_b 11.0211 _cell_length_c 8.7110 _exptl_crystal_F_000 224.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file is5027Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' fq10_0m in Pn' _shelx_refln_list_code 7 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status -2 0 0 550.04 21.72 65.96 556.81 2 0 0 90.72 2.42 66.11 -1. -4 0 0 28.13 13.03 40.44 5.43 4 0 0 50.8 5.05 40.6 -1. 0 1 0 10.56 2.6 16.21 6.71 -1 -1 0 4229.78 73.63 3910.79 1.75 1 1 0 4119.19 101.78 3890.44 1.74 -2 -1 0 477.93 9.71 119.68 340.92 2 1 0 143.1 2.1 117.53 -1. -3 -1 0 -0.27 5.7 1.31 2.47 3 1 0 0.01 0.63 1.38 -1. -4 -1 0 18.69 8.7 4.12 83.82 4 1 0 5.42 1.85 4.23 -1. -5 -1 0 5.69 4. 8.57 -1. 0 2 0 1069.72 10.06 617.65 255.44 -1 -2 0 1637.82 17.88 1533.44 60.02 1 2 0 1748.2 45.68 1531.05 59.95 -2 -2 0 30.01 3.27 18.85 9.24 2 2 0 24.49 1.05 18.95 -1. -3 -2 0 77.5 10.55 41.55 138.94 3 2 0 51. 1.95 41.04 -1. -4 -2 0 5. 1.82 3.29 -1. 4 2 0 3.72 1.58 3.24 -1. 0 3 0 140.05 1.81 156.11 64.56 -1 -3 0 1340.57 16.05 255.78 981.53 1 3 0 1281.52 19.82 252.59 984. -2 -3 0 449.84 12.75 408.26 89.3 2 3 0 383.31 5.04 409.85 -1. -3 -3 0 32.71 6.19 9.75 49.49 3 3 0 9.25 1.32 9.56 -1. -4 -3 0 27.41 2.19 29.3 -1. 4 3 0 27.67 2.25 29. -1. 0 4 0 4560.3 34.95 2862.82 1183.98 -1 -4 0 590.28 8.6 441.8 90.86 1 4 0 587.77 10.92 442.71 89.81 -2 -4 0 137.52 9.35 91.99 131.88 2 4 0 102.62 2.43 92.75 -1. -3 -4 0 482.87 26.05 464.19 14.43 3 4 0 494.75 8.05 462.94 -1. -4 -4 0 10.79 1.75 10.37 -1. 4 4 0 11.15 1.69 10.38 -1. 0 5 0 -0.58 0.65 1.4 0.58 -1 -5 0 383.85 4.21 92.38 255.27 1 5 0 376.5 5.57 89.61 253.03 -2 -5 0 433.88 10.89 360. 69.37 2 5 0 444.67 18.88 357.12 68.92 -3 -5 0 44.02 13.76 7.2 34.26 3 5 0 10.59 1.59 7.47 -1. -4 -5 0 54.12 3.12 47.95 -1. 4 5 0 57.02 3. 48.03 -1. 0 6 0 322.18 3.45 223.85 92.58 -1 -6 0 341.73 3.8 207.13 128.45 1 6 0 357.37 5.76 207.66 128.2 -2 -6 0 4.47 5.4 2.88 0.14 2 6 0 9.84 8.88 2.92 0.19 -3 -6 0 26.92 1.85 26.45 -1. 3 6 0 28.28 2.48 26.29 -1. -4 -6 0 3.11 1.43 1.77 -1. 4 6 0 2.09 1.56 1.73 -1. 0 7 0 6.99 0.84 6.74 2.79 -1 -7 0 822.68 7.65 427.67 375.97 1 7 0 847.36 9.6 433.06 377.29 -2 -7 0 332.94 15.92 331.21 3.93 2 7 0 350.51 19.81 332.78 3.8 -3 -7 0 7.67 1.37 7.32 -1. 3 7 0 6.8 1.66 7.29 -1. -4 -7 0 5.94 1.87 7.43 -1. 4 7 0 7.68 2.04 7.3 -1. 0 8 0 835.37 9.18 559.32 231.32 -1 -8 0 175.27 3.23 156.56 26.32 1 8 0 177.43 3.89 154.34 26.15 -2 -8 0 312.96 16.22 277.88 30.46 2 8 0 323.34 10.31 278.97 30.58 -3 -8 0 103.63 3.41 105.39 -1. 3 8 0 114.26 4.34 104.97 -1. -4 -8 0 21.13 2.84 26.11 -1. 4 8 0 30.15 3.59 26.31 -1. 0 9 0 156.19 3.37 115.03 47.57 -1 -9 0 416.02 5.98 418.07 8.63 1 9 0 447.71 7.66 422.91 8.17 -2 -9 0 36.38 8. 20.2 14.84 2 9 0 31.45 4.89 19.28 14.53 -3 -9 0 7.24 1.61 6.38 -1. 3 9 0 12.76 1.81 6.51 -1. 0 10 0 -1. 1.47 0.58 0.24 -1 -10 0 28.3 2.47 20.13 11.21 1 10 0 29.53 2.15 19.89 10.97 -2 -10 0 31.37 8.6 16.45 10.82 2 10 0 21.04 4.88 16.17 10.55 -3 -10 0 7.69 2.32 9.34 -1. 3 10 0 9.04 1.74 9.35 -1. 0 11 0 30.88 2.31 22.39 9.26 -1 -11 0 104.02 3.84 112.16 1.86 1 11 0 115.38 4.01 112.71 2.02 -2 -11 0 17.55 8.92 2.23 3.67 2 11 0 11.99 5.19 2.5 3.88 -3 -11 0 5.6 2.44 8.22 -1. 3 11 0 5.25 1.89 8.43 -1. 0 12 0 194.44 5.1 135.96 56.23 -1 -12 0 75.47 4.31 62.18 15.63 1 12 0 75.92 3.58 62.36 15.77 -2 -12 0 82.54 12.43 53.75 24.57 2 12 0 93.23 7.59 53.67 24.25 0 13 0 20.24 3.12 11.61 4.8 -1 -13 0 76.63 6.1 55.64 20.05 1 13 0 80.33 4.79 56.28 20.06 -2 -13 0 33.88 6.64 18.74 3.23 2 13 0 23.54 6.55 18.81 3.23 0 14 0 5.89 2.87 0.51 0.21 -1 -14 0 5.16 2.98 5.06 -1. 1 14 0 9.5 5.96 4.98 6.87 5 0 -1 8.26 4.37 4.63 -1. -5 0 1 -0.67 5.89 4.54 -1. 3 0 -1 453.78 6.36 428.32 -1. -3 0 1 411.26 5.68 426.17 -1. 1 0 -1 202.65 2.59 217.91 -1. -1 0 1 189.44 2.17 222.17 -1. -1 0 -1 11586.77 95.66 12388.8 -1. -3 0 -1 145.46 2.89 134.59 -1. 3 0 1 152.11 4.39 133.99 -1. -5 1 1 2.36 3.48 1.39 -1. 4 -1 -1 85.19 3.62 70.24 -1. -4 1 1 83.28 10.47 69.6 9.78 3 -1 -1 131.99 2.13 122.05 -1. -3 1 1 158.04 9.64 121.31 37.49 2 -1 -1 59.72 1.31 50.53 -1. -2 1 1 79.1 4.15 51.37 21.24 1 -1 -1 1972.48 36.02 4.2 1608.98 -1 1 1 2007.28 31.41 4.24 1617.4 0 -1 -1 1039.37 7.05 699.42 292.02 -1 -1 -1 93.43 2.21 5.65 87.85 1 1 1 90.37 4.86 5.04 86.87 -2 -1 -1 1902.49 27.56 1920.58 34.65 2 1 1 2059.92 31.18 1912.04 -1. -3 -1 -1 165.23 9.93 165.75 1.05 3 1 1 171.33 3.57 164.58 -1. -4 -1 -1 7.31 1.31 5.98 -1. 4 1 1 9.56 2.05 6.08 -1. 5 -2 -1 1.11 5.97 5.59 -1. -5 2 1 4.11 3.74 5.6 -1. 4 -2 -1 3.58 1.37 5.54 -1. -4 2 1 2.15 8.49 5.49 3.55 3 -2 -1 0.31 0.66 0.64 -1. -3 2 1 14.66 6.3 0.75 15.79 2 -2 -1 35.55 1.12 37.72 -1. -2 2 1 50.7 3.67 39.98 16.53 1 -2 -1 887.23 14.3 144.96 633.2 -1 2 1 885.15 12.48 145.13 634.19 0 -2 -1 569.91 3.7 373.74 158.65 0 2 1 615.38 8.33 383.62 154.57 -1 -2 -1 454.33 5.45 92.69 374.59 1 2 1 448.15 14.33 92.43 377.98 -2 -2 -1 942.03 21.52 971.2 19.02 2 2 1 957.55 15.64 976.57 -1. -3 -2 -1 47.32 1.45 43.89 -1. 3 2 1 49.61 2.85 43.99 -1. -4 -2 -1 2.43 1.22 0.83 -1. 4 2 1 1.47 1.64 0.8 -1. 4 -3 -1 112.61 3.52 90.31 -1. -4 3 1 106.42 16.34 90.36 14.95 3 -3 -1 8.15 0.99 8.02 -1. -3 3 1 92.8 11.21 7.72 157.62 2 -3 -1 21.95 0.99 20.7 -1. -2 3 1 28.41 3.44 20.26 8.38 1 -3 -1 2693.99 30.39 2379.28 104.47 -1 3 1 2531.9 31.1 2373.3 105.78 0 -3 -1 226.58 2.08 168.33 69.92 0 3 1 230.5 3.11 169.07 69.62 -1 -3 -1 161.19 2.31 133.41 47.35 1 3 1 172.49 3.83 132.35 47.45 -2 -3 -1 585.49 15.06 202.35 339.22 2 3 1 222.34 4.43 200.45 -1. -3 -3 -1 81.23 14.15 8.91 68. 3 3 1 7.79 1.49 8.1 -1. -4 -3 -1 12.11 1.63 13.75 -1. 4 3 1 12.68 2.19 13.69 -1. 4 -4 -1 0.16 1.2 0.02 -1. -4 4 1 7.66 13.82 0.02 20.18 3 -4 -1 82.33 2.69 78.6 -1. -3 4 1 90.6 8.47 78.22 16.65 2 -4 -1 1719.85 48.62 1168.71 483.35 -2 4 1 1728.18 31.3 1170.79 484.21 1 -4 -1 432.17 6.18 217.15 183.09 -1 4 1 467.14 5.19 219.69 182.72 0 -4 -1 2422.79 16.56 1521.49 629.2 0 4 1 2530.96 24.45 1521.37 629.25 -1 -4 -1 1626.85 12.54 1167.73 389.55 1 4 1 1670.43 26.86 1176.77 388.91 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210.75 86.16 -1 -6 -1 42.35 1.49 31.19 20.95 1 6 1 46.95 2.95 32.51 21.36 -2 -6 -1 57.1 6.94 14.11 73.18 2 6 1 95.5 11.84 14.77 73.3 -3 -6 -1 41.5 2.38 41.37 -1. 3 6 1 47.25 3.77 41.51 -1. -4 -6 -1 10.82 1.88 8.83 -1. 4 6 1 11.39 2.22 8.99 -1. 4 -7 -1 -1.27 1.27 0.15 -1. -4 7 1 0.54 1.38 0.13 -1. 3 -7 -1 4.12 1.28 7.54 -1. -3 7 1 13.03 13.6 7.7 12.23 2 -7 -1 324.36 17.9 229.94 95.1 -2 7 1 332.6 16.28 228.97 94.7 1 -7 -1 1104.58 9.45 912.26 179.1 -1 7 1 1105.33 11.45 909.07 176.87 0 -7 -1 184.83 2.91 128.21 51.76 0 7 1 189.62 2.59 125.15 53.02 -1 -7 -1 316.88 3.78 45.98 259.57 1 7 1 331.16 6.78 44.6 259.65 -2 -7 -1 341.45 15.72 201.93 112.74 2 7 1 338.74 19.59 204.15 112.28 -3 -7 -1 66.03 2.71 64.97 -1. 3 7 1 75.3 4.45 64.92 -1. -4 -7 -1 13.15 2.16 14.52 -1. 4 7 1 12.68 2.79 14.48 -1. 4 -8 -1 0.62 1.6 2.82 -1. -4 8 1 -0.73 1.39 2.89 -1. 3 -8 -1 101.88 3.45 108.43 -1. -3 8 1 94.94 3.72 108.16 -1. 2 -8 -1 308.13 18.77 217.76 90.06 -2 8 1 320.88 16.79 218.75 90.47 1 -8 -1 136.97 3.08 63.24 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79.23 32.06 -1 -10 -1 45.27 2.43 16.21 30.74 1 10 1 41.67 3.25 15.76 30.68 -2 -10 -1 130.51 8.84 20.08 97.47 2 10 1 124.57 7.5 19.91 97.97 -3 -10 -1 6.17 1.95 7.52 -1. 3 10 1 5.01 2.03 7.35 -1. 3 -11 -1 15.65 2.32 13. -1. -3 11 1 16.96 2.41 12.7 -1. 2 -11 -1 92.96 7.18 66.48 27.5 -2 11 1 90.1 11.72 66.23 27.39 1 -11 -1 55.26 2.7 4.89 46.62 -1 11 1 52.48 3.68 4.49 46.39 0 -11 -1 111.69 3.76 92.44 38.04 0 11 1 118.41 3.73 91.99 38.23 -1 -11 -1 160.91 4.66 108.92 59.99 1 11 1 173.65 5.93 108.2 59.56 -2 -11 -1 52.55 4.41 55.32 -1. 2 11 1 75.43 6.86 55.37 10.62 -3 -11 -1 11.83 2.92 5.34 -1. 3 11 1 5.24 1.9 5.57 -1. 2 -12 -1 65.82 6.71 49.06 20.29 -2 12 1 79.29 12.5 49.3 20.39 1 -12 -1 67.25 3.18 38.13 25.79 -1 12 1 71.22 4.26 37.8 25.72 0 -12 -1 114.23 4.11 83.03 34.42 0 12 1 117.63 4.86 83.22 34.34 -1 -12 -1 102.93 4.11 85.74 21.45 1 12 1 113.4 5.2 84.87 21.51 -2 -12 -1 18.12 3.07 17.69 -1. 2 12 1 30.35 6.1 17.83 4.97 2 -13 -1 120.78 9.03 76. 31.43 -2 13 1 121.83 6.08 75.09 31.06 1 -13 -1 69.02 4.53 48.5 23.28 -1 13 1 81.18 6.34 48.48 23.01 0 -13 -1 48.96 3.07 35.37 14.52 0 13 1 55.68 3.89 35.11 14.63 -1 -13 -1 55.36 4.14 5.05 52.63 1 13 1 64.36 4.35 5.02 52.82 1 -14 -1 15.64 5.81 16.62 2.06 -1 14 1 11.16 3.68 16.62 -1. 0 -14 -1 27.67 3.64 12.36 5.23 0 14 1 26.3 9.11 12.65 5.11 4 0 -2 4.61 2.08 1.66 -1. -4 0 2 0.98 11.41 1.39 0.57 2 0 -2 1310.71 11.72 1355.74 -1. -2 0 2 1147.24 25.71 1346.35 27.28 0 0 -2 434.46 4.38 336.85 141.77 0 0 2 408.96 10.19 342.8 139.31 -2 0 -2 1115.69 21.89 948.54 104.89 2 0 2 1029.23 28.85 956.5 -1. -4 0 -2 48.38 3.06 48.6 -1. 4 0 2 53.64 7.05 48.16 -1. 5 -1 -2 8.76 4.07 6.42 -1. -5 1 2 2.64 2.72 6.44 -1. 4 -1 -2 1.8 1.11 3.02 -1. -4 1 2 5.58 11.58 3.03 1.25 3 -1 -2 96.52 2.06 91.77 -1. -3 1 2 148.54 9.4 90.65 50.17 2 -1 -2 880.44 5.89 824.26 -1. -2 1 2 832.22 14.04 824.32 49.5 1 -1 -2 207.91 6.21 210.04 2.09 -1 1 2 193.45 4.45 212.41 2.34 0 -1 -2 22.68 0.64 18.07 7.94 0 1 2 21.76 1.69 19.2 7.47 -1 -1 -2 957.44 6.49 209.89 643.43 -2 -1 -2 0.85 0.34 0.89 -1. 2 1 2 -2.11 2.11 0.72 -1. -3 -1 -2 363.18 3.99 340.62 -1. -4 -1 -2 72.51 2.52 68.14 -1. 4 1 2 86.02 4.32 68. -1. 5 -2 -2 1.67 5.5 2.16 -1. -5 2 2 1.65 2.66 2.14 -1. 4 -2 -2 70.59 2.61 60.62 -1. -4 2 2 90.46 10.88 60.6 25.06 3 -2 -2 39.47 1.72 37.66 -1. -3 2 2 42.05 6.94 38.18 0.31 2 -2 -2 25.22 0.95 21.49 -1. -2 2 2 27.02 2.75 22.34 7.79 1 -2 -2 863.83 9.47 913.94 38.22 -1 2 2 845.39 13.32 905.75 38.33 0 -2 -2 1113.53 6.75 758.4 313.6 0 2 2 1118.86 14.9 758.28 313.66 -1 -2 -2 206.67 2.13 42.86 152. 1 2 2 203.63 5.58 42.84 151.12 -2 -2 -2 30.69 0.93 28.38 -1. 2 2 2 30.48 4.72 28.48 -1. -3 -2 -2 274.99 3.5 267.95 -1. 3 2 2 303.13 14.81 269.75 -1. -4 -2 -2 11.64 1.53 11.34 -1. 4 2 2 10.11 2.21 11.35 -1. 5 -3 -2 4.5 3.43 3.93 -1. -5 3 2 3.47 3.9 3.9 -1. 4 -3 -2 53.44 3.31 48.48 -1. -4 3 2 69.29 14.99 48.38 20.01 3 -3 -2 405.14 4.61 379.82 -1. -3 3 2 403.49 15.49 381.12 3.19 2 -3 -2 208.09 2.59 217.1 -1. -2 3 2 347.35 9.23 215.93 168.85 1 -3 -2 174.6 2.98 114.73 54.74 -1 3 2 181.86 5.69 114.48 55.17 0 -3 -2 2821.06 16.14 1889.95 783.14 0 3 2 3008.44 29.94 1893.59 781.63 -1 -3 -2 379.57 3.08 110.07 244.17 1 3 2 361.97 8.2 109.95 243.79 -2 -3 -2 43.88 1.19 46.67 -1. 2 3 2 51.21 3.49 45.85 -1. -3 -3 -2 79.45 1.79 77.04 -1. 3 3 2 82.69 5.16 76.86 -1. -4 -3 -2 26.7 2.49 27.83 -1. 4 3 2 35.49 4.13 27.64 -1. 4 -4 -2 6.58 1.48 4.55 -1. -4 4 2 7.09 1.57 4.46 -1. 3 -4 -2 41.39 1.83 40.03 -1. -3 4 2 68.74 8. 40.27 32.35 2 -4 -2 308.52 14.04 321.87 38.36 -2 4 2 323.74 9.28 318.88 38.05 1 -4 -2 1577.29 14.72 940.36 486.68 -1 4 2 1558.68 20.03 941.92 482.94 0 -4 -2 69.36 1.17 34.29 14.91 0 4 2 76.6 1.94 36.04 14.18 -1 -4 -2 1048.75 6.69 788.48 224.88 1 4 2 1110. 15.29 789.23 226.12 -2 -4 -2 87.44 1.65 93.93 -1. 2 4 2 100.13 3.78 95.75 -1. -3 -4 -2 11.21 1.06 11.34 -1. 3 4 2 10.01 2.52 11.34 -1. -4 -4 -2 1.69 1.37 1.65 -1. 4 4 2 1.33 1.67 1.63 -1. 4 -5 -2 69.86 2.75 67.06 -1. -4 5 2 79.63 16.98 67.31 27.84 3 -5 -2 28.15 1.78 29.93 -1. -3 5 2 86.31 8.66 29.41 62.79 2 -5 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146.87 60.78 0 10 3 201.22 5.59 146.96 60.74 -1 -10 -3 108.08 3.41 35.6 70.26 1 10 3 110.61 6.25 36.34 70.11 -2 -10 -3 134.92 6.89 20.66 104.46 2 10 3 138.06 8.09 19.99 103.35 -3 -10 -3 4.65 1.98 5.9 -1. 3 10 3 11.76 3.63 5.7 -1. 3 -11 -3 10.02 2.23 10.97 -1. -3 11 3 13.4 2.28 11.18 -1. 2 -11 -3 47.43 4.93 25.69 22.9 -2 11 3 45.6 5.5 25.43 22.88 1 -11 -3 88.58 3.39 80.3 9.02 -1 11 3 90.27 4.56 79.4 9.06 0 -11 -3 130.61 3.39 92.38 38.88 0 11 3 142.52 6.48 94.01 38.2 -1 -11 -3 69.09 3.27 69.8 6.46 1 11 3 79.16 5.83 69.43 6.53 -2 -11 -3 19.62 6.21 0.33 11.1 2 11 3 23.75 5.6 0.3 11.17 2 -12 -3 16. 3.55 12.01 7.37 -2 12 3 21.11 5.42 12.1 7.32 1 -12 -3 18.49 2.89 2.13 11.94 -1 12 3 17.51 4.72 2.27 11.81 0 -12 -3 23.97 2.44 18.32 7.47 0 12 3 29.32 7.88 18.07 7.57 -1 -12 -3 55.48 3.79 55.58 1.16 1 12 3 56.4 4.35 54.89 1.18 -2 -12 -3 9.38 6.74 0.95 1.82 2 12 3 11.31 5.9 1.02 1.83 1 -13 -3 21.69 3.22 14.56 4.57 -1 13 3 25.76 5.47 14.26 4.51 0 -13 -3 51.39 3.38 35.11 14.6 0 13 3 53.47 9.8 35.31 14.52 -1 -13 -3 44.36 3.83 37.96 13.35 1 13 3 49.01 5.81 38.08 13.28 4 0 -4 15.65 2.94 12.97 -1. -4 0 4 26.82 12.83 13.13 16.73 2 0 -4 298.49 3.85 250.55 -1. -2 0 4 607.36 16.06 253.61 392.29 0 0 -4 83.74 1.69 75.62 30.08 0 0 4 81.25 4.63 72.73 31.27 -2 0 -4 129.72 2.97 144.33 -1. -4 0 -4 2.27 1.51 1.91 -1. 5 -1 -4 9.69 2.86 6.57 -1. -5 1 4 19.69 8.5 6.6 3.55 4 -1 -4 238.56 4.68 203.12 -1. -4 1 4 233.36 14.36 202.68 1.7 3 -1 -4 3.1 0.87 2.41 -1. -3 1 4 63.4 7.95 2.54 68.55 2 -1 -4 3.53 0.5 1.09 -1. -2 1 4 1.69 2.34 1.17 0.37 1 -1 -4 911.63 5.95 897.19 70.28 -1 1 4 913.64 9.42 889.55 70.47 0 -1 -4 862.33 5.53 588.61 245.04 0 1 4 903.73 12.09 592.5 243.43 -1 -1 -4 82.25 1.53 75.2 9.66 1 1 4 86.96 4.42 78.48 9.27 -2 -1 -4 175.33 2.46 186.64 -1. -3 -1 -4 11.71 1.15 10.95 -1. -4 -1 -4 0.46 1.02 0.02 -1. 5 -2 -4 63.19 6.61 54.25 -1. -5 2 4 53.55 3.94 54.56 -1. 4 -2 -4 3.93 1.29 5.41 -1. -4 2 4 5.22 8.68 5.41 1.36 3 -2 -4 204.09 3.15 206.85 -1. -3 2 4 194.6 11.07 207.17 18.15 2 -2 -4 732.09 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5 9 26.46 4.22 21.06 1.31 0 -5 -9 14.1 1.64 9.51 3.95 0 5 9 15.38 3.46 9.56 3.93 -1 -5 -9 16.69 2.18 13.97 5.06 1 5 9 26.11 4.76 14.41 5.03 3 -6 -9 9.79 2.59 10.88 -1. -3 6 9 16.61 13.44 10.91 1.32 2 -6 -9 45.99 4.19 27.12 9.4 -2 6 9 40.54 7.43 26.8 9.45 1 -6 -9 7.96 1.99 6.94 3.17 -1 6 9 8.56 5.17 6.82 3.2 0 -6 -9 27.52 2.09 19.64 8.44 0 6 9 31.54 4.22 20.4 8.12 -1 -6 -9 40.98 2.71 26.4 13.87 1 6 9 46.09 4.29 26.51 14.04 2 -7 -9 -0.67 2.91 2.15 3.73 -2 7 9 1.93 6.94 2.32 3.62 1 -7 -9 10.41 2.1 9.63 3.1 -1 7 9 16.08 5.29 9.79 3.11 0 -7 -9 117.39 3.65 85.8 35.3 0 7 9 138.67 10.5 85.35 35.48 1 -8 -9 81.11 3.61 82.3 6. -1 8 9 78.57 8.14 82.83 6. 0 -8 -9 65.62 3.31 50.48 20.98 0 8 9 67.58 8.13 50.73 20.88 2 0 -10 128.77 11.17 2.65 92.1 -2 0 10 29.98 10.36 2.61 92.04 0 0 -10 197.22 4.84 137.53 56.46 0 0 10 207.7 12.81 136.52 56.88 3 -1 -10 6.22 2.1 11.17 -1. -3 1 10 8.83 8.55 11.11 0.08 2 -1 -10 11.82 4.27 8.39 2.36 -2 1 10 10.35 6.77 8.27 2.44 1 -1 -10 21.44 2.42 27.06 0.33 -1 1 10 32.42 4.83 27.07 0.32 0 -1 -10 114.04 2.67 80.88 33.56 0 1 10 114.86 6.88 81.15 33.45 -1 -1 -10 11.55 2.11 11.86 0.56 1 1 10 22.85 4.54 12.03 0.59 3 -2 -10 13.58 2.42 11.71 -1. -3 2 10 13.37 9.2 11.75 1.22 2 -2 -10 53.36 5.32 45.6 0.22 -2 2 10 38.54 11.39 45.45 0.22 1 -2 -10 32.46 2.43 31. 6.2 -1 2 10 37.92 4.85 31.55 6.17 0 -2 -10 1.99 1.45 2.14 0.91 0 2 10 4.74 3.3 2.2 0.88 -1 -2 -10 69.27 3.03 46.08 19.45 1 2 10 81.68 6.55 45.62 19.48 3 -3 -10 8.55 2.14 9.54 -1. -3 3 10 17.1 13.03 9.43 9.03 2 -3 -10 142.9 8.74 120.4 3.15 -2 3 10 130.29 16.12 120.07 3.31 1 -3 -10 148.6 3.88 117.35 27.32 -1 3 10 169.51 7.75 117.4 27.51 0 -3 -10 93.86 2.8 69.63 29.03 0 3 10 105.39 6.12 70.19 28.8 -1 -3 -10 27.52 2.56 3.85 18.23 1 3 10 20.96 4.59 3.9 18.35 2 -4 -10 24.63 3.68 1.18 17.27 -2 4 10 3.97 9.63 1.16 17.2 1 -4 -10 67.6 2.79 78.02 0.37 -1 4 10 81.35 5.95 78.09 0.34 0 -4 -10 54.31 2.56 35.28 14.33 0 4 10 68.93 5.31 34.64 14.59 2 -5 -10 94.64 4.96 104.05 0.24 -2 5 10 114.24 16.23 104.17 0.19 1 -5 -10 20.79 2.26 12.15 5.96 -1 5 10 31.85 5.04 12.25 5.78 0 -5 -10 7.42 2.2 5.32 2.18 0 5 10 8.47 3.77 5.26 2.2 1 -6 -10 49.91 3.02 33.95 10.96 -1 6 10 50.31 7.2 33.53 10.92 0 -6 -10 0.29 1.92 0.78 0.3 0 6 10 4.19 3.73 0.73 0.32 1 0 -11 18.32 6.43 20.91 -1. -1 0 11 23.64 7.95 20.79 -1. 2 -1 -11 -7.55 7.55 6.57 0.33 -2 1 11 0.76 8.91 6.64 0.33 1 -1 -11 0.88 3.67 1.42 4.98 -1 1 11 8.79 4.73 1.35 4.9 0 -1 -11 12.15 2.08 4.95 2. 0 1 11 13.03 4.19 4.83 2.05 1 -2 -11 69.15 4.06 47.11 18.87 -1 2 11 91.24 6.76 47.04 19.06 1 -3 -11 50.87 3.77 44.37 1.61 -1 3 11 59.22 6.48 44.08 1.59