#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:43:47 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181282 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/60/2236056.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236056_Fobs loop_ _publ_author_name 'Shikhaliyev, Namig G.' 'Maharramov, Abel M.' 'Muzalevskiy, Vasily M.' 'Nenajdenko, Valentine G.' 'Khrustalev, Victor N.' _publ_section_title ; [N-(1-Azanidyl-2,2,2-trichloroethylidene)-2,2,2-trichloroethanimidamide]copper(II) ; _journal_coeditor_code AA2069 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1220 _journal_page_last m1221 _journal_volume 68 _journal_year 2012 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 98.475 _cell_angle_beta 97.525 _cell_angle_gamma 103.662 _cell_length_a 5.9317 _cell_length_b 9.0782 _cell_length_c 10.8308 _exptl_crystal_F_000 327.00 _reflns_d_resolution_high 0.7828 _cod_data_source_file aa2069Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Namik4 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 115.64 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 969.74 827.20 15.12 o 2 0 0 1732.90 1563.93 40.17 o 3 0 0 1424.67 1416.32 30.72 o 4 0 0 327.87 333.05 7.64 o 5 0 0 472.67 496.83 14.94 o 6 0 0 2.34 2.42 1.40 o 7 0 0 116.52 133.82 5.47 o -7 1 0 0.10 1.91 1.57 o -6 1 0 78.40 105.20 4.44 o -5 1 0 253.71 319.87 10.05 o -4 1 0 433.78 459.84 26.01 o -3 1 0 458.94 449.87 24.14 o -2 1 0 43.56 50.20 1.76 o -1 1 0 192.13 233.80 5.15 o 0 1 0 465.18 658.54 12.02 o 1 1 0 7595.17 7812.63 172.05 o 2 1 0 233.40 204.11 5.58 o 3 1 0 28.58 30.30 1.85 o 4 1 0 10.17 11.14 2.06 o 5 1 0 155.70 162.05 4.20 o 6 1 0 177.82 189.43 7.55 o 7 1 0 0.14 0.00 2.22 o -7 2 0 14.93 18.80 2.79 o -6 2 0 25.70 22.12 2.24 o -5 2 0 182.14 182.99 6.33 o -4 2 0 1220.03 1176.49 36.68 o -3 2 0 125.11 125.66 3.08 o -2 2 0 1189.05 1207.47 26.13 o -1 2 0 1775.40 1678.43 36.19 o 0 2 0 1540.47 1941.97 50.16 o 1 2 0 1074.60 1347.21 45.17 o 2 2 0 1786.20 1979.74 42.68 o 3 2 0 2793.24 2843.61 61.46 o 4 2 0 9.40 12.69 0.98 o 5 2 0 0.74 1.26 0.62 o 6 2 0 272.46 255.32 12.56 o -7 3 0 39.93 41.80 3.23 o -6 3 0 14.92 6.57 1.59 o -5 3 0 35.51 22.99 2.16 o -4 3 0 191.45 198.16 4.75 o -3 3 0 2338.97 2317.09 49.95 o -2 3 0 185.17 193.97 4.43 o -1 3 0 771.34 708.43 15.41 o 0 3 0 24.57 34.52 1.45 o 1 3 0 3172.51 3609.98 93.46 o 2 3 0 455.61 491.92 19.86 o 3 3 0 191.48 185.12 4.53 o 4 3 0 231.33 215.57 5.32 o 5 3 0 23.17 24.51 1.57 o 6 3 0 36.22 36.11 5.71 o -7 4 0 21.90 26.16 4.31 o -6 4 0 19.19 12.87 1.89 o -5 4 0 183.72 181.90 6.41 o -4 4 0 116.73 119.99 3.11 o -3 4 0 63.55 56.67 1.74 o -2 4 0 825.57 762.10 16.64 o -1 4 0 835.54 819.83 17.89 o 0 4 0 53.60 88.23 2.98 o 1 4 0 1.37 11.02 1.13 o 2 4 0 523.02 510.61 11.43 o 3 4 0 244.68 242.44 5.77 o 4 4 0 58.11 73.07 2.39 o 5 4 0 135.81 150.77 4.15 o 6 4 0 23.02 25.13 3.68 o -7 5 0 8.91 11.55 1.95 o -6 5 0 195.60 236.00 10.79 o -5 5 0 4.65 3.93 1.22 o -4 5 0 1530.86 1546.50 33.63 o -3 5 0 43.32 38.63 1.72 o -2 5 0 1283.53 1196.75 26.14 o -1 5 0 1720.79 1799.75 39.05 o 0 5 0 2329.57 2780.02 71.86 o 1 5 0 1679.97 1931.02 49.93 o 2 5 0 299.41 336.18 9.48 o 3 5 0 924.16 944.54 20.84 o 4 5 0 29.57 32.33 2.18 o 5 5 0 1.29 2.07 1.90 o -7 6 0 0.06 0.41 1.52 o -6 6 0 32.45 43.75 3.30 o -5 6 0 95.22 118.93 4.79 o -4 6 0 24.70 27.10 1.39 o -3 6 0 662.63 633.06 14.11 o -2 6 0 35.32 32.27 1.37 o -1 6 0 3.64 5.79 0.65 o 0 6 0 208.39 225.99 6.71 o 1 6 0 435.43 503.30 13.84 o 2 6 0 120.46 112.78 4.13 o 3 6 0 70.00 77.28 3.40 o 4 6 0 342.27 388.83 11.27 o 5 6 0 79.17 95.60 4.24 o -6 7 0 6.90 6.49 1.73 o -5 7 0 48.20 48.93 3.07 o -4 7 0 11.36 11.19 1.35 o -3 7 0 542.00 507.04 11.55 o -2 7 0 74.37 71.17 2.24 o -1 7 0 579.53 557.36 15.21 o 0 7 0 632.17 689.68 18.56 o 1 7 0 194.68 214.55 6.74 o 2 7 0 426.47 477.21 13.53 o 3 7 0 250.40 238.96 7.65 o 4 7 0 7.57 5.90 1.84 o -6 8 0 10.85 9.82 1.85 o -5 8 0 6.13 6.88 1.57 o -4 8 0 19.98 17.31 1.90 o -3 8 0 1.75 0.00 0.84 o -2 8 0 110.01 108.76 3.15 o -1 8 0 179.34 152.41 5.18 o 0 8 0 170.04 172.63 5.73 o 1 8 0 0.51 0.00 0.94 o 2 8 0 122.09 117.16 8.25 o 3 8 0 100.96 103.60 4.76 o -6 9 0 27.67 27.34 3.11 o -5 9 0 13.90 13.47 1.88 o -4 9 0 0.21 0.00 0.69 o -3 9 0 1.39 3.13 0.77 o -2 9 0 28.71 22.96 2.92 o -1 9 0 106.16 132.56 8.00 o 0 9 0 73.38 66.68 3.22 o 1 9 0 56.64 43.41 2.81 o 2 9 0 275.78 257.21 8.32 o -5 10 0 31.98 35.15 3.68 o -4 10 0 30.75 28.68 4.82 o -3 10 0 91.95 88.24 3.80 o -2 10 0 10.15 7.89 1.35 o -1 10 0 169.37 152.96 5.52 o 0 10 0 26.28 34.37 4.38 o 1 10 0 4.25 3.60 2.54 o -3 11 0 11.85 6.56 1.48 o -2 11 0 12.23 14.42 1.76 o -1 11 0 1.32 3.05 1.33 o 0 11 0 25.77 27.23 2.48 o 0 -11 1 0.88 8.76 3.17 o 1 -11 1 9.51 8.59 1.63 o 2 -11 1 0.60 0.00 1.14 o 3 -11 1 16.39 15.89 2.54 o 4 -11 1 5.70 0.00 2.79 o -2 -10 1 54.05 51.52 3.30 o -1 -10 1 94.17 101.48 4.38 o 0 -10 1 136.53 127.56 5.90 o 1 -10 1 138.85 129.43 4.87 o 2 -10 1 9.51 9.73 1.44 o 3 -10 1 4.19 0.00 1.03 o 4 -10 1 53.05 48.97 3.68 o 5 -10 1 0.06 0.00 1.33 o -3 -9 1 0.26 0.00 3.74 o -2 -9 1 16.35 11.14 4.44 o -1 -9 1 1.94 3.01 1.21 o 0 -9 1 1.71 1.58 1.03 o 1 -9 1 254.18 251.25 7.78 o 2 -9 1 1.46 0.06 1.33 o 3 -9 1 0.60 2.28 0.76 o 4 -9 1 0.25 0.00 0.77 o 5 -9 1 18.66 12.67 1.90 o 6 -9 1 14.30 16.16 2.13 o -3 -8 1 119.83 134.87 5.23 o -2 -8 1 125.22 125.89 4.88 o -1 -8 1 0.81 0.67 1.05 o 0 -8 1 1495.40 1597.75 41.80 o 1 -8 1 391.46 384.09 18.85 o 2 -8 1 573.05 560.75 12.82 o 3 -8 1 447.52 413.43 9.66 o 4 -8 1 13.78 11.82 1.77 o 5 -8 1 33.51 42.14 3.05 o 6 -8 1 8.55 8.31 1.83 o -4 -7 1 5.21 6.30 1.78 o -3 -7 1 713.87 728.03 19.89 o -2 -7 1 267.12 273.40 8.35 o -1 -7 1 0.83 1.85 0.95 o 0 -7 1 0.50 0.00 0.71 o 1 -7 1 396.24 413.70 26.14 o 2 -7 1 139.89 132.61 3.56 o 3 -7 1 156.84 171.85 4.45 o 4 -7 1 165.44 154.72 4.14 o 5 -7 1 0.64 0.00 1.65 o 6 -7 1 20.60 21.44 4.76 o -5 -6 1 1.22 1.27 1.24 o -4 -6 1 5.77 4.36 1.25 o -3 -6 1 37.88 42.30 2.46 o -2 -6 1 54.09 62.33 2.96 o -1 -6 1 827.84 951.78 25.29 o 0 -6 1 83.57 98.25 3.57 o 1 -6 1 1.94 3.91 0.51 o 2 -6 1 179.75 187.32 4.62 o 3 -6 1 795.40 772.93 17.15 o 4 -6 1 80.98 80.75 2.47 o 5 -6 1 25.41 19.61 4.38 o 6 -6 1 12.37 7.53 1.83 o 7 -6 1 9.98 3.81 1.69 o -5 -5 1 54.00 60.43 5.46 o -4 -5 1 21.15 24.25 1.97 o -3 -5 1 226.19 208.53 5.53 o -2 -5 1 157.09 162.61 6.15 o -1 -5 1 17.33 17.59 2.73 o 0 -5 1 2230.89 2420.23 62.31 o 1 -5 1 910.14 1005.43 21.92 o 2 -5 1 14.43 11.04 1.14 o 3 -5 1 3.97 4.38 0.60 o 4 -5 1 143.14 158.37 4.08 o 5 -5 1 21.83 20.42 2.13 o 6 -5 1 35.61 43.50 3.20 o 7 -5 1 20.43 22.66 2.58 o -6 -4 1 22.66 16.88 3.30 o -5 -4 1 261.87 240.68 6.42 o -4 -4 1 40.40 34.81 1.67 o -3 -4 1 46.43 42.65 1.79 o -2 -4 1 1.21 0.75 0.38 o -1 -4 1 19.86 33.41 1.83 o 0 -4 1 627.23 768.26 20.14 o 1 -4 1 705.04 708.53 18.43 o 2 -4 1 1.03 1.76 0.82 o 3 -4 1 172.90 149.27 3.68 o 4 -4 1 197.45 204.89 5.02 o 5 -4 1 160.26 190.74 9.26 o 6 -4 1 60.07 81.28 4.03 o 7 -4 1 11.14 9.42 1.89 o -6 -3 1 12.96 5.81 1.48 o -5 -3 1 3.35 2.61 1.81 o -4 -3 1 1944.79 1918.89 41.58 o -3 -3 1 329.19 372.10 8.45 o -2 -3 1 1351.02 1563.69 33.67 o -1 -3 1 4081.08 4685.30 202.48 o 0 -3 1 1380.47 1836.90 47.84 o 1 -3 1 7843.71 7883.78 436.61 o 2 -3 1 159.30 113.55 4.09 o 3 -3 1 811.82 694.82 15.29 o 4 -3 1 24.99 32.89 1.40 o 5 -3 1 58.14 69.37 3.36 o 6 -3 1 172.75 210.09 7.40 o 7 -3 1 11.01 16.90 2.16 o -6 -2 1 63.47 82.27 3.95 o -5 -2 1 36.50 52.44 1.95 o -4 -2 1 38.23 29.93 1.41 o -3 -2 1 2320.60 2326.20 50.12 o -2 -2 1 2473.48 2649.22 57.08 o -1 -2 1 1436.22 1745.61 57.90 o 0 -2 1 2219.27 2840.23 54.01 o 1 -2 1 2455.17 2562.67 61.96 o 2 -2 1 1554.43 1432.92 31.36 o 3 -2 1 148.87 162.01 3.86 o 4 -2 1 647.56 630.72 21.15 o 5 -2 1 27.02 30.45 2.63 o 6 -2 1 9.15 8.97 2.35 o 7 -2 1 129.59 159.33 6.19 o -7 -1 1 35.33 38.34 4.44 o -6 -1 1 21.04 26.06 2.60 o -5 -1 1 275.79 293.41 6.97 o -4 -1 1 117.95 117.85 3.13 o -3 -1 1 191.63 186.35 4.41 o -2 -1 1 3184.77 3270.56 70.27 o -1 -1 1 3484.30 3517.38 76.23 o 0 -1 1 928.14 1081.97 20.68 o 1 -1 1 5679.90 5518.91 140.42 o 2 -1 1 2894.84 2680.80 58.11 o 3 -1 1 2112.42 1917.29 56.30 o 4 -1 1 167.81 118.46 4.06 o 5 -1 1 9.05 3.21 0.79 o 6 -1 1 101.08 89.45 4.08 o 7 -1 1 4.48 1.79 2.09 o -7 0 1 64.62 67.85 3.81 o -6 0 1 270.87 288.11 11.87 o -5 0 1 2.91 6.34 1.28 o -4 0 1 848.60 861.40 18.95 o -3 0 1 45.86 40.21 2.27 o -2 0 1 212.91 193.03 4.35 o -1 0 1 758.70 756.42 14.86 o 0 0 1 1210.61 962.47 44.73 o 1 0 1 6.82 8.27 0.68 o 2 0 1 5851.87 5731.63 123.20 o 3 0 1 2393.78 2436.71 57.64 o 4 0 1 81.68 76.14 2.61 o 5 0 1 8.45 11.19 2.31 o 6 0 1 0.30 0.00 1.27 o 7 0 1 21.25 20.21 2.29 o -7 1 1 18.12 18.32 2.22 o -6 1 1 28.38 19.67 2.15 o -5 1 1 456.83 406.22 12.52 o -4 1 1 92.97 84.11 3.78 o -3 1 1 116.71 88.79 2.20 o -2 1 1 64.09 59.81 2.20 o -1 1 1 428.37 412.00 7.48 o 0 1 1 1403.40 1435.22 56.18 o 1 1 1 22.20 13.60 0.50 o 2 1 1 883.97 846.87 20.42 o 3 1 1 147.28 112.93 2.93 o 4 1 1 1057.56 1137.79 24.93 o 5 1 1 269.69 292.57 7.02 o 6 1 1 7.86 11.54 1.78 o -7 2 1 4.26 5.02 1.76 o -6 2 1 19.15 23.71 2.44 o -5 2 1 584.02 600.98 17.95 o -4 2 1 740.26 660.48 19.38 o -3 2 1 2026.03 2113.27 59.76 o -2 2 1 9.31 12.85 0.62 o -1 2 1 4764.00 4734.89 102.34 o 0 2 1 2923.26 3128.75 96.60 o 1 2 1 133.43 103.28 4.04 o 2 2 1 649.27 606.28 13.28 o 3 2 1 151.15 145.49 3.66 o 4 2 1 45.61 34.86 1.54 o 5 2 1 5.99 7.32 0.88 o 6 2 1 128.75 145.51 10.15 o -7 3 1 23.39 35.33 3.11 o -6 3 1 9.97 11.49 1.77 o -5 3 1 39.59 25.26 2.28 o -4 3 1 404.53 396.40 12.02 o -3 3 1 168.93 172.99 4.07 o -2 3 1 1742.58 1673.28 36.16 o -1 3 1 1796.26 1883.73 40.93 o 0 3 1 482.74 507.05 11.14 o 1 3 1 2431.24 2744.43 59.31 o 2 3 1 28.08 14.27 0.85 o 3 3 1 692.32 715.56 15.82 o 4 3 1 14.36 17.81 1.22 o 5 3 1 80.63 101.71 3.13 o 6 3 1 0.19 0.12 1.36 o -7 4 1 14.33 18.03 2.25 o -6 4 1 59.60 71.53 3.76 o -5 4 1 63.15 67.77 3.40 o -4 4 1 12.67 15.40 1.71 o -3 4 1 699.22 627.80 13.83 o -2 4 1 3174.89 3065.89 66.29 o -1 4 1 2593.59 2445.73 53.16 o 0 4 1 39.36 33.80 2.04 o 1 4 1 641.95 819.16 21.51 o 2 4 1 2925.27 3357.45 72.34 o 3 4 1 25.73 21.66 1.68 o 4 4 1 152.52 128.37 3.57 o 5 4 1 9.42 6.98 1.52 o -7 5 1 15.92 19.60 2.60 o -6 5 1 135.60 153.81 8.25 o -5 5 1 15.24 14.93 1.88 o -4 5 1 28.18 21.35 2.55 o -3 5 1 292.07 285.16 6.61 o -2 5 1 44.36 33.20 1.43 o -1 5 1 569.87 581.28 12.91 o 0 5 1 110.10 121.49 3.96 o 1 5 1 204.41 216.96 6.49 o 2 5 1 224.81 225.97 6.80 o 3 5 1 76.11 78.95 3.26 o 4 5 1 263.26 260.81 7.86 o 5 5 1 5.60 6.42 1.52 o -7 6 1 16.26 13.95 2.16 o -6 6 1 56.49 53.18 3.93 o -5 6 1 88.49 86.99 3.88 o -4 6 1 0.29 0.48 0.45 o -3 6 1 25.44 17.67 1.11 o -2 6 1 1318.72 1303.73 42.65 o -1 6 1 1.67 1.98 0.95 o 0 6 1 1413.95 1468.47 46.83 o 1 6 1 1155.55 1240.85 32.50 o 2 6 1 3.81 1.89 0.94 o 3 6 1 42.20 56.43 2.96 o 4 6 1 179.15 193.78 6.52 o -6 7 1 12.94 9.63 1.85 o -5 7 1 166.57 151.89 6.28 o -4 7 1 272.86 281.21 6.70 o -3 7 1 7.09 10.07 0.89 o -2 7 1 48.56 49.76 1.80 o -1 7 1 166.14 169.87 7.40 o 0 7 1 284.64 316.29 9.15 o 1 7 1 137.29 146.69 5.06 o 2 7 1 9.22 7.14 1.28 o 3 7 1 0.53 0.00 1.27 o 4 7 1 0.68 0.00 1.27 o -6 8 1 11.27 14.05 1.97 o -5 8 1 3.96 2.97 1.40 o -4 8 1 77.60 70.28 2.44 o -3 8 1 264.09 272.35 6.65 o -2 8 1 18.47 9.87 0.87 o -1 8 1 7.78 2.81 1.00 o 0 8 1 147.50 139.76 4.85 o 1 8 1 659.78 647.19 17.76 o 2 8 1 24.27 24.23 2.17 o 3 8 1 168.57 170.25 6.16 o -5 9 1 46.61 52.29 3.35 o -4 9 1 19.82 12.62 1.61 o -3 9 1 133.95 106.64 4.06 o -2 9 1 362.25 347.05 17.07 o -1 9 1 1.84 2.46 1.09 o 0 9 1 52.26 61.37 3.03 o 1 9 1 6.55 7.27 2.41 o 2 9 1 100.30 108.38 7.74 o -5 10 1 3.69 2.08 2.28 o -4 10 1 0.42 1.65 2.79 o -3 10 1 0.52 0.00 0.95 o -2 10 1 1.86 0.47 1.02 o -1 10 1 0.21 0.63 1.33 o 0 10 1 2.75 2.43 1.24 o 1 10 1 46.86 37.14 2.75 o -3 11 1 20.07 18.95 2.13 o -2 11 1 37.51 36.87 3.87 o -1 11 1 72.05 66.77 7.49 o 0 -11 2 16.76 12.96 4.25 o 1 -11 2 86.46 94.46 4.13 o 2 -11 2 75.44 70.44 3.52 o 3 -11 2 14.10 9.71 1.59 o -2 -10 2 73.42 66.13 3.71 o -1 -10 2 3.14 0.41 1.27 o 0 -10 2 86.62 77.26 3.61 o 1 -10 2 20.93 15.87 4.31 o 2 -10 2 52.79 58.00 3.05 o 3 -10 2 15.92 10.72 1.55 o 4 -10 2 26.04 25.22 2.79 o 5 -10 2 4.53 2.96 1.53 o -3 -9 2 0.45 0.00 2.41 o -2 -9 2 91.14 102.84 4.48 o -1 -9 2 142.81 134.07 5.04 o 0 -9 2 0.43 0.00 1.71 o 1 -9 2 395.53 380.66 15.10 o 2 -9 2 85.72 86.25 3.54 o 3 -9 2 82.31 86.58 3.06 o 4 -9 2 118.21 118.12 3.67 o 5 -9 2 15.69 13.07 3.30 o -4 -8 2 341.90 351.32 10.76 o -3 -8 2 65.11 57.68 3.25 o -2 -8 2 35.70 33.59 2.36 o -1 -8 2 154.11 169.86 5.88 o 0 -8 2 59.14 64.10 3.13 o 1 -8 2 132.56 120.99 5.52 o 2 -8 2 93.19 84.70 2.67 o 3 -8 2 63.28 81.86 2.72 o 4 -8 2 15.95 13.00 1.12 o 5 -8 2 9.23 9.51 1.76 o 6 -8 2 18.63 20.83 4.31 o -4 -7 2 40.11 48.67 2.96 o -3 -7 2 98.76 109.40 4.32 o -2 -7 2 16.96 10.43 1.45 o -1 -7 2 418.47 423.14 12.04 o 0 -7 2 214.56 252.65 7.68 o 1 -7 2 5.27 4.80 0.61 o 2 -7 2 272.32 219.79 5.40 o 3 -7 2 74.37 81.17 2.60 o 4 -7 2 74.98 77.84 2.56 o 5 -7 2 37.36 26.02 4.89 o 6 -7 2 1.88 3.12 1.57 o -5 -6 2 100.27 98.72 4.09 o -4 -6 2 91.06 84.76 3.59 o -3 -6 2 205.68 215.66 6.68 o -2 -6 2 530.13 572.03 15.63 o -1 -6 2 1014.08 1158.68 30.49 o 0 -6 2 91.55 94.30 3.59 o 1 -6 2 172.53 166.34 4.17 o 2 -6 2 863.33 798.51 19.14 o 3 -6 2 360.75 326.40 7.61 o 4 -6 2 11.87 8.10 0.85 o 5 -6 2 11.27 12.27 1.68 o 6 -6 2 15.16 14.02 3.05 o 7 -6 2 3.29 4.70 1.76 o -5 -5 2 79.12 78.73 6.79 o -4 -5 2 185.70 207.74 6.39 o -3 -5 2 1.90 0.00 0.95 o -2 -5 2 340.47 391.57 16.69 o -1 -5 2 95.65 102.86 3.59 o 0 -5 2 2.05 4.31 1.90 o 1 -5 2 136.78 130.99 6.51 o 2 -5 2 104.23 96.38 4.77 o 3 -5 2 1592.64 1519.42 33.07 o 4 -5 2 53.84 53.63 1.94 o 5 -5 2 53.87 68.42 3.36 o 6 -5 2 0.33 0.30 1.48 o 7 -5 2 6.37 6.57 1.76 o -6 -4 2 81.42 72.97 5.46 o -5 -4 2 322.63 324.86 9.61 o -4 -4 2 96.73 76.86 2.36 o -3 -4 2 97.63 105.26 2.87 o -2 -4 2 1383.19 1422.41 30.80 o -1 -4 2 4630.44 5549.73 142.67 o 0 -4 2 590.92 637.86 14.04 o 1 -4 2 328.33 325.75 17.08 o 2 -4 2 2628.11 2581.61 55.72 o 3 -4 2 208.77 202.11 5.28 o 4 -4 2 1105.58 1064.47 38.53 o 5 -4 2 139.58 133.03 4.76 o 6 -4 2 10.08 11.19 1.80 o 7 -4 2 1.81 1.02 1.50 o -6 -3 2 21.25 18.53 2.19 o -5 -3 2 608.59 635.90 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