#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:46:20 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181288 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/66/2236696.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236696_Fobs loop_ _publ_author_name 'Yang, Hexiong' 'Jenkins, Neil G.' 'Downs, Robert T.' _publ_section_title ; Redetermination of junitoite, CaZn~2~Si~2~O~7~·H~2~O ; _journal_coeditor_code WM2677 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first i73 _journal_volume 68 _journal_year 2012 _space_group_IT_number 41 _symmetry_space_group_name_Hall 'A 2 -2ab' _symmetry_space_group_name_H-M 'A b a 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 12.5302 _cell_length_b 6.3056 _cell_length_c 8.5617 _exptl_crystal_F_000 696.00 _reflns_d_resolution_high 0.6482 _cod_data_source_file wm2677Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' juni in Aba2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 343.69 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z' 'x, y+1/2, z+1/2' '-x, -y+1/2, z+1/2' 'x+1/2, -y+1, z+1/2' '-x+1/2, y+1, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 -12 5299.08 5283.48 227.24 o 4 2 -12 10381.57 10885.37 442.16 o 5 2 -12 7.81 4.33 19.93 o 6 2 -12 1450.04 1490.92 82.59 o 2 1 -11 128.82 104.00 21.67 o 3 1 -11 675.74 614.46 43.39 o 4 1 -11 10.39 18.22 11.93 o 5 1 -11 419.78 440.88 42.50 o 6 1 -11 147.44 166.01 18.07 o 7 1 -11 2292.71 2268.36 77.32 o 8 1 -11 50.80 41.15 14.39 o 9 1 -11 1727.72 1719.88 63.05 o 10 1 -11 108.45 122.48 18.07 o 2 3 -11 26.76 59.78 20.79 o 3 3 -11 340.19 369.38 39.02 o 4 3 -11 8.25 6.93 18.19 o 5 3 -11 101.02 107.45 24.26 o 6 3 -11 84.47 95.32 24.26 o 7 3 -11 2045.26 1977.47 70.49 o 8 3 -11 50.93 49.32 15.00 o 2 5 -11 29.58 18.19 20.79 o 3 5 -11 631.64 719.28 53.79 o 2 0 -10 5847.21 6113.27 261.54 o 4 0 -10 16977.78 17649.99 695.16 o 6 0 -10 2841.18 2777.76 125.71 o 8 0 -10 5490.33 5431.47 228.43 o 10 0 -10 3005.87 2826.13 129.17 o 12 0 -10 7301.38 7257.60 300.53 o 0 2 -10 6388.52 6669.42 274.18 o 1 2 -10 5.22 7.80 13.86 o 2 2 -10 8082.72 8413.96 320.55 o 3 2 -10 77.61 57.19 19.06 o 4 2 -10 1620.04 1620.49 58.14 o 5 2 -10 70.94 65.91 13.16 o 6 2 -10 8479.49 8591.70 247.01 o 7 2 -10 5.45 2.17 10.41 o 8 2 -10 5490.12 5482.69 163.66 o 9 2 -10 9.43 6.37 11.22 o 10 2 -10 3965.75 3946.77 122.47 o 11 2 -10 45.43 46.01 14.31 o 0 4 -10 3837.87 3939.84 158.36 o 1 4 -10 73.16 64.12 19.93 o 2 4 -10 3964.57 4080.94 188.16 o 3 4 -10 168.08 166.41 26.87 o 4 4 -10 11464.65 12122.07 490.19 o 5 4 -10 152.81 153.40 26.00 o 6 4 -10 1921.86 1911.59 96.62 o 7 4 -10 57.39 54.59 14.70 o 8 4 -10 3471.46 3434.75 109.34 o 9 4 -10 13.76 7.36 12.87 o 1 6 -10 26.16 32.92 20.79 o 2 6 -10 4338.25 4521.57 189.93 o 3 6 -10 265.31 276.54 35.54 o 4 6 -10 771.98 773.32 53.81 o 1 1 -9 430.08 457.79 19.34 o 2 1 -9 88.68 95.29 11.94 o 3 1 -9 1903.44 1905.89 61.00 o 4 1 -9 23.99 25.85 9.48 o 5 1 -9 3067.23 2940.70 90.86 o 6 1 -9 313.42 298.64 20.53 o 7 1 -9 80.71 82.83 13.16 o 8 1 -9 72.53 69.28 12.55 o 9 1 -9 581.40 523.39 27.61 o 10 1 -9 11.70 3.90 10.41 o 11 1 -9 678.88 640.79 32.11 o 12 1 -9 92.82 106.55 15.62 o 13 1 -9 1381.23 1313.42 50.07 o 1 3 -9 77.14 68.09 12.46 o 2 3 -9 51.79 17.33 13.86 o 3 3 -9 691.66 705.73 45.14 o 4 3 -9 15.07 1.73 10.40 o 5 3 -9 1547.53 1606.42 56.59 o 6 3 -9 142.17 152.65 16.84 o 7 3 -9 79.96 58.55 12.87 o 8 3 -9 56.23 56.77 13.16 o 9 3 -9 214.15 209.45 19.61 o 10 3 -9 9.58 19.15 11.93 o 11 3 -9 195.87 174.83 26.87 o 12 3 -9 97.89 83.77 15.54 o 1 5 -9 526.82 541.15 31.88 o 2 5 -9 48.50 37.26 18.20 o 3 5 -9 1788.41 1726.76 87.90 o 4 5 -9 13.70 -8.66 14.73 o 5 5 -9 2517.18 2521.41 118.57 o 6 5 -9 90.38 86.65 21.66 o 7 5 -9 111.20 91.86 23.40 o 8 5 -9 60.41 62.16 15.32 o 9 5 -9 615.81 630.62 36.01 o 10 5 -9 87.41 99.65 22.53 o 1 7 -9 41.23 13.86 19.93 o 2 7 -9 4.02 -1.73 20.79 o 0 0 -8 50306.88 49114.28 1895.35 o 2 0 -8 8270.78 8135.77 224.14 o 4 0 -8 4966.04 5004.10 212.17 o 6 0 -8 6045.90 6113.40 248.88 o 8 0 -8 24577.69 23795.32 927.64 o 10 0 -8 1551.19 1543.45 75.69 o 12 0 -8 1208.65 1237.53 65.18 o 14 0 -8 2481.07 2464.83 113.31 o 0 2 -8 3994.59 3856.68 99.61 o 1 2 -8 21.61 6.79 6.16 o 2 2 -8 14059.70 14062.58 325.36 o 3 2 -8 73.61 82.17 11.03 o 4 2 -8 6361.13 6684.65 195.24 o 5 2 -8 79.70 68.99 10.71 o 6 2 -8 11108.77 11265.37 316.38 o 7 2 -8 15.60 3.34 8.25 o 8 2 -8 4783.49 4846.92 142.49 o 9 2 -8 30.57 33.84 10.20 o 10 2 -8 12928.71 12767.90 358.24 o 11 2 -8 44.41 66.91 16.46 o 12 2 -8 4039.90 3994.96 120.97 o 13 2 -8 38.04 38.58 12.21 o 14 2 -8 4179.69 4276.15 144.38 o 0 4 -8 27750.78 28490.65 1081.02 o 1 4 -8 98.82 112.27 14.39 o 2 4 -8 5144.22 5027.00 188.60 o 3 4 -8 378.44 357.33 33.82 o 4 4 -8 4525.88 4512.50 185.14 o 5 4 -8 239.07 257.92 45.08 o 6 4 -8 3845.44 3868.91 178.60 o 7 4 -8 45.95 42.68 11.94 o 8 4 -8 14386.01 14609.36 409.55 o 9 4 -8 36.32 42.28 12.21 o 10 4 -8 1108.16 1077.20 42.95 o 11 4 -8 188.86 184.50 18.11 o 12 4 -8 1375.50 1347.72 50.91 o 13 4 -8 65.98 71.40 14.56 o 1 6 -8 156.98 149.40 17.77 o 2 6 -8 6362.73 6234.75 192.68 o 3 6 -8 159.90 175.94 26.00 o 4 6 -8 4358.51 4479.28 203.21 o 5 6 -8 191.73 185.49 28.60 o 6 6 -8 5181.86 5090.84 216.72 o 7 6 -8 142.39 131.73 24.27 o 8 6 -8 1668.71 1570.93 80.90 o 9 6 -8 185.87 166.17 18.88 o 1 1 -7 741.83 730.87 19.20 o 2 1 -7 227.22 243.18 10.51 o 3 1 -7 8450.37 8346.57 194.12 o 4 1 -7 59.18 49.77 8.58 o 5 1 -7 4978.61 4788.43 141.45 o 6 1 -7 100.73 93.10 15.17 o 7 1 -7 999.75 985.58 35.65 o 8 1 -7 63.01 51.54 9.48 o 9 1 -7 753.83 735.11 29.47 o 10 1 -7 291.65 282.87 22.54 o 11 1 -7 1937.40 1844.76 60.66 o 12 1 -7 215.37 210.17 16.85 o 13 1 -7 3864.07 3916.06 117.55 o 14 1 -7 117.64 109.89 14.09 o 15 1 -7 272.55 274.10 19.92 o 16 1 -7 81.17 64.84 12.82 o 1 3 -7 1879.26 1889.75 48.47 o 2 3 -7 148.96 161.78 11.57 o 3 3 -7 5261.40 5347.04 127.21 o 4 3 -7 39.96 34.10 6.59 o 5 3 -7 2747.30 2663.87 63.38 o 6 3 -7 84.25 89.94 11.64 o 7 3 -7 1579.87 1552.02 52.93 o 8 3 -7 61.19 48.99 10.71 o 9 3 -7 1467.45 1450.66 63.07 o 10 3 -7 239.64 231.06 18.01 o 11 3 -7 1216.92 1230.58 44.81 o 12 3 -7 162.64 177.16 16.51 o 13 3 -7 2528.76 2488.51 79.74 o 14 3 -7 68.43 71.83 12.91 o 15 3 -7 510.21 545.57 37.30 o 1 5 -7 104.44 125.62 42.03 o 2 5 -7 57.60 82.77 12.87 o 3 5 -7 4838.48 4882.16 145.32 o 4 5 -7 33.43 22.53 14.73 o 5 5 -7 3337.15 3474.31 107.27 o 6 5 -7 32.70 40.33 17.76 o 7 5 -7 350.08 343.07 16.62 o 8 5 -7 39.97 44.64 12.21 o 9 5 -7 229.20 208.32 18.63 o 10 5 -7 161.66 163.49 17.65 o 11 5 -7 1599.35 1485.51 54.03 o 12 5 -7 113.84 97.30 15.40 o 1 7 -7 936.61 1000.35 42.06 o 2 7 -7 62.12 80.48 15.32 o 3 7 -7 2127.80 2079.84 104.51 o 4 7 -7 8.33 21.66 18.19 o 5 7 -7 1149.24 1133.78 66.03 o 6 7 -7 10.44 19.93 17.33 o 7 7 -7 777.55 841.07 54.68 o 8 7 -7 28.31 21.66 18.19 o 0 0 -6 8554.48 8760.99 360.47 o 2 0 -6 23596.79 23397.39 624.01 o 4 0 -6 27089.85 26779.04 560.39 o 6 0 -6 13227.25 13092.46 506.88 o 8 0 -6 6994.79 6799.60 271.35 o 10 0 -6 13854.06 13932.06 546.13 o 12 0 -6 10938.00 10662.66 422.26 o 14 0 -6 3081.01 2875.74 124.88 o 16 0 -6 2072.18 2146.33 97.52 o 0 2 -6 43608.39 44457.57 1234.45 o 1 2 -6 153.82 152.35 7.88 o 2 2 -6 16759.41 16814.77 291.54 o 3 2 -6 83.14 88.24 6.33 o 4 2 -6 9661.47 9351.08 160.86 o 5 2 -6 42.53 49.42 8.58 o 6 2 -6 14043.34 14137.09 396.98 o 7 2 -6 86.02 82.02 11.70 o 8 2 -6 21917.38 21953.75 604.08 o 9 2 -6 76.96 77.36 10.36 o 10 2 -6 4777.13 4523.03 131.71 o 11 2 -6 33.38 38.34 9.75 o 12 2 -6 5789.78 5683.02 163.65 o 13 2 -6 8.10 11.95 8.74 o 14 2 -6 5943.96 5908.81 170.98 o 15 2 -6 31.87 26.28 10.82 o 16 2 -6 6618.45 6504.28 187.28 o 0 4 -6 4113.47 4111.96 173.93 o 1 4 -6 461.63 498.75 19.15 o 2 4 -6 13727.38 13934.62 303.59 o 3 4 -6 55.04 41.09 7.47 o 4 4 -6 16725.65 16962.04 385.52 o 5 4 -6 62.72 65.76 7.52 o 6 4 -6 8357.31 8467.98 182.59 o 7 4 -6 355.11 354.39 14.60 o 8 4 -6 3519.90 3416.55 103.33 o 9 4 -6 253.78 259.84 22.11 o 10 4 -6 9072.42 9156.58 259.83 o 11 4 -6 35.74 48.40 11.22 o 12 4 -6 7756.24 7605.69 217.98 o 13 4 -6 36.19 22.91 10.83 o 14 4 -6 2390.30 2331.80 111.54 o 15 4 -6 123.46 115.66 14.56 o 0 6 -6 15574.04 16032.26 628.13 o 1 6 -6 369.28 416.36 25.12 o 2 6 -6 6153.11 6068.75 241.46 o 3 6 -6 266.72 298.45 22.07 o 4 6 -6 2908.85 2806.85 79.88 o 5 6 -6 171.35 131.75 21.67 o 6 6 -6 5819.58 5781.19 173.86 o 7 6 -6 230.70 226.17 19.24 o 8 6 -6 9883.78 10215.03 221.84 o 9 6 -6 239.93 223.80 13.11 o 10 6 -6 2069.70 2085.94 188.96 o 11 6 -6 136.56 126.01 16.24 o 12 6 -6 2279.21 2261.77 75.22 o 0 8 -6 1182.72 1160.79 65.16 o 1 8 -6 445.10 451.63 30.35 o 2 8 -6 4514.20 4433.36 131.60 o 3 8 -6 127.67 142.13 26.87 o 4 8 -6 5885.33 5901.28 260.05 o 5 8 -6 126.51 136.93 25.13 o 6 8 -6 3091.72 2906.02 133.52 o 1 1 -5 3199.08 3224.97 55.80 o 2 1 -5 322.07 314.96 7.58 o 3 1 -5 51.59 58.53 7.25 o 4 1 -5 46.87 37.30 6.55 o 5 1 -5 2276.00 2118.67 55.04 o 6 1 -5 38.28 46.06 7.03 o 7 1 -5 1799.53 1729.52 52.74 o 8 1 -5 205.30 218.23 16.47 o 9 1 -5 2847.08 2840.48 147.84 o 10 1 -5 418.88 414.25 18.99 o 11 1 -5 129.78 124.80 11.33 o 12 1 -5 179.54 160.74 12.87 o 13 1 -5 424.93 403.73 19.87 o 14 1 -5 96.12 109.44 12.21 o 15 1 -5 327.43 345.43 20.12 o 16 1 -5 256.53 299.66 23.41 o 17 1 -5 1202.57 1198.05 41.72 o 1 3 -5 6501.16 6577.11 99.55 o 2 3 -5 217.07 223.94 6.99 o 3 3 -5 936.57 904.65 21.68 o 4 3 -5 62.28 65.07 7.38 o 5 3 -5 2889.49 2821.18 57.98 o 6 3 -5 119.79 125.74 7.86 o 7 3 -5 3343.24 3266.62 97.27 o 8 3 -5 144.06 141.20 12.21 o 9 3 -5 4367.10 4339.22 126.35 o 10 3 -5 285.10 280.08 28.18 o 11 3 -5 136.69 165.52 15.60 o 12 3 -5 136.47 135.51 16.47 o 13 3 -5 963.31 980.63 36.35 o 14 3 -5 149.85 151.58 13.74 o 15 3 -5 830.22 802.39 31.64 o 16 3 -5 147.28 188.46 23.83 o 1 5 -5 959.00 921.34 35.03 o 2 5 -5 10.51 21.59 6.96 o 3 5 -5 95.48 86.07 10.48 o 4 5 -5 13.88 15.10 7.16 o 5 5 -5 1066.88 1091.57 47.77 o 6 5 -5 60.71 61.00 7.86 o 7 5 -5 432.20 482.18 17.43 o 8 5 -5 75.06 79.32 8.08 o 9 5 -5 1060.84 1015.42 38.58 o 10 5 -5 69.04 72.06 12.28 o 11 5 -5 258.14 231.05 17.71 o 12 5 -5 131.60 134.55 16.47 o 13 5 -5 172.22 190.53 16.82 o 14 5 -5 138.93 139.26 14.42 o 1 7 -5 2676.14 2549.33 84.18 o 2 7 -5 122.04 124.30 16.16 o 3 7 -5 313.35 320.78 35.98 o 4 7 -5 32.90 43.10 12.21 o 5 7 -5 1121.43 1100.01 62.56 o 6 7 -5 223.88 267.86 29.47 o 8 7 -5 39.94 59.05 13.53 o 9 7 -5 1971.62 1967.02 49.98 o 10 7 -5 79.48 67.44 16.90 o 11 7 -5 137.27 137.22 16.90 o 0 0 -4 3320.60 2848.35 134.54 o 2 0 -4 46418.12 46497.21 978.39 o 4 0 -4 9349.47 9260.64 338.40 o 6 0 -4 49640.72 50544.47 1945.83 o 8 0 -4 10199.79 10066.39 393.75 o 10 0 -4 21416.27 21507.41 833.03 o 12 0 -4 5253.42 5406.61 216.55 o 14 0 -4 18134.52 18174.36 707.19 o 16 0 -4 2298.02 2287.48 98.47 o 18 0 -4 3148.81 3110.78 130.05 o 0 2 -4 21752.88 21968.96 462.95 o 1 2 -4 387.86 389.24 9.52 o 2 2 -4 16468.54 16966.47 351.43 o 3 2 -4 38.23 40.72 4.14 o 4 2 -4 107637.84 113647.31 3683.76 o 5 2 -4 45.70 45.98 5.75 o 6 2 -4 5400.24 5168.25 144.10 o 7 2 -4 243.17 252.03 13.94 o 8 2 -4 5430.74 5312.24 150.29 o 9 2 -4 74.00 75.85 8.51 o 10 2 -4 4888.78 4780.06 136.30 o 11 2 -4 5.63 8.91 6.24 o 12 2 -4 26929.46 26820.53 734.77 o 13 2 -4 13.47 16.46 13.00 o 14 2 -4 929.87 992.16 38.22 o 15 2 -4 76.30 62.96 10.83 o 16 2 -4 2046.46 2048.70 63.55 o 17 2 -4 13.53 10.00 6.93 o 0 4 -4 7886.96 7986.16 228.68 o 1 4 -4 313.92 305.79 12.28 o 2 4 -4 23175.05 23244.65 432.06 o 3 4 -4 174.38 163.42 8.17 o 4 4 -4 2885.76 2905.96 66.08 o 5 4 -4 243.05 250.78 9.97 o 6 4 -4 27361.03 27848.55 515.19 o 7 4 -4 264.34 261.88 11.63 o 8 4 -4 9325.62 9525.13 203.73 o 9 4 -4 241.81 231.71 21.67 o 10 4 -4 12927.86 12588.56 350.18 o 11 4 -4 97.93 100.72 11.66 o 12 4 -4 2388.96 2284.08 71.05 o 13 4 -4 137.41 125.42 12.18 o 14 4 -4 12915.43 12862.74 513.36 o 15 4 -4 92.93 106.90 21.23 o 16 4 -4 2275.68 2161.10 103.66 o 0 6 -4 10186.40 9924.05 397.50 o 1 6 -4 657.97 667.42 29.77 o 2 6 -4 5555.40 5470.04 153.25 o 3 6 -4 286.62 274.52 38.59 o 4 6 -4 27649.78 27129.65 617.59 o 5 6 -4 261.82 261.85 15.50 o 6 6 -4 2131.13 2211.54 189.14 o 7 6 -4 487.64 521.34 19.23 o 8 6 -4 4205.56 4273.74 115.56 o 9 6 -4 175.54 191.06 11.38 o 10 6 -4 1960.03 2020.15 66.90 o 11 6 -4 65.64 70.57 16.03 o 12 6 -4 9781.78 9997.93 283.41 o 13 6 -4 103.08 93.54 13.43 o 0 8 -4 4253.79 4315.69 184.78 o 1 8 -4 130.60 151.33 17.77 o 2 8 -4 6222.01 6261.66 186.97 o 3 8 -4 434.87 490.62 30.24 o 4 8 -4 519.78 479.84 28.34 o 5 8 -4 478.98 446.70 39.03 o 6 8 -4 8323.72 8320.51 338.55 o 7 8 -4 142.64 149.06 24.27 o 8 8 -4 4563.42 4210.79 179.54 o 9 8 -4 186.59 182.01 24.27 o 1 1 -3 11915.47 11667.31 175.98 o 2 1 -3 151.62 162.76 5.90 o 3 1 -3 4157.69 4372.10 84.35 o 4 1 -3 41.13 14.73 7.37 o 5 1 -3 6003.63 6327.38 186.16 o 6 1 -3 388.82 395.22 20.83 o 7 1 -3 7023.52 6919.70 192.17 o 8 1 -3 360.60 337.81 14.75 o 9 1 -3 5177.92 4992.28 140.27 o 10 1 -3 156.98 159.41 10.37 o 11 1 -3 1023.32 1005.49 33.13 o 12 1 -3 170.41 185.06 11.85 o 13 1 -3 815.81 821.78 28.78 o 14 1 -3 343.46 334.98 16.42 o 15 1 -3 554.32 534.17 22.99 o 16 1 -3 350.51 354.33 17.08 o 17 1 -3 2463.34 2405.60 71.09 o 18 1 -3 158.47 192.40 20.80 o 1 3 -3 14349.64 14564.28 283.24 o 2 3 -3 19.52 16.97 3.66 o 3 3 -3 137.99 130.55 7.25 o 4 3 -3 49.31 39.87 4.76 o 5 3 -3 2803.70 2794.77 54.84 o 6 3 -3 383.24 387.09 11.19 o 7 3 -3 8181.31 8212.56 176.25 o 8 3 -3 248.60 236.58 13.32 o 9 3 -3 6953.23 6777.58 190.01 o 10 3 -3 113.14 111.01 9.58 o 11 3 -3 207.34 201.57 12.66 o 12 3 -3 114.81 141.63 10.74 o 13 3 -3 392.64 401.63 18.10 o 14 3 -3 294.94 291.50 33.38 o 15 3 -3 1360.58 1360.61 69.55 o 16 3 -3 248.53 260.93 27.74 o 17 3 -3 3033.46 2942.67 130.03 o 1 5 -3 2574.62 2642.21 65.96 o 2 5 -3 62.56 60.85 7.63 o 3 5 -3 2088.11 2054.40 52.24 o 4 5 -3 19.59 15.76 4.62 o 5 5 -3 3384.35 3322.62 65.68 o 6 5 -3 210.34 218.14 9.96 o 7 5 -3 2262.64 2317.13 54.94 o 8 5 -3 110.59 120.76 8.41 o 9 5 -3 1921.04 1956.75 46.61 o 10 5 -3 12.47 9.04 8.32 o 11 5 -3 1070.20 1051.33 57.35 o 12 5 -3 131.80 144.85 13.87 o 13 5 -3 1010.06 995.97 36.10 o 14 5 -3 267.71 285.99 15.93 o 15 5 -3 100.70 71.92 21.66 o 1 7 -3 3912.47 3792.84 115.49 o 2 7 -3 143.99 151.62 16.90 o 3 7 -3 31.20 51.24 27.73 o 4 7 -3 23.34 29.83 10.71 o 5 7 -3 807.18 843.97 79.01 o 6 7 -3 212.57 227.41 18.27 o 7 7 -3 3003.82 3018.76 139.72 o 8 7 -3 78.81 63.73 13.59 o 9 7 -3 2785.86 2891.91 81.75 o 10 7 -3 105.42 113.78 18.63 o 11 7 -3 93.11 80.46 13.74 o 12 7 -3 60.71 65.51 12.47 o 1 9 -3 939.72 928.10 42.37 o 2 9 -3 22.62 25.03 14.31 o 3 9 -3 480.00 474.12 31.12 o 4 9 -3 3.91 18.19 17.33 o 5 9 -3 989.85 1055.09 59.92 o 0 0 -2 21341.51 21752.78 783.84 o 2 0 -2 51539.90 54133.59 1845.00 o 4 0 -2 83856.06 93102.45 3594.82 o 6 0 -2 24242.28 24720.68 952.38 o 8 0 -2 16583.30 17413.24 475.55 o 10 0 -2 20749.33 20977.04 810.43 o 12 0 -2 20355.24 20915.95 809.11 o 14 0 -2 4330.80 4118.53 164.92 o 16 0 -2 4001.45 3933.42 158.46 o 18 0 -2 6124.96 6125.43 239.14 o 0 2 -2 78002.09 70584.80 1907.68 o 1 2 -2 77.43 53.73 5.32 o 2 2 -2 34659.53 35045.62 723.39 o 3 2 -2 367.89 359.64 9.89 o 4 2 -2 15163.91 15920.19 305.51 o 5 2 -2 205.36 196.13 6.67 o 6 2 -2 29454.79 30826.42 673.27 o 7 2 -2 81.31 73.20 7.46 o 8 2 -2 35019.50 37161.33 826.69 o 9 2 -2 47.95 48.57 4.55 o 10 2 -2 8759.72 8917.27 246.94 o 11 2 -2 108.46 110.66 8.50 o 12 2 -2 5806.10 5756.50 161.49 o 13 2 -2 49.58 56.53 7.80 o 14 2 -2 10362.32 10567.38 418.06 o 15 2 -2 15.31 10.40 11.26 o 16 2 -2 8253.44 8042.28 322.01 o 17 2 -2 12.86 14.73 13.00 o 18 2 -2 1780.85 1639.19 76.56 o 0 4 -2 7984.95 7485.64 204.11 o 1 4 -2 480.08 475.89 14.30 o 2 4 -2 23739.66 23013.45 524.02 o 3 4 -2 356.38 343.84 13.65 o 4 4 -2 37416.43 36774.22 824.42 o 5 4 -2 363.58 356.18 11.53 o 6 4 -2 12494.72 12453.79 234.46 o 7 4 -2 304.25 308.09 10.63 o 8 4 -2 6866.01 6913.45 148.59 o 9 4 -2 182.08 164.07 11.39 o 10 4 -2 12584.07 12692.41 351.82 o 11 4 -2 150.93 149.00 11.15 o 12 4 -2 13440.01 13453.96 372.41 o 13 4 -2 128.85 147.33 21.67 o 14 4 -2 2833.26 2629.68 118.70 o 15 4 -2 109.97 98.79 20.80 o 16 4 -2 2360.84 2153.11 101.08 o 17 4 -2 41.45 55.45 17.33 o 0 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4 8254.70 8368.44 229.32 o 1 4 4 337.48 337.20 11.80 o 2 4 4 23800.99 23201.53 448.39 o 3 4 4 157.43 173.48 8.85 o 4 4 4 1833.80 1757.00 55.14 o 5 4 4 228.03 228.56 11.99 o 6 4 4 27807.33 27362.84 613.71 o 7 4 4 272.44 270.26 13.81 o 8 4 4 9412.33 9333.35 260.81 o 9 4 4 253.60 218.49 13.47 o 10 4 4 13092.02 13420.32 371.59 o 11 4 4 89.89 110.92 19.93 o 12 4 4 1759.01 1825.45 87.05 o 13 4 4 125.83 113.53 20.80 o 14 4 4 13205.52 12923.55 514.62 o 15 4 4 97.32 136.05 22.53 o 16 4 4 2308.96 2487.95 114.12 o 0 6 4 10288.91 9981.52 396.72 o 1 6 4 682.96 691.77 23.89 o 2 6 4 5210.56 5063.32 124.14 o 3 6 4 256.97 247.42 14.74 o 4 6 4 28082.91 27678.43 614.64 o 5 6 4 234.13 251.05 14.79 o 6 6 4 1788.31 1827.57 109.76 o 7 6 4 511.91 490.79 70.71 o 8 6 4 4428.77 4339.36 128.84 o 9 6 4 201.25 201.47 31.21 o 10 6 4 1872.80 1865.72 61.11 o 11 6 4 51.99 79.71 21.66 o 12 6 4 10125.55 10046.71 409.25 o 13 6 4 90.11 112.65 25.13 o 0 8 4 4324.21 4195.58 183.94 o 1 8 4 152.63 157.29 18.07 o 2 8 4 6497.23 6412.07 187.11 o 3 8 4 424.95 434.07 27.90 o 4 8 4 81.42 120.45 26.00 o 5 8 4 459.29 449.43 28.28 o 6 8 4 8561.58 8483.50 343.16 o 7 8 4 149.96 160.38 17.49 o 8 8 4 4536.32 4600.97 139.51 o 9 8 4 199.75 169.02 31.20 o 1 1 5 3104.70 3149.18 45.18 o 2 1 5 329.05 320.37 6.88 o 3 1 5 54.96 53.21 3.48 o 4 1 5 52.79 50.78 3.28 o 5 1 5 2428.63 2378.40 41.23 o 6 1 5 20.63 18.81 3.96 o 7 1 5 1661.71 1640.32 41.56 o 8 1 5 190.71 197.07 11.85 o 9 1 5 2780.91 2766.48 80.37 o 10 1 5 433.19 423.65 17.66 o 11 1 5 138.56 130.62 9.58 o 12 1 5 202.76 178.88 18.64 o 13 1 5 487.83 492.25 18.75 o 14 1 5 81.86 59.79 12.13 o 15 1 5 347.88 373.73 25.15 o 16 1 5 232.00 221.05 19.07 o 17 1 5 1119.89 1190.10 52.99 o 1 3 5 6388.37 6399.95 129.69 o 2 3 5 228.80 236.98 10.89 o 3 3 5 1016.12 957.34 23.03 o 4 3 5 64.29 63.96 5.13 o 5 3 5 3039.20 2977.90 57.40 o 6 3 5 97.28 101.27 11.26 o 7 3 5 3160.94 3172.09 89.84 o 8 3 5 137.17 147.99 11.22 o 9 3 5 4341.26 4398.36 125.93 o 10 3 5 320.20 322.17 22.11 o 11 3 5 186.81 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12 4 6 8322.14 8663.19 243.49 o 13 4 6 47.60 88.38 20.79 o 14 4 6 2075.71 2114.97 101.87 o 15 4 6 110.40 116.12 22.53 o 0 6 6 16133.71 15738.82 627.24 o 1 6 6 364.18 332.35 22.38 o 2 6 6 6857.44 6677.47 152.70 o 3 6 6 303.66 313.76 17.96 o 4 6 6 2200.79 2127.14 61.72 o 5 6 6 182.59 186.10 14.23 o 6 6 6 6198.98 5979.14 141.10 o 7 6 6 208.19 218.11 21.94 o 8 6 6 9696.05 9579.69 206.80 o 9 6 6 220.75 251.85 48.54 o 10 6 6 2100.16 2503.17 240.79 o 11 6 6 153.38 175.57 15.35 o 12 6 6 1472.74 1584.01 86.07 o 0 8 6 864.68 853.42 59.04 o 1 8 6 443.21 453.81 64.61 o 2 8 6 3961.71 3974.32 129.52 o 3 8 6 99.67 124.53 18.01 o 4 8 6 6465.72 6336.04 210.26 o 5 8 6 110.93 120.79 19.93 o 6 8 6 2708.40 2729.91 123.81 o 1 1 7 684.81 685.57 14.12 o 2 1 7 213.67 207.55 7.12 o 3 1 7 8564.43 8420.04 142.07 o 4 1 7 58.72 68.67 6.58 o 5 1 7 4994.84 4922.43 99.13 o 6 1 7 129.89 132.40 9.64 o 7 1 7 1034.04 1023.27 35.63 o 8 1 7 62.98 61.90 9.13 o 9 1 7 687.76 698.50 27.27 o 10 1 7 252.24 221.42 14.67 o 11 1 7 1974.76 1923.01 60.03 o 12 1 7 217.23 216.16 14.16 o 13 1 7 3895.37 3931.71 114.13 o 14 1 7 153.39 181.64 12.70 o 15 1 7 265.16 290.67 14.75 o 16 1 7 83.71 51.12 13.86 o 1 3 7 1804.89 1764.54 41.16 o 2 3 7 140.97 146.59 7.78 o 3 3 7 5397.45 5407.89 104.30 o 4 3 7 41.83 44.87 8.25 o 5 3 7 2848.75 2869.63 57.01 o 6 3 7 113.39 118.22 11.36 o 7 3 7 1562.24 1568.40 51.94 o 8 3 7 59.89 43.09 9.13 o 9 3 7 1392.47 1377.38 46.55 o 10 3 7 216.05 218.39 15.55 o 11 3 7 1247.13 1274.37 43.56 o 12 3 7 160.94 153.97 12.47 o 13 3 7 2648.56 2740.70 82.29 o 14 3 7 96.16 101.39 19.93 o 15 3 7 474.02 475.29 39.03 o 1 5 7 78.89 76.85 10.14 o 2 5 7 57.69 52.57 11.71 o 3 5 7 4893.42 4917.34 118.33 o 4 5 7 29.80 29.84 8.26 o 5 5 7 3288.22 3287.78 119.18 o 6 5 7 20.59 22.13 7.37 o 7 5 7 397.00 395.82 16.89 o 8 5 7 44.28 54.63 11.38 o 9 5 7 205.17 194.39 17.34 o 10 5 7 161.72 155.07 15.07 o 11 5 7 1633.79 1673.92 56.96 o 12 5 7 110.03 114.39 12.23 o 1 7 7 889.15 937.12 41.12 o 2 7 7 64.02 65.13 14.05 o 3 7 7 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262.26 256.16 11.33 o 6 4 8 3704.92 3600.64 81.76 o 7 4 8 26.68 26.35 9.94 o 8 4 8 14954.67 14737.21 412.00 o 9 4 8 22.61 -3.58 9.13 o 10 4 8 720.85 736.92 31.47 o 11 4 8 204.28 200.92 25.57 o 12 4 8 1621.29 1667.43 57.84 o 13 4 8 81.53 99.92 11.36 o 0 6 8 510.29 575.15 45.98 o 1 6 8 139.96 154.44 17.46 o 2 6 8 6795.60 6867.55 193.20 o 3 6 8 183.16 194.79 19.30 o 4 6 8 4634.61 4799.37 121.21 o 5 6 8 213.73 196.24 15.81 o 6 6 8 5354.52 5249.26 156.98 o 7 6 8 127.44 128.26 16.02 o 8 6 8 950.02 1007.23 56.88 o 9 6 8 157.49 164.48 22.53 o 1 1 9 494.68 504.55 14.10 o 2 1 9 85.40 83.34 6.50 o 3 1 9 1772.54 1753.41 41.89 o 4 1 9 22.54 18.97 7.41 o 5 1 9 3008.39 3009.76 92.69 o 6 1 9 321.33 317.92 24.28 o 7 1 9 91.03 89.22 12.55 o 8 1 9 77.41 69.15 11.59 o 9 1 9 639.38 638.47 28.49 o 10 1 9 2.14 4.27 9.13 o 11 1 9 628.03 605.46 27.26 o 12 1 9 84.50 99.96 12.55 o 13 1 9 1319.83 1282.66 44.81 o 1 3 9 98.76 102.64 9.31 o 2 3 9 50.60 61.85 9.83 o 3 3 9 623.54 610.47 23.51 o 4 3 9 13.19 9.13 5.46 o 5 3 9 1515.19 1542.76 34.36 o 6 3 9 146.28 137.54 14.93 o 7 3 9 60.42 47.59 11.21 o 8 3 9 61.83 57.94 11.84 o 9 3 9 253.24 237.31 18.88 o 10 3 9 2.17 11.26 9.76 o 11 3 9 187.70 178.23 16.45 o 12 3 9 87.86 90.35 17.33 o 1 5 9 588.59 595.71 29.75 o 2 5 9 42.78 57.30 11.48 o 3 5 9 1666.77 1637.54 48.48 o 4 5 9 14.01 22.91 9.93 o 5 5 9 2480.02 2540.93 68.58 o 6 5 9 105.56 104.01 8.64 o 7 5 9 147.36 184.13 18.95 o 8 5 9 60.72 59.24 13.53 o 9 5 9 646.86 613.50 31.48 o 1 7 9 43.17 27.44 28.16 o 2 7 9 2.72 22.27 14.39 o 0 0 10 4774.91 5025.40 210.75 o 2 0 10 6700.16 6582.63 187.55 o 4 0 10 18005.35 17655.13 695.16 o 6 0 10 3141.02 2953.82 130.17 o 8 0 10 3825.20 3776.94 161.86 o 10 0 10 3376.19 3348.48 145.02 o 12 0 10 7472.52 7342.46 298.00 o 0 2 10 6622.18 6671.80 194.31 o 1 2 10 10.12 5.13 6.81 o 2 2 10 7218.27 7458.57 179.67 o 3 2 10 69.83 67.52 7.11 o 4 2 10 1841.33 1795.04 49.87 o 5 2 10 65.78 70.03 13.16 o 6 2 10 8184.85 8316.34 239.00 o 7 2 10 10.56 17.76 10.41 o 8 2 10 6096.42 6158.91 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