#------------------------------------------------------------------------------
#$Date: 2016-04-03 06:46:43 +0300 (Sun, 03 Apr 2016) $
#$Revision: 181289 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/67/2236704.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2236704_Fobs
loop_
_publ_author_name
'Levytskyy, Volodymyr'
'Babizhetskyy, Volodymyr'
'Kotur, Bohdan'
'Smetana, Volodymyr'
_publ_section_title
;
 Redetermination of dysprosium trinickel from single-crystal X-ray data
;
_journal_coeditor_code           WM2688
_journal_issue                   11
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              i83
_journal_volume                  68
_journal_year                    2012
_space_group_IT_number           166
_symmetry_space_group_name_Hall  '-R 3 2"'
_symmetry_space_group_name_H-M   'R -3 m :H'
_cell_angle_alpha                90.000
_cell_angle_beta                 90.000
_cell_angle_gamma                120.000
_cell_length_a                   4.9660
_cell_length_b                   4.9660
_cell_length_c                   24.3700
_exptl_crystal_F_000             1350.00
_reflns_d_resolution_high        0.7465
_cod_data_source_file            wm2688Isup2.hkl
_cod_data_source_block           I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     '                                  DyNi3'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            692.91
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'x-y, -y, -z'
'-x, -x+y, -z'
'y, x, -z'
'x+2/3, y+1/3, z+1/3'
'-y+2/3, x-y+1/3, z+1/3'
'-x+y+2/3, -x+1/3, z+1/3'
'x-y+2/3, -y+1/3, -z+1/3'
'-x+2/3, -x+y+1/3, -z+1/3'
'y+2/3, x+1/3, -z+1/3'
'x+1/3, y+2/3, z+2/3'
'-y+1/3, x-y+2/3, z+2/3'
'-x+y+1/3, -x+2/3, z+2/3'
'x-y+1/3, -y+2/3, -z+2/3'
'-x+1/3, -x+y+2/3, -z+2/3'
'y+1/3, x+2/3, -z+2/3'
'-x, -y, -z'
'y, -x+y, -z'
'x-y, x, -z'
'-x+y, y, z'
'x, x-y, z'
'-y, -x, z'
'-x+2/3, -y+1/3, -z+1/3'
'y+2/3, -x+y+1/3, -z+1/3'
'x-y+2/3, x+1/3, -z+1/3'
'-x+y+2/3, y+1/3, z+1/3'
'x+2/3, x-y+1/3, z+1/3'
'-y+2/3, -x+1/3, z+1/3'
'-x+1/3, -y+2/3, -z+2/3'
'y+1/3, -x+y+2/3, -z+2/3'
'x-y+1/3, x+2/3, -z+2/3'
'-x+y+1/3, y+2/3, z+2/3'
'x+1/3, x-y+2/3, z+2/3'
'-y+1/3, -x+2/3, z+2/3'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
-1 2 0 288550.25 301720.97 4286.78 o
0 3 0 165835.19 176286.50 2056.53 o
-2 4 0 480129.16 507834.63 7087.22 o
-1 5 0 71398.60 71518.73 1752.86 o
-3 6 0 48988.19 48677.18 2370.18 o
-1 1 1 16334.80 16265.54 455.24 o
0 2 1 293708.00 306364.09 3717.96 o
-2 3 1 11073.17 11594.86 406.61 o
-4 4 1 111753.59 115215.74 2687.53 o
-1 4 1 8051.13 7730.18 539.76 o
-3 5 1 7317.52 7818.39 693.66 o
0 5 1 5674.70 5318.91 1031.14 o
-5 6 1 3660.71 3747.90 1158.48 o
-2 6 1 56290.57 56262.18 2356.08 o
0 1 2 1320.09 1487.67 141.62 o
-2 2 2 81618.62 86927.77 1483.81 o
-1 3 2 1167.01 1254.93 203.47 o
-3 4 2 693.21 758.08 246.72 o
0 4 2 30058.95 29354.79 1550.98 o
-5 5 2 791.70 349.21 669.26 o
-2 5 2 634.81 895.82 386.64 o
-4 6 2 14918.75 16306.51 1230.38 o
-1 6 2 400.45 1211.91 1315.08 o
0 0 3 2093.05 2113.40 253.69 o
-1 2 3 3134.89 3146.95 203.06 o
-3 3 3 1895.02 1938.37 331.00 o
0 3 3 2394.05 2406.32 425.09 o
-2 4 3 1155.90 924.38 271.71 o
-4 5 3 1379.22 1730.51 458.38 o
-1 5 3 1130.70 1284.82 407.02 o
-3 6 3 986.70 1033.56 538.48 o
-1 1 4 6570.19 6240.50 280.52 o
0 2 4 85722.02 88340.63 2247.89 o
-2 3 4 3954.54 4013.55 304.72 o
-4 4 4 30656.26 31029.18 1438.14 o
-1 4 4 2197.79 2022.12 362.42 o
-3 5 4 1591.95 1472.57 395.48 o
0 5 4 1458.08 1947.86 710.75 o
-5 6 4 764.88 1103.99 1206.02 o
-2 6 4 14591.78 14214.68 1114.70 o
0 1 5 1083.33 1018.01 169.66 o
-2 2 5 132114.48 141304.56 1691.60 o
-1 3 5 835.00 844.25 177.84 o
-3 4 5 753.01 882.82 276.55 o
0 4 5 43628.07 42319.90 1614.01 o
-5 5 5 313.00 -142.73 725.06 o
-2 5 5 378.14 326.50 343.12 o
-4 6 5 19643.17 20285.32 1476.60 o
-1 6 5 491.33 375.75 3098.01 o
0 0 6 18259.43 15984.13 1086.86 o
-1 2 6 364279.50 365306.22 2736.34 o
-3 3 6 202104.20 211890.16 3563.36 o
0 3 6 202988.59 201300.72 6034.10 o
-2 4 6 7349.23 7894.12 541.60 o
-4 5 6 88804.23 84252.91 2637.75 o
-1 5 6 88419.66 87556.74 1847.13 o
-3 6 6 64743.43 60770.05 2009.68 o
-1 1 7 218787.16 209534.05 3506.58 o
0 2 7 185.25 235.02 155.15 o
-2 3 7 127536.56 128776.49 1937.01 o
-4 4 7 634.49 1100.37 565.99 o
-1 4 7 84708.88 81580.52 1529.92 o
-3 5 7 56778.57 56857.21 1405.01 o
0 5 7 41905.55 41636.77 2055.12 o
-5 6 7 33317.93 38752.60 4816.92 o
-2 6 7 718.23 129.67 493.75 o
0 1 8 219004.80 220621.55 1942.01 o
-2 2 8 24703.12 24352.52 690.20 o
-1 3 8 123873.28 124032.15 1477.62 o
-3 4 8 83104.77 83540.79 2146.99 o
0 4 8 12728.31 11664.20 1108.79 o
-5 5 8 39342.33 37897.17 2224.07 o
-2 5 8 57405.63 55004.93 1439.97 o
-4 6 8 7366.60 8563.76 1273.04 o
0 0 9 36116.60 32618.97 1322.59 o
-1 2 9 39105.85 38715.25 739.86 o
-3 3 9 22065.40 22596.18 1041.22 o
0 3 9 23567.40 22426.44 1148.96 o
-2 4 9 12237.83 12859.64 675.92 o
-4 5 9 10497.78 11316.59 1034.58 o
-1 5 9 9827.42 9037.17 757.76 o
-3 6 9 7273.97 7572.46 872.83 o
-1 1 10 17166.17 16525.78 563.78 o
0 2 10 3670.37 3577.18 448.75 o
-2 3 10 9224.35 9206.97 512.41 o
-4 4 10 1312.29 1875.06 661.94 o
-1 4 10 6203.23 6069.69 579.97 o
-3 5 10 4040.69 4668.01 617.52 o
0 5 10 2407.90 1599.98 734.98 o
-2 6 10 668.62 488.02 665.85 o
0 1 11 121245.21 115745.12 1543.73 o
-2 2 11 503.18 579.71 247.04 o
-1 3 11 68988.21 64819.24 1177.37 o
-3 4 11 44306.05 44867.23 1181.74 o
0 4 11 140.82 -142.79 448.57 o
-5 5 11 19731.62 20382.60 1841.83 o
-2 5 11 28381.12 28417.04 1164.28 o
-4 6 11 76.74 -448.04 2034.63 o
0 0 12 284209.06 273061.34 4685.13 o
-1 2 12 3030.07 2874.46 281.81 o
-3 3 12 1977.26 1785.07 543.19 o
0 3 12 1831.05 1520.21 500.40 o
-2 4 12 95713.13 93306.29 1698.96 o
-4 5 12 565.41 542.38 447.89 o
-1 5 12 621.16 937.83 478.70 o
-3 6 12 256.44 818.58 958.04 o
-1 1 13 872.85 1296.69 255.16 o
0 2 13 134380.14 129836.09 2623.60 o
-2 3 13 849.90 1183.58 368.30 o
-4 4 13 59536.93 60467.36 2682.83 o
-1 4 13 837.42 999.14 366.60 o
-3 5 13 1126.78 830.82 516.06 o
0 5 13 852.08 441.48 889.15 o
0 1 14 93076.92 89789.21 1510.99 o
-2 2 14 237008.28 233239.09 2860.95 o
-1 3 14 61905.14 59902.09 1309.91 o
-3 4 14 41954.33 42693.62 1306.37 o
0 4 14 107466.24 104567.92 2814.67 o
-5 5 14 24744.63 27568.22 2342.28 o
-2 5 14 30957.98 28964.68 1341.33 o
0 0 15 191645.41 185583.34 4055.05 o
-1 2 15 113591.99 112987.35 1446.37 o
-3 3 15 75399.45 76240.37 2230.56 o
0 3 15 73066.88 71744.96 2145.69 o
-2 4 15 79229.10 77091.30 1726.59 o
-4 5 15 36153.39 37387.45 1644.50 o
-1 5 15 37302.43 37129.98 1440.91 o
-1 1 16 35346.81 34667.43 1011.59 o
0 2 16 2363.86 2040.57 581.65 o
-2 3 16 22721.63 22581.80 937.01 o
-4 4 16 1533.43 1822.09 754.13 o
-1 4 16 16450.70 16317.76 935.30 o
-3 5 16 11857.11 11605.75 1109.99 o
0 1 17 3617.99 3168.18 487.87 o
-2 2 17 85666.02 85975.88 2114.68 o
-1 3 17 2141.30 1978.03 431.42 o
-3 4 17 1239.68 2363.42 664.69 o
0 4 17 36996.86 37391.64 1916.84 o
-2 5 17 1012.39 1113.60 478.32 o
0 0 18 55097.96 52532.66 2293.45 o
-1 2 18 8697.56 8748.04 670.43 o
-3 3 18 4463.00 4518.36 918.49 o
0 3 18 4731.66 4066.56 797.13 o
-2 4 18 24987.48 26025.23 1252.26 o
-4 5 18 2097.96 2986.20 1295.68 o
-1 5 18 1969.55 1285.88 1182.75 o
-1 1 19 760.51 973.98 405.41 o
0 2 19 82001.52 79521.15 2286.38 o
-2 3 19 363.76 596.22 399.67 o
-4 4 19 36978.41 36805.68 2378.91 o
-1 4 19 205.26 420.20 442.16 o
-3 5 19 257.18 -78.14 648.39 o
0 1 20 35110.19 35243.09 1376.01 o
-2 2 20 34.07 207.84 577.07 o
-1 3 20 23467.19 24092.45 1210.82 o
-3 4 20 17760.03 18343.72 1381.53 o
0 4 20 20.77 539.52 619.01 o
-2 5 20 12983.79 14257.66 2457.14 o
0 0 21 69933.03 72176.20 2865.89 o
-1 2 21 83878.45 85299.76 1712.20 o
-3 3 21 57107.17 58204.41 4212.07 o
0 3 21 58810.25 55708.32 2101.09 o
-2 4 21 33936.79 33988.74 1622.75 o
-1 1 22 55502.37 56967.28 1973.94 o
0 2 22 85699.37 86038.53 2516.30 o
-2 3 22 39989.46 40172.63 1536.35 o
-4 4 22 44986.40 46104.96 3722.41 o
-1 4 22 28853.12 28302.73 1425.53 o
0 1 23 528.65 629.00 535.13 o
-2 2 23 37080.41 36209.93 2165.10 o
-1 3 23 538.00 499.91 447.52 o
-3 4 23 429.12 892.74 568.33 o
0 0 24 73740.69 81492.97 4921.35 o
-1 2 24 652.43 632.72 471.20 o
-3 3 24 521.36 156.32 798.65 o
0 3 24 434.71 664.76 657.30 o
-2 4 24 34519.68 34847.20 2291.22 o
-1 1 25 33914.29 36475.82 1901.49 o
0 2 25 793.17 947.24 663.95 o
-2 3 25 24021.22 29070.42 1857.54 o
-1 4 25 17285.10 17376.95 2639.56 o
0 1 26 5241.92 5046.26 989.11 o
-2 2 26 4731.55 6220.70 1323.33 o
-1 3 26 3398.93 4759.65 769.82 o
0 0 27 21055.79 24090.64 4083.17 o
-1 2 27 7480.92 9363.78 1132.66 o
-3 3 27 5633.17 5913.06 2921.35 o
0 3 27 5211.49 5191.43 2392.49 o
-1 1 28 35290.08 38975.27 2633.61 o
0 2 28 16255.15 17768.02 1697.79 o
-2 3 28 25861.63 26801.05 5347.85 o
0 1 29 28327.31 29811.95 3391.74 o
-2 2 29 1638.22 1693.08 1252.41 o
-1 3 29 21229.10 25483.09 4192.91 o
0 0 30 3593.78 2043.99 2232.08 o
-1 2 30 44026.23 49939.59 2715.48 o
-1 1 31 107.77 -246.60 1657.23 o