#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:52:03 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181304 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/82/2238291.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2238291_Fobs loop_ _publ_author_name 'Hu, Feng' 'Xu, Chao' 'Shi, Hua-Tian' 'Chen, Qun' 'Zhang, Qian-Feng' _publ_section_title ; \m-(Acetic acid)-di-\m-chlorido-bis[triphenyltellurium(IV)] monohydrate ; _journal_coeditor_code XU5713 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1171 _journal_volume 69 _journal_year 2013 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.584 _cell_angle_gamma 90.000 _cell_length_a 13.9469 _cell_length_b 9.3616 _cell_length_c 27.7941 _exptl_crystal_F_000 1704.00 _reflns_d_resolution_high 0.7692 _cod_data_source_file xu5713Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' I in space group P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 447.00 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 33.04 87.80 12.59 o 4 0 0 58392.81 58685.36 1058.50 o 6 0 0 33.31 57.66 41.38 o 8 0 0 21882.91 21897.95 453.28 o 10 0 0 1499.84 1310.76 84.53 o 12 0 0 3182.60 3262.60 140.20 o 14 0 0 1441.85 1726.60 209.81 o 16 0 0 2015.50 2184.72 257.93 o 1 1 0 28201.20 29814.85 309.41 o 2 1 0 257.97 499.25 15.21 o 3 1 0 38198.82 38520.23 565.97 o 4 1 0 718.27 617.57 30.34 o 6 1 0 769.80 727.63 38.90 o 7 1 0 4172.78 3852.70 85.24 o 8 1 0 5192.07 5095.78 107.60 o 9 1 0 1.74 41.11 27.09 o 10 1 0 691.78 775.82 51.39 o 11 1 0 7472.84 7482.56 152.66 o 12 1 0 3561.56 3680.12 131.66 o 13 1 0 292.08 236.38 55.80 o 14 1 0 563.93 468.13 96.52 o 15 1 0 1185.22 1165.57 133.81 o 16 1 0 80.47 317.47 98.66 o 17 1 0 609.64 658.00 193.45 o 0 2 0 4323.28 3999.87 132.82 o 1 2 0 21484.90 20565.80 312.53 o 2 2 0 8250.59 8789.70 125.56 o 3 2 0 24959.72 26807.56 307.51 o 4 2 0 57184.11 58701.97 859.05 o 5 2 0 1209.47 1071.13 35.94 o 6 2 0 7428.33 7381.13 128.47 o 7 2 0 2552.75 2693.73 84.46 o 8 2 0 18826.46 18875.86 284.06 o 9 2 0 15369.36 14929.54 312.00 o 10 2 0 352.71 312.19 37.99 o 11 2 0 2321.64 2310.48 153.65 o 12 2 0 4742.35 4521.01 148.09 o 13 2 0 5709.91 5862.25 177.72 o 14 2 0 2582.66 2904.22 134.32 o 15 2 0 892.49 988.65 125.13 o 16 2 0 1017.69 1177.64 138.33 o 17 2 0 1511.65 1718.90 242.53 o 1 3 0 263.96 235.68 30.60 o 2 3 0 1777.99 1810.50 68.78 o 3 3 0 2249.46 2654.53 116.18 o 4 3 0 8547.72 8406.75 116.85 o 5 3 0 2463.75 2223.34 147.77 o 6 3 0 2151.03 2334.04 68.07 o 7 3 0 6981.89 7292.45 122.37 o 8 3 0 7359.24 7633.44 160.10 o 9 3 0 50.77 24.23 32.23 o 10 3 0 1883.91 1953.38 163.41 o 11 3 0 71.32 75.77 44.69 o 12 3 0 3896.87 4125.36 145.54 o 13 3 0 670.48 749.68 134.51 o 14 3 0 1733.75 1935.53 122.37 o 15 3 0 199.42 153.91 59.99 o 16 3 0 2516.00 2602.52 198.03 o 17 3 0 479.24 679.48 175.16 o 0 4 0 1460.66 1545.67 92.39 o 1 4 0 20171.91 21679.15 423.27 o 2 4 0 17514.38 18100.42 361.86 o 3 4 0 102.29 151.52 20.21 o 4 4 0 1487.91 1583.50 42.19 o 5 4 0 28806.21 28719.63 350.12 o 6 4 0 3794.86 3573.54 85.06 o 7 4 0 5.41 -16.19 16.19 o 8 4 0 6504.26 6431.60 197.66 o 9 4 0 15487.21 15751.54 326.75 o 10 4 0 3968.56 4083.10 136.72 o 11 4 0 4.32 45.57 45.35 o 12 4 0 1933.87 1890.43 115.64 o 13 4 0 9351.87 9128.04 241.57 o 14 4 0 862.81 936.29 92.39 o 15 4 0 187.87 292.10 71.88 o 16 4 0 91.15 177.32 135.70 o 1 5 0 12935.73 13262.49 290.57 o 2 5 0 2.68 -17.41 29.85 o 3 5 0 227.64 177.00 32.47 o 4 5 0 10978.12 11535.10 204.73 o 5 5 0 5316.59 5203.97 130.78 o 6 5 0 727.73 730.02 47.63 o 7 5 0 2943.26 2921.68 92.87 o 8 5 0 3887.95 3503.01 235.39 o 9 5 0 203.17 241.80 49.35 o 10 5 0 393.01 415.95 60.35 o 11 5 0 0.73 -12.83 43.41 o 12 5 0 2128.71 1984.09 121.84 o 13 5 0 232.33 299.55 67.39 o 14 5 0 322.56 272.70 68.60 o 15 5 0 8.73 15.92 56.45 o 16 5 0 1202.31 1213.16 205.00 o 0 6 0 6995.93 6971.86 273.33 o 1 6 0 8253.84 8033.34 210.92 o 2 6 0 7755.87 7579.73 202.58 o 3 6 0 2953.72 2982.13 97.54 o 4 6 0 2423.84 2243.75 153.36 o 5 6 0 14449.50 14009.31 246.96 o 6 6 0 11926.94 11926.95 287.09 o 7 6 0 1352.10 1293.61 67.14 o 8 6 0 93.25 62.25 42.50 o 9 6 0 10132.86 9843.01 238.51 o 10 6 0 2965.03 2903.79 124.30 o 11 6 0 2006.14 1809.05 116.45 o 12 6 0 80.52 148.84 58.85 o 13 6 0 2715.05 2920.22 142.31 o 14 6 0 77.95 130.38 63.15 o 15 6 0 453.62 481.76 100.03 o 1 7 0 4709.29 4528.20 191.52 o 2 7 0 285.07 303.26 54.39 o 3 7 0 3906.49 3784.87 169.09 o 4 7 0 77.91 101.59 48.44 o 5 7 0 7770.81 7253.77 177.21 o 6 7 0 3.00 -37.31 40.66 o 7 7 0 833.32 738.68 89.71 o 8 7 0 269.56 354.20 76.30 o 9 7 0 1737.43 1609.06 117.99 o 10 7 0 74.51 93.72 53.58 o 11 7 0 1047.06 1006.47 95.96 o 12 7 0 399.92 292.97 70.68 o 13 7 0 1.62 -17.70 53.23 o 14 7 0 384.25 516.24 100.03 o 0 8 0 9139.46 9093.06 359.95 o 1 8 0 3091.90 3287.15 162.65 o 2 8 0 1913.89 1968.86 126.60 o 3 8 0 10103.19 10153.09 216.27 o 4 8 0 1824.59 1957.19 97.57 o 5 8 0 2131.13 2156.73 105.62 o 6 8 0 2318.03 2262.69 143.01 o 7 8 0 6969.13 7422.72 256.11 o 8 8 0 2828.23 2779.82 167.30 o 9 8 0 1063.81 1088.14 121.77 o 10 8 0 1037.19 1034.51 143.40 o 11 8 0 1911.88 2017.89 166.70 o 12 8 0 322.68 190.78 84.08 o 13 8 0 305.38 263.94 99.13 o 1 9 0 1119.53 1053.30 104.70 o 2 9 0 894.42 1106.25 87.27 o 3 9 0 1187.20 1118.30 113.87 o 4 9 0 447.24 513.50 70.35 o 5 9 0 1365.70 1372.89 103.85 o 6 9 0 923.81 748.76 101.39 o 7 9 0 649.59 808.97 110.51 o 8 9 0 88.18 66.28 63.73 o 9 9 0 539.42 285.34 85.23 o 10 9 0 1438.41 1385.22 146.92 o 11 9 0 114.14 -19.25 105.87 o 12 9 0 31.42 -90.47 90.47 o 0 10 0 1454.09 1532.19 182.86 o 1 10 0 3297.76 3454.67 171.43 o 2 10 0 78.56 73.31 90.70 o 3 10 0 4352.62 4224.35 156.42 o 4 10 0 1130.57 1102.16 124.42 o 5 10 0 1.26 43.59 69.06 o 6 10 0 435.96 496.29 101.39 o 7 10 0 3294.63 3531.96 278.14 o 8 10 0 347.12 519.05 85.22 o 9 10 0 0.23 -25.12 68.64 o 10 10 0 156.73 11.18 67.12 o 1 11 0 40.55 -20.64 51.44 o 2 11 0 198.29 185.18 65.55 o 3 11 0 0.56 94.00 78.91 o 4 11 0 135.99 121.20 76.82 o 5 11 0 182.83 135.58 179.97 o 6 11 0 176.84 269.48 132.82 o 7 11 0 3.26 11.55 111.64 o 0 12 0 37.83 86.62 111.64 o 1 12 0 332.88 375.80 163.61 o 2 12 0 1528.21 1493.69 215.58 o 3 12 0 435.00 477.37 155.91 o -17 0 1 5364.10 5231.78 350.33 o -15 0 1 654.04 854.64 161.69 o -13 0 1 6598.36 6803.70 334.93 o -11 0 1 1403.17 1433.20 101.48 o -9 0 1 17943.27 17756.95 389.16 o -7 0 1 707.45 928.51 65.86 o -5 0 1 2324.69 2258.51 407.11 o -3 0 1 9524.91 10547.92 202.43 o -1 0 1 1634.72 1643.98 39.47 o 1 0 1 60029.94 71252.80 1239.26 o 3 0 1 3120.92 3017.74 78.92 o 7 0 1 929.49 728.15 56.84 o 9 0 1 11068.77 11368.09 272.30 o 11 0 1 8579.14 8181.77 228.42 o 13 0 1 3142.70 3337.71 248.31 o 15 0 1 2012.53 1917.16 232.91 o 17 0 1 948.19 1014.40 194.41 o -17 1 1 91.51 84.90 90.44 o -16 1 1 197.14 220.10 90.92 o -15 1 1 63.14 -67.12 67.12 o -14 1 1 2329.42 2687.25 124.56 o -13 1 1 835.23 983.74 84.62 o -12 1 1 12.41 21.98 41.12 o -11 1 1 1889.72 1741.59 75.12 o -10 1 1 8209.11 8137.25 173.89 o -9 1 1 7650.49 7390.07 143.82 o -8 1 1 661.81 682.90 44.16 o -7 1 1 5544.92 5705.11 111.21 o -6 1 1 12903.92 13146.61 200.74 o -5 1 1 8583.86 8282.50 152.40 o -4 1 1 75485.47 75300.05 953.88 o -3 1 1 23.27 9.85 11.37 o -2 1 1 1573.10 1608.95 24.83 o -1 1 1 13619.73 12048.48 140.25 o 0 1 1 85435.45 91443.05 1587.67 o 1 1 1 4024.98 3828.54 51.08 o 2 1 1 5157.66 4487.24 52.42 o 3 1 1 27879.57 29892.86 442.79 o 4 1 1 75450.62 75636.05 1094.96 o 5 1 1 570.67 597.70 37.46 o 6 1 1 91.56 96.37 19.81 o 7 1 1 12799.65 13383.28 207.04 o 8 1 1 20788.71 20304.13 299.38 o 9 1 1 1114.34 1002.18 52.31 o 10 1 1 716.06 832.80 51.84 o 11 1 1 0.93 32.61 30.24 o 12 1 1 18056.29 17861.06 352.20 o 13 1 1 30.54 43.53 47.65 o 14 1 1 330.21 257.83 128.00 o 15 1 1 127.32 75.46 76.18 o 16 1 1 6474.42 6572.69 278.28 o 17 1 1 549.37 431.99 271.41 o -17 2 1 2168.76 2319.10 540.89 o -16 2 1 403.46 658.92 115.37 o -15 2 1 298.79 271.19 115.49 o -14 2 1 23.73 -8.19 49.47 o -13 2 1 5996.18 5833.32 267.91 o -12 2 1 5971.21 6031.28 173.32 o -11 2 1 28.06 35.72 33.06 o -10 2 1 827.72 885.65 54.84 o -9 2 1 6849.49 6983.91 139.81 o -8 2 1 32986.15 32968.60 460.16 o -7 2 1 8448.18 8170.48 144.31 o -6 2 1 10791.39 11275.86 178.39 o -5 2 1 5922.42 5900.90 100.22 o -4 2 1 4775.06 4596.33 78.19 o -3 2 1 5907.94 6263.99 84.52 o -1 2 1 5561.44 6170.12 109.26 o 0 2 1 11186.57 10239.38 204.04 o 1 2 1 75997.87 77972.38 1919.09 o 2 2 1 40048.87 42836.09 548.87 o 3 2 1 1801.42 2016.43 54.73 o 4 2 1 26269.39 27590.84 359.06 o 5 2 1 21204.89 21879.96 293.10 o 6 2 1 694.54 651.77 38.70 o 7 2 1 1067.90 1100.27 46.82 o 8 2 1 3869.70 4202.41 94.24 o 9 2 1 6540.38 6311.08 140.31 o 10 2 1 1.39 1.08 31.95 o 11 2 1 2926.09 2898.94 189.21 o 12 2 1 569.17 566.37 69.51 o 13 2 1 1177.04 1122.41 91.51 o 14 2 1 735.66 827.18 84.91 o 15 2 1 850.97 941.71 124.49 o 16 2 1 841.62 1061.96 136.09 o 17 2 1 180.97 215.58 130.89 o -17 3 1 216.43 271.41 130.89 o -16 3 1 1.27 -3.87 75.89 o -15 3 1 32.28 -1.51 54.45 o -14 3 1 1757.13 1883.20 121.03 o -13 3 1 6212.21 6253.14 227.48 o -12 3 1 251.51 394.88 82.18 o -11 3 1 90.92 42.86 42.11 o -10 3 1 2674.91 2410.24 101.69 o -9 3 1 16031.04 15900.22 255.58 o -8 3 1 3305.92 3473.18 89.43 o -7 3 1 6920.44 6803.87 129.02 o -6 3 1 3614.81 3437.89 66.03 o -5 3 1 22803.50 22292.73 302.61 o -4 3 1 10849.86 10834.67 180.28 o -3 3 1 19898.04 19507.42 805.19 o -1 3 1 26983.39 27741.27 515.16 o 0 3 1 59.22 32.60 21.27 o 1 3 1 1839.74 1866.04 64.55 o 2 3 1 12729.74 13282.32 270.61 o 3 3 1 63632.71 66032.59 833.24 o 4 3 1 24397.89 23408.45 323.58 o 5 3 1 1107.95 1177.75 43.93 o 6 3 1 1291.01 1388.45 50.01 o 7 3 1 10775.21 11162.43 168.45 o 8 3 1 18744.70 18603.78 318.24 o 9 3 1 2477.75 2397.84 102.21 o 10 3 1 1054.92 1038.95 94.93 o 11 3 1 41.12 35.87 41.86 o 12 3 1 5150.60 5130.01 163.74 o 13 3 1 5675.26 5404.59 192.27 o 14 3 1 904.21 878.61 88.65 o 15 3 1 69.23 3.92 74.82 o 16 3 1 738.54 889.72 130.66 o -16 4 1 1380.36 1302.88 116.08 o -15 4 1 189.12 206.17 66.08 o -14 4 1 1.59 73.18 54.80 o -13 4 1 927.99 914.75 89.98 o -12 4 1 5069.02 4776.86 161.19 o -11 4 1 1840.39 1715.16 119.35 o -10 4 1 814.01 828.84 103.71 o -9 4 1 350.09 339.71 44.45 o -8 4 1 22412.05 21966.29 373.77 o -7 4 1 9029.50 9315.32 185.90 o -6 4 1 635.02 613.78 45.56 o -5 4 1 4986.86 4902.05 84.57 o -4 4 1 44445.08 44697.01 586.88 o -3 4 1 3242.95 3331.21 95.30 o -2 4 1 10206.49 10237.68 226.47 o -1 4 1 7387.24 7418.86 177.62 o 0 4 1 32343.85 33371.37 885.44 o 1 4 1 90.75 195.63 33.95 o 2 4 1 4281.59 4093.40 98.06 o 3 4 1 2851.23 3090.10 201.15 o 4 4 1 9080.65 9118.40 129.29 o 5 4 1 233.41 269.04 29.15 o 6 4 1 634.68 674.52 52.51 o 7 4 1 255.56 247.86 45.01 o 8 4 1 4372.16 4202.95 109.40 o 9 4 1 62.77 39.99 58.17 o 10 4 1 1774.98 1614.21 117.78 o 11 4 1 712.82 675.17 71.89 o 12 4 1 26.06 -23.06 46.32 o 13 4 1 46.74 149.64 68.39 o 14 4 1 526.00 669.58 86.05 o 15 4 1 425.56 367.39 75.39 o 16 4 1 726.94 619.81 159.76 o -16 5 1 515.54 553.67 115.49 o -15 5 1 24.57 -54.08 54.08 o -14 5 1 33.99 101.11 60.81 o -13 5 1 2003.03 2151.28 130.06 o -12 5 1 1357.40 1329.41 101.29 o -11 5 1 57.15 92.34 93.93 o -10 5 1 12.76 0.71 45.20 o -9 5 1 7827.73 7595.71 193.45 o -8 5 1 3025.74 3202.08 101.37 o -7 5 1 170.95 193.14 37.11 o -6 5 1 364.16 401.05 29.65 o -5 5 1 21309.79 21584.22 309.03 o -4 5 1 89.96 79.70 22.88 o -3 5 1 2049.71 2026.79 59.90 o -2 5 1 5386.59 5537.39 154.44 o -1 5 1 23077.30 23905.51 476.37 o 0 5 1 134.12 90.97 36.67 o 1 5 1 2523.60 2851.49 105.42 o 2 5 1 14795.34 15044.85 267.08 o 3 5 1 11174.94 10268.67 199.21 o 4 5 1 10.38 10.55 12.40 o 5 5 1 13706.59 14713.71 233.82 o 6 5 1 11084.77 10574.74 182.94 o 7 5 1 8071.53 7930.52 152.48 o 8 5 1 88.98 134.07 64.13 o 9 5 1 3568.19 3474.60 169.73 o 10 5 1 4566.12 4333.84 146.52 o 11 5 1 2894.24 2910.23 126.28 o 12 5 1 11.10 84.62 53.87 o 13 5 1 1354.17 1345.84 145.10 o 14 5 1 1427.76 1521.78 121.40 o 15 5 1 432.96 422.43 79.09 o 16 5 1 10.76 46.52 121.27 o -15 6 1 982.41 1069.43 227.13 o -14 6 1 357.25 272.14 90.11 o -13 6 1 424.68 441.92 77.47 o -12 6 1 1880.18 1844.07 121.78 o -11 6 1 2029.62 2107.06 143.52 o -10 6 1 342.72 401.76 81.99 o -9 6 1 4.58 29.71 39.84 o -8 6 1 6820.09 6712.99 180.41 o -7 6 1 159.78 91.83 32.78 o -6 6 1 783.75 853.90 76.13 o -5 6 1 1452.86 1424.20 61.10 o -4 6 1 13042.80 12895.31 208.24 o -3 6 1 132.74 208.60 40.84 o -2 6 1 298.24 294.35 50.30 o -1 6 1 91.41 107.69 92.39 o 0 6 1 6325.36 6608.98 165.36 o 1 6 1 3764.59 3402.44 127.40 o 2 6 1 245.82 414.22 53.03 o 3 6 1 2687.17 2644.90 92.19 o 4 6 1 925.94 978.49 52.21 o 5 6 1 3298.24 3144.61 122.49 o 6 6 1 1131.43 1192.53 88.26 o 7 6 1 5382.39 5409.93 124.83 o 8 6 1 48.75 13.30 37.65 o 9 6 1 1879.88 1793.12 106.93 o 10 6 1 18.42 27.29 59.97 o 11 6 1 4976.32 4767.60 224.65 o 12 6 1 489.55 448.99 72.74 o 13 6 1 666.09 742.26 102.82 o 14 6 1 11.29 17.87 55.54 o 15 6 1 439.14 319.48 91.81 o -14 7 1 400.68 404.30 95.89 o -13 7 1 488.33 427.35 78.98 o -12 7 1 1420.98 1460.28 123.57 o -11 7 1 947.86 1069.11 96.71 o -10 7 1 90.00 115.19 52.07 o -9 7 1 1364.15 1331.80 113.02 o -8 7 1 63.47 59.14 58.26 o -7 7 1 881.21 911.99 71.36 o -6 7 1 130.55 107.24 41.48 o -5 7 1 2942.95 2792.83 103.80 o -4 7 1 1942.93 2034.49 70.75 o -3 7 1 3905.75 4047.63 101.34 o -2 7 1 1271.43 1149.03 89.83 o -1 7 1 8854.77 8877.93 196.30 o 0 7 1 102.12 95.13 76.03 o 1 7 1 2950.99 3147.74 136.67 o 2 7 1 2264.29 2094.40 93.06 o 3 7 1 8618.19 8899.93 200.27 o 4 7 1 1903.40 1882.45 89.99 o 5 7 1 5085.48 4983.72 215.11 o 6 7 1 9108.33 9031.47 204.01 o 7 7 1 3280.00 2967.35 163.61 o 8 7 1 4020.50 4052.89 199.22 o 9 7 1 3716.36 3537.92 140.37 o 10 7 1 4241.87 4023.22 164.18 o 11 7 1 3433.45 3307.12 155.21 o 12 7 1 1876.01 1742.43 124.29 o 13 7 1 1005.68 1053.15 107.14 o 14 7 1 732.69 919.62 123.50 o -13 8 1 595.47 765.14 116.22 o -12 8 1 748.46 679.23 114.66 o -11 8 1 724.01 860.31 117.79 o -10 8 1 1180.99 1230.19 130.47 o -9 8 1 47.88 110.48 67.28 o -8 8 1 276.98 285.54 74.89 o -7 8 1 39.55 0.68 57.55 o -6 8 1 4166.49 4307.09 140.23 o -5 8 1 1.61 2.75 39.73 o -4 8 1 10.71 53.37 41.70 o -3 8 1 188.63 227.85 50.23 o -2 8 1 4836.79 4963.60 165.91 o -1 8 1 438.98 358.63 70.09 o 0 8 1 547.14 529.05 76.89 o 1 8 1 2840.01 2613.23 135.78 o 2 8 1 2253.94 2371.39 102.86 o 3 8 1 408.89 479.38 62.42 o 4 8 1 801.28 743.21 61.96 o 5 8 1 2520.19 2524.40 107.87 o 6 8 1 390.64 424.07 164.58 o 7 8 1 3891.37 3749.97 235.80 o 8 8 1 25.42 0.27 57.35 o 9 8 1 3495.72 3163.80 171.69 o 10 8 1 31.89 8.46 69.70 o 11 8 1 1784.23 1724.10 154.26 o 12 8 1 12.82 77.62 59.01 o 13 8 1 549.87 555.55 131.85 o -12 9 1 10.01 117.42 103.94 o -11 9 1 750.77 706.43 161.69 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