data_2239766 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 12.3530 _cell_length_b 4.5092 _cell_length_c 19.7780 _exptl_crystal_F_000 552.00 _reflns_d_resolution_high 0.8394 _[local]_cod_data_source_file nk2224Isup2.hkl _[local]_cod_data_source_block I _shelx_title ' I in Pca2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 196.42 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' '-x+1/2, y, z+1/2' 'x+1/2, -y, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 -23 836.17 795.09 108.52 o 1 1 -23 14.06 62.62 29.35 o 0 0 -22 303.88 271.56 83.81 o 2 0 -22 1208.25 1313.59 135.95 o 4 0 -22 37.36 34.84 51.39 o 0 1 -22 970.10 852.51 103.53 o 1 1 -22 134.85 145.00 40.41 o 2 1 -22 379.54 368.28 45.72 o 3 1 -22 44.64 74.76 31.86 o 4 1 -22 174.06 206.53 44.67 o 2 0 -21 788.40 756.28 76.28 o 4 0 -21 939.22 1059.94 89.69 o 6 0 -21 152.34 73.13 38.33 o 1 1 -21 53.15 56.72 33.33 o 2 1 -21 725.44 742.15 52.66 o 3 1 -21 17.79 37.78 29.14 o 4 1 -21 722.70 676.25 55.25 o 5 1 -21 61.30 78.65 32.82 o 6 1 -21 82.71 85.22 31.95 o 1 2 -21 116.36 51.89 30.75 o 2 2 -21 504.95 483.13 47.38 o 3 2 -21 1.72 13.74 26.89 o 0 0 -20 4241.32 4098.38 253.32 o 2 0 -20 503.92 558.44 73.80 o 4 0 -20 226.42 127.27 49.50 o 6 0 -20 1010.06 936.38 69.10 o 0 1 -20 1244.26 1166.74 97.01 o 1 1 -20 26.55 68.88 34.10 o 2 1 -20 395.88 339.14 42.61 o 3 1 -20 17.27 35.66 32.40 o 4 1 -20 58.35 91.12 32.52 o 5 1 -20 42.99 56.23 28.43 o 6 1 -20 732.06 801.84 77.23 o 7 1 -20 9.33 40.47 28.79 o 0 2 -20 873.59 818.31 75.73 o 1 2 -20 72.31 87.28 28.98 o 2 2 -20 343.17 344.59 43.75 o 3 2 -20 94.70 94.72 26.90 o 4 2 -20 271.82 277.27 37.97 o 5 2 -20 49.98 61.16 28.83 o 2 0 -19 829.04 812.41 87.25 o 4 0 -19 1282.01 1233.52 78.67 o 6 0 -19 166.47 150.53 45.16 o 8 0 -19 194.42 238.41 80.01 o 1 1 -19 202.91 244.10 34.43 o 2 1 -19 1216.58 1215.82 62.13 o 3 1 -19 54.01 46.53 30.47 o 4 1 -19 1376.51 1420.70 66.99 o 5 1 -19 5.99 54.51 30.43 o 6 1 -19 52.35 66.62 29.65 o 7 1 -19 56.51 50.38 29.07 o 8 1 -19 399.12 420.14 43.57 o 1 2 -19 88.27 120.55 31.06 o 2 2 -19 317.06 296.23 41.16 o 3 2 -19 17.27 4.55 26.54 o 4 2 -19 590.06 692.33 48.76 o 5 2 -19 137.29 121.25 40.07 o 6 2 -19 288.09 270.84 36.27 o 1 3 -19 222.12 227.79 40.11 o 2 3 -19 378.45 429.09 57.13 o 0 0 -18 4104.67 4200.16 247.73 o 2 0 -18 333.29 327.39 66.51 o 4 0 -18 428.82 423.56 62.46 o 6 0 -18 946.97 1059.53 80.83 o 8 0 -18 445.13 398.99 107.07 o 0 1 -18 1200.71 1207.61 88.51 o 1 1 -18 311.34 300.93 35.23 o 2 1 -18 1018.76 937.27 78.16 o 3 1 -18 190.91 209.17 41.28 o 4 1 -18 100.33 82.56 30.41 o 5 1 -18 89.17 74.59 28.70 o 6 1 -18 1124.01 1146.77 57.59 o 7 1 -18 6.61 7.79 26.71 o 8 1 -18 234.58 256.49 35.59 o 9 1 -18 53.65 60.68 25.88 o 0 2 -18 1129.00 1149.03 79.65 o 1 2 -18 187.14 153.18 34.38 o 2 2 -18 289.66 367.89 42.70 o 3 2 -18 469.61 510.52 56.38 o 4 2 -18 16.73 43.69 29.38 o 5 2 -18 66.29 66.80 27.06 o 6 2 -18 794.86 760.92 54.69 o 7 2 -18 19.81 65.03 26.74 o 0 3 -18 579.95 585.38 65.11 o 1 3 -18 12.68 38.14 27.04 o 2 3 -18 135.54 115.71 27.14 o 3 3 -18 244.03 299.38 39.04 o 4 3 -18 15.81 50.92 26.44 o 2 0 -17 2433.53 2604.32 113.59 o 4 0 -17 2461.01 2613.31 99.56 o 6 0 -17 93.67 140.30 45.24 o 8 0 -17 226.89 221.27 68.26 o 10 0 -17 603.59 639.97 71.93 o 1 1 -17 13.49 60.38 34.47 o 2 1 -17 1579.05 1618.30 62.83 o 3 1 -17 5.10 31.20 31.08 o 4 1 -17 1355.84 1357.61 62.95 o 5 1 -17 36.19 51.95 28.16 o 6 1 -17 292.40 392.88 41.00 o 7 1 -17 142.87 139.08 28.84 o 8 1 -17 219.66 212.30 33.38 o 9 1 -17 80.85 92.81 28.83 o 1 2 -17 277.17 330.54 40.65 o 2 2 -17 1390.89 1383.34 63.42 o 3 2 -17 1.16 -13.72 27.15 o 4 2 -17 635.23 682.42 47.02 o 5 2 -17 180.10 219.64 36.15 o 6 2 -17 40.09 41.47 26.89 o 7 2 -17 40.43 38.86 23.34 o 8 2 -17 139.11 175.53 30.30 o 1 3 -17 174.78 208.03 39.26 o 2 3 -17 321.23 306.52 42.29 o 3 3 -17 3.05 31.74 25.62 o 4 3 -17 443.04 412.23 41.53 o 5 3 -17 115.76 89.34 28.98 o 6 3 -17 54.20 47.28 23.78 o 0 0 -16 2585.11 2719.44 169.98 o 2 0 -16 902.44 941.26 84.23 o 4 0 -16 280.49 278.25 47.54 o 6 0 -16 1843.93 1847.38 104.59 o 8 0 -16 1003.50 1087.04 82.73 o 10 0 -16 16.29 67.66 43.79 o 0 1 -16 5797.05 5806.58 178.26 o 1 1 -16 163.85 158.76 33.68 o 2 1 -16 433.05 426.62 41.03 o 3 1 -16 80.57 137.62 39.89 o 4 1 -16 473.18 410.22 38.82 o 5 1 -16 261.90 220.19 32.43 o 6 1 -16 907.43 936.16 58.57 o 7 1 -16 13.73 84.12 28.65 o 8 1 -16 1010.05 909.60 50.93 o 9 1 -16 111.94 117.85 30.25 o 10 1 -16 21.73 27.96 20.12 o 0 2 -16 1158.64 1075.96 80.60 o 1 2 -16 4.81 30.85 29.79 o 2 2 -16 789.96 774.06 60.07 o 3 2 -16 178.33 200.30 40.77 o 4 2 -16 64.13 63.83 29.17 o 5 2 -16 222.53 220.26 35.25 o 6 2 -16 949.54 890.53 59.69 o 7 2 -16 143.78 160.36 30.72 o 8 2 -16 397.19 393.46 44.58 o 9 2 -16 56.15 44.23 27.22 o 0 3 -16 437.45 462.39 57.99 o 1 3 -16 96.75 107.48 35.16 o 2 3 -16 196.37 257.78 41.14 o 3 3 -16 285.18 284.72 33.86 o 4 3 -16 77.47 43.78 26.55 o 5 3 -16 66.83 78.69 33.11 o 6 3 -16 606.41 623.68 43.69 o 7 3 -16 44.98 52.00 23.65 o 2 0 -15 2227.64 2278.10 133.09 o 4 0 -15 1967.18 2090.48 102.42 o 6 0 -15 198.73 247.86 53.43 o 8 0 -15 704.81 718.16 86.44 o 10 0 -15 970.44 1031.35 71.64 o 1 1 -15 119.00 151.03 33.06 o 2 1 -15 1608.46 1565.83 77.10 o 3 1 -15 35.67 85.56 39.24 o 4 1 -15 2155.89 2131.78 71.50 o 5 1 -15 270.83 272.63 32.05 o 6 1 -15 71.53 71.60 26.61 o 7 1 -15 59.74 77.73 28.98 o 8 1 -15 289.76 325.69 34.41 o 9 1 -15 8.60 22.36 22.84 o 10 1 -15 601.54 619.04 40.69 o 11 1 -15 4.68 25.80 21.27 o 1 2 -15 415.16 381.18 39.76 o 2 2 -15 463.30 480.82 42.83 o 3 2 -15 235.91 228.36 34.50 o 4 2 -15 2296.09 2254.54 83.13 o 5 2 -15 112.15 96.13 28.85 o 6 2 -15 92.64 124.47 30.31 o 7 2 -15 561.77 562.45 41.72 o 8 2 -15 324.00 318.59 35.13 o 9 2 -15 35.32 61.93 22.61 o 1 3 -15 299.89 378.98 38.89 o 2 3 -15 496.10 522.48 43.98 o 3 3 -15 26.77 68.73 27.73 o 4 3 -15 585.42 578.70 43.97 o 5 3 -15 92.32 93.56 25.69 o 6 3 -15 91.72 104.83 28.88 o 7 3 -15 254.26 260.92 29.62 o 1 4 -15 345.80 359.90 38.32 o 2 4 -15 5.45 52.58 24.00 o 0 0 -14 5154.81 4917.64 158.20 o 2 0 -14 1653.36 1610.81 80.42 o 4 0 -14 344.69 310.72 64.52 o 6 0 -14 1720.25 1777.43 118.45 o 8 0 -14 1377.79 1379.05 72.76 o 10 0 -14 232.79 175.33 41.94 o 0 1 -14 4773.70 4835.79 117.23 o 1 1 -14 63.55 62.50 32.90 o 2 1 -14 1002.01 896.78 52.35 o 3 1 -14 500.62 482.51 39.63 o 4 1 -14 285.63 279.34 31.21 o 5 1 -14 38.57 48.32 32.40 o 6 1 -14 2277.25 2290.21 70.62 o 7 1 -14 56.21 80.52 25.83 o 8 1 -14 1091.90 1087.51 66.99 o 9 1 -14 68.74 101.67 27.59 o 10 1 -14 64.28 25.61 20.49 o 11 1 -14 37.11 47.71 22.89 o 0 2 -14 3642.37 3469.94 127.07 o 1 2 -14 375.85 412.08 38.44 o 2 2 -14 237.70 306.08 39.61 o 3 2 -14 564.97 526.78 40.69 o 4 2 -14 156.48 169.08 31.10 o 5 2 -14 151.90 123.11 47.38 o 6 2 -14 1052.46 1163.15 64.18 o 7 2 -14 3.37 32.85 27.85 o 8 2 -14 525.96 570.19 58.14 o 9 2 -14 85.55 78.20 22.73 o 10 2 -14 1.00 25.28 21.11 o 0 3 -14 946.05 919.29 79.55 o 1 3 -14 54.46 67.33 33.33 o 2 3 -14 334.06 379.42 37.72 o 3 3 -14 504.89 573.03 41.47 o 4 3 -14 13.81 50.79 22.78 o 5 3 -14 144.19 142.57 27.73 o 6 3 -14 321.31 363.20 34.30 o 7 3 -14 81.95 74.00 21.82 o 8 3 -14 369.58 372.15 39.41 o 0 4 -14 253.57 239.39 46.08 o 1 4 -14 143.50 148.59 32.06 o 2 4 -14 113.07 114.45 29.76 o 3 4 -14 156.21 199.41 33.01 o 4 4 -14 39.21 35.55 25.23 o 2 0 -13 5096.48 5189.92 195.39 o 4 0 -13 2694.39 2696.11 96.61 o 6 0 -13 203.59 263.88 92.09 o 8 0 -13 799.64 850.28 64.46 o 10 0 -13 2492.60 2494.25 167.59 o 12 0 -13 169.96 281.39 48.48 o 1 1 -13 111.87 111.60 34.26 o 2 1 -13 3543.22 3635.11 72.21 o 3 1 -13 123.20 134.15 37.49 o 4 1 -13 3063.54 2966.85 70.05 o 5 1 -13 142.26 158.10 32.83 o 6 1 -13 277.18 318.84 40.30 o 7 1 -13 129.45 98.67 23.17 o 8 1 -13 103.86 99.59 28.17 o 9 1 -13 46.43 57.60 22.79 o 10 1 -13 1346.83 1379.13 56.11 o 11 1 -13 3.35 56.11 23.30 o 1 2 -13 248.72 267.64 55.81 o 2 2 -13 2364.26 2280.14 72.32 o 3 2 -13 128.31 149.62 39.47 o 4 2 -13 1766.75 1822.24 64.66 o 5 2 -13 149.49 184.96 33.10 o 6 2 -13 174.50 193.65 31.21 o 7 2 -13 438.60 358.04 34.61 o 8 2 -13 229.96 210.28 27.11 o 9 2 -13 40.83 25.83 22.40 o 10 2 -13 519.01 525.65 34.96 o 1 3 -13 205.57 232.64 31.77 o 2 3 -13 247.84 280.97 34.28 o 3 3 -13 5.08 25.45 23.58 o 4 3 -13 716.51 680.89 44.51 o 5 3 -13 119.40 168.39 32.30 o 6 3 -13 127.58 137.04 28.58 o 7 3 -13 233.39 265.43 29.01 o 8 3 -13 223.58 234.82 36.76 o 9 3 -13 61.31 53.72 26.41 o 1 4 -13 443.62 463.04 39.31 o 2 4 -13 267.61 241.24 50.62 o 3 4 -13 41.03 83.10 24.28 o 4 4 -13 106.41 105.68 25.88 o 5 4 -13 150.89 119.97 23.71 o 0 0 -12 4767.30 4929.01 222.49 o 2 0 -12 810.77 843.82 63.88 o 4 0 -12 349.18 460.68 54.07 o 6 0 -12 3566.29 3741.51 171.02 o 8 0 -12 2431.43 2572.45 100.20 o 10 0 -12 411.70 405.76 46.76 o 12 0 -12 292.29 320.68 51.56 o 0 1 -12 4843.02 4977.67 149.15 o 1 1 -12 106.51 119.40 32.48 o 2 1 -12 1524.99 1552.62 58.77 o 3 1 -12 309.59 341.40 38.80 o 4 1 -12 694.64 696.14 44.77 o 5 1 -12 97.36 127.61 31.85 o 6 1 -12 3231.64 3260.36 102.72 o 7 1 -12 32.41 80.82 31.71 o 8 1 -12 224.96 230.04 31.46 o 9 1 -12 280.54 271.46 31.60 o 10 1 -12 42.48 64.20 24.37 o 11 1 -12 7.95 67.82 26.13 o 12 1 -12 209.54 220.09 29.15 o 0 2 -12 2383.21 2285.27 84.00 o 1 2 -12 477.56 462.79 41.89 o 2 2 -12 791.15 844.12 49.20 o 3 2 -12 604.07 604.35 42.45 o 4 2 -12 151.82 171.21 33.83 o 5 2 -12 66.84 53.13 44.79 o 6 2 -12 1355.26 1344.35 48.65 o 7 2 -12 80.76 85.13 30.48 o 8 2 -12 850.67 862.59 41.29 o 9 2 -12 270.49 236.52 29.69 o 10 2 -12 0.76 12.45 15.80 o 11 2 -12 54.51 38.50 23.32 o 0 3 -12 554.62 612.90 68.79 o 1 3 -12 158.36 116.90 29.72 o 2 3 -12 1081.94 1038.16 50.55 o 3 3 -12 1100.27 1155.16 76.73 o 4 3 -12 111.49 107.45 25.37 o 5 3 -12 176.56 199.73 28.71 o 6 3 -12 724.69 704.65 42.33 o 7 3 -12 36.48 48.99 19.09 o 8 3 -12 216.31 206.75 24.92 o 9 3 -12 91.58 68.25 54.96 o 0 4 -12 200.00 287.31 56.82 o 1 4 -12 45.55 39.21 27.75 o 2 4 -12 207.64 147.21 41.03 o 3 4 -12 326.95 332.07 38.35 o 4 4 -12 7.73 44.91 23.36 o 5 4 -12 121.96 101.04 25.56 o 6 4 -12 198.45 171.96 30.83 o 2 0 -11 3311.65 3321.75 116.50 o 4 0 -11 4806.62 4875.62 145.91 o 6 0 -11 379.25 355.06 49.31 o 8 0 -11 741.78 747.69 56.86 o 10 0 -11 966.92 998.68 80.64 o 12 0 -11 299.23 345.43 46.22 o 1 1 -11 158.03 195.29 31.30 o 2 1 -11 3264.50 3442.30 82.08 o 3 1 -11 40.47 49.87 28.88 o 4 1 -11 3683.19 3697.33 87.71 o 5 1 -11 70.63 68.37 30.23 o 6 1 -11 280.89 286.37 37.22 o 7 1 -11 590.73 604.41 39.89 o 8 1 -11 952.02 980.35 44.94 o 9 1 -11 207.39 196.16 26.96 o 10 1 -11 1001.38 1027.40 42.31 o 11 1 -11 52.09 60.06 22.58 o 12 1 -11 176.05 184.78 27.71 o 1 2 -11 610.41 630.99 41.61 o 2 2 -11 1755.94 1849.04 64.24 o 3 2 -11 211.33 185.22 30.65 o 4 2 -11 1880.82 1882.85 55.21 o 5 2 -11 266.00 270.48 31.68 o 6 2 -11 358.04 355.36 33.69 o 7 2 -11 192.36 191.71 25.28 o 8 2 -11 358.31 412.51 36.15 o 9 2 -11 61.87 88.86 22.07 o 10 2 -11 675.85 746.74 50.42 o 11 2 -11 43.83 55.22 26.38 o 1 3 -11 624.65 652.84 44.76 o 2 3 -11 1480.26 1426.26 57.46 o 3 3 -11 0.59 21.20 23.59 o 4 3 -11 2048.70 2106.61 73.12 o 5 3 -11 293.04 308.39 32.10 o 6 3 -11 83.45 65.15 25.50 o 7 3 -11 265.97 247.68 29.91 o 8 3 -11 105.36 107.89 23.45 o 9 3 -11 28.87 30.33 25.54 o 10 3 -11 276.86 347.97 68.46 o 1 4 -11 226.50 263.24 33.41 o 2 4 -11 290.33 249.33 33.24 o 3 4 -11 50.72 50.33 18.58 o 4 4 -11 218.46 239.35 29.43 o 5 4 -11 143.31 83.19 27.14 o 6 4 -11 37.16 50.72 28.20 o 7 4 -11 196.79 206.53 45.17 o 0 0 -10 10713.02 10855.81 337.87 o 2 0 -10 5671.67 6119.14 175.63 o 4 0 -10 6635.96 7511.54 213.22 o 6 0 -10 3317.36 3351.83 89.53 o 8 0 -10 1161.82 1195.84 77.04 o 10 0 -10 287.71 339.57 48.76 o 12 0 -10 563.91 548.66 56.43 o 0 1 -10 4023.11 4141.75 128.22 o 1 1 -10 75.67 40.80 31.05 o 2 1 -10 3088.29 3158.96 78.52 o 3 1 -10 123.06 128.05 28.40 o 4 1 -10 154.97 149.78 28.48 o 5 1 -10 79.37 80.69 26.13 o 6 1 -10 1814.09 1798.31 52.09 o 7 1 -10 48.31 58.10 28.84 o 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495.99 37.88 o 4 4 -10 22.24 29.21 14.26 o 5 4 -10 160.05 207.30 80.93 o 6 4 -10 118.41 148.74 32.22 o 7 4 -10 24.88 45.51 27.26 o 2 0 -9 2165.76 2093.42 109.26 o 4 0 -9 7972.79 8658.33 430.60 o 6 0 -9 698.24 703.78 55.30 o 8 0 -9 1470.53 1543.60 75.03 o 10 0 -9 1095.90 1119.91 96.03 o 12 0 -9 393.38 347.13 45.89 o 1 1 -9 447.51 484.73 32.74 o 2 1 -9 4746.28 4787.56 88.32 o 3 1 -9 384.64 425.33 33.29 o 4 1 -9 4603.61 4615.85 98.12 o 5 1 -9 132.10 128.68 25.22 o 6 1 -9 407.80 393.88 30.48 o 7 1 -9 192.35 174.31 23.42 o 8 1 -9 2166.75 2133.09 68.80 o 9 1 -9 176.05 161.18 26.82 o 10 1 -9 778.49 733.55 44.38 o 11 1 -9 68.38 48.92 21.83 o 12 1 -9 230.62 169.22 27.54 o 13 1 -9 103.73 100.82 30.20 o 1 2 -9 1396.78 1433.90 48.66 o 2 2 -9 927.69 998.00 47.96 o 3 2 -9 8.48 54.90 33.12 o 4 2 -9 2372.45 2489.13 55.60 o 5 2 -9 237.33 250.61 28.81 o 6 2 -9 661.75 633.36 60.26 o 7 2 -9 63.05 83.02 18.16 o 8 2 -9 629.00 646.79 33.28 o 9 2 -9 288.59 307.68 27.01 o 10 2 -9 941.71 1040.76 41.66 o 11 2 -9 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176.11 39.14 o 5 5 1 206.86 208.69 89.26 o 2 0 2 9937.10 10292.53 160.71 o 4 0 2 2887.70 2976.14 74.35 o 8 0 2 2436.93 2427.82 110.94 o 10 0 2 6.66 29.80 31.74 o 12 0 2 1395.80 1367.65 70.59 o 14 0 2 296.85 438.91 68.80 o 0 1 2 19130.77 19603.08 302.25 o 1 1 2 679.52 652.20 26.39 o 2 1 2 2315.95 2328.72 45.93 o 3 1 2 1038.09 1028.77 22.91 o 4 1 2 2185.98 2143.81 54.41 o 5 1 2 1775.18 1808.15 65.97 o 6 1 2 3798.80 3806.20 132.52 o 7 1 2 40.12 49.54 23.53 o 8 1 2 1450.88 1510.36 42.54 o 9 1 2 131.19 150.98 28.22 o 10 1 2 1.10 13.73 12.13 o 11 1 2 48.96 58.51 14.54 o 12 1 2 366.53 395.80 25.59 o 13 1 2 22.71 51.06 25.05 o 14 1 2 480.45 606.06 79.44 o 0 2 2 5263.17 5407.31 185.12 o 1 2 2 149.56 139.77 23.63 o 2 2 2 1680.55 1507.06 196.57 o 3 2 2 2430.24 2440.08 97.44 o 4 2 2 611.84 593.21 68.66 o 5 2 2 400.36 413.03 24.22 o 6 2 2 3843.93 3655.43 173.48 o 7 2 2 177.82 163.92 59.24 o 8 2 2 1450.95 1325.42 109.86 o 9 2 2 96.70 73.92 43.49 o 11 2 2 320.45 384.65 81.52 o 12 2 2 436.21 396.91 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1097.93 26.93 o 4 1 3 6358.94 6328.44 90.62 o 5 1 3 950.58 1018.84 29.75 o 6 1 3 998.24 968.14 48.30 o 7 1 3 142.25 121.00 22.33 o 8 1 3 875.20 868.56 37.25 o 9 1 3 98.88 76.56 16.10 o 10 1 3 3102.22 3292.37 114.64 o 11 1 3 56.90 67.37 18.57 o 12 1 3 520.85 543.42 28.45 o 13 1 3 14.17 47.62 20.68 o 14 1 3 98.22 150.05 60.52 o 1 2 3 1375.90 1393.64 67.01 o 2 2 3 5573.76 5519.52 130.35 o 3 2 3 66.98 93.10 22.19 o 4 2 3 4422.27 4557.49 167.35 o 5 2 3 211.15 214.58 23.31 o 6 2 3 159.56 166.40 24.07 o 7 2 3 478.66 417.30 79.23 o 8 2 3 475.74 453.25 76.81 o 12 2 3 342.58 337.60 92.83 o 13 2 3 27.13 117.20 62.61 o 1 3 3 521.30 487.10 43.19 o 2 3 3 762.80 712.15 47.76 o 3 3 3 30.89 57.27 34.68 o 4 3 3 1071.10 1024.65 82.23 o 5 3 3 470.49 441.95 50.99 o 6 3 3 1000.22 947.60 67.55 o 11 3 3 106.15 157.32 61.93 o 12 3 3 6.68 46.45 59.37 o 1 4 3 314.74 288.74 39.96 o 2 4 3 316.71 327.85 46.54 o 3 4 3 3.00 5.39 28.54 o 4 4 3 497.14 490.68 62.67 o 5 4 3 554.12 652.11 73.78 o 6 4 3 45.34 32.76 13.37 o 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119.95 28.98 o 8 2 4 673.49 761.97 91.22 o 9 2 4 334.24 345.27 70.41 o 13 2 4 12.53 6.40 51.16 o 0 3 4 1192.04 1112.16 86.23 o 1 3 4 476.89 465.75 44.98 o 2 3 4 581.39 639.58 49.11 o 3 3 4 772.40 700.75 61.46 o 4 3 4 244.94 243.08 34.87 o 5 3 4 361.63 351.63 38.88 o 6 3 4 768.60 738.52 63.28 o 7 3 4 95.65 118.82 18.51 o 0 4 4 1385.64 1257.30 96.33 o 1 4 4 192.92 181.82 40.86 o 2 4 4 78.13 93.42 33.42 o 3 4 4 735.91 729.25 74.79 o 4 4 4 27.81 23.83 26.39 o 5 4 4 172.44 181.76 33.39 o 6 4 4 319.44 346.71 29.01 o 3 5 4 251.72 255.13 54.80 o 4 5 4 34.35 12.12 23.83 o 2 0 5 5724.68 5625.33 108.38 o 4 0 5 7321.37 7697.79 141.05 o 6 0 5 1183.12 1178.08 116.12 o 8 0 5 2247.22 2158.21 85.09 o 10 0 5 2307.21 2300.86 111.21 o 12 0 5 362.42 355.44 52.91 o 14 0 5 261.31 358.94 67.12 o 1 1 5 1468.32 1439.89 35.67 o 2 1 5 4861.44 5003.11 109.09 o 3 1 5 77.54 72.42 15.42 o 4 1 5 6965.06 7249.21 110.10 o 5 1 5 663.22 649.86 25.21 o 6 1 5 58.23 71.82 17.63 o 7 1 5 114.97 138.71 20.62 o 8 1 5 1394.33 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6 156.41 148.44 33.05 o 8 3 6 710.91 830.57 70.15 o 0 4 6 445.10 381.36 63.01 o 1 4 6 410.09 381.28 42.80 o 2 4 6 233.08 169.17 55.74 o 3 4 6 120.86 122.72 46.92 o 4 4 6 129.94 163.72 42.07 o 5 4 6 270.37 252.44 39.11 o 2 0 7 10463.76 10833.08 189.52 o 4 0 7 7565.43 7892.99 267.22 o 6 0 7 334.14 332.80 35.40 o 8 0 7 3270.02 3473.04 90.01 o 10 0 7 1557.36 1467.46 92.49 o 12 0 7 366.05 401.42 68.73 o 14 0 7 56.16 64.69 49.95 o 1 1 7 399.98 393.28 25.30 o 2 1 7 4579.96 5041.05 151.70 o 3 1 7 27.06 57.77 25.75 o 4 1 7 5786.92 6167.29 102.06 o 5 1 7 120.06 138.66 20.29 o 6 1 7 1827.82 1774.22 47.06 o 7 1 7 154.37 175.05 20.68 o 8 1 7 930.14 922.89 35.48 o 9 1 7 44.45 55.19 22.93 o 10 1 7 1867.02 1907.10 72.75 o 11 1 7 53.72 58.23 43.82 o 12 1 7 394.44 402.90 45.84 o 13 1 7 43.21 10.03 21.34 o 1 2 7 1155.08 1187.43 42.18 o 2 2 7 7026.00 7660.54 146.39 o 3 2 7 1022.07 992.13 52.72 o 4 2 7 2502.38 2396.91 58.57 o 5 2 7 491.63 482.36 27.37 o 6 2 7 339.56 362.79 27.65 o 7 2 7 114.87 88.57 17.67 o 8 2 7 237.06 226.90 22.43 o 9 2 7 49.25 33.40 9.46 o 10 2 7 678.88 635.82 52.17 o 1 3 7 481.67 555.19 61.18 o 2 3 7 798.03 748.12 55.03 o 3 3 7 10.32 37.08 34.94 o 4 3 7 754.50 716.91 66.24 o 5 3 7 388.55 308.45 46.31 o 6 3 7 147.36 214.34 43.49 o 7 3 7 269.18 174.76 32.38 o 8 3 7 216.82 220.67 30.70 o 1 4 7 313.89 269.48 44.67 o 3 4 7 239.34 206.19 50.62 o 4 4 7 125.20 91.28 38.44 o 5 4 7 278.30 263.15 47.73 o 0 0 8 8262.22 8850.21 234.00 o 2 0 8 4097.00 4141.19 97.22 o 4 0 8 785.10 803.94 48.78 o 6 0 8 5172.65 5226.97 331.44 o 8 0 8 2071.79 2028.49 101.38 o 10 0 8 495.10 562.91 61.26 o 12 0 8 321.90 297.28 51.90 o 0 1 8 5021.17 5289.66 129.18 o 1 1 8 216.25 216.15 20.72 o 2 1 8 3149.83 3470.70 93.35 o 3 1 8 5.86 4.86 22.03 o 4 1 8 928.90 927.08 37.76 o 5 1 8 487.08 496.70 29.97 o 6 1 8 3573.82 3561.51 75.81 o 7 1 8 29.06 32.53 20.58 o 8 1 8 1425.38 1430.31 47.33 o 9 1 8 532.41 450.90 51.58 o 10 1 8 202.61 175.34 23.83 o 11 1 8 19.20 20.94 22.15 o 12 1 8 350.26 318.21 44.16 o 13 1 8 18.63 35.27 26.12 o 0 2 8 910.90 934.83 56.85 o 1 2 8 2497.23 2487.92 63.75 o 2 2 8 3125.14 3261.86 72.64 o 3 2 8 1420.14 1448.81 47.53 o 4 2 8 262.13 289.85 29.57 o 5 2 8 323.17 312.23 26.47 o 6 2 8 2640.35 2548.26 58.28 o 7 2 8 22.77 39.64 20.43 o 8 2 8 925.89 957.41 42.44 o 9 2 8 234.64 237.89 22.30 o 10 2 8 3.62 8.37 37.19 o 0 3 8 1526.91 1479.24 102.86 o 1 3 8 437.38 364.93 37.84 o 2 3 8 1264.80 1201.70 52.86 o 3 3 8 630.04 685.99 62.91 o 4 3 8 218.59 225.91 43.80 o 5 3 8 223.27 249.28 46.99 o 6 3 8 906.98 878.36 56.01 o 7 3 8 17.66 37.70 29.49 o 8 3 8 345.45 378.66 39.85 o 0 4 8 339.43 303.74 63.95 o 1 4 8 54.71 55.67 41.20 o 2 4 8 215.28 131.00 46.25 o 3 4 8 536.09 422.15 59.11 o 4 4 8 20.34 31.44 28.00 o 5 4 8 170.18 126.96 39.99 o 2 0 9 2555.87 2669.15 88.47 o 4 0 9 8056.77 8692.80 221.39 o 6 0 9 633.06 600.66 44.51 o 8 0 9 1244.56 1231.57 58.62 o 10 0 9 1529.83 1533.87 76.47 o 12 0 9 417.08 334.37 55.27 o 1 1 9 439.96 428.97 27.79 o 2 1 9 5206.34 5372.91 95.68 o 3 1 9 389.65 381.08 27.56 o 4 1 9 4665.98 4891.30 103.13 o 5 1 9 157.65 172.31 23.24 o 6 1 9 362.45 399.15 31.85 o 7 1 9 141.48 142.87 24.47 o 8 1 9 1978.01 1976.38 80.68 o 9 1 9 178.45 123.02 23.40 o 10 1 9 893.49 877.00 52.52 o 11 1 9 62.45 55.77 23.11 o 1 2 9 1242.23 1238.14 47.62 o 2 2 9 933.43 949.97 46.91 o 3 2 9 11.79 53.92 24.93 o 4 2 9 2348.16 2447.45 56.90 o 5 2 9 262.05 246.29 23.94 o 6 2 9 733.97 758.22 38.54 o 7 2 9 66.92 62.12 23.18 o 8 2 9 619.14 597.66 33.06 o 9 2 9 272.61 304.96 51.97 o 10 2 9 995.43 995.22 70.48 o 1 3 9 897.60 937.11 45.96 o 2 3 9 2899.46 2887.51 72.88 o 3 3 9 10.77 17.56 20.48 o 4 3 9 690.53 692.02 42.32 o 5 3 9 486.49 504.84 38.62 o 6 3 9 15.21 18.57 17.89 o 7 3 9 268.86 330.19 52.71 o 8 3 9 60.55 34.33 19.39 o 1 4 9 170.84 120.63 40.79 o 2 4 9 98.84 123.19 51.03 o 3 4 9 44.28 64.29 43.55 o 4 4 9 432.51 309.73 64.09 o 5 4 9 125.80 92.49 41.87 o 0 0 10 10757.48 11245.45 412.05 o 2 0 10 5291.41 5703.68 143.42 o 4 0 10 6359.47 7067.45 296.40 o 6 0 10 3338.95 3548.81 163.92 o 8 0 10 1502.71 1446.04 87.61 o 10 0 10 296.07 345.11 42.81 o 12 0 10 544.57 430.16 59.24 o 0 1 10 4299.66 4445.95 224.37 o 1 1 10 51.43 63.09 26.55 o 2 1 10 3118.71 3196.74 77.53 o 3 1 10 162.59 120.95 24.80 o 4 1 10 221.83 233.71 28.21 o 5 1 10 80.82 91.15 26.11 o 6 1 10 1816.21 1771.73 48.47 o 7 1 10 59.80 57.56 22.40 o 8 1 10 3502.75 3563.45 86.84 o 9 1 10 33.25 22.93 19.08 o 10 1 10 28.91 37.44 25.40 o 11 1 10 76.78 90.31 27.98 o 0 2 10 5415.34 5474.85 318.41 o 1 2 10 170.73 137.88 23.26 o 2 2 10 1449.09 1448.76 56.54 o 3 2 10 322.97 380.12 36.06 o 4 2 10 382.56 354.02 31.57 o 5 2 10 194.98 203.94 26.08 o 6 2 10 1702.54 1714.98 53.62 o 7 2 10 474.60 439.39 42.65 o 8 2 10 675.54 668.70 49.28 o 9 2 10 129.94 99.73 47.09 o 10 2 10 1.87 36.85 15.96 o 0 3 10 2249.73 2271.27 151.03 o 1 3 10 534.19 546.28 38.26 o 2 3 10 6.65 62.89 33.23 o 3 3 10 99.88 104.14 21.81 o 4 3 10 56.87 32.69 22.30 o 5 3 10 147.65 140.39 28.27 o 6 3 10 530.32 531.22 44.03 o 7 3 10 35.08 45.16 25.92 o 8 3 10 478.73 420.87 52.24 o 2 4 10 40.59 10.91 32.45 o 3 4 10 474.04 439.25 71.42 o 4 4 10 18.91 29.28 29.08 o 5 4 10 159.17 127.16 42.14 o 2 0 11 3164.60 3121.40 108.76 o 4 0 11 4569.04 4353.20 129.03 o 6 0 11 371.10 313.96 42.18 o 8 0 11 647.69 510.79 63.01 o 10 0 11 910.72 870.50 71.72 o 1 1 11 158.38 150.98 24.13 o 2 1 11 3212.99 3387.64 76.75 o 3 1 11 37.09 46.52 24.32 o 4 1 11 3585.60 3645.15 83.15 o 5 1 11 60.29 101.88 31.26 o 6 1 11 261.28 210.41 24.86 o 7 1 11 691.31 741.51 40.26 o 8 1 11 985.10 887.30 39.45 o 9 1 11 191.40 153.84 23.59 o 10 1 11 1024.79 1025.34 129.82 o 11 1 11 48.00 31.31 19.06 o 1 2 11 596.76 615.98 38.28 o 2 2 11 1788.44 1875.43 83.13 o 3 2 11 225.91 193.56 32.37 o 4 2 11 1944.67 1885.89 53.32 o 5 2 11 244.62 268.78 28.71 o 6 2 11 275.67 256.32 31.39 o 7 2 11 225.65 217.49 27.89 o 8 2 11 358.22 344.89 66.24 o 9 2 11 69.27 40.76 17.80 o 10 2 11 627.43 515.65 69.14 o 1 3 11 703.23 702.98 42.21 o 2 3 11 1087.99 1022.47 46.15 o 3 3 11 1.84 27.27 30.02 o 4 3 11 2455.69 2541.52 144.71 o 5 3 11 324.07 296.28 39.21 o 6 3 11 86.88 100.77 24.74 o 7 3 11 285.82 264.53 30.24 o 3 4 11 43.68 26.32 30.29 o 4 4 11 232.12 65.10 30.29 o 0 0 12 5288.98 5446.76 229.82 o 2 0 12 539.22 538.75 64.02 o 4 0 12 427.14 455.17 43.18 o 6 0 12 3513.67 3482.25 99.12 o 8 0 12 2679.39 2831.33 120.65 o 10 0 12 399.71 459.71 65.43 o 0 1 12 4914.63 4874.88 142.43 o 1 1 12 87.84 104.71 33.91 o 2 1 12 1601.47 1672.90 55.23 o 3 1 12 343.08 410.31 34.26 o 4 1 12 683.67 656.87 39.53 o 5 1 12 95.59 62.04 26.46 o 6 1 12 3149.22 3222.24 78.84 o 7 1 12 36.30 39.08 20.95 o 8 1 12 260.62 187.98 28.95 o 9 1 12 233.62 148.20 47.59 o 10 1 12 45.40 34.14 20.92 o 11 1 12 10.80 48.12 21.32 o 0 2 12 2794.25 2578.54 132.01 o 1 2 12 492.92 474.40 41.31 o 2 2 12 757.79 741.60 41.88 o 3 2 12 537.64 494.81 39.99 o 4 2 12 167.27 181.94 24.17 o 5 2 12 69.12 90.90 24.54 o 6 2 12 1347.05 1355.70 59.12 o 7 2 12 98.13 75.21 25.30 o 8 2 12 824.34 840.17 44.58 o 9 2 12 301.14 289.51 33.50 o 0 3 12 594.55 550.89 100.40 o 1 3 12 97.24 90.42 24.33 o 2 3 12 950.90 854.05 51.36 o 3 3 12 1049.84 981.64 60.22 o 4 3 12 86.20 84.81 32.98 o 5 3 12 193.64 178.00 33.67 o 6 3 12 742.20 678.31 153.48 o 7 3 12 40.93 50.78 19.64 o 2 0 13 4950.49 4980.04 150.03 o 4 0 13 2798.33 2711.63 91.16 o 6 0 13 203.74 146.83 41.30 o 8 0 13 558.05 473.07 56.28 o 10 0 13 2742.53 2436.10 148.84 o 1 1 13 113.31 88.92 25.17 o 2 1 13 3931.21 4128.29 108.31 o 3 1 13 124.38 138.83 27.54 o 4 1 13 3056.24 3040.33 69.83 o 5 1 13 176.36 141.89 29.21 o 6 1 13 211.61 174.81 24.23 o 7 1 13 95.27 71.37 23.02 o 8 1 13 73.46 59.29 33.37 o 9 1 13 41.82 76.89 33.06 o 10 1 13 1377.61 1185.41 73.65 o 1 2 13 147.50 133.98 26.64 o 2 2 13 2208.15 2213.15 67.77 o 3 2 13 139.16 151.37 26.31 o 4 2 13 1699.22 1686.77 80.63 o 5 2 13 149.79 135.07 28.50 o 6 2 13 230.18 152.47 29.60 o 7 2 13 456.97 442.39 47.26 o 8 2 13 242.91 234.88 40.29 o 9 2 13 31.71 42.41 25.44 o 1 3 13 198.77 200.91 38.21 o 2 3 13 397.88 332.21 43.47 o 3 3 13 3.60 24.23 28.86 o 4 3 13 631.48 581.47 66.34 o 5 3 13 124.43 84.21 27.53 o 6 3 13 119.02 56.78 26.40 o 7 3 13 259.42 171.93 54.53 o 0 0 14 5381.48 5410.81 177.32 o 2 0 14 1676.72 1628.76 80.05 o 4 0 14 375.69 367.20 114.31 o 6 0 14 1814.35 1623.67 79.31 o 8 0 14 1008.54 897.55 99.56 o 0 1 14 4785.64 4927.59 137.29 o 1 1 14 60.69 100.12 33.98 o 2 1 14 758.39 751.00 46.14 o 3 1 14 505.51 516.82 36.77 o 4 1 14 190.94 185.34 27.75 o 5 1 14 38.32 59.35 24.17 o 6 1 14 2262.93 2114.87 66.88 o 7 1 14 50.67 70.51 29.56 o 8 1 14 1162.04 1076.43 111.55 o 9 1 14 98.95 29.89 45.37 o 10 1 14 61.23 50.89 38.37 o 0 2 14 3346.20 3157.74 128.44 o 1 2 14 313.95 274.37 29.73 o 2 2 14 311.82 286.76 49.89 o 3 2 14 682.81 710.00 55.47 o 4 2 14 160.34 159.92 36.87 o 5 2 14 176.22 113.06 29.89 o 6 2 14 1198.15 1334.86 128.31 o 7 2 14 6.74 50.01 29.74 o 8 2 14 436.68 464.10 72.91 o 9 2 14 77.25 73.38 29.62 o 1 3 14 73.32 78.83 40.32 o 2 3 14 402.42 512.83 77.48 o 3 3 14 534.05 521.17 60.72 o 4 3 14 9.26 51.28 26.89 o 5 3 14 138.11 96.08 22.68 o 6 3 14 346.60 275.29 36.51 o 2 0 15 2377.11 2428.07 112.82 o 4 0 15 1909.37 1689.26 82.65 o 6 0 15 190.38 216.70 52.58 o 1 1 15 119.74 108.46 29.33 o 2 1 15 1453.70 1381.14 55.63 o 3 1 15 38.26 72.61 25.92 o 4 1 15 2147.09 1891.66 73.85 o 5 1 15 237.50 188.63 38.04 o 6 1 15 121.22 75.18 41.97 o 7 1 15 75.35 86.96 31.32 o 8 1 15 279.71 193.20 44.90 o 9 1 15 9.71 18.65 31.17 o 1 2 15 469.67 452.19 39.12 o 2 2 15 552.96 473.77 45.38 o 3 2 15 224.85 188.73 39.60 o 4 2 15 2364.17 2266.09 116.90 o 5 2 15 108.05 68.25 25.96 o 6 2 15 54.25 42.15 26.17 o 7 2 15 570.26 431.93 43.69 o 8 2 15 262.64 231.44 46.52 o 2 3 15 493.39 423.50 73.04 o 3 3 15 29.47 25.31 46.85 o 4 3 15 549.49 713.37 93.64 o 5 3 15 93.91 83.14 37.77 o 6 3 15 87.66 83.47 31.91 o 0 0 16 2675.08 2394.70 135.44 o 2 0 16 955.66 948.26 122.75 o 4 0 16 261.87 244.63 53.52 o 0 1 16 6040.61 5992.83 179.57 o 1 1 16 145.06 132.68 29.09 o 2 1 16 481.90 443.14 63.31 o 3 1 16 42.57 30.33 36.19 o 4 1 16 553.37 568.10 54.37 o 5 1 16 277.83 316.80 66.38 o 6 1 16 911.65 758.20 88.79 o 7 1 16 16.96 41.60 33.66 o 8 1 16 972.80 851.57 86.23 o 9 1 16 131.85 60.05 43.15 o 1 2 16 6.39 13.06 39.18 o 2 2 16 717.00 751.87 86.77 o 4 2 16 36.35 41.54 41.27 o 5 2 16 195.91 146.55 42.07 o 6 2 16 864.25 777.25 76.61 o 7 2 16 140.04 63.62 26.12 o 4 3 16 98.23 86.57 39.45 o 5 3 16 57.78 15.69 39.25 o 1 1 17 2.32 16.90 44.36 o 3 1 17 5.74 44.90 44.16 o 4 1 17 1405.27 1168.77 103.20 o 5 2 17 208.46 209.29 52.98 o 6 2 17 67.04 28.34 30.63 o 7 2 17 15.78 61.06 37.90 o