#------------------------------------------------------------------------------ #$Date: 2016-04-06 17:06:23 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181905 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/05/2240597.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2240597 _cell_angle_alpha 90.000 _cell_angle_beta 94.036 _cell_angle_gamma 90.000 _cell_length_a 3.7792 _cell_length_b 29.8913 _cell_length_c 7.0139 _exptl_crystal_F_000 414.00 _reflns_d_resolution_high 0.8000 _cod_data_source_file cq2014Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' qo115 in P21/n (14) sir97' _shelx_refln_list_code 4 _shelx_f_calc_maximum 108.05 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4292.57 4406.74 89.69 o 4 0 0 16.30 -1.40 10.27 o 1 1 0 7961.76 7919.71 70.60 o 2 1 0 590.59 645.97 17.85 o 3 1 0 814.74 938.84 37.31 o 4 1 0 8.33 -7.19 7.19 o 1 2 0 5265.36 5330.53 53.58 o 2 2 0 6538.79 6956.58 145.05 o 3 2 0 29.79 35.10 7.49 o 4 2 0 197.23 179.33 20.94 o 1 3 0 28.30 43.58 2.53 o 2 3 0 2297.10 2475.49 61.39 o 3 3 0 1832.48 1996.99 58.54 o 4 3 0 32.08 30.03 13.62 o 1 4 0 4599.91 4644.48 47.05 o 2 4 0 3241.55 3237.34 50.43 o 3 4 0 268.43 343.11 21.75 o 4 4 0 115.15 116.74 14.53 o 1 5 0 324.10 379.47 8.74 o 2 5 0 47.99 59.82 5.46 o 3 5 0 700.41 757.31 33.10 o 4 5 0 373.48 333.12 24.81 o 1 6 0 752.82 817.16 17.10 o 2 6 0 95.23 76.66 9.08 o 3 6 0 645.75 650.51 24.11 o 4 6 0 38.71 51.76 10.49 o 1 7 0 599.81 545.52 9.51 o 2 7 0 1186.55 1149.96 32.43 o 3 7 0 5.84 5.61 4.22 o 4 7 0 241.99 257.75 40.58 o 0 8 0 574.45 546.12 13.86 o 1 8 0 584.34 600.04 14.99 o 2 8 0 549.91 489.91 17.48 o 3 8 0 820.85 854.41 28.48 o 4 8 0 45.82 43.25 9.85 o 1 9 0 378.90 336.71 7.31 o 2 9 0 882.14 900.49 25.93 o 3 9 0 524.69 549.42 22.73 o 4 9 0 96.82 72.47 13.01 o 0 10 0 261.38 242.10 16.44 o 1 10 0 665.17 640.37 12.04 o 2 10 0 314.41 304.51 13.81 o 3 10 0 513.27 553.60 31.10 o 4 10 0 228.46 247.65 17.72 o 1 11 0 4939.98 4790.39 54.66 o 2 11 0 335.87 316.75 14.36 o 3 11 0 293.07 312.22 17.24 o 4 11 0 322.87 333.58 20.63 o 0 12 0 514.55 465.55 14.37 o 1 12 0 49.84 55.59 3.30 o 2 12 0 717.29 712.96 22.68 o 3 12 0 186.80 190.49 16.71 o 4 12 0 470.55 501.60 25.58 o 1 13 0 4200.15 4245.45 49.93 o 2 13 0 766.81 804.40 28.72 o 3 13 0 432.86 441.12 25.81 o 4 13 0 28.63 54.06 14.39 o 0 14 0 65.85 56.77 4.36 o 1 14 0 146.19 156.67 5.52 o 2 14 0 181.94 189.51 12.88 o 3 14 0 75.40 61.79 23.77 o 4 14 0 519.34 501.06 26.05 o 1 15 0 4104.74 3995.47 49.55 o 2 15 0 0.23 7.20 3.84 o 3 15 0 648.15 671.17 32.94 o 4 15 0 64.01 58.58 10.32 o 0 16 0 447.95 391.78 26.87 o 1 16 0 21.29 39.64 5.30 o 2 16 0 606.02 602.34 21.56 o 3 16 0 0.03 6.79 5.96 o 4 16 0 567.91 580.12 31.04 o 1 17 0 7264.49 7216.61 111.50 o 2 17 0 0.38 -3.24 3.85 o 3 17 0 322.72 330.50 23.49 o 4 17 0 48.10 61.02 10.57 o 0 18 0 78.40 55.94 11.67 o 1 18 0 36.81 71.79 11.54 o 2 18 0 595.43 595.73 22.44 o 3 18 0 37.14 35.49 11.53 o 4 18 0 919.91 876.82 36.60 o 1 19 0 3194.26 3198.60 61.49 o 2 19 0 48.87 56.03 7.70 o 3 19 0 1613.88 1612.34 56.88 o 4 19 0 36.96 49.26 10.22 o 0 20 0 562.17 541.84 29.81 o 1 20 0 33.01 56.60 12.96 o 2 20 0 1177.50 1229.86 38.25 o 3 20 0 98.27 97.70 25.72 o 1 21 0 4020.23 3997.84 74.58 o 2 21 0 1669.44 1703.77 43.76 o 3 21 0 199.14 179.69 18.62 o 0 22 0 1395.57 1319.15 28.53 o 1 22 0 0.09 19.95 11.01 o 2 22 0 228.20 238.43 15.42 o 3 22 0 456.76 467.62 30.20 o 1 23 0 1725.89 1829.65 49.36 o 2 23 0 16.58 14.21 4.61 o 3 23 0 19.14 14.29 7.00 o 0 24 0 932.03 975.67 53.87 o 1 24 0 1625.94 1637.57 68.98 o 2 24 0 64.48 64.23 12.27 o 3 24 0 428.46 419.09 29.88 o 1 25 0 90.47 116.17 14.50 o 2 25 0 163.12 146.42 12.66 o 3 25 0 281.29 264.41 24.24 o 0 26 0 686.31 608.48 43.71 o 1 26 0 106.60 116.34 14.06 o 2 26 0 368.69 374.35 20.73 o 3 26 0 305.86 263.42 46.39 o 1 27 0 11.63 18.21 7.48 o 2 27 0 522.01 521.91 25.28 o 3 27 0 135.50 160.68 24.74 o 0 28 0 2276.12 2121.57 93.03 o 1 28 0 133.26 112.13 14.09 o 2 28 0 171.83 172.08 17.11 o 3 28 0 102.15 90.74 15.48 o 1 29 0 71.22 85.95 12.89 o 2 29 0 306.74 275.36 18.78 o 0 30 0 2555.07 2569.61 108.57 o 1 30 0 296.74 294.88 23.46 o 2 30 0 514.49 506.73 34.11 o 1 31 0 232.18 235.30 21.78 o 2 31 0 31.33 48.38 12.39 o 0 32 0 2101.03 2056.68 98.42 o 1 32 0 0.26 -2.72 6.80 o 2 32 0 1335.31 1272.75 57.46 o 1 33 0 73.82 78.36 13.73 o 2 33 0 6.91 37.14 22.47 o 0 34 0 1988.93 2093.79 102.92 o 1 34 0 3.03 7.97 6.95 o 1 35 0 109.96 109.66 16.23 o 0 36 0 873.56 771.76 61.31 o 1 36 0 30.18 29.59 10.66 o -3 0 1 1861.35 1893.06 74.82 o -1 0 1 8891.61 8665.54 140.99 o 1 0 1 125.35 189.22 11.25 o 3 0 1 28.48 23.05 8.15 o -4 1 1 48.04 11.44 6.99 o -3 1 1 53.45 59.54 5.49 o -2 1 1 75.52 65.78 5.97 o -1 1 1 3197.76 3316.13 42.34 o 1 1 1 433.85 399.92 9.29 o 2 1 1 3681.31 3679.94 54.81 o 3 1 1 0.32 -1.31 3.50 o 4 1 1 809.77 892.71 33.82 o -4 2 1 4.90 -8.22 8.22 o -3 2 1 2377.98 2402.52 70.17 o -2 2 1 64.66 51.24 5.16 o -1 2 1 1963.03 2017.49 33.70 o 1 2 1 25.98 23.85 2.43 o 2 2 1 10.77 15.09 4.12 o 3 2 1 9.30 4.74 3.33 o 4 2 1 59.02 29.91 14.87 o -4 3 1 1.85 -2.55 7.44 o -3 3 1 26.00 31.48 5.93 o -2 3 1 148.66 123.91 7.89 o -1 3 1 1167.98 1271.22 23.31 o 1 3 1 11675.71 11808.13 134.27 o 2 3 1 3505.47 3602.56 53.97 o 3 3 1 10.85 7.92 3.14 o 4 3 1 506.63 512.48 25.21 o -4 4 1 69.22 48.19 28.94 o -3 4 1 1939.33 1948.61 45.18 o -2 4 1 81.44 68.49 4.98 o -1 4 1 5782.26 5749.75 81.03 o 1 4 1 5228.16 5127.44 81.36 o 2 4 1 982.51 1029.18 29.87 o 3 4 1 113.86 111.59 8.74 o 4 4 1 228.56 211.03 22.76 o -4 5 1 255.43 248.46 22.19 o -3 5 1 174.53 197.99 12.92 o -2 5 1 321.78 291.02 13.22 o -1 5 1 3278.21 3433.78 52.91 o 0 5 1 292.52 298.73 5.78 o 1 5 1 4009.98 4003.71 69.84 o 2 5 1 9532.38 9815.33 122.57 o 3 5 1 183.01 164.50 10.69 o 4 5 1 671.52 705.76 30.09 o -4 6 1 71.23 38.83 9.04 o -3 6 1 2083.72 2236.21 60.17 o -2 6 1 279.36 233.03 12.00 o -1 6 1 468.41 460.76 11.61 o 0 6 1 2396.02 2575.74 27.47 o 1 6 1 287.81 257.42 7.31 o 2 6 1 198.72 224.56 12.10 o 3 6 1 1059.39 1064.31 44.76 o 4 6 1 502.61 490.88 25.19 o -4 7 1 124.34 96.63 14.64 o -3 7 1 93.59 102.95 9.63 o -2 7 1 1666.91 1665.70 79.79 o -1 7 1 3142.00 3266.15 46.93 o 0 7 1 4008.49 3860.14 36.38 o 1 7 1 17.20 15.91 2.43 o 2 7 1 605.61 593.87 22.84 o 3 7 1 109.00 129.65 9.83 o 4 7 1 729.36 733.01 26.32 o -4 8 1 5.34 0.50 7.66 o -3 8 1 481.52 526.35 22.05 o -2 8 1 4.91 9.39 2.32 o -1 8 1 6032.01 6054.11 72.23 o 0 8 1 3668.47 3703.49 38.20 o 1 8 1 1187.25 1081.14 21.63 o 2 8 1 743.89 763.30 23.28 o 3 8 1 266.61 277.00 14.27 o 4 8 1 407.02 386.68 18.94 o -4 9 1 180.61 200.73 24.32 o -3 9 1 0.12 -3.31 4.76 o -2 9 1 1241.79 1161.91 61.60 o -1 9 1 2698.03 2853.65 63.35 o 0 9 1 2735.56 2674.20 31.87 o 1 9 1 2433.31 2357.22 43.50 o 2 9 1 105.34 84.27 7.49 o 3 9 1 674.47 679.98 22.75 o 4 9 1 71.32 86.60 9.00 o -4 10 1 43.49 50.83 11.29 o -3 10 1 2.66 7.79 5.06 o -2 10 1 1963.79 1969.33 77.73 o -1 10 1 845.96 780.11 15.40 o 0 10 1 268.70 244.09 5.99 o 1 10 1 1851.44 1751.83 43.06 o 2 10 1 194.81 207.99 21.98 o 3 10 1 234.56 275.56 14.23 o 4 10 1 0.64 3.92 4.66 o -4 11 1 287.30 300.55 37.70 o -3 11 1 6.11 5.16 4.72 o -2 11 1 797.96 692.38 21.70 o -1 11 1 221.54 202.92 8.29 o 0 11 1 550.82 496.99 9.47 o 1 11 1 117.35 111.99 5.38 o 2 11 1 590.96 546.04 19.76 o 3 11 1 97.17 99.74 7.89 o 4 11 1 19.39 10.37 5.06 o -4 12 1 13.91 19.68 9.80 o -3 12 1 57.39 56.98 9.06 o -2 12 1 359.55 345.50 13.29 o -1 12 1 8.90 6.20 1.53 o 0 12 1 5280.50 5382.25 59.74 o 1 12 1 5919.22 5845.12 72.30 o 2 12 1 190.72 170.55 11.23 o 3 12 1 1659.44 1733.10 44.59 o 4 12 1 26.08 28.19 6.59 o -4 13 1 650.04 734.66 41.49 o -3 13 1 0.35 -5.46 7.35 o -2 13 1 2641.21 2774.37 50.54 o -1 13 1 5.02 11.49 4.28 o 0 13 1 2233.95 2220.97 28.60 o 1 13 1 94.18 107.18 5.57 o 2 13 1 6.45 4.03 3.77 o 3 13 1 25.22 40.92 7.16 o 4 13 1 14.73 8.84 5.31 o -4 14 1 0.90 24.45 22.37 o -3 14 1 4.74 4.22 5.90 o -2 14 1 187.86 219.00 11.58 o -1 14 1 3601.28 3676.49 60.24 o 0 14 1 2377.54 2615.67 38.46 o 1 14 1 1946.24 1782.07 28.46 o 2 14 1 106.74 93.03 7.38 o 3 14 1 1317.18 1412.67 39.91 o 4 14 1 3.76 11.33 5.67 o -4 15 1 1229.11 1262.79 56.22 o -3 15 1 50.69 55.65 10.30 o -2 15 1 4021.52 4294.45 93.97 o -1 15 1 75.59 96.56 11.19 o 0 15 1 1192.44 1130.88 23.01 o 1 15 1 44.45 39.07 3.25 o 2 15 1 4.72 3.11 2.38 o 3 15 1 32.34 53.90 8.48 o 4 15 1 234.48 210.31 16.48 o -4 16 1 0.37 51.22 30.34 o -3 16 1 79.51 74.33 11.49 o -2 16 1 422.62 471.14 18.19 o -1 16 1 646.00 713.82 22.05 o 0 16 1 449.63 495.34 13.18 o 1 16 1 4476.93 4453.19 55.95 o 2 16 1 14.02 17.07 3.95 o 3 16 1 3005.88 3235.86 68.32 o 4 16 1 132.19 134.20 16.05 o -4 17 1 913.09 976.34 49.56 o -3 17 1 0.75 12.76 7.23 o -2 17 1 2430.95 2539.75 52.35 o -1 17 1 12.64 17.91 4.38 o 0 17 1 857.20 847.79 18.91 o 1 17 1 34.84 40.32 4.81 o 2 17 1 209.00 208.42 11.01 o 3 17 1 219.27 259.51 22.27 o 4 17 1 24.31 16.95 6.09 o -4 18 1 40.20 47.03 10.17 o -3 18 1 7.20 9.13 6.61 o -2 18 1 607.46 596.12 21.77 o -1 18 1 71.39 71.33 7.46 o 0 18 1 8.38 25.28 6.76 o 1 18 1 3660.29 3583.27 53.87 o 2 18 1 161.50 151.72 9.48 o 3 18 1 1828.26 1998.20 58.44 o 4 18 1 20.61 18.78 8.15 o -4 19 1 635.35 674.71 32.83 o -3 19 1 0.02 3.13 5.53 o -2 19 1 1448.24 1520.35 58.11 o -1 19 1 94.73 72.51 9.59 o 0 19 1 981.26 974.64 25.47 o 1 19 1 417.03 429.94 14.00 o 2 19 1 186.96 189.61 10.64 o 3 19 1 292.97 288.67 22.62 o -3 20 1 46.35 37.08 9.43 o -2 20 1 179.50 198.16 14.89 o -1 20 1 1880.97 1873.82 43.59 o 0 20 1 742.35 801.90 22.97 o 1 20 1 2627.06 2578.51 43.11 o 2 20 1 465.58 454.26 16.88 o 3 20 1 280.93 321.25 24.42 o -3 21 1 46.07 34.45 9.76 o -2 21 1 1098.41 1094.55 32.77 o -1 21 1 215.25 220.14 15.74 o 0 21 1 1509.02 1630.27 36.27 o 1 21 1 3.42 15.95 4.01 o 2 21 1 136.46 154.34 12.43 o 3 21 1 299.70 329.85 24.76 o -3 22 1 101.09 94.65 35.79 o -2 22 1 273.64 262.40 16.38 o -1 22 1 160.89 154.39 13.93 o 0 22 1 1519.63 1539.97 44.27 o 1 22 1 322.69 301.65 12.53 o 2 22 1 592.54 615.67 25.50 o 3 22 1 654.46 664.81 36.23 o -3 23 1 73.71 56.47 11.27 o -2 23 1 1034.54 1024.88 32.92 o -1 23 1 394.94 425.91 24.27 o 0 23 1 204.78 235.20 12.16 o 1 23 1 69.81 59.87 10.09 o 2 23 1 362.88 380.68 20.13 o 3 23 1 87.33 76.69 13.43 o -3 24 1 211.18 210.24 21.44 o -2 24 1 329.81 335.35 18.48 o -1 24 1 1344.63 1382.21 47.77 o 0 24 1 1671.15 1678.94 37.78 o 1 24 1 936.57 927.05 38.14 o 2 24 1 45.06 46.87 8.68 o 3 24 1 259.32 276.10 23.83 o -3 25 1 0.92 -3.64 9.60 o -2 25 1 238.52 241.57 21.83 o -1 25 1 61.05 85.46 13.01 o 0 25 1 1198.28 1287.48 46.43 o 1 25 1 530.96 499.10 28.21 o 2 25 1 767.34 767.12 30.27 o 3 25 1 19.26 22.68 7.89 o -3 26 1 604.59 574.77 36.46 o -2 26 1 52.43 48.51 11.70 o -1 26 1 278.53 284.09 17.81 o 0 26 1 687.16 694.88 37.07 o 1 26 1 761.86 752.63 35.77 o 2 26 1 99.93 111.29 12.39 o 3 26 1 192.82 163.33 19.26 o -3 27 1 24.65 57.33 12.63 o -2 27 1 120.75 136.90 17.17 o -1 27 1 1222.61 1202.97 38.62 o 0 27 1 997.84 991.00 41.67 o 1 27 1 54.86 77.31 12.70 o 2 27 1 1321.45 1353.26 43.04 o 3 27 1 17.90 1.19 6.43 o -3 28 1 600.29 610.63 61.10 o -2 28 1 101.52 111.59 21.11 o -1 28 1 722.24 757.98 30.59 o 0 28 1 14.37 51.65 11.01 o 1 28 1 178.11 214.26 20.07 o 2 28 1 3.66 6.24 5.80 o 3 28 1 80.11 63.07 13.29 o -2 29 1 68.49 65.89 13.18 o -1 29 1 251.12 273.99 28.38 o 0 29 1 142.26 163.18 19.00 o 1 29 1 1260.25 1245.13 62.16 o 2 29 1 999.09 988.14 45.11 o -2 30 1 0.07 0.94 7.02 o -1 30 1 772.05 789.63 39.06 o 0 30 1 0.24 48.38 11.81 o 1 30 1 25.00 31.78 19.52 o 2 30 1 140.63 119.94 16.31 o -2 31 1 13.92 6.07 5.58 o -1 31 1 70.03 77.81 13.58 o 0 31 1 1312.52 1374.58 54.11 o 1 31 1 126.37 126.61 24.82 o 2 31 1 267.41 269.46 47.69 o -2 32 1 15.60 10.44 8.40 o -1 32 1 696.13 704.04 49.52 o 0 32 1 9.75 43.85 14.51 o 1 32 1 92.45 116.91 29.07 o 2 32 1 38.50 60.45 12.75 o -2 33 1 16.09 24.85 13.42 o -1 33 1 8.58 22.83 9.39 o 0 33 1 311.89 263.16 24.19 o 1 33 1 106.33 112.26 18.97 o 2 33 1 1388.28 1371.63 87.15 o -1 34 1 235.67 247.38 23.98 o 0 34 1 38.82 64.89 13.60 o 1 34 1 98.90 105.50 16.18 o -1 35 1 33.14 33.97 10.79 o 0 35 1 412.17 415.68 37.79 o 1 35 1 0.02 -4.92 8.37 o -1 36 1 557.61 555.41 39.57 o 0 36 1 189.77 214.49 23.01 o 1 36 1 95.19 98.04 16.31 o 0 37 1 480.57 474.98 34.52 o -4 0 2 247.22 219.91 29.43 o -2 0 2 1261.70 1124.48 76.32 o 0 0 2 1444.80 1237.65 22.94 o 2 0 2 24.10 15.88 6.13 o 4 0 2 810.42 892.20 65.32 o -4 1 2 33.01 11.54 7.88 o -3 1 2 1351.52 1426.94 54.98 o -2 1 2 129.90 117.62 5.14 o -1 1 2 11522.56 11395.77 105.34 o 0 1 2 0.13 2.21 1.19 o 1 1 2 3387.01 2835.40 111.48 o 2 1 2 171.43 172.33 8.04 o 3 1 2 44.37 48.54 5.75 o 4 1 2 5.06 12.61 8.43 o -4 2 2 549.96 561.02 34.64 o -3 2 2 394.96 389.21 25.76 o -2 2 2 5.03 5.98 1.41 o -1 2 2 2.24 5.86 1.44 o 0 2 2 633.69 649.70 17.64 o 1 2 2 955.30 836.11 24.78 o 2 2 2 1241.14 1213.89 24.53 o 3 2 2 1.51 -3.02 3.02 o 4 2 2 479.37 555.95 36.04 o -4 3 2 27.80 -17.19 29.20 o -3 3 2 1058.00 1061.71 41.02 o -2 3 2 110.81 114.07 7.73 o -1 3 2 6408.70 6478.36 69.18 o 0 3 2 0.14 2.60 1.37 o 1 3 2 3805.73 3370.08 99.33 o 2 3 2 237.45 217.16 9.22 o 3 3 2 33.10 32.14 5.31 o 4 3 2 11.49 31.31 9.58 o -4 4 2 283.25 268.74 24.24 o -3 4 2 266.91 275.39 14.49 o -2 4 2 177.13 158.15 13.91 o -1 4 2 232.20 227.61 6.53 o 0 4 2 641.48 603.29 13.07 o 1 4 2 98.78 100.07 7.43 o 2 4 2 501.66 457.19 14.90 o 3 4 2 590.08 590.51 22.74 o 4 4 2 430.89 439.66 32.39 o -4 5 2 168.77 163.83 22.71 o -3 5 2 757.12 752.17 25.45 o -2 5 2 821.71 807.15 23.28 o -1 5 2 1543.76 1457.59 49.67 o 0 5 2 825.14 864.48 13.57 o 1 5 2 3039.50 2771.82 55.92 o 2 5 2 397.80 370.97 13.11 o 3 5 2 175.56 197.37 11.34 o 4 5 2 111.37 117.34 17.55 o -4 6 2 249.89 284.33 24.88 o -3 6 2 457.65 452.72 19.67 o -2 6 2 192.22 172.63 10.40 o -1 6 2 13.84 20.52 2.63 o 0 6 2 4.92 9.24 1.70 o 1 6 2 3626.50 3539.82 47.56 o 2 6 2 701.06 720.32 21.84 o 3 6 2 207.26 206.22 11.64 o 4 6 2 639.93 684.62 40.30 o -4 7 2 490.50 465.40 48.87 o -3 7 2 247.53 231.85 22.06 o -2 7 2 635.46 654.37 29.73 o -1 7 2 4129.64 4109.42 71.58 o 0 7 2 86.70 82.75 3.92 o 1 7 2 1417.47 1329.22 26.69 o 2 7 2 487.58 488.24 21.13 o 3 7 2 1217.88 1208.58 35.70 o 4 7 2 64.74 58.45 12.86 o -4 8 2 53.02 35.43 14.07 o -3 8 2 71.48 64.75 10.00 o -2 8 2 782.61 755.10 28.10 o -1 8 2 9.72 8.89 2.30 o 0 8 2 3499.88 3488.57 42.76 o 1 8 2 399.48 376.91 10.00 o 2 8 2 4649.26 4757.46 79.05 o 3 8 2 762.60 795.81 26.49 o 4 8 2 488.35 488.90 35.49 o -4 9 2 520.10 548.87 35.26 o -3 9 2 437.46 444.36 20.62 o -2 9 2 653.00 678.33 27.12 o -1 9 2 768.01 806.24 24.84 o 0 9 2 287.18 292.84 9.11 o 1 9 2 5701.66 5629.62 104.54 o 2 9 2 1972.66 1935.14 41.72 o 3 9 2 1594.29 1584.31 42.80 o 4 9 2 0.09 24.90 9.22 o -4 10 2 98.08 118.93 17.74 o -3 10 2 571.54 630.90 32.44 o -2 10 2 2966.34 3273.20 119.87 o -1 10 2 75.73 56.37 4.88 o 0 10 2 6976.18 7061.00 78.14 o 1 10 2 42.34 28.62 3.83 o 2 10 2 728.09 740.96 23.22 o 3 10 2 529.20 564.16 20.11 o 4 10 2 318.46 294.30 27.09 o -4 11 2 121.79 105.41 16.29 o -3 11 2 364.18 413.53 20.61 o -2 11 2 199.10 219.80 16.02 o -1 11 2 2989.48 3202.55 53.92 o 0 11 2 2048.73 2182.76 30.33 o 1 11 2 1150.12 1147.27 23.28 o 2 11 2 426.98 412.69 16.99 o 3 11 2 431.94 464.92 18.54 o 4 11 2 18.35 24.21 8.09 o -4 12 2 209.36 209.25 22.49 o -3 12 2 481.94 500.23 23.05 o -2 12 2 2300.78 2395.74 62.33 o -1 12 2 54.78 56.49 5.57 o 0 12 2 8754.72 8847.09 87.69 o 1 12 2 1484.64 1503.28 28.18 o 2 12 2 1170.45 1106.12 30.15 o 3 12 2 37.48 48.32 7.09 o 4 12 2 18.40 23.37 7.38 o -4 13 2 18.73 38.91 30.62 o -3 13 2 159.28 151.67 18.20 o -2 13 2 14.80 21.35 3.75 o -1 13 2 65.54 52.03 5.29 o 0 13 2 563.65 603.01 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