data_2240640 _cell_angle_alpha 90.000 _cell_angle_beta 90.939 _cell_angle_gamma 90.000 _cell_length_a 14.8595 _cell_length_b 8.3873 _cell_length_c 22.0138 _exptl_crystal_F_000 1152.00 _reflns_d_resolution_high 0.8101 _cod_data_source_file sj5456RNSBsup3.hkl _cod_data_source_block RNSB _shelx_title ' RNSBra in P21 # 4 RELABEL ISOR's C13,C33 oztf set' _shelx_refln_list_code 4 _shelx_f_calc_maximum 175.15 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 -10 0 182.70 456.60 58.35 o 1 -10 0 98.58 407.63 54.63 o 2 -10 0 19.29 108.31 37.87 o 3 -10 0 156.24 281.42 24.81 o 1 -9 0 577.56 644.28 37.20 o 2 -9 0 120.52 170.20 28.66 o 3 -9 0 88.84 38.97 22.51 o 4 -9 0 85.90 68.23 39.40 o 5 -9 0 155.26 190.19 176.75 o 6 -9 0 3.54 11.17 22.26 o 7 -9 0 29.65 150.22 39.63 o 8 -9 0 79.13 153.25 33.93 o 9 -9 0 0.29 121.99 26.61 o 0 -8 0 1219.99 1534.55 117.42 o 1 -8 0 154.59 254.99 37.81 o 2 -8 0 289.14 404.51 55.60 o 3 -8 0 815.33 1015.22 50.41 o 4 -8 0 22.30 41.91 23.77 o 5 -8 0 444.20 392.00 46.74 o 6 -8 0 191.24 239.62 63.40 o 7 -8 0 136.37 120.19 57.08 o 8 -8 0 15.73 48.09 72.62 o 9 -8 0 9.47 18.40 24.88 o 10 -8 0 20.69 79.37 23.48 o 11 -8 0 7.39 59.72 56.17 o 1 -7 0 430.29 477.67 31.77 o 2 -7 0 289.95 320.52 37.00 o 3 -7 0 470.56 590.70 40.58 o 4 -7 0 733.02 739.30 45.61 o 5 -7 0 173.09 231.71 32.20 o 6 -7 0 304.23 237.80 54.45 o 7 -7 0 529.47 587.58 110.64 o 8 -7 0 442.03 587.42 119.46 o 9 -7 0 193.52 311.25 53.00 o 10 -7 0 2.57 4.98 23.77 o 11 -7 0 68.41 111.00 31.59 o 12 -7 0 10.28 16.12 34.84 o 13 -7 0 40.43 12.89 43.67 o 0 -6 0 691.63 1014.93 205.37 o 1 -6 0 300.36 392.08 35.61 o 2 -6 0 248.27 334.75 29.91 o 3 -6 0 41.16 77.82 22.73 o 4 -6 0 622.75 530.67 66.86 o 5 -6 0 1410.45 1346.44 72.07 o 6 -6 0 3.79 13.46 21.05 o 7 -6 0 141.53 175.27 61.37 o 8 -6 0 38.28 86.45 39.05 o 9 -6 0 327.35 285.63 57.67 o 10 -6 0 7.06 308.00 56.52 o 11 -6 0 99.60 410.49 65.31 o 12 -6 0 220.32 246.04 26.43 o 13 -6 0 130.02 239.40 38.00 o 14 -6 0 25.91 77.15 17.67 o 1 -5 0 836.87 1059.51 63.24 o 2 -5 0 3678.81 4079.91 193.47 o 3 -5 0 335.16 417.48 47.66 o 4 -5 0 847.60 862.22 70.34 o 5 -5 0 108.35 125.64 47.32 o 6 -5 0 99.01 119.40 35.93 o 7 -5 0 133.36 190.55 26.89 o 8 -5 0 2165.86 2025.38 80.78 o 9 -5 0 480.33 532.18 38.63 o 10 -5 0 144.61 349.82 42.40 o 11 -5 0 56.67 228.33 37.51 o 12 -5 0 141.69 179.56 37.54 o 13 -5 0 27.37 55.49 28.62 o 14 -5 0 27.96 73.46 20.15 o 15 -5 0 19.41 122.38 17.59 o 16 -5 0 47.40 75.19 15.64 o 0 -4 0 3783.85 4461.72 113.53 o 1 -4 0 1134.91 1118.06 41.42 o 2 -4 0 1034.47 1030.98 42.29 o 3 -4 0 46.92 53.76 16.29 o 4 -4 0 363.27 354.71 33.65 o 5 -4 0 1670.21 1584.36 70.72 o 6 -4 0 61.72 23.08 40.36 o 7 -4 0 67.63 114.37 69.28 o 8 -4 0 337.85 423.53 76.26 o 9 -4 0 94.14 670.60 104.70 o 10 -4 0 10.64 79.02 25.43 o 11 -4 0 212.20 349.32 50.03 o 12 -4 0 652.37 818.01 86.06 o 13 -4 0 58.19 220.12 52.91 o 14 -4 0 2.73 7.22 22.75 o 15 -4 0 4.17 36.65 16.08 o 16 -4 0 5.59 45.71 14.58 o 1 -3 0 2566.40 2727.78 80.59 o 2 -3 0 2835.20 2953.33 47.87 o 3 -3 0 2650.99 2531.10 106.40 o 4 -3 0 816.72 727.88 41.07 o 5 -3 0 146.07 123.74 21.82 o 6 -3 0 1384.22 1421.53 75.11 o 7 -3 0 349.48 366.88 63.88 o 8 -3 0 2839.41 3064.27 160.46 o 9 -3 0 130.33 189.33 52.29 o 10 -3 0 272.13 309.43 36.02 o 11 -3 0 1.05 71.75 25.52 o 12 -3 0 140.95 495.46 75.27 o 13 -3 0 221.07 244.15 56.36 o 14 -3 0 183.36 128.19 46.06 o 15 -3 0 64.79 150.50 34.05 o 16 -3 0 66.09 75.46 20.16 o 17 -3 0 17.28 35.28 16.48 o 0 -2 0 17763.27 19364.39 110.79 o 1 -2 0 27.86 62.50 9.41 o 2 -2 0 6330.45 6158.73 62.95 o 3 -2 0 1626.96 1396.01 49.46 o 4 -2 0 2804.60 2535.35 65.25 o 5 -2 0 146.97 130.06 15.30 o 6 -2 0 1738.84 1584.70 76.35 o 7 -2 0 1649.71 1875.48 123.30 o 8 -2 0 1181.62 1264.39 103.77 o 9 -2 0 752.88 864.37 92.18 o 10 -2 0 24.61 151.11 51.23 o 11 -2 0 400.89 534.99 57.16 o 12 -2 0 9.77 419.43 67.73 o 13 -2 0 36.38 404.92 72.24 o 14 -2 0 37.95 108.56 45.90 o 15 -2 0 32.19 64.58 38.24 o 16 -2 0 185.70 212.56 30.49 o 17 -2 0 26.74 44.45 27.82 o 1 -1 0 1045.15 1129.72 17.65 o 2 -1 0 8013.47 7431.51 155.52 o 3 -1 0 14706.81 13687.20 350.00 o 4 -1 0 6117.47 5588.21 87.38 o 5 -1 0 1064.90 998.35 43.34 o 6 -1 0 1319.40 1147.83 76.59 o 7 -1 0 606.11 662.27 132.80 o 8 -1 0 645.97 844.11 138.33 o 9 -1 0 155.83 346.26 65.64 o 10 -1 0 109.07 107.16 41.35 o 11 -1 0 36.68 85.53 28.00 o 12 -1 0 196.11 231.60 40.73 o 13 -1 0 46.35 179.52 54.89 o 14 -1 0 211.29 325.51 59.25 o 15 -1 0 21.93 415.34 64.84 o 16 -1 0 29.49 99.91 36.78 o 17 -1 0 38.24 48.30 20.88 o 18 -1 0 37.93 65.25 20.63 o 2 0 0 16764.08 13968.97 130.39 o 3 0 0 4391.79 4054.46 88.25 o 4 0 0 22476.76 18707.03 225.11 o 5 0 0 261.97 264.92 31.02 o 6 0 0 651.25 711.33 116.43 o 7 0 0 1743.45 1966.77 142.26 o 8 0 0 659.73 799.55 213.87 o 9 0 0 209.10 415.71 172.56 o 10 0 0 6.64 184.87 44.48 o 11 0 0 0.00 210.24 51.92 o 12 0 0 15.18 35.61 26.56 o 13 0 0 133.50 152.16 33.88 o 14 0 0 0.70 67.52 36.07 o 15 0 0 12.42 212.39 45.98 o 16 0 0 158.47 205.74 40.06 o 18 0 0 22.22 24.14 18.86 o 4 1 0 6102.56 4780.50 105.48 o 5 1 0 1068.49 749.93 130.75 o 6 1 0 1312.27 1132.33 86.62 o 7 1 0 607.48 663.77 80.01 o 8 1 0 645.10 774.56 155.33 o 9 1 0 154.04 380.80 80.40 o 10 1 0 108.31 110.18 31.84 o 11 1 0 36.30 89.94 33.68 o 12 1 0 195.99 137.69 43.70 o 13 1 0 45.89 229.84 90.09 o 18 1 0 36.97 78.46 25.75 o 4 2 0 2808.34 2317.96 65.40 o 5 2 0 144.94 129.78 23.06 o 6 2 0 1742.21 1638.42 76.09 o 7 2 0 1655.01 1994.06 91.57 o 8 2 0 1186.28 1292.56 114.37 o 9 2 0 752.42 848.83 66.95 o 10 2 0 23.79 169.85 98.54 o 11 2 0 396.01 526.74 148.28 o 12 2 0 9.73 460.04 149.18 o 7 3 0 353.19 465.91 151.89 o 8 3 0 2843.06 3420.75 348.26 o 9 3 0 131.37 253.74 116.33 o 10 3 0 274.31 351.27 137.50 o 11 3 0 0.91 88.41 84.23 o 17 3 0 16.94 47.70 23.55 o 6 4 0 61.83 210.72 113.71 o 7 4 0 66.15 1052.99 221.85 o 8 4 0 334.65 485.48 146.85 o 9 4 0 93.95 1016.50 231.24 o 10 4 0 10.68 130.55 99.67 o 16 4 0 5.12 27.32 23.00 o 1 5 0 842.06 1056.18 134.24 o 2 5 0 3695.57 4469.50 326.01 o 3 5 0 335.70 427.19 119.59 o 4 5 0 851.53 1039.45 188.89 o 5 5 0 106.90 301.18 169.85 o 6 5 0 100.01 287.93 133.40 o 7 5 0 131.42 229.44 115.32 o 8 5 0 2155.66 3058.89 367.66 o 9 5 0 483.94 767.61 196.36 o 4 6 0 622.81 839.86 197.44 o 5 6 0 1408.45 2026.08 286.02 o 6 6 0 3.61 18.11 74.60 o 7 6 0 139.89 305.41 155.20 o 0 -10 1 376.65 438.38 58.58 o 1 -10 1 17.49 130.49 27.38 o 2 -10 1 98.62 210.93 33.92 o 3 -10 1 115.46 260.58 109.86 o 4 -10 1 63.87 89.32 50.40 o -9 -9 1 51.71 97.92 25.22 o -8 -9 1 4.49 84.68 27.76 o -7 -9 1 66.64 219.07 43.86 o -6 -9 1 27.87 242.41 49.96 o -5 -9 1 17.71 213.66 51.89 o -4 -9 1 363.52 397.51 36.04 o -3 -9 1 79.37 80.37 19.67 o -2 -9 1 28.85 46.34 17.16 o -1 -9 1 156.19 161.06 20.97 o 0 -9 1 5.46 6.35 12.76 o 1 -9 1 93.57 110.37 31.88 o 2 -9 1 397.96 444.96 39.32 o 3 -9 1 79.43 160.69 38.63 o 4 -9 1 109.65 95.18 74.50 o 5 -9 1 35.71 126.67 89.37 o 6 -9 1 134.15 75.67 30.75 o 7 -9 1 90.92 234.91 45.26 o 8 -9 1 116.25 248.03 41.56 o 9 -9 1 30.53 152.64 27.82 o -11 -8 1 110.29 132.38 40.71 o -10 -8 1 61.26 79.95 22.58 o -9 -8 1 78.95 64.75 49.62 o -8 -8 1 242.50 228.73 36.62 o -7 -8 1 67.01 62.89 50.29 o -6 -8 1 497.62 582.48 50.17 o -5 -8 1 94.54 117.21 31.67 o -4 -8 1 269.11 319.56 38.66 o -3 -8 1 235.10 282.42 33.43 o -2 -8 1 254.31 375.30 65.59 o -1 -8 1 488.97 661.19 42.25 o 0 -8 1 294.91 312.06 54.67 o 1 -8 1 707.32 850.83 50.44 o 2 -8 1 151.32 195.63 41.55 o 3 -8 1 64.27 139.38 35.35 o 4 -8 1 2.97 27.48 22.62 o 5 -8 1 60.79 116.85 54.49 o 6 -8 1 179.00 183.57 42.72 o 7 -8 1 52.30 88.31 32.29 o 8 -8 1 33.08 36.73 62.74 o 9 -8 1 13.15 5.91 30.63 o 10 -8 1 121.99 119.63 25.44 o 11 -8 1 6.72 28.69 30.54 o -13 -7 1 18.14 56.16 30.87 o -12 -7 1 84.02 25.01 53.46 o -11 -7 1 150.86 145.81 35.59 o -10 -7 1 37.92 27.67 25.73 o -9 -7 1 142.38 195.48 44.43 o -8 -7 1 487.95 550.09 74.31 o -7 -7 1 283.72 390.89 45.93 o -6 -7 1 100.09 92.55 25.75 o -5 -7 1 452.10 460.21 33.32 o -4 -7 1 131.80 129.32 21.35 o -3 -7 1 1685.25 1738.66 68.98 o -2 -7 1 46.19 59.71 21.53 o -1 -7 1 478.83 518.47 33.33 o 0 -7 1 68.29 151.06 21.53 o 1 -7 1 136.77 242.62 33.79 o 2 -7 1 473.51 648.61 37.51 o 3 -7 1 475.65 583.54 58.53 o 4 -7 1 623.88 759.82 60.18 o 5 -7 1 959.88 939.77 70.19 o 6 -7 1 356.54 238.17 30.49 o 7 -7 1 61.33 157.22 36.37 o 8 -7 1 1.82 145.74 92.52 o 9 -7 1 439.20 501.64 59.59 o 10 -7 1 49.54 25.58 24.99 o 11 -7 1 32.52 4.30 22.69 o 12 -7 1 1.50 -21.90 55.29 o 13 -7 1 39.02 24.98 46.27 o -14 -6 1 80.24 88.74 16.90 o -13 -6 1 13.32 105.21 18.89 o -12 -6 1 74.23 164.22 26.30 o -11 -6 1 424.20 604.58 45.06 o -10 -6 1 237.20 219.52 47.49 o -9 -6 1 6.42 97.86 41.63 o -8 -6 1 39.57 93.22 40.90 o -7 -6 1 241.57 182.77 47.98 o -6 -6 1 23.91 36.92 26.03 o -5 -6 1 281.57 332.70 55.30 o -4 -6 1 736.87 673.37 66.20 o -3 -6 1 1197.96 1214.27 49.48 o -2 -6 1 234.11 273.85 38.42 o -1 -6 1 207.07 349.10 52.35 o 0 -6 1 90.27 74.02 28.75 o 1 -6 1 133.40 241.86 25.59 o 2 -6 1 396.64 631.47 39.32 o 3 -6 1 373.58 446.30 35.28 o 4 -6 1 87.85 147.85 24.62 o 5 -6 1 264.48 251.20 51.10 o 6 -6 1 71.05 41.86 20.36 o 7 -6 1 713.45 581.93 91.22 o 8 -6 1 111.59 97.33 40.33 o 9 -6 1 24.43 132.24 33.20 o 10 -6 1 633.15 578.35 59.24 o 11 -6 1 235.57 354.47 37.16 o 12 -6 1 3.16 166.73 33.88 o 13 -6 1 207.58 278.07 29.70 o 14 -6 1 12.17 47.94 15.14 o -16 -5 1 1.73 72.36 22.80 o -15 -5 1 107.68 129.00 22.08 o -14 -5 1 56.81 77.56 18.53 o -13 -5 1 12.99 26.71 25.97 o -12 -5 1 59.96 208.24 40.98 o -11 -5 1 367.13 455.68 54.37 o -10 -5 1 289.36 369.23 43.79 o -9 -5 1 197.13 330.02 34.54 o -8 -5 1 310.85 686.04 55.50 o -7 -5 1 289.55 277.47 31.87 o -6 -5 1 192.49 190.37 32.63 o -5 -5 1 1806.16 1857.54 148.89 o -4 -5 1 102.82 103.30 40.66 o -3 -5 1 8.43 15.13 27.80 o -2 -5 1 229.33 216.69 53.06 o -1 -5 1 1530.50 1746.16 137.75 o 0 -5 1 919.27 921.65 82.39 o 1 -5 1 1500.48 1633.43 81.06 o 2 -5 1 1011.03 1040.01 69.21 o 3 -5 1 1058.59 1063.26 76.02 o 4 -5 1 44.86 30.22 26.47 o 5 -5 1 236.94 227.04 46.45 o 6 -5 1 734.80 780.57 75.72 o 7 -5 1 29.88 76.99 23.09 o 8 -5 1 396.73 867.49 118.90 o 9 -5 1 163.98 313.57 32.91 o 10 -5 1 487.57 435.44 44.75 o 11 -5 1 163.55 142.15 41.14 o 12 -5 1 130.24 207.03 43.20 o 13 -5 1 114.30 350.56 50.55 o 14 -5 1 23.52 31.13 17.00 o 15 -5 1 87.54 75.22 17.64 o 16 -5 1 28.36 82.78 22.56 o -16 -4 1 12.42 25.67 15.02 o -15 -4 1 14.98 16.08 24.25 o -14 -4 1 18.21 46.84 37.18 o -13 -4 1 135.61 102.28 41.64 o -12 -4 1 68.76 350.50 64.40 o -11 -4 1 281.11 493.79 64.16 o -10 -4 1 57.81 334.35 54.87 o -9 -4 1 1375.84 1464.88 81.74 o -8 -4 1 237.33 259.97 52.65 o -7 -4 1 99.98 103.21 36.31 o -6 -4 1 621.15 603.64 64.31 o -5 -4 1 113.28 134.67 30.96 o -4 -4 1 485.67 473.61 37.45 o -3 -4 1 751.66 749.63 44.20 o -2 -4 1 5294.51 5457.29 259.82 o -1 -4 1 2437.10 2617.08 96.60 o 0 -4 1 491.59 487.08 29.09 o 1 -4 1 407.40 418.23 25.93 o 2 -4 1 1077.91 1029.15 53.14 o 3 -4 1 171.38 170.90 21.71 o 4 -4 1 664.16 675.63 43.60 o 5 -4 1 165.92 262.55 37.62 o 6 -4 1 663.06 687.81 58.07 o 7 -4 1 4005.97 3948.51 176.13 o 8 -4 1 412.95 488.26 54.81 o 9 -4 1 1035.55 1005.53 56.20 o 10 -4 1 63.43 193.01 36.64 o 11 -4 1 127.10 174.01 47.91 o 12 -4 1 365.61 578.32 165.09 o 13 -4 1 288.59 303.78 57.21 o 14 -4 1 72.50 56.69 23.67 o 15 -4 1 34.19 35.67 15.76 o 16 -4 1 4.66 65.95 16.52 o -17 -3 1 26.29 29.31 13.48 o -16 -3 1 15.32 15.20 26.28 o -15 -3 1 58.20 104.11 40.69 o -14 -3 1 69.68 93.20 41.43 o -13 -3 1 25.89 143.65 49.23 o -12 -3 1 453.20 704.05 103.94 o -11 -3 1 148.88 252.81 36.34 o -10 -3 1 161.24 410.43 52.21 o -9 -3 1 116.60 326.88 69.43 o -8 -3 1 627.67 827.15 97.55 o -7 -3 1 621.10 646.79 74.42 o -6 -3 1 84.61 94.86 32.28 o -5 -3 1 126.65 92.15 23.32 o -4 -3 1 540.54 477.37 34.13 o -3 -3 1 5255.52 5557.02 148.36 o -2 -3 1 2083.19 1899.19 54.55 o -1 -3 1 2367.94 2483.30 87.76 o 0 -3 1 3161.07 3092.06 91.24 o 1 -3 1 1932.70 2051.88 37.58 o 2 -3 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13999.48 286.44 o 1 -2 1 7247.11 7325.41 75.60 o 2 -2 1 10272.96 10405.34 201.74 o 3 -2 1 1172.36 1193.60 42.72 o 4 -2 1 606.16 650.33 35.06 o 5 -2 1 4409.48 3978.50 96.44 o 6 -2 1 1637.52 1494.96 77.77 o 7 -2 1 2170.44 2603.86 141.46 o 8 -2 1 1017.92 1198.52 108.84 o 9 -2 1 755.26 897.55 100.62 o 10 -2 1 103.83 122.60 29.98 o 11 -2 1 286.36 431.56 61.29 o 12 -2 1 390.30 480.60 52.77 o 13 -2 1 268.79 233.29 53.52 o 14 -2 1 77.81 276.37 66.52 o 15 -2 1 8.88 43.38 35.51 o 16 -2 1 111.17 202.35 27.58 o 17 -2 1 140.18 105.98 40.45 o -18 -1 1 22.17 65.36 20.05 o -17 -1 1 4.39 28.49 17.95 o -16 -1 1 85.84 81.91 43.89 o -15 -1 1 61.41 192.92 56.79 o -14 -1 1 142.84 256.70 56.86 o -13 -1 1 311.51 418.25 78.28 o -12 -1 1 15.64 167.35 37.50 o -11 -1 1 106.10 132.13 35.15 o -10 -1 1 32.80 173.88 55.47 o -9 -1 1 551.76 652.95 78.57 o -8 -1 1 91.88 187.40 44.92 o -7 -1 1 1119.92 1273.69 71.17 o -6 -1 1 600.61 498.74 43.78 o -5 -1 1 2000.83 1889.77 71.49 o -4 -1 1 81.18 65.61 14.83 o -3 -1 1 6085.66 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