#------------------------------------------------------------------------------ #$Date: 2018-03-10 10:13:29 +0200 (Sat, 10 Mar 2018) $ #$Revision: 206893 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/24/24/2242426.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2242426 loop_ _publ_author_name 'Gelbrich, Thomas' 'Langes, Christoph' 'Stefinovic, Marijan' 'Griesser, Ulrich J.' _publ_section_title ; Naloxegol hydrogen oxalate displaying an hydrogen-bonded layer structure ; _journal_coeditor_code FY2125 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first 474 _journal_page_last 477 _journal_paper_doi 10.1107/S2056989018003675 _journal_volume 74 _journal_year 2018 _chemical_formula_iupac 'C34 H54 N O11 +, C2 H O4 -' _chemical_formula_moiety 'C34 H54 N O11 +, C2 H O4 -' _chemical_formula_sum 'C36 H55 N O15' _chemical_formula_weight 741.81 _chemical_name_common 'Naloxegol hydrogen oxalate' _chemical_name_systematic ; (5\a,6\a)-6-[(2,5,8,11,14,17,20-Heptaoxadocosan-22-yl)oxy]-3,14-dihydroxy-17-\ (prop-2-en-1-yl)-4,5-epoxymorphinan-17-ium hydrogen oxalate ; _space_group_crystal_system orthorhombic _space_group_IT_number 19 _space_group_name_Hall 'P 2ac 2ab' _space_group_name_H-M_alt 'P 21 21 21' _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2014/6 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 10.35810(10) _cell_length_b 13.40390(10) _cell_length_c 26.1689(2) _cell_measurement_reflns_used 31215 _cell_measurement_temperature 173(2) _cell_measurement_theta_max 67.5060 _cell_measurement_theta_min 3.3600 _cell_volume 3633.26(5) _computing_cell_refinement ; CrysAlis PRO (Rigaku OD, 2015) ; _computing_data_collection ; CrysAlis PRO (Rigaku OD, 2015) ; _computing_data_reduction ; CrysAlis PRO (Rigaku OD, 2015) ; _computing_molecular_graphics ; XP in SHELXTL (Sheldrick, 2008), Mercury (Macrae et al., 2006) and TOPOS (Blatov, 2006) ; _computing_publication_material ; PLATON (Spek, 2009), publCIF (Westrip, 2010) and TOPOS (Blatov, 2006) ; _computing_structure_refinement ; SHELXL2014 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT (Sheldrick, 2015a) ; _diffrn_ambient_temperature 173(2) _diffrn_detector_area_resol_mean 10.3575 _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'Riguaku Oxford Diffraction Xcalibur Ruby Gemini Ultra' _diffrn_measurement_method '\w scans' _diffrn_radiation_monochromator mirror _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0563 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 31 _diffrn_reflns_limit_l_min -31 _diffrn_reflns_number 58082 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 67.541 _diffrn_reflns_theta_min 3.378 _exptl_absorpt_coefficient_mu 0.881 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.80917 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (CrysAlis PRO; Rigaku OD, 2015) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.356 _exptl_crystal_description plate _exptl_crystal_F_000 1592 _exptl_crystal_size_max 0.250 _exptl_crystal_size_mid 0.150 _exptl_crystal_size_min 0.050 _refine_diff_density_max 0.731 _refine_diff_density_min -0.428 _refine_ls_abs_structure_details ; Flack x determined using 2777 quotients [(I^+^)-(I^-^)]/[(I^+^)+(I^-^)] (Parsons et al., 2013) ; _refine_ls_abs_structure_Flack 0.00(4) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.034 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 488 _refine_ls_number_reflns 6563 _refine_ls_number_restraints 4 _refine_ls_restrained_S_all 1.034 _refine_ls_R_factor_all 0.0484 _refine_ls_R_factor_gt 0.0476 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0807P)^2^+1.8400P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1251 _refine_ls_wR_factor_ref 0.1262 _reflns_number_gt 6429 _reflns_number_total 6563 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file fy2125sup1.cif _cod_data_source_block I _cod_database_code 2242426 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.810 _shelx_estimated_absorpt_t_max 0.957 _shelx_hkl_file ; 0 0 2 2403.62 58.18 0 0 3 -0.01 0.15 0 0 4 1948.91 48.95 0 0 5 0.95 0.49 0 0 6 9999.00 240.34 0 0 7 0.33 0.93 0 0 8 368.27 13.75 0 0 9 1.17 0.94 0 0 10 182.94 9.56 0 0 11 0.47 0.93 0 0 12 114.75 8.11 0 0 13 -0.12 1.31 0 0 14 1274.26 41.47 0 0 15 -0.19 0.90 0 0 -15 0.22 0.39 0 0 15 0.42 0.31 0 0 15 0.36 0.34 0 0 15 0.46 0.43 0 0 16 138.96 6.22 0 0 -16 144.18 6.18 0 0 16 137.74 6.12 0 0 16 138.21 6.13 0 0 -17 0.13 0.29 0 0 17 -0.05 0.43 0 0 17 0.19 0.47 0 0 17 0.32 0.27 0 0 -17 0.10 0.18 0 0 17 0.77 1.07 0 0 17 -0.61 0.41 0 0 17 0.13 0.37 0 0 18 53.70 3.69 0 0 18 52.59 3.60 0 0 18 54.29 7.20 0 0 -18 51.32 3.57 0 0 -18 50.27 3.51 0 0 -18 39.27 3.09 0 0 18 49.17 3.49 0 0 18 43.61 3.30 0 0 19 0.78 0.73 0 0 19 0.27 0.37 0 0 19 1.23 0.78 0 0 -19 0.85 0.59 0 0 19 2.10 0.88 0 0 -19 0.94 0.45 0 0 19 -0.88 0.98 0 0 -20 388.31 13.04 0 0 20 398.82 13.10 0 0 20 396.70 13.12 0 0 20 309.90 12.38 0 0 -20 337.77 12.67 0 0 20 411.09 13.38 0 0 20 373.83 22.31 0 0 -21 1.35 0.69 0 0 21 1.57 0.92 0 0 -21 1.66 0.82 0 0 21 1.67 1.53 0 0 21 1.38 0.78 0 0 21 2.27 0.95 0 0 -21 0.92 1.21 0 0 22 226.36 9.27 0 0 -22 179.37 16.39 0 0 -22 210.27 9.15 0 0 22 163.04 15.19 0 0 22 229.72 9.51 0 0 22 229.18 9.33 0 0 23 0.22 0.63 0 0 23 0.60 0.62 0 0 -23 0.65 0.60 0 0 -24 37.07 3.32 0 0 24 36.55 3.31 0 0 24 33.59 3.24 0 0 24 44.59 3.70 0 0 -25 0.30 0.46 0 0 25 0.42 0.34 0 0 25 -0.87 0.82 0 0 26 21.52 2.42 0 0 26 26.35 2.79 0 0 -26 26.53 2.87 0 0 -26 20.33 2.35 0 0 -27 -0.04 0.59 0 0 27 -0.13 0.58 0 0 27 -0.50 0.52 0 0 -28 25.54 2.65 0 0 28 22.92 2.45 0 0 29 0.60 0.59 0 0 -29 -0.31 0.56 0 0 -30 3.14 0.86 0 0 -31 0.03 0.25 0 -1 0 0.05 0.10 0 1 0 0.22 0.18 0 1 -1 301.50 8.14 0 1 -1 284.30 8.28 0 -1 1 288.18 8.36 0 1 1 292.60 8.33 0 1 2 124.16 4.27 0 1 -2 125.68 4.26 0 1 2 125.22 3.88 0 -1 2 123.19 4.58 0 1 3 122.30 4.84 0 -1 3 122.30 4.86 0 1 -3 118.94 3.76 0 1 3 117.27 4.13 0 1 -3 121.52 4.13 0 1 4 215.10 7.55 0 1 4 198.36 6.20 0 1 -4 202.46 6.20 0 -1 4 211.28 7.52 0 1 5 276.52 9.74 0 -1 5 268.51 9.63 0 1 6 498.58 15.59 0 -1 6 465.59 15.31 0 -1 7 5249.83 131.56 0 1 7 5453.77 131.90 0 1 8 392.51 14.34 0 -1 8 372.91 14.11 0 1 9 503.65 17.97 0 -1 9 496.83 17.77 0 -1 10 4.10 1.43 0 1 10 6.44 1.94 0 1 11 77.76 6.28 0 -1 11 77.97 6.20 0 -1 12 200.41 10.98 0 1 12 200.21 10.90 0 1 13 2641.93 73.29 0 -1 13 2610.61 73.12 0 1 14 7.90 2.30 0 -1 14 6.13 2.05 0 1 -15 46.08 3.09 0 1 15 47.65 3.17 0 -1 15 49.55 3.23 0 -1 15 49.10 3.18 0 -1 15 46.76 3.12 0 -1 15 58.87 6.63 0 1 15 46.28 3.09 0 1 15 45.06 3.13 0 -1 -16 0.41 0.40 0 1 16 0.01 0.28 0 1 16 0.50 0.49 0 -1 16 0.36 0.33 0 1 16 0.07 0.21 0 -1 16 -0.36 0.46 0 -1 16 -0.35 1.16 0 -1 16 0.03 0.37 0 1 16 -0.14 1.38 0 1 -16 0.54 0.50 0 1 -16 1.08 0.55 0 1 16 -0.22 0.32 0 -1 -16 0.28 0.33 0 1 17 312.17 17.49 0 1 17 223.57 8.70 0 -1 -17 220.79 8.84 0 -1 -17 233.62 8.88 0 1 17 242.59 9.02 0 1 -17 240.43 9.10 0 1 17 189.13 8.48 0 1 17 252.86 9.25 0 -1 17 249.47 9.18 0 -1 17 306.09 17.39 0 -1 17 257.50 9.31 0 -1 17 253.64 9.22 0 1 -17 248.41 9.12 0 1 17 248.76 9.25 0 1 18 9.36 1.50 0 1 18 8.71 1.45 0 -1 -18 9.89 1.53 0 -1 18 11.64 3.18 0 1 18 11.40 3.35 0 1 -18 10.94 1.63 0 1 -18 10.46 1.54 0 1 18 7.29 1.32 0 1 18 10.84 1.67 0 -1 18 9.05 1.48 0 -1 -18 11.87 1.63 0 -1 18 8.22 1.42 0 -1 18 8.86 1.48 0 -1 18 10.04 1.56 0 1 18 7.56 1.30 0 -1 19 225.46 8.84 0 1 19 220.47 8.69 0 1 19 226.15 8.88 0 1 19 230.96 16.39 0 -1 19 232.52 16.53 0 -1 19 181.60 8.25 0 1 19 198.81 8.25 0 -1 19 220.17 8.70 0 -1 -19 210.90 8.55 0 -1 -19 205.19 8.55 0 1 19 219.22 8.60 0 1 -19 211.68 8.70 0 1 -19 216.08 8.62 0 1 19 179.61 8.18 0 -1 19 224.33 8.73 0 -1 -19 197.24 8.32 0 -1 -20 201.90 8.67 0 -1 20 229.98 9.08 0 1 -20 219.04 8.85 0 -1 -20 200.18 8.56 0 1 20 220.45 8.96 0 -1 20 216.57 8.83 0 1 20 219.05 8.90 0 1 -20 215.70 8.92 0 -1 -20 203.63 8.61 0 1 20 220.20 8.75 0 -1 -20 205.37 8.71 0 -1 20 210.37 16.37 0 -1 20 178.09 8.28 0 -1 20 221.14 8.88 0 1 -20 194.06 15.99 0 1 -21 166.87 7.52 0 1 21 162.32 7.33 0 -1 -21 129.72 6.83 0 1 21 167.52 7.64 0 -1 21 156.57 7.42 0 1 -21 158.34 7.51 0 -1 -21 140.41 7.06 0 -1 21 169.57 7.56 0 -1 21 136.89 13.49 0 -1 -21 149.80 7.20 0 1 -21 127.55 13.24 0 -1 21 171.20 7.69 0 1 21 158.85 7.62 0 1 -22 55.82 4.12 0 1 -22 29.25 6.54 0 1 -22 54.19 4.11 0 -1 -22 51.22 3.87 0 -1 -22 37.30 7.45 0 -1 22 34.68 6.81 0 1 22 59.79 4.30 0 -1 22 57.89 4.15 0 1 22 55.52 4.18 0 -1 22 59.64 4.28 0 1 22 54.67 3.98 0 -1 -22 47.78 3.76 0 -1 22 56.15 4.12 0 -1 -23 149.32 7.46 0 -1 23 174.60 7.98 0 -1 -23 155.19 7.56 0 -1 23 180.66 8.13 0 -1 23 185.24 8.26 0 1 -23 165.05 7.97 0 1 23 180.19 8.01 0 1 23 181.20 8.23 0 1 23 161.06 7.85 0 1 24 324.59 12.57 0 1 -24 349.31 12.93 0 -1 24 378.48 13.09 0 -1 24 377.36 13.26 0 1 24 386.80 13.37 0 -1 -24 297.81 12.05 0 -1 25 43.35 3.69 0 -1 25 39.53 3.39 0 -1 -25 40.87 3.78 0 1 -25 35.03 3.26 0 1 25 40.45 3.58 0 1 25 30.77 3.02 0 -1 26 14.04 1.97 0 -1 -26 17.15 2.32 0 1 -26 13.54 1.93 0 1 26 10.85 1.68 0 1 26 14.66 2.09 0 -1 26 19.09 2.34 0 1 -27 4.11 1.05 0 1 -27 3.53 1.16 0 -1 27 3.52 0.97 0 -1 -27 4.16 1.20 0 -1 27 4.14 1.06 0 1 27 3.69 1.08 0 1 27 2.39 0.74 0 1 -28 1.76 0.65 0 -1 28 0.75 0.44 0 -1 28 0.62 0.49 0 -1 -28 0.82 0.55 0 1 -28 0.84 0.76 0 -1 29 4.18 1.04 0 -1 -29 2.55 0.78 0 1 -29 4.63 1.08 0 1 -30 0.53 0.53 0 -1 -30 -0.25 0.48 0 1 -31 46.22 3.10 0 -1 -31 48.31 3.18 0 1 -31 48.75 3.15 0 2 0 18.19 1.70 0 -2 0 15.28 1.27 0 2 0 15.37 1.57 0 2 0 17.68 1.08 0 -2 1 644.19 17.27 0 2 -1 712.03 18.48 0 2 -1 663.62 16.60 0 2 1 677.19 18.61 0 2 -1 648.16 18.45 0 2 2 200.17 7.21 0 2 -2 201.21 5.93 0 -2 2 192.77 7.24 0 2 -2 202.86 6.91 0 2 -2 204.30 7.25 0 2 -3 763.22 20.76 0 2 -3 766.13 19.80 0 2 3 778.48 20.87 0 -2 3 751.64 21.21 0 2 3 725.35 19.85 0 2 -4 105.02 4.55 0 2 -4 107.87 4.74 0 2 4 109.34 4.80 0 -2 4 111.88 5.29 0 2 -4 102.54 4.15 0 2 4 103.48 4.10 0 2 5 1904.04 46.93 0 2 5 1754.83 45.70 0 2 -5 1843.62 45.82 0 2 -5 1838.31 46.74 0 2 6 1227.73 31.86 0 2 -6 1242.81 31.69 0 2 7 785.38 21.65 0 -2 7 949.82 25.67 0 -2 8 28.30 3.16 0 2 8 24.50 2.95 0 2 9 124.42 7.50 0 -2 9 129.09 7.61 0 2 10 4258.54 109.01 0 -2 10 4245.41 108.86 0 2 11 2511.07 68.50 0 -2 11 2494.38 68.35 0 -2 12 915.21 29.83 0 2 12 913.10 29.93 0 2 13 134.89 9.49 0 -2 13 135.01 9.41 0 2 13 117.58 7.23 0 2 14 23.62 2.16 0 2 -14 25.25 2.13 0 -2 14 28.19 4.36 0 2 14 31.95 4.72 0 -2 15 66.32 3.88 0 -2 15 66.79 3.85 0 2 15 63.57 3.80 0 2 -15 64.76 3.86 0 2 -15 65.42 3.78 0 2 15 68.44 3.96 0 -2 15 67.28 3.88 0 2 15 62.47 3.72 0 2 15 68.93 4.01 0 -2 16 408.48 12.65 0 2 16 395.15 12.58 0 2 16 401.84 12.80 0 2 -16 391.91 12.47 0 2 16 294.63 11.79 0 2 16 393.06 12.44 0 2 16 397.28 12.68 0 -2 16 401.02 12.63 0 -2 16 491.83 21.84 0 -2 -16 322.44 11.77 0 2 -16 373.50 12.50 0 -2 16 398.24 12.66 0 2 -17 862.73 24.02 0 -2 17 872.19 24.18 0 2 -17 924.98 35.07 0 2 17 867.72 24.09 0 2 17 688.47 23.35 0 -2 17 876.53 24.16 0 -2 -17 752.15 23.35 0 -2 17 883.07 24.26 0 2 17 848.31 24.37 0 -2 -17 862.80 24.25 0 -2 17 1020.77 36.31 0 2 17 885.29 24.40 0 2 17 854.38 23.92 0 2 -17 874.45 24.33 0 2 17 869.07 24.25 0 -2 18 64.07 4.14 0 -2 18 61.49 4.05 0 2 18 60.31 4.14 0 -2 18 73.23 8.59 0 -2 18 60.01 4.03 0 -2 -18 55.86 3.77 0 2 -18 62.87 7.97 0 2 -18 64.23 4.17 0 -2 -18 63.51 4.18 0 2 18 61.70 4.09 0 2 18 64.55 4.06 0 2 18 66.05 4.26 0 2 -18 64.86 4.09 0 2 18 65.05 4.19 0 -2 19 128.33 6.23 0 2 19 121.69 6.20 0 -2 -19 111.79 5.77 0 -2 -19 119.73 6.18 0 -2 19 120.27 6.05 0 2 -19 121.52 6.21 0 2 -19 125.52 6.12 0 2 -19 100.84 10.84 0 -2 19 115.52 11.49 0 2 19 115.28 6.17 0 -2 19 121.71 6.14 0 2 19 127.29 6.15 0 2 19 115.71 5.90 0 2 20 45.28 3.63 0 2 -20 46.57 3.65 0 2 -20 32.02 6.25 0 2 20 42.32 3.54 0 -2 -20 34.07 3.02 0 -2 20 42.50 7.14 0 -2 20 39.87 3.30 0 -2 20 44.95 3.56 0 2 -20 47.25 3.58 0 -2 20 49.00 3.70 0 -2 20 45.21 3.53 0 -2 -20 44.64 3.56 0 2 20 46.54 3.57 0 -2 21 38.35 3.34 0 2 -21 39.55 3.46 0 -2 21 39.67 7.15 0 2 -21 36.31 3.23 0 2 21 35.72 3.22 0 2 21 34.26 3.19 0 -2 -21 38.79 3.35 0 -2 21 36.23 3.24 0 -2 21 39.85 3.39 0 2 21 34.78 3.22 0 -2 21 31.41 2.94 0 2 -22 184.42 8.40 0 -2 22 194.15 8.42 0 2 22 171.70 8.12 0 2 -22 103.45 12.23 0 -2 22 190.61 8.34 0 -2 22 186.68 8.24 0 2 -22 187.44 8.26 0 -2 -22 154.96 7.74 0 2 22 190.70 8.46 0 -2 22 130.84 13.64 0 -2 -22 178.10 8.12 0 -2 -23 6.63 1.67 0 -2 -23 3.07 0.94 0 2 23 3.53 1.10 0 2 -23 4.81 1.32 0 -2 23 3.02 1.08 0 -2 23 4.66 1.20 0 2 23 4.51 1.45 0 -2 23 4.20 1.25 0 -2 -23 2.93 0.92 0 2 24 85.74 5.37 0 -2 24 102.57 5.83 0 -2 24 98.38 5.74 0 -2 -24 87.73 5.39 0 2 24 99.42 5.82 0 -2 -24 100.12 6.04 0 2 -24 90.61 5.65 0 -2 24 99.02 5.71 0 -2 25 458.94 15.42 0 2 25 469.41 15.57 0 2 -25 444.80 15.39 0 -2 -25 499.95 16.24 0 -2 25 459.66 15.30 0 2 26 22.71 2.60 0 2 26 16.62 2.06 0 2 -26 20.21 2.46 0 -2 -26 23.72 2.79 0 -2 26 23.19 2.62 0 -2 27 26.47 2.69 0 -2 -27 24.31 2.75 0 -2 27 17.00 2.05 0 2 -27 20.43 2.36 0 -2 -28 -0.08 0.50 0 -2 28 0.56 0.46 0 2 -28 -0.98 0.76 0 -2 28 -0.70 0.65 0 2 -28 -0.19 0.44 0 -2 29 3.21 0.86 0 -2 -29 4.04 0.97 0 2 -29 3.33 0.79 0 2 -29 4.31 1.06 0 2 -30 8.17 1.30 0 -2 -30 7.89 1.31 0 2 -30 8.18 1.36 0 -2 30 9.71 1.41 0 -2 -31 53.56 3.31 0 2 -31 49.27 3.16 0 3 0 0.25 0.55 0 -3 0 0.57 0.42 0 3 0 1.40 0.73 0 -3 -1 282.24 9.64 0 -3 1 276.59 9.06 0 3 1 296.49 10.53 0 3 -1 314.21 10.60 0 3 -1 284.71 8.10 0 3 -1 295.73 10.51 0 -3 2 119.54 5.79 0 3 -2 123.22 5.68 0 3 2 122.11 5.92 0 3 -2 121.08 5.85 0 3 -2 113.00 3.91 0 3 -3 364.73 10.74 0 3 3 395.18 13.08 0 -3 3 387.66 13.14 0 3 -3 398.40 13.05 0 3 -3 393.83 12.52 0 3 -4 1780.57 46.35 0 3 -4 1691.83 44.40 0 -3 4 1849.52 47.01 0 3 4 1844.39 46.61 0 3 -5 1107.90 29.52 0 3 5 1141.47 30.88 0 -3 5 1164.57 31.68 0 3 -5 1042.00 29.33 0 3 -5 1122.00 30.70 0 -3 6 1399.72 36.37 0 3 -6 1200.96 33.10 0 3 6 1328.39 34.93 0 3 -6 1227.38 34.18 0 3 -6 1279.15 34.59 0 3 -7 52.16 3.11 0 -3 7 59.18 4.69 0 3 -7 57.01 4.06 0 3 -8 3.03 1.01 0 -3 8 2.36 1.19 0 -3 9 474.08 17.54 0 3 -9 428.67 16.30 0 -3 10 8.78 2.37 0 3 10 6.80 1.78 0 3 -10 8.12 1.91 0 3 -11 30.50 3.91 0 3 11 28.64 3.63 0 -3 11 32.19 4.16 0 -3 12 153.09 9.89 0 3 12 138.95 8.67 0 3 -12 137.51 9.11 0 3 -13 1052.70 35.64 0 3 13 1050.67 33.87 0 -3 13 1161.01 37.07 0 3 -14 201.19 7.81 0 3 -14 202.93 7.72 0 3 14 206.30 7.94 0 3 -14 226.23 13.07 0 3 14 196.43 7.70 0 -3 14 193.01 7.63 0 3 14 218.71 11.43 0 -3 14 202.88 7.74 0 3 14 200.87 7.70 0 3 -15 148.41 6.37 0 -3 15 173.85 12.08 0 3 15 146.70 6.32 0 3 15 145.88 6.49 0 3 -15 145.34 6.44 0 3 15 139.63 6.29 0 -3 15 149.86 6.40 0 3 -15 156.35 11.29 0 -3 15 144.82 6.28 0 3 15 126.98 6.19 0 -3 15 154.75 6.47 0 3 16 108.04 5.51 0 3 -16 105.68 5.30 0 3 -16 105.50 9.55 0 3 -16 105.67 5.43 0 -3 16 105.06 5.31 0 3 16 109.72 5.37 0 -3 16 100.65 5.22 0 -3 16 102.91 5.25 0 -3 16 122.44 10.51 0 3 16 101.44 5.34 0 3 16 103.82 5.31 0 -3 17 14.24 3.72 0 3 17 15.74 1.90 0 -3 17 16.07 1.93 0 -3 17 16.86 1.99 0 3 -17 11.77 3.22 0 3 17 15.64 1.96 0 3 17 14.23 1.83 0 3 -17 15.08 1.92 0 -3 17 15.30 1.93 0 3 -17 15.97 1.92 0 -3 -17 14.81 1.91 0 3 17 14.27 1.88 0 3 -18 20.88 4.56 0 -3 -18 22.00 2.43 0 3 18 20.72 2.37 0 3 -18 22.25 2.33 0 3 18 24.36 2.52 0 -3 18 26.01 2.55 0 -3 18 29.42 5.43 0 3 -18 23.26 2.46 0 -3 18 22.16 2.35 0 -3 18 26.16 2.56 0 3 18 23.85 2.44 0 3 18 23.16 2.39 0 -3 19 121.34 6.16 0 3 19 127.93 6.46 0 -3 19 130.36 6.39 0 -3 19 124.08 12.03 0 -3 19 125.12 6.27 0 3 -19 117.25 6.03 0 3 -19 126.72 6.41 0 -3 -19 123.57 6.34 0 3 19 112.97 6.16 0 3 -20 10.38 1.71 0 3 20 11.87 1.85 0 3 -20 7.12 2.18 0 -3 20 9.85 1.63 0 3 20 10.48 1.77 0 3 -20 9.05 1.56 0 3 -20 9.36 1.56 0 -3 -20 7.48 1.47 0 -3 20 11.22 3.94 0 -3 20 12.90 1.90 0 -3 20 9.08 1.60 0 -3 21 3.71 2.46 0 -3 -21 5.22 1.28 0 3 -21 6.78 1.42 0 3 21 6.84 1.38 0 3 -21 6.68 1.50 0 -3 21 5.37 1.31 0 3 -21 4.57 1.12 0 -3 21 5.64 1.24 0 -3 -21 5.90 1.44 0 3 21 6.32 1.41 0 -3 21 5.79 1.29 0 -3 21 7.55 1.50 0 3 22 49.51 3.98 0 3 22 40.44 3.56 0 -3 -22 52.31 4.25 0 3 -22 47.85 3.80 0 -3 22 48.91 3.90 0 -3 22 46.86 3.79 0 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418.34 18.24 0 7 5 406.85 18.21 0 7 6 374.20 17.68 0 7 6 323.61 10.86 0 7 -6 304.38 10.61 0 7 6 317.45 10.83 0 7 -6 299.85 10.62 0 -7 -6 374.77 17.14 0 7 -6 312.35 10.74 0 -7 6 366.95 17.27 0 7 -6 329.06 15.25 0 7 -7 126.16 5.78 0 7 7 133.29 6.00 0 -7 7 158.75 10.84 0 7 7 136.88 6.07 0 7 -7 123.53 5.77 0 7 -7 132.01 5.98 0 7 -7 138.70 9.03 0 7 7 150.59 10.81 0 7 7 129.75 5.91 0 -7 -7 157.49 10.84 0 7 7 119.22 5.65 0 7 -7 131.30 5.91 0 -7 -8 135.13 10.38 0 -7 8 155.71 10.89 0 7 8 110.02 5.41 0 7 -8 129.79 8.59 0 7 -8 116.71 5.55 0 7 -8 125.31 5.71 0 7 -8 123.78 5.79 0 7 8 158.66 11.21 0 7 8 127.46 5.89 0 7 -8 101.68 5.24 0 7 -8 126.99 5.75 0 7 -9 2.74 0.78 0 7 -9 1.85 0.57 0 7 -9 0.70 0.34 0 7 -9 1.27 0.49 0 -7 9 1.15 1.20 0 7 9 0.92 0.40 0 7 9 1.74 1.21 0 7 -9 1.84 0.57 0 7 9 1.26 0.50 0 7 9 3.96 0.98 0 -7 -9 0.12 0.74 0 7 -10 46.39 3.37 0 7 -10 40.31 3.07 0 7 10 44.92 3.37 0 7 -10 42.90 3.33 0 7 10 50.18 6.54 0 7 -10 48.75 3.39 0 7 -10 47.69 3.32 0 -7 10 43.37 3.08 0 -7 10 50.60 6.41 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0.66 0 7 -18 -0.08 0.65 0 -7 18 0.61 0.59 0 7 -19 430.60 14.62 0 -7 19 415.32 14.31 0 7 -19 415.46 14.75 0 7 -19 446.58 14.81 0 -7 -19 428.82 14.54 0 -7 19 372.29 13.74 0 7 -19 389.18 13.91 0 7 19 354.56 13.58 0 -7 -19 376.28 14.13 0 7 -20 9.35 1.83 0 -7 20 10.39 1.89 0 7 -20 7.07 1.60 0 7 -20 8.02 1.50 0 -7 -20 8.94 1.77 0 -7 -20 6.37 1.44 0 -7 20 6.51 1.33 0 7 -20 7.88 1.46 0 -7 -21 112.50 6.18 0 -7 21 107.72 6.05 0 7 -21 109.50 6.28 0 -7 -21 99.10 5.94 0 7 -21 113.18 6.25 0 7 -21 114.90 6.30 0 -7 21 91.73 5.52 0 -7 22 14.78 2.02 0 7 -22 15.97 2.20 0 -7 -22 16.23 2.24 0 -7 -22 14.85 2.07 0 -7 22 13.21 1.91 0 7 -22 16.95 2.22 0 -7 -22 12.38 1.87 0 7 -22 14.47 2.16 0 7 -23 61.75 4.36 0 7 23 53.86 4.04 0 7 -23 60.04 4.38 0 -7 -23 62.61 4.34 0 -7 -23 50.72 3.95 0 7 -23 56.75 4.17 0 -7 23 55.82 4.09 0 -7 -23 55.14 3.90 0 7 -24 5.11 1.18 0 7 -24 4.98 1.10 0 7 -24 3.44 1.08 0 -7 -24 5.16 1.26 0 -7 -24 4.83 1.18 0 -7 24 4.60 1.18 0 7 24 6.06 1.22 0 7 -24 3.66 1.09 0 -7 -25 -0.06 0.43 0 7 25 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3.27 0 8 -2 19.53 2.02 0 8 -2 14.48 1.74 0 8 2 16.60 1.83 0 8 2 20.20 2.04 0 8 -2 15.25 1.79 0 8 2 18.49 2.02 0 8 2 18.13 1.97 0 8 2 18.89 1.98 0 8 -2 18.63 1.96 0 8 -2 17.84 1.95 0 8 -2 19.96 2.04 0 8 2 17.15 1.90 0 -8 2 22.55 3.99 0 8 2 19.10 2.03 0 8 -2 17.72 1.97 0 8 3 164.48 6.96 0 8 3 165.29 6.91 0 8 3 188.83 12.47 0 8 -3 161.32 6.75 0 -8 3 196.94 12.68 0 8 -3 163.43 6.85 0 8 3 168.69 6.93 0 8 -3 169.15 6.93 0 8 -3 140.17 6.39 0 8 -3 177.02 7.07 0 8 -3 164.86 6.95 0 8 -3 161.90 6.85 0 8 -3 147.61 6.69 0 8 3 142.08 6.44 0 8 3 164.62 6.91 0 8 3 157.63 6.92 0 -8 -3 180.71 11.20 0 8 -3 146.66 6.64 0 8 -4 70.25 4.18 0 8 -4 85.07 4.51 0 8 -4 75.20 4.26 0 -8 4 84.36 8.09 0 8 -4 61.31 3.89 0 8 -4 61.57 3.83 0 8 -4 75.97 4.30 0 8 4 73.93 4.26 0 8 -4 70.15 4.06 0 8 4 85.72 8.20 0 8 4 74.63 4.30 0 8 4 59.25 3.77 0 8 -4 66.54 4.01 0 8 4 80.78 4.40 0 8 -4 78.61 4.42 0 8 4 78.31 4.45 0 8 4 78.37 4.36 0 8 -4 82.23 4.50 0 -8 -4 85.58 7.71 0 -8 5 53.44 6.55 0 8 -5 48.59 3.39 0 -8 -5 58.88 6.46 0 8 5 49.86 3.41 0 8 -5 42.73 3.19 0 8 5 49.41 3.41 0 8 5 51.89 6.42 0 8 -5 45.09 3.29 0 8 5 50.37 3.43 0 8 5 50.50 3.52 0 8 -5 55.47 6.19 0 8 -5 45.58 3.28 0 8 5 35.45 2.83 0 8 -5 44.16 3.12 0 8 -5 52.19 3.50 0 8 -5 50.39 3.41 0 8 -5 51.35 3.46 0 8 -5 51.93 3.56 0 8 5 44.94 3.26 0 8 -5 37.82 2.90 0 8 -6 29.15 2.51 0 8 -6 37.28 5.03 0 8 6 33.99 2.79 0 -8 6 33.83 5.10 0 8 -6 24.94 2.30 0 8 6 35.59 2.88 0 8 -6 36.06 2.86 0 8 6 35.53 2.94 0 8 6 34.28 2.80 0 8 -6 33.77 2.82 0 8 -6 36.93 2.95 0 8 6 46.32 6.10 0 8 6 36.09 2.92 0 8 -6 37.80 2.97 0 -8 -6 37.74 5.33 0 8 -6 36.64 2.90 0 8 -6 33.91 2.79 0 8 6 32.82 2.76 0 -8 7 -0.53 1.47 0 8 7 -0.06 0.26 0 8 -7 -2.18 1.25 0 8 -7 0.47 0.37 0 -8 -7 0.01 0.52 0 8 -7 -0.07 0.54 0 8 7 -0.60 0.59 0 8 -7 3.39 0.94 0 8 -7 -0.09 0.35 0 8 -7 1.47 0.68 0 8 7 2.61 1.65 0 8 -7 0.45 0.36 0 8 7 0.33 0.34 0 8 -7 1.39 0.66 0 -8 7 -0.01 0.38 0 8 -7 0.20 0.38 0 8 7 0.58 0.33 0 8 7 0.29 0.38 0 8 7 0.36 0.35 0 8 -8 195.36 7.80 0 8 -8 173.63 7.41 0 8 8 142.01 6.89 0 8 8 181.51 7.68 0 8 8 190.10 7.83 0 -8 -8 197.30 13.63 0 8 -8 188.64 7.70 0 8 8 183.54 7.67 0 -8 8 145.68 6.70 0 8 -8 182.13 7.51 0 8 8 200.98 13.81 0 8 8 181.99 7.56 0 8 8 187.36 7.80 0 -8 8 202.09 13.80 0 8 -8 156.53 7.22 0 8 -8 190.63 7.83 0 8 -8 181.87 7.67 0 8 9 1.72 0.73 0 -8 9 -0.08 1.14 0 8 -9 1.45 0.66 0 8 9 1.01 0.52 0 8 9 2.44 0.87 0 -8 9 0.10 0.42 0 8 -9 0.74 0.49 0 8 9 1.81 0.70 0 8 9 1.56 1.14 0 8 -9 1.54 0.78 0 -8 -9 3.33 1.82 0 8 -9 0.91 0.52 0 8 -9 1.53 0.61 0 8 9 0.45 0.47 0 8 -9 0.22 0.41 0 8 10 8.43 1.42 0 8 -10 10.73 1.69 0 -8 10 13.80 3.78 0 8 -10 9.52 1.46 0 -8 10 11.92 1.66 0 8 -10 11.75 1.74 0 8 10 11.01 1.63 0 8 10 11.10 1.67 0 -8 -10 12.73 3.49 0 8 -10 12.09 1.74 0 8 10 10.93 1.63 0 -8 10 10.85 1.55 0 8 -10 10.91 1.64 0 8 10 12.50 3.35 0 8 10 10.54 1.72 0 8 -10 11.01 1.62 0 8 -11 37.37 3.14 0 8 -11 40.77 3.35 0 -8 11 39.49 3.15 0 8 11 39.87 3.33 0 8 11 34.65 6.02 0 8 -11 40.26 3.27 0 -8 -11 34.25 6.11 0 8 11 37.39 3.20 0 8 -11 34.94 3.13 0 8 11 35.71 3.04 0 -8 11 39.61 6.43 0 8 -11 37.59 3.14 0 8 -11 38.91 3.14 0 -8 11 35.42 2.97 0 8 11 38.24 3.29 0 8 12 4.10 1.06 0 8 -12 3.13 0.89 0 8 -12 3.41 1.01 0 -8 12 2.85 0.91 0 8 -12 1.78 0.59 0 8 12 4.62 2.48 0 -8 12 0.95 1.86 0 8 -12 2.96 0.98 0 -8 12 2.28 0.78 0 8 12 3.66 1.04 0 -8 -12 3.65 2.16 0 8 -12 3.00 1.00 0 -8 12 2.33 0.80 0 8 -12 2.82 0.94 0 -8 13 7.06 2.79 0 8 13 4.86 2.13 0 8 -13 4.52 1.13 0 8 13 6.92 1.38 0 -8 13 5.03 1.22 0 8 13 4.79 1.18 0 8 -13 5.44 1.28 0 8 13 6.35 1.29 0 8 -13 4.84 1.21 0 -8 13 5.27 1.16 0 8 -13 5.20 1.29 0 -8 -13 6.39 2.74 0 -8 13 4.59 1.12 0 8 -13 5.60 1.38 0 8 -14 0.49 0.42 0 -8 14 -0.14 0.45 0 8 -14 0.90 0.73 0 -8 14 0.47 0.49 0 8 14 0.50 0.71 0 8 -14 0.02 0.55 0 8 -14 0.87 0.75 0 8 14 -1.42 1.40 0 -8 -14 0.91 0.81 0 8 -14 1.70 0.78 0 8 14 0.55 0.50 0 8 -14 0.56 0.55 0 -8 14 0.63 1.26 0 8 15 -0.85 1.21 0 8 15 -0.04 0.32 0 8 -15 0.07 0.48 0 8 -15 0.05 0.61 0 -8 -15 1.22 0.84 0 8 -15 0.37 0.58 0 -8 15 0.70 1.12 0 -8 15 -0.27 0.38 0 -8 15 0.33 0.57 0 -8 15 -0.07 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5.49 0 9 -6 31.38 2.75 0 9 -6 33.52 2.92 0 9 -6 29.55 2.78 0 9 -6 33.91 2.97 0 9 6 32.40 5.68 0 9 -7 118.14 5.96 0 9 -7 112.46 5.98 0 9 7 108.11 5.68 0 9 -7 109.10 5.79 0 9 -7 110.54 5.81 0 -9 7 101.04 5.32 0 -9 -7 120.46 10.74 0 9 7 101.93 5.54 0 9 7 111.26 5.83 0 9 -7 111.48 5.84 0 9 7 107.24 10.54 0 9 7 100.07 5.70 0 9 7 104.28 5.69 0 9 7 111.77 5.84 0 9 -7 108.00 5.67 0 9 -7 104.18 5.70 0 -9 7 108.18 10.64 0 -9 8 630.58 20.50 0 9 8 716.83 21.69 0 9 8 724.67 21.53 0 9 8 767.24 21.88 0 9 -8 715.32 21.48 0 9 8 690.70 31.43 0 9 8 649.45 20.91 0 9 -8 739.65 21.64 0 9 8 735.50 21.67 0 9 -8 724.79 21.37 0 -9 -8 733.93 31.50 0 9 -8 711.81 21.56 0 -9 8 750.04 32.48 0 9 -8 734.12 21.88 0 9 -8 724.30 21.70 0 9 8 733.67 21.65 0 9 -8 736.62 21.61 0 9 -9 180.91 7.94 0 -9 -9 161.73 13.54 0 9 -9 154.49 7.49 0 9 -9 178.51 8.01 0 9 9 175.33 14.25 0 9 9 184.42 8.08 0 9 -9 174.48 7.78 0 9 -9 175.68 7.90 0 9 9 171.05 7.80 0 -9 9 188.51 7.86 0 9 9 183.32 7.98 0 9 -9 183.27 7.93 0 -9 9 173.41 14.07 0 9 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18.35 2.14 0 10 -1 19.84 2.25 0 10 2 33.16 3.00 0 10 2 32.21 3.00 0 10 2 34.81 3.08 0 10 2 33.99 3.05 0 10 -2 28.77 2.80 0 10 2 29.96 2.84 0 10 2 33.66 3.07 0 10 -2 33.09 2.98 0 -10 2 31.14 5.95 0 10 -2 36.95 6.22 0 10 -2 33.50 3.01 0 10 -2 27.52 2.71 0 10 -2 32.28 2.95 0 10 -2 33.36 2.97 0 10 -2 36.03 3.12 0 -10 -2 28.80 5.86 0 10 -2 36.69 3.20 0 10 -3 38.72 3.22 0 10 -3 44.08 3.52 0 10 -3 45.98 3.55 0 10 -3 47.67 3.67 0 10 -3 43.21 3.47 0 10 -3 42.56 3.47 0 10 -3 44.92 3.58 0 10 3 43.48 3.43 0 10 -3 41.47 6.53 0 10 3 44.95 3.60 0 10 3 48.56 3.71 0 -10 3 46.76 7.21 0 10 3 46.40 3.64 0 -10 -3 43.33 7.12 0 10 -3 42.76 3.51 0 10 3 46.52 3.62 0 10 -3 35.88 3.08 0 10 3 46.89 3.66 0 10 -3 43.08 3.43 0 10 -4 190.88 8.21 0 10 -4 174.97 7.98 0 10 4 188.94 8.34 0 10 4 190.82 8.20 0 10 -4 193.88 8.40 0 10 -4 161.74 7.62 0 10 -4 171.46 7.79 0 10 4 190.45 8.31 0 -10 4 173.83 7.76 0 10 -4 183.35 7.95 0 10 -4 190.73 8.19 0 -10 4 188.95 15.07 0 10 -4 187.83 8.27 0 10 4 188.03 8.22 0 10 4 171.85 7.77 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0.26 0.62 0 11 -1 51.39 3.97 0 11 1 53.52 4.02 0 11 1 53.34 4.06 0 11 -1 50.29 3.88 0 11 -1 50.41 3.95 0 11 -1 49.91 3.91 0 11 1 51.38 3.96 0 11 -1 50.65 3.94 0 -11 1 38.88 7.15 0 11 1 56.37 4.14 0 11 1 53.19 4.04 0 -11 -1 41.16 7.31 0 11 -1 41.99 3.47 0 11 -1 37.67 6.80 0 11 -2 -0.29 0.74 0 11 -2 1.44 0.75 0 11 2 1.83 0.86 0 -11 -2 1.57 0.69 0 11 -2 1.11 0.63 0 11 2 1.28 0.74 0 11 -2 1.30 0.65 0 11 2 1.37 0.71 0 11 -2 2.42 1.00 0 11 2 2.12 1.13 0 11 -2 0.88 0.55 0 -11 2 0.50 1.17 0 11 -2 0.72 0.63 0 11 2 0.53 0.70 0 11 -2 1.75 0.72 0 11 3 145.16 7.11 0 11 3 134.60 6.95 0 -11 3 113.01 12.31 0 11 -3 126.25 6.69 0 -11 -3 114.31 12.66 0 11 -3 118.06 6.39 0 11 -3 123.96 6.54 0 11 -3 141.12 7.06 0 11 -3 130.39 6.77 0 11 -3 89.42 10.61 0 11 -3 120.89 6.52 0 11 3 136.78 6.94 0 11 3 140.52 6.98 0 -11 3 125.10 6.53 0 11 -3 130.15 6.75 0 11 3 137.11 6.90 0 11 -3 143.50 7.08 0 11 -4 55.55 4.14 0 11 -4 52.84 4.01 0 11 4 56.34 4.25 0 11 -4 61.50 4.33 0 11 4 56.30 4.24 0 11 -4 50.97 3.99 0 -11 4 43.67 7.58 0 11 -4 55.23 4.14 0 -11 4 50.64 3.85 0 11 4 56.14 4.18 0 11 -4 31.31 6.24 0 11 -4 52.99 3.95 0 11 4 55.14 4.15 0 11 -4 54.71 4.21 0 11 4 58.41 4.23 0 -11 -4 49.85 8.43 0 11 -5 17.39 2.18 0 11 -5 17.99 2.21 0 11 5 21.50 2.54 0 11 -5 18.72 2.39 0 11 5 20.44 2.48 0 11 5 19.36 2.37 0 -11 5 14.44 1.96 0 11 5 18.35 2.42 0 11 -5 19.92 2.49 0 11 -5 19.79 2.50 0 11 -5 19.84 2.48 0 -11 5 18.84 5.08 0 -11 -5 10.50 3.62 0 11 5 21.93 2.63 0 11 -5 18.95 2.27 0 11 -5 20.41 2.50 0 11 -6 234.87 9.72 0 -11 6 223.03 9.33 0 -11 6 189.13 16.37 0 11 -6 205.96 9.16 0 11 6 231.52 9.67 0 11 -6 219.63 9.36 0 11 -6 240.52 9.87 0 11 6 230.60 9.64 0 11 -6 231.68 9.82 0 -11 -6 210.44 17.85 0 11 6 228.25 9.66 0 11 6 226.78 9.77 0 11 -6 203.72 8.97 0 11 -6 233.20 9.83 0 11 6 234.82 9.82 0 11 -6 222.25 9.53 0 11 7 6.44 1.51 0 11 -7 5.87 1.35 0 11 -7 5.35 1.26 0 11 -7 5.56 1.36 0 -11 7 5.18 1.23 0 11 -7 3.67 1.08 0 11 7 5.90 1.58 0 11 -7 4.90 1.14 0 11 7 5.88 1.26 0 -11 7 4.89 2.55 0 11 7 6.55 1.49 0 11 7 6.66 1.50 0 11 -7 6.54 1.36 0 11 -7 4.22 1.11 0 11 8 68.90 4.75 0 11 -8 65.00 4.61 0 11 8 67.24 4.75 0 11 -8 70.75 4.82 0 -11 8 59.83 4.20 0 11 8 60.46 4.46 0 11 -8 61.01 4.45 0 11 8 67.66 4.70 0 -11 8 64.40 4.45 0 11 -8 66.95 4.69 0 11 -8 70.45 4.91 0 11 8 65.72 4.69 0 11 -8 66.36 4.62 0 11 -8 62.81 4.53 0 11 -9 97.47 5.69 0 11 9 93.67 5.67 0 11 -9 89.71 5.57 0 -11 9 88.42 5.37 0 11 -9 102.22 6.01 0 11 -9 88.73 5.54 0 11 9 92.93 5.64 0 11 -9 91.24 5.58 0 11 9 101.14 5.85 0 11 9 101.44 5.88 0 11 9 93.91 5.79 0 11 -9 93.75 5.65 0 11 -9 98.14 5.81 0 -11 9 94.11 5.68 0 11 10 56.69 4.33 0 11 10 59.22 4.41 0 11 -10 53.20 4.20 0 11 -10 53.12 4.06 0 11 10 57.89 4.33 0 11 10 49.96 3.98 0 11 10 49.51 3.97 0 11 -10 56.71 4.19 0 11 -10 57.61 4.40 0 -11 10 49.37 3.99 0 11 -10 54.36 4.22 0 -11 10 52.05 3.96 0 11 -10 50.61 4.04 0 11 11 172.87 8.16 0 11 -11 171.96 8.00 0 11 11 191.25 8.71 0 11 -11 176.13 8.36 0 11 11 189.89 8.52 0 11 -11 181.64 8.39 0 -11 11 194.23 8.50 0 11 11 166.49 7.93 0 -11 11 171.56 7.98 0 -11 -11 149.79 7.55 0 11 -11 178.85 8.34 0 -11 11 173.05 8.08 0 11 11 192.47 8.64 0 11 -11 183.01 8.35 0 11 -11 190.69 8.67 0 11 12 2.93 1.00 0 -11 12 3.74 1.23 0 11 -12 2.25 0.99 0 -11 12 3.27 1.07 0 -11 12 3.68 1.16 0 -11 -12 2.72 0.91 0 11 12 2.18 1.12 0 11 -12 2.10 0.72 0 11 -12 2.71 1.04 0 11 12 2.30 0.88 0 11 -12 3.47 1.16 0 11 12 2.34 0.88 0 11 13 3.21 1.07 0 -11 13 2.61 0.96 0 -11 13 2.32 0.83 0 11 13 2.75 1.27 0 11 -13 4.96 1.36 0 -11 13 1.73 0.72 0 11 13 3.15 1.02 0 11 13 1.81 0.95 0 11 -13 2.63 1.00 0 -11 -13 1.89 0.87 0 11 -13 3.02 1.14 0 11 14 506.24 16.88 0 11 -14 538.63 17.08 0 11 14 439.10 15.98 0 11 14 532.88 17.29 0 -11 -14 478.14 16.42 0 11 14 493.63 16.53 0 -11 14 466.61 16.06 0 -11 14 532.92 16.90 0 11 -14 517.59 16.88 0 11 -14 521.52 17.09 0 11 -14 503.88 16.81 0 -11 15 13.75 2.00 0 11 -15 17.45 2.27 0 11 15 13.52 1.90 0 11 -15 15.98 2.24 0 11 15 14.70 2.24 0 -11 -15 12.71 1.92 0 11 -15 14.92 2.11 0 11 15 9.84 1.63 0 -11 -15 16.44 2.32 0 11 15 13.31 2.04 0 11 -15 14.57 2.18 0 11 16 8.63 1.46 0 11 16 10.00 1.83 0 11 -16 7.77 1.53 0 11 16 7.97 1.54 0 11 -16 11.18 1.76 0 -11 -16 9.20 1.69 0 -11 16 8.15 1.55 0 11 -16 8.58 1.51 0 11 16 6.58 1.30 0 -11 -16 9.40 1.63 0 11 -16 10.63 1.84 0 11 -17 81.20 4.97 0 11 -17 81.43 4.96 0 11 -17 77.39 4.81 0 -11 -17 72.30 4.68 0 11 -17 74.94 4.74 0 11 17 71.22 4.60 0 -11 17 68.68 4.49 0 -11 -17 81.71 4.95 0 11 17 77.80 4.96 0 11 -18 10.67 1.72 0 -11 -18 12.24 1.80 0 11 -18 11.97 1.81 0 11 18 9.06 1.62 0 -11 -18 10.41 1.70 0 -11 -18 10.24 1.67 0 11 -18 9.66 1.61 0 11 18 9.63 1.56 0 11 -18 10.19 1.66 0 11 19 6.43 1.22 0 11 -19 6.57 1.26 0 11 19 7.03 1.42 0 -11 -19 7.34 1.39 0 11 -19 7.25 1.31 0 -11 -19 6.24 1.26 0 -11 -19 6.00 1.25 0 11 -19 6.51 1.31 0 -11 -20 31.44 2.74 0 11 -20 32.27 2.78 0 11 20 32.64 2.88 0 -11 -20 33.35 2.87 0 11 -20 29.81 2.66 0 -11 -20 31.90 2.79 0 11 20 22.53 2.17 0 11 -20 31.58 2.80 0 -11 -21 15.53 1.84 0 11 -21 14.48 1.74 0 -11 -21 14.50 1.76 0 11 -21 14.41 1.76 0 11 -21 15.75 1.81 0 11 21 14.16 1.81 0 11 -22 1.52 0.53 0 11 -22 1.98 0.62 0 -11 -22 2.43 0.66 0 -11 -22 2.20 0.65 0 11 22 1.56 0.60 0 11 -22 0.94 0.47 0 12 0 219.45 9.55 0 12 0 217.97 9.55 0 12 0 215.99 9.55 0 12 0 219.60 9.61 0 12 0 226.91 9.68 0 12 -1 75.74 5.04 0 12 -1 76.79 5.14 0 12 1 69.44 4.89 0 -12 1 67.93 4.78 0 12 -1 76.25 5.07 0 12 -1 70.79 4.89 0 12 -1 73.98 5.01 0 12 1 72.07 4.92 0 12 1 73.72 5.06 0 12 1 74.75 5.05 0 12 1 73.85 5.00 0 12 2 202.10 9.09 0 -12 2 188.58 8.77 0 12 -2 191.86 8.83 0 12 -2 207.87 9.15 0 12 -2 215.60 9.36 0 12 2 201.79 9.12 0 12 2 205.84 9.16 0 12 -2 200.54 9.07 0 12 2 203.91 9.12 0 12 2 207.97 9.19 0 12 -2 221.41 9.40 0 -12 -3 54.63 4.06 0 12 3 65.91 4.65 0 12 3 64.53 4.69 0 12 -3 59.17 4.36 0 12 -3 62.21 4.49 0 12 3 66.41 4.65 0 -12 3 60.34 4.38 0 12 3 65.49 4.68 0 12 3 63.16 4.53 0 12 -3 64.67 4.71 0 12 4 5.10 1.28 0 -12 -4 5.02 1.20 0 12 -4 5.87 1.45 0 12 4 7.23 1.68 0 12 4 6.51 1.38 0 12 4 6.61 1.62 0 12 4 7.58 1.67 0 12 -4 5.87 1.36 0 -12 4 5.87 1.41 0 12 -4 4.99 1.33 0 12 -5 228.50 9.69 0 12 5 227.15 9.60 0 -12 5 209.66 9.19 0 12 5 230.05 9.75 0 12 -5 219.17 9.64 0 12 5 219.28 9.61 0 12 5 231.22 9.67 0 12 -5 217.09 9.39 0 12 5 220.93 9.52 0 12 -5 204.20 8.97 0 -12 -5 197.34 9.08 0 12 -6 33.30 3.43 0 -12 6 33.03 3.10 0 12 6 37.70 3.48 0 12 6 35.04 3.39 0 12 -6 31.14 3.14 0 -12 -6 27.97 2.93 0 12 -6 35.77 3.33 0 12 -6 31.21 2.98 0 12 6 31.31 3.17 0 12 6 30.88 3.25 0 12 -6 34.87 3.39 0 12 -7 439.41 14.74 0 12 -7 399.83 14.29 0 12 7 408.89 14.34 0 12 -7 349.61 13.46 0 12 7 420.74 14.60 0 12 -7 412.31 14.48 0 12 7 404.26 14.40 0 -12 -7 387.22 14.16 0 12 -7 404.65 14.19 0 12 -7 361.70 13.58 0 -12 7 376.38 13.62 0 12 7 416.65 14.43 0 -12 8 10.60 1.76 0 12 8 8.79 1.69 0 12 -8 9.21 1.72 0 12 -8 10.77 1.89 0 12 -8 7.27 1.47 0 12 -8 8.62 1.66 0 -12 -8 9.10 1.72 0 12 -8 6.57 1.42 0 12 8 9.24 1.66 0 12 -8 11.28 1.85 0 12 8 9.73 1.76 0 12 8 8.16 1.59 0 12 -9 8.55 1.69 0 12 9 8.64 1.60 0 -12 9 10.13 1.79 0 12 -9 8.12 1.61 0 12 9 9.62 1.80 0 12 -9 7.67 1.67 0 12 -9 6.36 1.29 0 12 -9 8.79 1.69 0 12 9 9.24 1.66 0 12 9 7.95 1.56 0 -12 -9 8.91 1.69 0 -12 -9 7.60 1.43 0 12 -9 7.26 1.44 0 -12 10 21.20 2.56 0 12 10 16.37 2.15 0 -12 -10 16.64 2.23 0 12 10 19.68 2.47 0 -12 -10 18.01 2.44 0 12 -10 19.04 2.41 0 12 -10 17.03 2.21 0 -12 10 17.58 2.32 0 12 -10 16.25 2.16 0 12 10 17.69 2.28 0 12 -10 17.35 2.29 0 12 -10 15.57 2.15 0 12 10 19.40 2.46 0 12 -11 19.83 2.33 0 12 -11 18.64 2.38 0 12 11 20.13 2.54 0 12 11 21.38 2.41 0 12 -11 18.75 2.34 0 12 11 20.32 2.56 0 -12 -11 22.95 2.65 0 -12 11 23.10 2.57 0 12 -11 23.98 2.68 0 12 -11 22.88 2.63 0 -12 -11 20.89 2.45 0 12 11 23.13 2.61 0 -12 11 23.80 2.75 0 12 12 32.25 3.06 0 -12 -12 30.31 2.99 0 12 12 33.80 3.22 0 -12 -12 33.56 3.22 0 12 -12 33.35 3.14 0 12 -12 37.76 3.41 0 12 -12 30.37 3.01 0 -12 12 30.35 3.00 0 -12 12 30.40 2.97 0 12 12 35.15 3.29 0 12 -12 29.28 2.94 0 -12 13 256.17 10.32 0 12 13 291.91 11.22 0 -12 -13 270.48 10.78 0 -12 13 285.45 10.94 0 12 -13 294.43 11.04 0 12 -13 249.39 10.41 0 12 -13 281.70 11.02 0 -12 -13 305.17 11.34 0 12 -13 277.33 10.82 0 12 13 266.79 10.68 0 12 13 284.16 10.95 0 12 14 2.38 0.83 0 12 14 4.12 1.24 0 -12 -14 1.94 0.73 0 12 -14 2.01 0.84 0 -12 -14 1.73 0.82 0 12 -14 3.34 1.09 0 12 -14 2.14 0.88 0 12 -14 1.76 0.82 0 12 14 2.58 0.97 0 -12 14 1.97 0.84 0 12 15 27.22 2.62 0 -12 -15 33.29 3.09 0 -12 -15 28.87 2.83 0 -12 15 27.78 2.72 0 12 15 32.39 3.06 0 -12 -15 26.26 2.58 0 12 -15 30.37 2.83 0 12 15 30.47 2.88 0 12 -15 28.75 2.77 0 12 -15 29.06 2.79 0 12 -15 30.53 2.89 0 -12 -16 4.99 1.17 0 12 -16 6.39 1.24 0 -12 -16 5.28 1.10 0 12 -16 6.45 1.34 0 -12 -16 5.93 1.36 0 12 16 5.61 1.20 0 12 -16 5.32 1.25 0 12 16 5.85 1.25 0 -12 16 4.69 1.12 0 12 17 10.14 1.65 0 -12 -17 9.44 1.57 0 12 -17 9.12 1.47 0 -12 -17 11.97 1.75 0 12 17 9.28 1.47 0 12 -17 9.65 1.51 0 12 -17 9.21 1.48 0 12 -18 8.21 1.29 0 12 -18 6.39 1.11 0 -12 -18 11.07 1.63 0 -12 -18 9.33 1.48 0 12 18 10.20 1.60 0 12 18 8.60 1.36 0 12 -18 10.39 1.52 0 12 -18 10.30 1.55 0 -12 -19 1.36 0.60 0 -12 -19 2.71 0.79 0 12 19 2.47 0.70 0 12 -19 1.96 0.76 0 -12 -19 2.35 0.76 0 12 19 1.43 0.53 0 12 -19 2.57 0.75 0 12 -19 1.92 0.62 0 -12 -20 1.16 0.48 0 12 -20 1.91 0.61 0 12 -20 1.26 0.54 0 12 20 1.27 0.53 0 -12 -20 2.21 0.67 0 12 -20 2.38 0.66 0 13 0 -0.27 0.93 0 -13 0 1.49 1.08 0 13 0 -0.16 0.51 0 13 0 -0.41 0.62 0 13 0 0.80 0.73 0 13 -1 4.92 1.41 0 13 1 5.60 1.30 0 13 -1 4.73 1.12 0 13 -1 6.42 1.53 0 -13 1 3.72 0.91 0 13 1 4.15 1.12 0 13 1 5.63 1.35 0 13 1 5.60 1.31 0 -13 -1 4.81 1.37 0 13 1 4.58 1.39 0 -13 2 18.90 2.42 0 13 2 18.41 2.29 0 13 2 22.31 2.69 0 13 2 20.99 2.54 0 -13 -2 21.33 2.60 0 13 -2 21.34 2.68 0 13 -2 19.19 2.38 0 13 2 19.59 2.45 0 13 -2 18.71 2.37 0 13 2 20.67 2.50 0 13 3 3.31 1.05 0 13 -3 3.70 1.32 0 -13 -3 4.67 1.14 0 13 -3 2.40 0.91 0 13 3 3.84 1.28 0 13 -3 3.49 1.03 0 -13 3 2.92 0.94 0 13 3 2.49 1.03 0 13 3 3.29 0.91 0 13 3 3.58 1.12 0 -13 3 4.02 1.20 0 13 -4 53.20 3.97 0 13 4 55.96 4.32 0 13 -4 62.62 4.56 0 -13 4 57.78 4.25 0 13 -4 66.26 4.56 0 13 4 66.40 4.61 0 13 4 60.06 4.39 0 13 4 62.45 4.50 0 13 5 1.50 0.89 0 13 5 1.02 0.89 0 -13 -5 0.99 0.49 0 13 5 1.24 0.78 0 13 5 0.53 0.45 0 13 -5 -0.01 0.77 0 -13 5 1.00 0.59 0 13 6 57.03 4.25 0 13 6 55.22 4.13 0 -13 -6 47.64 3.79 0 13 6 50.81 4.03 0 -13 6 48.03 3.69 0 13 6 55.32 4.15 0 13 -6 53.43 4.14 0 13 7 -0.41 0.60 0 -13 7 0.67 0.83 0 13 7 0.60 0.66 0 13 7 0.72 0.58 0 -13 -7 -0.32 0.59 0 13 7 -1.09 0.71 0 13 -7 -0.16 0.57 0 13 8 30.08 2.94 0 -13 -8 31.57 3.07 0 13 8 32.92 3.15 0 13 8 37.61 3.39 0 -13 8 35.15 3.28 0 13 -8 30.38 2.80 0 13 -8 34.61 3.17 0 13 8 31.35 3.06 0 13 9 3.40 1.00 0 -13 -9 3.82 1.15 0 13 9 3.91 1.20 0 13 -9 4.10 1.23 0 13 9 3.79 1.02 0 13 9 3.39 1.18 0 13 -9 3.47 1.05 0 -13 9 4.14 1.16 0 -13 9 5.07 1.31 0 13 -10 7.23 1.34 0 13 10 9.69 1.65 0 13 10 11.33 1.80 0 -13 -10 8.21 1.51 0 13 -10 6.64 1.32 0 13 10 9.65 1.70 0 13 10 7.59 1.43 0 -13 10 11.14 1.79 0 -13 10 7.96 1.52 0 -13 11 62.19 4.18 0 13 -11 56.35 3.97 0 13 11 65.61 4.44 0 13 11 53.46 3.77 0 13 -11 58.41 4.14 0 13 11 70.44 4.48 0 -13 11 65.52 4.38 0 13 11 62.35 4.28 0 -13 -11 66.74 4.48 0 -13 12 24.40 2.47 0 13 12 27.02 2.65 0 -13 -12 21.08 2.26 0 -13 -12 27.60 2.76 0 13 12 27.02 2.74 0 13 -12 22.25 2.38 0 -13 12 29.25 2.81 0 13 -12 26.96 2.67 0 13 12 27.67 2.73 0 -13 -13 28.39 2.77 0 13 -13 26.53 2.65 0 -13 13 28.27 2.68 0 -13 -13 22.27 2.31 0 13 13 27.56 2.66 0 13 -13 21.17 2.21 0 13 -13 23.72 2.42 0 13 13 30.15 2.82 0 -13 -14 13.06 1.73 0 -13 14 16.96 1.97 0 13 -14 18.08 2.01 0 13 -14 12.24 1.62 0 13 14 17.51 2.06 0 13 14 18.81 2.20 0 -13 -14 17.18 2.10 0 13 -14 16.08 2.01 0 13 -15 8.59 1.37 0 -13 -15 7.01 1.19 0 13 15 9.00 1.51 0 -13 15 8.30 1.35 0 13 -15 7.64 1.24 0 -13 -15 10.52 1.65 0 13 15 10.09 1.52 0 13 -15 10.48 1.60 0 13 16 99.44 5.09 0 -13 -16 89.45 4.68 0 13 -16 97.95 4.88 0 -13 -16 103.42 5.09 0 13 -16 99.33 4.89 0 13 16 96.72 4.90 0 13 -17 6.53 1.11 0 -13 -17 5.28 1.06 0 13 17 4.43 0.92 0 13 -17 3.11 0.75 0 13 17 4.96 1.02 0 -13 -17 5.66 1.06 0 -13 -17 5.16 1.01 0 13 -18 24.00 2.05 0 13 18 21.42 2.02 0 -13 -18 27.04 2.24 0 -14 0 206.70 8.82 0 14 0 192.91 8.44 0 14 0 201.33 8.68 0 14 0 213.27 8.96 0 14 1 7.14 1.48 0 -14 1 8.41 1.58 0 14 1 5.11 1.17 0 -14 -1 6.28 1.40 0 14 1 5.77 1.34 0 14 -1 5.56 1.22 0 14 -1 10.35 1.82 0 14 -1 5.69 1.32 0 -14 1 5.85 1.32 0 -14 2 36.67 3.15 0 -14 -2 42.41 3.55 0 14 -2 38.25 3.29 0 14 2 40.93 3.44 0 -14 2 42.39 3.45 0 14 2 35.02 3.00 0 14 -2 35.74 3.11 0 14 2 39.35 3.36 0 14 -2 44.13 3.60 0 14 3 43.39 3.60 0 14 3 44.63 3.63 0 -14 -3 49.48 3.91 0 14 -3 42.12 3.31 0 -14 3 41.69 3.40 0 14 3 49.42 3.81 0 14 -3 45.89 3.69 0 -14 4 108.86 5.79 0 14 4 120.90 6.35 0 -14 -4 123.73 6.53 0 14 4 121.76 6.31 0 14 -4 123.25 6.42 0 14 4 123.22 6.31 0 -14 -5 0.79 0.49 0 -14 -5 0.38 0.78 0 14 5 0.49 0.67 0 14 5 0.35 0.48 0 14 -5 0.36 0.51 0 14 5 0.66 0.65 0 -14 5 1.59 0.83 0 14 -6 90.77 5.32 0 14 6 92.39 5.29 0 -14 6 93.96 5.44 0 14 6 90.80 5.31 0 -14 -6 81.47 4.89 0 -14 -6 94.28 5.44 0 14 6 90.54 5.24 0 -14 7 4.92 1.25 0 -14 -7 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4.31 2 10 -10 54.10 4.03 -2 10 9 118.78 6.49 2 10 -9 128.98 6.68 -2 10 9 139.71 7.00 -2 10 9 130.06 6.85 2 10 -9 128.81 6.68 2 -10 9 102.27 11.68 -2 10 9 130.33 6.83 2 10 -9 135.32 6.93 -2 -10 -9 127.95 6.76 2 10 -9 129.42 6.73 -2 10 9 100.48 11.42 -2 -10 -9 128.75 6.71 -2 -10 -9 95.73 11.31 -2 10 9 135.90 7.01 2 10 -8 94.11 5.52 2 10 -8 87.38 5.32 -2 10 8 93.21 5.50 2 10 -8 83.91 5.33 -2 -10 -8 60.96 8.85 2 -10 8 73.80 9.76 -2 10 8 86.78 5.39 -2 10 8 88.24 5.38 -2 -10 -8 86.44 5.34 2 10 -8 87.41 5.35 -2 -10 -8 77.54 5.03 -2 10 8 89.73 5.48 2 10 -8 87.90 5.37 -2 -10 -8 60.88 8.72 -2 10 8 87.17 10.42 -2 10 8 84.81 5.30 2 10 -7 21.08 2.50 -2 10 7 16.36 2.06 2 -10 7 16.42 4.71 -2 10 7 19.16 2.36 2 10 -7 18.61 2.36 2 10 -7 15.64 2.16 -2 10 7 18.12 2.33 -2 -10 -7 17.55 2.28 2 10 -7 18.20 2.30 -2 10 7 20.33 2.41 -2 -10 -7 11.76 3.92 -2 -10 -7 18.33 2.29 -2 10 7 19.01 2.38 -2 10 7 16.70 4.49 -2 10 7 17.13 2.19 2 10 -7 17.17 2.25 2 10 -6 182.11 8.34 -2 10 6 195.73 8.48 2 10 -6 195.88 8.52 2 10 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10 2 37.30 3.27 -2 10 -2 33.24 3.00 -2 10 -2 40.88 3.43 -2 -10 3 4.70 1.07 -2 10 -3 5.76 1.22 2 10 3 6.04 1.38 -2 10 -3 2.72 1.82 -2 10 -3 6.72 1.36 2 10 3 8.45 3.15 2 10 3 4.47 1.09 2 10 3 4.51 1.08 2 10 3 4.84 1.13 -2 10 -3 6.15 1.37 -2 -10 3 7.90 1.55 -2 -10 3 4.39 1.01 2 10 3 6.24 1.29 2 10 3 6.09 1.23 -2 -10 3 2.46 1.92 -2 10 -3 5.94 1.42 2 10 4 111.63 6.13 2 10 4 92.27 10.61 -2 -10 4 102.85 5.73 -2 10 -4 97.83 10.63 2 10 4 106.93 5.93 -2 10 -4 118.23 6.15 -2 10 -4 111.23 6.07 2 10 4 110.40 5.94 -2 -10 4 104.64 5.80 2 10 4 102.78 5.72 -2 -10 4 91.70 10.45 2 10 4 117.16 6.06 -2 -10 4 94.70 5.33 -2 10 -4 99.73 5.69 2 10 4 107.22 6.02 -2 10 -4 111.13 5.94 -2 10 -4 105.01 5.88 2 10 5 21.61 2.48 -2 -10 5 20.32 2.33 -2 10 -5 17.34 4.28 -2 -10 5 18.14 4.54 2 10 5 22.27 2.48 2 10 5 23.02 2.57 -2 10 -5 23.22 2.60 2 10 5 22.24 5.14 -2 10 -5 23.65 2.66 -2 -10 5 21.99 2.48 -2 10 -5 23.29 2.52 2 10 5 24.00 2.62 2 10 5 22.11 2.50 -2 -10 5 22.35 2.51 2 10 5 25.15 2.71 -2 10 -5 22.55 2.51 -2 10 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4.84 -2 10 -12 85.21 5.39 -2 10 -12 79.77 5.25 -2 10 -13 24.11 2.74 -2 10 -13 20.03 2.54 -2 -10 13 21.12 2.52 2 10 13 20.68 2.60 2 10 13 24.91 2.83 -2 10 -13 22.97 2.67 -2 10 -13 23.86 2.76 -2 -10 13 21.34 2.54 -2 -10 13 23.03 2.62 2 10 13 23.42 2.71 -2 10 -14 17.93 2.30 -2 10 -14 14.88 2.15 -2 -10 14 12.92 2.00 -2 -10 14 14.93 2.13 -2 10 -14 15.46 2.19 2 10 14 17.59 2.42 2 10 14 12.98 2.01 -2 -10 14 13.68 1.94 2 10 14 16.41 2.27 -2 10 -14 12.27 2.01 -2 10 -15 90.63 5.53 -2 -10 15 90.13 5.45 2 10 15 83.90 5.48 -2 10 -15 94.77 5.72 2 10 15 90.08 5.67 -2 10 -15 88.64 5.46 -2 -10 15 88.20 5.41 2 10 15 88.94 5.55 -2 -10 15 93.38 5.54 2 10 15 86.13 5.41 -2 10 -15 91.42 5.58 -2 10 -16 14.21 2.10 -2 10 -16 13.88 2.03 -2 -10 16 17.07 2.22 2 10 16 16.16 2.28 2 10 16 12.72 1.91 2 10 16 16.59 2.34 -2 -10 16 13.32 1.94 -2 10 -16 13.02 1.88 -2 -10 16 14.39 2.03 2 10 16 13.87 2.12 -2 10 -16 14.38 2.11 2 -10 -16 15.77 2.19 -2 10 -16 15.49 2.15 -2 10 -17 37.95 3.36 2 -10 -17 42.43 3.62 -2 -10 17 36.76 3.29 -2 10 -17 39.33 3.49 -2 10 -17 37.38 3.40 2 10 17 35.95 3.39 2 10 17 42.07 3.57 2 10 17 34.96 3.13 2 10 17 33.86 3.25 -2 10 -17 35.83 3.08 -2 -10 17 40.77 3.47 -2 10 -17 38.28 3.45 -2 10 -18 9.03 1.65 -2 10 -18 10.16 1.77 2 10 18 9.47 1.72 -2 10 -18 9.83 1.73 2 10 18 10.95 1.71 -2 -10 18 7.37 1.37 2 -10 -18 7.69 1.54 2 10 18 6.72 1.32 -2 -10 18 10.40 1.67 2 10 18 9.38 1.65 -2 10 -18 9.30 1.59 2 10 19 17.06 2.24 -2 10 -19 19.81 2.30 -2 -10 19 14.96 1.89 -2 10 -19 17.48 2.16 2 -10 -19 19.73 2.36 -2 10 -19 21.51 2.48 -2 -10 19 19.66 2.30 2 10 19 17.57 2.17 2 10 19 17.17 2.12 -2 10 -19 20.04 2.32 -2 10 -20 3.54 1.01 -2 10 -20 3.46 1.03 2 10 20 2.90 0.88 2 10 20 3.12 0.90 -2 10 -20 4.17 1.08 2 -10 -20 2.92 0.90 -2 10 -20 2.80 0.88 -2 -10 20 3.23 0.86 2 10 20 2.35 0.87 2 10 21 23.61 2.36 -2 10 -21 24.10 2.41 2 10 21 27.61 2.66 -2 10 -21 25.70 2.52 2 10 21 22.89 2.30 -2 -10 21 26.31 2.49 2 -10 -21 31.73 2.81 -2 10 -21 27.81 2.60 -2 10 -21 30.76 2.70 -2 10 -22 5.76 1.15 -2 10 -22 4.69 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11 -18 3.31 0.93 -2 11 18 2.43 0.72 -2 -11 -18 4.15 1.10 -2 -11 -18 3.86 1.10 -2 -11 -17 64.22 4.30 -2 11 17 61.94 4.25 -2 11 17 55.05 3.79 2 11 -17 62.20 4.20 2 11 -17 50.78 3.76 2 11 -17 56.78 4.12 -2 -11 -17 57.42 3.92 -2 -11 -17 66.23 4.35 2 11 -17 60.92 4.15 2 11 -16 36.05 3.16 2 11 -16 42.93 3.58 -2 11 16 47.47 3.70 -2 11 16 34.68 3.09 -2 -11 -16 36.87 3.27 -2 -11 -16 39.33 3.43 -2 -11 -16 44.47 3.59 2 11 -16 42.80 3.49 2 11 -16 47.82 3.68 2 11 -15 116.02 6.14 -2 11 15 110.68 6.09 2 11 -15 107.25 5.97 2 11 -15 111.57 6.10 2 11 -15 105.07 6.02 -2 -11 -15 115.52 6.21 -2 -11 -15 113.79 6.17 2 11 -15 91.19 5.49 -2 -11 -15 104.08 5.90 -2 11 15 98.93 5.70 2 11 -14 5.51 1.28 2 11 -14 4.54 1.13 2 11 -14 5.93 1.41 -2 11 14 4.00 1.19 2 11 -14 8.19 1.52 -2 11 14 7.37 1.46 -2 -11 -14 7.30 1.54 2 11 -14 6.81 1.57 -2 -11 -14 5.32 1.32 2 11 -14 7.30 1.38 2 11 -13 13.39 1.93 2 11 -13 16.44 2.25 2 11 -13 13.59 2.06 2 11 -13 14.39 2.11 -2 11 13 16.59 2.32 2 11 -13 13.98 2.05 -2 11 13 14.26 2.14 -2 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103.00 6.05 2 11 -8 103.89 6.04 -2 11 8 110.03 6.23 -2 -11 -8 99.60 5.86 2 11 -8 104.81 6.06 -2 -11 -8 112.22 6.27 -2 11 8 111.38 6.24 2 11 -8 107.69 6.14 2 11 -8 103.04 6.04 -2 11 7 46.01 3.83 2 11 -7 48.29 3.91 2 11 -7 45.02 3.73 2 11 -7 43.74 3.63 -2 -11 -7 42.52 3.71 -2 11 7 48.73 3.98 -2 -11 -7 44.11 3.61 -2 11 7 45.98 3.81 2 11 -7 44.84 3.77 2 11 -7 49.42 4.02 -2 11 7 42.78 3.74 2 11 -7 45.28 3.85 2 11 -6 61.41 4.31 2 11 -6 63.05 4.45 -2 11 6 67.29 4.69 -2 -11 -6 41.45 7.45 2 -11 6 50.23 8.40 -2 11 6 67.69 4.66 2 11 -6 67.80 4.71 -2 -11 -6 61.07 4.30 2 11 -6 69.00 4.78 -2 11 6 62.02 4.30 -2 11 6 73.46 4.92 -2 -11 -6 65.39 4.60 2 11 -6 66.44 4.71 -2 11 6 67.91 4.77 2 11 -6 69.75 4.82 2 11 -5 81.13 5.20 2 11 -5 76.91 5.07 -2 11 5 77.39 5.03 2 11 -5 73.08 4.71 -2 11 5 60.47 8.87 -2 11 5 78.83 5.06 2 11 -5 73.48 4.93 2 11 -5 71.94 4.86 -2 -11 -5 67.37 4.72 2 -11 5 64.57 9.60 -2 11 5 65.33 4.50 -2 11 5 72.88 4.90 -2 -11 -5 47.30 8.06 -2 11 5 77.49 5.10 -2 11 4 54.84 8.36 2 11 -4 63.54 4.40 -2 11 4 70.26 4.75 2 11 -4 63.78 4.61 2 -11 4 46.06 8.10 2 11 -4 63.89 4.55 2 11 -4 61.94 4.48 -2 -11 -4 61.49 4.41 -2 -11 -4 49.41 8.04 -2 11 4 62.62 4.42 -2 11 4 66.90 4.64 2 11 -4 68.20 4.69 -2 11 4 70.56 4.71 -2 11 4 63.04 4.61 2 11 -3 176.98 8.26 2 11 -3 169.32 7.94 -2 -11 -3 121.53 12.95 -2 11 3 183.16 8.29 2 11 -3 163.82 7.88 -2 11 3 125.00 13.11 -2 -11 -3 177.30 8.10 -2 -11 -3 166.58 7.82 -2 11 3 169.30 7.97 -2 11 3 186.13 8.26 2 11 -3 167.03 7.96 2 -11 3 131.88 14.10 -2 -11 -3 179.02 8.24 2 11 -3 170.65 8.06 -2 11 3 181.81 8.37 2 11 -2 177.30 8.23 2 11 -2 168.32 7.88 2 11 -2 180.73 8.14 -2 -11 -2 129.74 13.39 -2 11 2 190.89 8.37 2 11 -2 158.25 7.57 2 -11 2 146.08 14.79 2 11 -2 178.02 8.15 -2 -11 -2 169.85 7.95 -2 11 2 172.07 8.05 -2 -11 -2 154.48 7.52 -2 11 2 186.88 8.30 -2 -11 -2 175.47 8.15 -2 11 2 144.69 14.03 2 11 -2 171.83 7.96 -2 -11 -2 176.48 8.08 2 11 -2 148.51 7.55 -2 11 2 180.85 8.34 -2 -11 -1 106.44 6.05 -2 11 1 105.69 6.00 -2 11 1 111.51 6.10 2 11 -1 99.02 5.66 2 11 -1 91.39 5.53 -2 11 1 115.74 6.23 2 11 -1 99.38 5.72 -2 -11 -1 78.12 10.11 2 11 -1 105.37 6.09 2 11 -1 104.66 5.91 2 11 -1 91.46 5.49 2 11 -1 111.53 6.07 -2 -11 -1 100.51 5.80 -2 -11 -1 103.99 5.88 -2 11 1 90.89 11.00 2 11 -1 108.22 6.04 2 -11 1 93.22 11.68 -2 11 1 104.96 6.10 2 11 0 151.25 7.48 2 11 0 151.31 7.35 -2 11 0 155.73 7.45 2 11 0 115.09 12.51 -2 11 0 120.96 12.83 -2 11 0 160.28 7.53 -2 -11 0 155.67 7.50 -2 11 0 152.04 7.44 2 11 0 138.15 7.03 -2 -11 0 121.00 12.75 2 11 0 147.33 7.29 2 -11 0 138.52 14.30 2 11 0 131.34 6.81 2 11 0 146.68 7.09 -2 -11 0 143.62 7.12 2 11 0 132.59 6.76 2 11 0 148.97 7.38 -2 -11 0 136.55 6.98 -2 11 0 152.77 7.46 2 11 1 106.21 6.03 -2 -11 1 99.10 5.69 2 11 1 108.13 6.02 2 11 1 96.01 5.58 -2 11 -1 113.99 6.20 -2 11 -1 110.41 6.15 2 11 1 99.60 5.78 -2 -11 1 78.39 10.08 -2 -11 1 104.65 5.97 2 -11 -1 90.10 11.54 2 11 1 84.31 5.22 2 11 1 109.50 6.05 -2 -11 1 100.38 5.70 2 11 1 74.75 10.03 2 11 1 105.08 6.00 -2 11 -1 107.36 6.08 -2 11 -1 84.68 10.63 -2 11 -2 131.95 13.50 2 11 2 176.54 8.14 2 11 2 168.93 8.09 2 11 2 168.17 7.83 -2 -11 2 177.15 8.17 -2 11 -2 182.57 8.29 2 11 2 168.48 7.99 -2 -11 2 135.19 13.53 2 -11 -2 154.51 15.38 -2 -11 2 176.28 7.99 2 11 2 141.34 14.13 -2 11 -2 194.03 8.48 2 11 2 174.99 8.16 -2 -11 2 166.94 7.77 2 11 2 179.27 8.29 -2 11 -2 178.18 8.32 2 11 3 181.10 8.35 -2 11 -3 195.60 8.54 -2 11 -3 127.37 13.18 2 11 3 148.62 14.53 -2 -11 3 159.98 7.54 -2 -11 3 175.11 8.08 -2 11 -3 163.33 7.70 -2 11 -3 184.98 8.45 -2 -11 3 138.29 13.74 2 -11 -3 145.53 15.08 -2 11 -3 177.74 8.17 2 11 3 182.60 8.29 2 11 3 159.82 7.74 2 11 3 172.10 8.11 2 11 3 180.31 8.18 2 11 3 175.75 8.23 -2 -11 3 160.51 7.69 2 11 4 67.72 4.71 2 11 4 64.40 4.56 2 11 4 57.32 4.23 -2 11 -4 74.80 4.99 -2 11 -4 67.59 4.64 2 11 4 49.19 8.29 2 11 4 66.06 4.63 -2 -11 4 60.51 4.40 -2 -11 4 62.89 4.35 -2 -11 4 46.75 7.68 2 -11 -4 40.52 7.75 2 11 4 65.59 4.60 2 11 4 63.85 4.57 -2 -11 4 64.56 4.46 -2 11 -4 41.93 7.33 -2 11 -4 56.20 4.16 2 11 5 74.96 4.96 2 11 5 56.54 8.79 2 11 5 75.50 4.97 -2 11 -5 72.57 4.86 -2 11 -5 76.93 5.13 2 11 5 78.07 4.96 2 11 5 77.06 5.01 2 11 5 78.27 5.17 -2 -11 5 71.77 4.79 -2 -11 5 71.77 4.75 2 -11 -5 59.59 9.52 -2 -11 5 78.27 4.99 2 11 5 75.46 5.02 -2 -11 5 61.78 8.92 -2 11 -5 67.25 4.65 2 11 6 72.99 4.95 -2 11 -6 73.39 4.98 2 11 6 70.73 4.81 -2 11 -6 64.05 4.56 -2 11 -6 69.25 4.75 -2 11 -6 63.91 4.54 -2 -11 6 67.04 4.55 -2 -11 6 59.73 4.33 2 11 6 65.77 4.60 2 11 6 71.99 4.85 2 11 6 61.02 4.44 -2 -11 6 73.81 4.81 2 11 6 60.78 4.48 2 11 7 48.10 3.94 2 11 7 41.75 3.58 -2 -11 7 42.58 3.53 -2 -11 7 48.97 3.96 -2 11 -7 49.03 4.01 2 11 7 44.89 3.76 2 11 7 46.81 3.91 -2 -11 7 48.69 3.78 -2 11 -7 45.25 3.77 -2 11 -7 48.29 3.96 2 11 7 51.30 4.03 -2 11 -7 40.88 3.55 -2 11 -7 47.00 3.89 2 11 7 43.89 3.66 -2 -11 7 45.96 3.76 2 11 8 107.08 6.25 2 11 8 118.54 6.40 -2 -11 8 105.03 5.90 -2 11 -8 117.01 6.44 -2 11 -8 108.39 6.21 -2 11 -8 109.97 6.20 2 11 8 94.07 5.71 -2 -11 8 114.77 6.24 2 11 8 96.07 5.70 -2 -11 8 103.18 5.91 2 11 8 108.30 6.24 2 11 8 101.69 5.95 -2 11 -8 104.05 6.06 2 11 9 63.42 4.67 2 11 9 56.92 4.25 -2 11 -9 64.84 4.71 -2 -11 9 70.97 4.71 2 11 9 68.61 4.81 -2 11 -9 72.79 4.95 2 11 9 68.53 4.75 -2 -11 9 66.46 4.53 -2 11 -9 71.80 4.86 -2 -11 9 71.83 4.82 2 11 9 62.05 4.54 -2 11 -9 67.94 4.75 2 11 10 106.36 6.09 2 11 10 100.09 5.97 2 11 10 85.86 5.30 -2 11 -10 103.27 5.95 -2 -11 10 105.76 6.01 2 11 10 102.26 6.02 -2 11 -10 103.20 6.05 -2 -11 10 99.00 5.73 -2 -11 10 99.97 5.89 2 11 10 88.81 5.62 -2 11 -10 98.80 5.82 -2 11 -10 97.31 5.78 2 11 10 94.89 5.76 2 11 11 21.99 2.66 -2 -11 11 21.68 2.55 2 11 11 21.94 2.60 -2 -11 11 23.03 2.70 -2 11 -11 22.69 2.63 2 11 11 21.45 2.56 -2 -11 11 22.84 2.60 -2 -11 11 21.04 2.41 -2 11 -11 21.98 2.66 2 11 11 22.34 2.64 -2 11 -11 19.96 2.45 2 11 11 19.32 2.40 -2 -11 12 27.12 2.83 -2 -11 12 28.92 2.96 2 11 12 26.11 2.87 -2 11 -12 30.56 3.16 -2 11 -12 24.42 2.75 2 -11 -12 25.25 2.73 -2 11 -12 29.36 3.07 2 11 12 29.03 2.98 2 11 12 28.20 2.99 -2 -11 12 25.85 2.81 2 11 12 30.79 3.05 -2 -11 12 25.15 2.67 2 11 12 22.32 2.54 2 11 13 18.13 2.43 2 11 13 16.38 2.24 2 -11 -13 14.80 2.06 2 11 13 14.41 2.10 2 11 13 16.01 2.26 -2 11 -13 14.31 2.04 -2 -11 13 15.37 2.13 -2 11 -13 14.79 2.12 -2 -11 13 16.74 2.22 -2 -11 13 15.20 2.16 -2 11 -13 15.85 2.18 -2 11 -14 6.20 1.45 2 11 14 4.19 1.31 -2 11 -14 6.04 1.36 2 11 14 5.84 1.39 -2 -11 14 6.72 1.41 2 11 14 4.71 1.30 2 -11 -14 6.36 1.40 -2 -11 14 6.23 1.39 -2 11 -14 5.20 1.23 -2 11 -14 4.75 1.19 -2 -11 14 6.91 1.45 2 11 14 6.89 1.54 -2 11 -15 113.00 6.13 -2 -11 15 109.82 6.01 -2 11 -15 108.33 6.04 2 11 15 106.02 5.98 -2 -11 15 104.62 5.87 2 -11 -15 103.90 5.90 2 11 15 115.22 6.21 2 11 15 104.98 5.91 -2 11 -15 104.49 5.83 -2 -11 15 104.92 5.92 2 11 15 99.65 5.91 -2 11 -15 109.85 6.03 2 11 16 36.22 3.29 -2 11 -16 42.36 3.50 -2 11 -16 44.08 3.60 2 11 16 41.12 3.47 2 -11 -16 40.97 3.49 -2 -11 16 42.01 3.42 -2 11 -16 40.08 3.28 2 11 16 42.37 3.41 -2 -11 16 43.41 3.50 2 11 16 40.90 3.43 -2 11 -16 41.06 3.45 -2 -11 16 42.28 3.44 2 11 17 55.43 4.06 -2 11 -17 61.49 4.16 -2 -11 17 63.54 4.21 2 11 17 63.37 4.29 2 -11 -17 59.80 4.18 2 11 17 55.05 3.95 -2 11 -17 53.21 3.71 2 11 17 53.84 3.79 -2 -11 17 64.76 4.26 -2 11 -17 64.36 4.31 -2 11 -17 62.76 4.18 -2 11 -18 3.05 0.99 2 11 18 2.51 0.84 2 -11 -18 1.81 0.54 -2 -11 18 2.75 0.87 2 11 18 3.43 1.01 -2 11 -18 3.05 0.98 2 11 18 2.70 0.77 -2 -11 18 3.12 0.94 -2 11 -18 2.69 0.88 2 11 18 1.52 0.64 -2 11 -19 8.31 1.43 2 11 19 8.59 1.45 -2 11 -19 10.82 1.65 -2 11 -19 7.89 1.40 2 -11 -19 9.79 1.55 2 11 19 7.04 1.30 -2 -11 19 9.88 1.50 2 11 19 7.51 1.32 -2 11 -20 6.29 1.19 -2 11 -20 6.67 1.23 2 11 20 5.03 1.04 2 11 20 4.59 0.97 -2 -11 20 5.23 1.02 2 11 20 4.90 1.01 2 -11 -20 8.13 1.38 2 -11 -20 5.33 1.12 -2 11 -21 11.01 1.47 2 11 21 7.98 1.18 -2 -11 21 8.61 1.25 2 -11 -21 11.18 1.49 2 -11 -21 11.04 1.47 2 11 21 7.66 1.21 -2 11 -21 11.66 1.50 2 11 21 7.15 1.12 -2 11 -22 2.72 0.74 2 -11 -22 0.42 0.33 2 -11 -22 1.90 0.62 2 12 -20 1.88 0.58 -2 -12 -20 2.42 0.66 -2 12 20 1.01 0.44 2 12 -19 1.65 0.57 -2 -12 -19 1.44 0.54 2 12 -19 2.10 0.68 -2 -12 -19 1.76 0.60 -2 -12 -19 2.02 0.65 2 12 -19 2.49 0.72 -2 -12 -19 2.07 0.67 -2 12 19 1.26 0.57 -2 12 18 18.78 2.06 2 12 -18 20.22 2.09 2 12 -18 17.60 1.97 -2 -12 -18 19.69 2.10 -2 -12 -18 19.67 2.08 -2 -12 -18 18.33 1.98 2 12 -18 19.12 2.03 -2 12 17 8.34 1.47 -2 -12 -17 8.36 1.41 2 12 -17 7.43 1.31 -2 -12 -17 6.33 1.17 -2 12 17 6.08 1.07 2 12 -17 8.72 1.43 2 12 -17 8.45 1.41 -2 -12 -17 8.82 1.45 -2 -12 -17 10.36 1.57 2 12 -16 1.50 0.64 -2 12 16 -0.11 0.29 -2 -12 -16 0.39 0.57 -2 12 16 1.31 0.69 -2 -12 -16 0.40 0.38 2 12 -16 0.90 0.62 2 12 -16 1.49 0.77 -2 -12 -15 21.18 2.40 -2 12 15 19.67 2.27 2 12 -15 16.34 2.10 -2 -12 -15 18.97 2.28 -2 12 15 15.31 1.98 2 12 -15 20.17 2.27 -2 -12 -15 18.33 2.21 2 12 -15 18.82 2.20 2 12 -14 6.94 1.37 -2 -12 -14 7.78 1.49 -2 -12 -14 8.83 1.57 -2 12 14 8.11 1.52 -2 12 14 5.67 1.23 -2 -12 -14 11.69 1.91 2 12 -14 8.59 1.55 2 12 -14 6.78 1.35 -2 12 13 27.92 2.77 -2 -12 -13 31.50 3.06 -2 -12 -13 27.79 2.88 2 12 -13 24.08 2.65 2 12 -13 31.11 2.93 -2 12 13 30.12 2.95 2 12 -13 26.37 2.63 -2 -12 -13 27.37 2.83 2 12 -13 25.67 2.67 -2 -12 -12 83.39 5.19 -2 12 12 80.17 5.03 -2 -12 -12 72.47 4.83 2 12 -12 70.61 4.78 2 12 -12 81.68 5.05 2 12 -12 77.05 4.95 -2 -12 -12 86.43 5.30 -2 12 12 82.01 5.09 2 12 -12 74.66 4.79 2 12 -12 69.96 4.67 2 12 -11 158.05 7.47 -2 12 11 155.20 7.45 2 12 -11 138.20 7.13 -2 -12 -11 152.08 7.51 -2 -12 -11 134.76 7.01 2 12 -11 152.56 7.33 -2 12 11 151.03 7.34 -2 -12 -11 155.76 7.55 2 12 -11 149.24 7.28 2 12 -11 137.75 6.99 2 12 -10 76.87 4.94 -2 12 10 72.84 4.89 2 12 -10 64.02 4.52 -2 -12 -10 73.23 4.96 -2 -12 -10 76.16 4.98 2 12 -10 68.36 4.68 -2 -12 -10 62.54 4.43 -2 12 10 64.66 4.38 -2 12 10 78.25 4.97 2 12 -10 73.76 4.86 2 12 -10 64.94 4.43 2 12 -10 69.23 4.60 2 12 -9 69.12 4.68 2 12 -9 70.39 4.79 -2 -12 -9 60.95 4.35 2 -12 9 61.88 4.29 -2 12 9 66.27 4.60 2 12 -9 67.67 4.60 -2 12 9 69.55 4.78 -2 -12 -9 67.36 4.69 -2 -12 -9 70.26 4.79 2 12 -9 57.76 4.27 -2 12 9 62.79 4.41 2 12 -9 61.93 4.39 2 12 -9 54.33 4.10 2 12 -8 67.56 4.64 -2 -12 -8 61.84 4.59 -2 -12 -8 55.61 4.13 -2 12 8 69.21 4.73 2 12 -8 67.62 4.63 -2 -12 -8 66.55 4.72 -2 12 8 71.42 4.82 2 12 -8 70.96 4.81 2 12 -8 62.42 4.41 -2 12 8 60.69 4.44 2 12 -8 60.60 4.28 2 12 -8 66.83 4.64 -2 12 7 52.92 4.13 -2 -12 -7 51.02 4.09 2 12 -7 49.31 3.96 2 12 -7 51.23 4.02 -2 -12 -7 49.23 4.01 -2 12 7 49.93 4.04 -2 12 7 54.03 4.18 2 12 -7 52.30 4.11 2 12 -7 51.92 4.15 -2 12 6 220.30 9.61 -2 12 6 227.05 9.61 -2 12 6 235.65 9.79 -2 -12 -6 210.15 9.39 2 12 -6 223.06 9.52 -2 12 6 194.45 8.74 2 12 -6 230.28 9.73 -2 -12 -6 227.18 9.65 -2 -12 -6 229.01 9.73 2 12 -6 204.64 9.21 2 12 -6 226.43 9.72 2 12 -5 1.76 0.69 2 12 -5 3.00 0.96 -2 12 5 3.69 1.10 -2 12 5 4.08 1.33 -2 -12 -5 3.55 1.06 -2 -12 -5 3.09 1.36 -2 12 5 3.79 1.07 2 12 -5 3.38 1.11 -2 -12 -5 5.33 1.36 2 12 -5 2.33 0.82 -2 12 5 2.13 0.99 -2 -12 -5 3.56 1.08 2 12 -5 2.68 1.15 -2 -12 -4 120.80 6.55 -2 -12 -4 97.93 5.74 -2 12 4 115.43 6.36 -2 -12 -4 101.38 5.88 -2 12 4 114.46 6.35 2 12 -4 95.67 5.75 2 12 -4 100.26 5.80 2 12 -4 107.72 6.09 -2 12 4 104.25 5.92 -2 -12 -4 113.52 6.28 2 12 -4 111.27 6.28 -2 12 4 107.80 6.28 2 12 -4 115.17 6.42 -2 12 3 32.57 3.16 -2 12 3 39.11 3.53 -2 12 3 41.03 3.64 -2 -12 -3 35.34 3.44 2 12 -3 35.27 3.27 -2 -12 -3 33.50 3.12 2 12 -3 36.14 3.31 -2 12 3 41.22 3.66 -2 -12 -3 36.53 3.35 2 12 -3 37.40 3.45 2 12 -3 32.56 3.13 2 12 -3 39.91 3.65 -2 -12 -2 67.87 4.69 -2 12 2 73.99 4.98 2 12 -2 67.41 4.68 2 12 -2 68.71 4.60 -2 12 2 72.94 4.96 2 12 -2 60.85 4.30 -2 -12 -2 76.92 5.14 -2 12 2 65.99 4.62 2 12 -2 60.12 4.35 -2 12 2 72.98 4.91 2 12 -2 71.79 4.88 2 12 -2 74.93 5.03 2 12 -1 46.60 3.87 -2 12 1 53.99 4.23 -2 12 1 54.18 4.19 -2 -12 -1 51.59 4.17 2 12 -1 40.31 3.46 2 12 -1 42.01 3.51 -2 12 1 48.26 3.94 -2 -12 -1 42.93 3.69 2 12 -1 46.72 3.87 2 12 -1 43.85 3.63 -2 12 1 53.17 4.16 2 12 -1 50.64 4.17 2 12 0 76.29 5.11 -2 -12 0 75.62 5.09 -2 12 0 77.92 5.12 2 12 0 68.96 4.67 2 12 0 69.92 4.78 2 12 0 74.56 5.01 -2 12 0 77.82 5.08 -2 -12 0 69.87 4.74 -2 12 0 74.32 4.99 2 12 0 76.71 5.08 -2 12 0 76.97 5.11 2 12 1 50.04 4.09 2 12 1 51.64 4.05 -2 12 -1 53.14 4.16 2 12 1 48.77 3.82 -2 -12 1 51.89 4.18 2 12 1 47.81 3.88 -2 -12 1 45.87 3.73 -2 12 -1 53.08 4.25 -2 12 -1 52.08 4.05 2 12 1 48.84 4.01 -2 12 -1 54.31 4.19 2 12 1 53.75 4.16 2 12 2 74.01 5.05 2 12 2 74.27 4.95 2 12 2 70.84 4.78 -2 12 -2 76.11 4.98 2 12 2 66.01 4.67 -2 -12 2 74.80 4.99 -2 12 -2 75.59 4.97 -2 -12 2 64.70 4.45 2 12 2 62.23 4.45 2 12 2 67.88 4.78 -2 12 -2 73.20 5.00 2 12 3 35.49 3.43 2 12 3 37.46 3.39 2 12 3 34.23 3.32 -2 -12 3 36.03 3.40 2 12 3 38.92 3.53 2 12 3 35.20 3.22 -2 12 -3 36.89 3.42 2 12 3 40.05 3.57 -2 12 -3 38.33 3.51 -2 -12 3 38.97 3.50 -2 12 -3 34.80 3.38 2 12 4 110.39 6.33 2 12 4 97.70 5.80 2 12 4 104.03 6.02 -2 12 -4 111.75 6.24 2 12 4 106.29 6.14 2 12 4 113.46 6.33 -2 -12 4 107.71 6.12 2 12 4 102.65 6.04 -2 -12 4 112.03 6.28 -2 12 -4 115.83 6.46 -2 12 -5 4.90 1.41 2 12 5 2.78 0.96 2 12 5 3.52 1.20 2 12 5 3.91 1.21 -2 -12 5 3.62 1.04 -2 12 -5 3.48 1.12 2 12 5 2.02 0.86 2 12 5 4.36 1.25 2 12 5 1.41 0.72 -2 -12 5 2.84 1.05 -2 12 -6 196.72 8.90 2 12 6 193.57 8.91 2 12 6 209.63 9.24 -2 12 -6 215.96 9.31 2 12 6 223.62 9.57 -2 -12 6 240.05 9.76 2 12 6 227.13 9.58 2 12 6 201.10 9.04 -2 -12 6 199.41 8.98 -2 -12 6 223.54 9.42 -2 12 -6 236.38 9.84 2 12 6 233.85 9.80 2 12 7 42.33 3.61 2 12 7 44.91 3.73 2 12 7 53.62 4.13 -2 12 -7 42.11 3.60 2 12 7 51.77 4.10 -2 -12 7 53.79 4.13 2 12 7 47.76 3.82 -2 -12 7 56.01 4.15 -2 12 -7 49.75 4.05 2 12 7 53.70 4.22 2 12 8 55.77 4.13 2 12 8 52.79 4.02 -2 12 -8 67.57 4.71 2 12 8 70.08 4.79 -2 -12 8 68.80 4.70 2 12 8 61.76 4.43 -2 -12 8 67.36 4.64 -2 -12 8 68.97 4.64 -2 12 -8 63.21 4.46 2 12 8 68.67 4.79 2 12 8 63.82 4.61 2 12 9 50.42 3.88 2 12 9 68.10 4.70 2 12 9 68.12 4.72 2 12 9 70.64 4.77 -2 -12 9 70.55 4.73 -2 -12 9 71.85 4.78 2 12 9 60.19 4.39 -2 -12 9 64.82 4.49 -2 12 -9 61.04 4.39 2 12 9 63.21 4.55 -2 -12 10 72.88 4.88 2 12 10 66.12 4.59 2 12 10 75.23 4.93 2 12 10 72.35 4.84 2 12 10 60.39 4.40 -2 -12 10 76.19 4.96 2 12 10 76.26 5.03 -2 -12 10 75.48 4.96 -2 12 -10 72.66 4.85 -2 12 -10 71.25 4.79 -2 -12 10 71.78 4.68 -2 12 -10 71.17 4.76 -2 12 -11 140.21 7.10 -2 -12 11 148.20 7.28 2 12 11 133.87 6.96 -2 -12 11 156.20 7.38 -2 12 -11 152.04 7.36 2 12 11 157.04 7.49 -2 -12 11 156.69 7.41 -2 12 -11 140.62 7.13 2 12 11 147.85 7.32 2 12 11 154.12 7.44 -2 -12 11 135.43 6.78 2 12 11 127.32 6.72 2 12 12 81.02 5.05 2 12 12 66.76 4.60 2 12 12 77.28 4.94 -2 -12 12 79.94 4.98 2 12 12 75.23 4.93 -2 -12 12 79.52 5.00 -2 12 -12 83.38 5.10 -2 -12 12 77.98 4.97 -2 12 -12 76.53 4.87 -2 12 -12 79.59 4.95 2 12 12 69.45 4.50 2 12 13 22.99 2.55 -2 -12 13 27.23 2.73 -2 -12 13 30.28 2.86 -2 12 -13 26.58 2.71 2 12 13 27.14 2.82 -2 -12 13 24.98 2.65 2 -12 -13 22.88 2.40 -2 12 -13 30.09 2.88 2 12 13 29.18 2.89 2 12 13 27.29 2.76 -2 12 -13 27.69 2.83 -2 12 -14 6.80 1.57 2 12 14 6.42 1.29 2 12 14 7.20 1.39 -2 -12 14 6.06 1.36 2 12 14 6.74 1.36 -2 -12 14 6.84 1.40 2 -12 -14 4.80 1.10 2 12 14 6.05 1.31 -2 -12 14 7.04 1.33 -2 12 -14 8.75 1.53 -2 12 -14 6.04 1.29 2 12 15 16.95 2.09 -2 12 -15 22.13 2.39 -2 -12 15 17.68 2.08 2 12 15 18.05 2.18 -2 -12 15 23.00 2.43 2 12 15 19.97 2.35 -2 -12 15 18.31 2.14 -2 12 -15 20.56 2.25 2 12 15 17.35 2.14 2 -12 -15 17.79 2.07 -2 12 -15 18.47 2.19 -2 12 -16 0.41 0.46 2 12 16 2.15 0.81 -2 -12 16 1.85 0.70 2 12 16 0.32 0.40 2 12 16 0.29 0.36 2 12 16 0.40 0.44 -2 -12 16 0.64 0.44 -2 12 -16 0.13 0.34 2 -12 -16 0.77 0.58 -2 12 -16 0.51 0.51 -2 12 -17 8.73 1.43 2 12 17 8.93 1.47 2 12 17 5.35 1.00 -2 12 -17 8.32 1.42 2 12 17 7.79 1.30 -2 -12 17 8.29 1.31 2 -12 -17 7.93 1.36 2 -12 -17 7.96 1.41 -2 12 -17 4.95 0.98 -2 -12 17 8.12 1.31 2 12 17 7.15 1.25 2 12 18 18.16 1.97 2 -12 -18 15.69 1.79 2 -12 -18 20.11 2.12 -2 -12 18 14.70 1.71 -2 12 -18 19.28 2.00 -2 12 -18 16.92 1.90 2 12 18 14.08 1.73 2 -12 -19 -0.08 0.23 2 -12 -19 1.16 0.46 2 12 19 0.90 0.46 2 12 19 1.43 0.54 -2 12 -19 1.71 0.63 2 -12 -19 0.81 0.47 -2 -12 19 1.34 0.50 2 -12 -20 1.74 0.60 -2 -13 -17 2.02 0.63 -2 13 17 2.88 0.75 -2 -13 -16 13.41 1.65 -2 13 16 11.35 1.50 2 13 -16 9.60 1.33 -2 -13 -16 8.31 1.25 -2 13 16 9.35 1.27 -2 -13 -16 11.74 1.54 -2 -13 -16 10.67 1.40 2 13 -16 12.13 1.51 2 13 -16 11.37 1.44 -2 13 15 24.90 2.36 2 13 -15 20.27 2.04 2 13 -15 25.26 2.36 -2 -13 -15 25.64 2.34 -2 -13 -15 23.11 2.24 -2 -13 -15 25.25 2.38 -2 -13 -15 27.57 2.52 -2 13 15 22.37 2.14 2 13 -15 23.12 2.16 -2 13 14 7.68 1.35 -2 -13 -14 7.84 1.43 -2 13 14 6.90 1.26 2 13 -14 6.35 1.18 2 13 -14 8.41 1.39 -2 -13 -14 7.36 1.33 2 13 -14 5.00 1.00 -2 -13 -14 6.21 1.19 -2 -13 -14 6.61 1.28 -2 -13 -13 9.38 1.48 2 13 -13 6.78 1.22 2 13 -13 7.30 1.26 -2 13 13 9.17 1.43 -2 -13 -13 14.13 1.94 -2 -13 -13 9.95 1.57 2 13 -13 10.26 1.55 -2 13 13 10.06 1.58 -2 -13 -13 9.79 1.55 -2 -13 -12 40.67 3.36 -2 13 12 41.67 3.33 -2 13 12 39.65 3.21 -2 -13 -12 46.14 3.51 2 13 -12 39.17 3.16 2 13 -12 33.01 2.85 -2 -13 -12 34.88 2.95 -2 -13 -12 42.60 3.35 2 13 -12 31.82 2.77 2 13 -11 1.52 0.64 -2 13 11 0.77 0.62 -2 -13 -11 1.42 0.79 -2 13 11 2.72 0.94 -2 -13 -11 1.83 0.69 2 13 -11 2.15 0.84 -2 -13 -11 1.80 0.77 2 13 -11 1.14 0.58 2 13 -11 0.72 0.31 2 13 -10 7.97 1.36 2 13 -10 7.93 1.37 2 13 -10 9.45 1.60 -2 13 10 9.19 1.58 -2 -13 -10 12.95 2.05 -2 -13 -10 8.29 1.55 -2 -13 -10 9.54 1.71 -2 13 10 9.90 1.69 2 13 -10 10.68 1.79 -2 -13 -9 15.77 2.11 -2 13 9 12.90 1.84 2 13 -9 15.49 2.06 2 13 -9 13.69 1.96 -2 -13 -9 16.11 2.11 -2 13 9 15.23 2.05 2 13 -9 14.84 1.99 -2 -13 -9 17.65 2.41 2 13 -9 14.02 1.89 2 13 -8 13.94 1.97 -2 -13 -8 19.01 2.55 -2 -13 -8 13.19 1.95 -2 13 8 18.26 2.28 -2 13 8 16.61 2.21 2 13 -8 16.41 2.13 -2 -13 -8 16.32 2.24 2 13 -8 15.40 2.09 2 13 -8 18.43 2.30 -2 13 8 14.55 2.00 -2 13 7 28.27 2.85 -2 13 7 32.45 3.10 2 13 -7 29.02 2.83 -2 13 7 31.75 3.03 -2 -13 -7 34.27 3.28 2 -13 7 28.06 2.82 2 13 -7 26.49 2.75 -2 -13 -7 24.91 2.71 -2 -13 -7 30.87 3.04 2 13 -7 31.17 3.07 2 13 -7 28.71 2.91 -2 -13 -6 73.16 4.93 -2 13 6 73.95 4.83 -2 -13 -6 61.93 4.38 -2 13 6 69.54 4.67 -2 -13 -6 66.07 4.60 2 13 -6 61.89 4.38 2 13 -6 60.11 4.29 2 13 -6 71.09 4.80 -2 13 6 67.01 4.60 2 13 -6 68.27 4.66 -2 -13 -5 92.74 5.57 -2 13 5 92.80 5.45 -2 13 5 79.27 4.82 -2 -13 -5 77.37 4.95 -2 13 5 86.96 5.34 2 13 -5 79.98 5.05 2 13 -5 78.19 4.94 -2 -13 -5 87.88 5.38 -2 13 5 92.26 5.48 2 13 -5 95.71 5.58 2 13 -5 90.99 5.51 -2 13 4 70.56 4.69 -2 13 4 65.27 4.52 -2 13 4 60.77 4.45 -2 -13 -4 70.64 4.76 -2 -13 -4 62.67 4.43 2 13 -4 58.84 4.19 -2 13 4 51.96 3.90 2 13 -4 66.26 4.56 -2 -13 -4 55.05 4.00 2 13 -4 53.02 3.95 2 13 -4 66.17 4.65 2 13 -3 7.51 1.41 2 13 -3 8.90 1.74 -2 13 3 9.20 1.66 -2 -13 -3 10.60 1.96 -2 -13 -3 7.51 1.59 -2 13 3 7.23 1.62 2 13 -3 6.46 1.33 2 13 -3 7.89 1.65 -2 13 3 8.01 1.65 -2 13 3 7.75 1.48 -2 -13 -2 40.05 3.46 -2 13 2 38.85 3.40 -2 13 2 42.15 3.62 2 13 -2 37.15 3.33 -2 13 2 45.00 3.75 2 13 -2 33.67 3.04 2 13 -2 40.73 3.59 -2 -13 -2 43.92 3.76 -2 13 2 41.18 3.60 2 13 -2 43.83 3.72 -2 13 1 10.75 1.89 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57.37 4.25 2 13 4 63.32 4.47 2 13 4 61.37 4.44 -2 13 -4 63.94 4.46 -2 13 -4 66.04 4.69 2 13 4 63.45 4.59 2 13 5 89.86 5.43 -2 13 -5 91.04 5.57 -2 -13 5 94.98 5.58 -2 13 -5 91.79 5.47 2 13 5 92.77 5.54 2 13 5 73.97 4.85 2 13 5 82.80 5.20 -2 -13 5 89.66 5.40 2 13 5 91.57 5.54 2 13 6 63.75 4.52 -2 -13 6 76.55 4.97 2 13 6 56.32 4.10 -2 13 -6 70.93 4.65 2 13 6 68.17 4.62 2 13 6 59.23 4.25 -2 -13 6 64.77 4.47 -2 13 -6 66.05 4.61 2 13 6 69.15 4.67 2 13 7 24.33 2.58 -2 13 -7 29.66 2.95 2 13 7 29.76 2.96 2 13 7 26.98 2.84 -2 -13 7 30.15 2.95 -2 -13 7 28.26 2.85 2 13 7 24.50 2.56 -2 -13 7 28.25 2.83 2 13 7 28.32 2.90 -2 13 -8 16.46 2.12 -2 -13 8 12.07 1.85 -2 -13 8 17.80 2.29 2 13 8 14.87 2.04 -2 -13 8 15.27 2.06 2 13 8 12.65 1.80 2 13 8 15.45 2.18 2 13 8 16.19 2.17 2 13 9 12.85 1.90 2 13 9 13.11 1.84 -2 -13 9 13.32 1.90 -2 -13 9 14.54 2.01 2 13 9 15.00 2.07 -2 -13 9 15.13 2.03 2 13 9 14.23 2.05 -2 13 -9 14.32 2.12 -2 -13 9 14.65 1.98 -2 -13 10 10.92 1.75 2 13 10 8.13 1.47 -2 13 -10 10.56 1.76 2 13 10 7.11 1.37 2 13 10 8.51 1.52 -2 -13 10 9.18 1.53 -2 -13 10 10.09 1.68 -2 -13 10 8.57 1.49 2 13 10 8.93 1.62 2 13 11 1.23 0.60 -2 -13 11 1.63 0.72 2 13 11 1.71 0.77 -2 13 -11 2.23 0.83 2 13 11 1.20 0.73 -2 -13 11 0.83 0.50 -2 -13 11 2.32 0.82 2 13 11 1.89 0.74 2 13 12 36.60 3.14 -2 -13 12 46.20 3.43 2 13 12 43.17 3.40 -2 -13 12 44.01 3.41 -2 13 -12 43.84 3.36 -2 -13 12 38.16 3.12 2 13 13 7.99 1.34 -2 -13 13 11.80 1.70 2 13 13 10.80 1.58 2 -13 -13 11.16 1.72 -2 13 -13 11.21 1.67 -2 -13 13 10.42 1.66 2 13 13 9.26 1.50 -2 -13 13 10.41 1.57 -2 13 -14 7.59 1.28 2 13 14 6.98 1.25 -2 -13 14 8.46 1.42 2 13 14 4.00 0.92 -2 -13 14 7.70 1.28 2 13 14 5.85 1.14 2 -13 -14 8.19 1.40 -2 -13 14 8.17 1.36 -2 -13 15 25.74 2.35 2 -13 -15 16.40 1.77 2 -13 -15 24.20 2.35 -2 13 -15 23.72 2.19 2 13 15 23.11 2.15 -2 -13 15 19.53 1.97 2 13 15 28.37 2.49 2 13 15 14.11 1.69 2 -13 -16 12.51 1.60 2 13 16 11.53 1.54 -2 -13 16 6.94 1.11 2 13 16 9.28 1.27 -2 13 -16 9.96 1.33 2 -13 -17 3.95 0.87 2 13 17 2.35 0.69 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-2 -14 -4 0.28 0.59 -2 14 4 0.87 0.52 -2 14 4 1.38 0.67 -2 14 4 0.46 0.60 -2 -14 -4 0.44 0.37 -2 14 3 24.86 2.57 -2 -14 -3 26.54 2.76 -2 -14 -3 20.50 2.28 2 14 -3 26.46 2.67 -2 14 3 26.01 2.66 -2 14 3 18.71 2.12 2 14 -3 25.35 2.63 -2 14 2 6.14 1.32 2 14 -2 7.64 1.45 -2 14 2 7.25 1.47 -2 -14 -2 6.09 1.20 -2 14 2 7.49 1.37 -2 -14 -2 5.85 1.24 2 14 -2 5.47 1.28 -2 -14 -2 5.77 1.24 -2 -14 -1 40.85 3.43 -2 -14 -1 41.51 3.43 -2 14 1 42.38 3.40 -2 14 1 35.02 3.07 -2 -14 -1 33.22 2.92 2 14 -1 41.41 3.42 -2 14 1 37.47 3.23 2 14 -1 42.60 3.49 -2 14 0 33.17 2.98 2 14 0 22.83 2.37 -2 -14 0 36.55 3.26 -2 -14 0 31.28 2.98 -2 14 0 31.98 2.98 2 14 0 32.15 2.95 2 14 0 32.83 3.03 -2 14 0 34.04 3.06 2 14 0 33.04 3.03 2 14 1 35.39 3.00 2 -14 -1 33.01 2.97 -2 14 -1 38.83 3.29 -2 -14 1 39.59 3.36 2 14 1 37.22 3.21 2 14 1 39.19 3.32 -2 -14 1 42.22 3.47 -2 14 -1 36.92 3.19 -2 14 -1 44.53 3.52 2 14 1 41.44 3.41 -2 14 -2 5.81 1.30 2 14 2 6.15 1.32 2 -14 -2 4.91 1.08 -2 14 -2 5.72 1.33 -2 14 -2 5.68 1.24 2 14 2 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2.52 4 12 9 21.51 2.49 -4 -12 9 18.40 2.30 -4 -12 9 23.65 2.65 4 12 10 1.66 0.76 4 12 10 1.49 0.67 4 12 10 1.48 0.72 -4 -12 10 2.15 0.87 4 12 10 2.00 0.88 -4 -12 10 1.31 0.59 -4 12 -10 2.02 0.82 4 12 10 1.77 0.94 -4 -12 10 2.37 0.99 4 12 11 86.76 5.22 -4 -12 11 113.30 5.80 4 12 11 108.48 5.99 -4 -12 11 116.37 5.98 -4 12 -11 107.21 5.85 4 12 11 114.49 6.08 -4 -12 11 113.53 5.89 4 12 11 113.70 6.03 4 12 11 94.94 5.46 4 12 12 19.64 2.17 -4 -12 12 24.12 2.48 4 12 12 25.32 2.68 4 -12 -12 21.59 2.27 -4 -12 12 26.72 2.66 -4 12 -12 24.34 2.53 4 12 12 25.27 2.65 -4 -12 12 24.30 2.53 4 12 12 23.84 2.53 4 12 12 18.78 2.13 -4 -12 13 60.48 3.91 4 12 13 57.59 4.01 4 -12 -13 45.43 3.37 -4 -12 13 57.98 3.94 -4 12 -13 56.98 3.84 4 12 13 61.08 4.07 -4 -12 13 59.99 3.95 4 12 13 57.29 3.94 -4 -12 14 12.50 1.70 4 12 14 13.19 1.84 4 -12 -14 9.38 1.48 -4 12 -14 11.54 1.65 4 12 14 14.29 1.85 -4 -12 14 12.94 1.78 4 12 14 11.37 1.67 -4 -12 15 3.18 0.90 4 12 15 2.48 0.79 -4 -12 15 2.87 0.91 4 -12 -15 2.09 0.71 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3.99 1.11 4 13 6 3.33 1.04 -4 -13 6 3.61 1.09 4 13 6 3.74 1.08 -4 -13 6 3.32 0.99 -4 -13 6 4.37 1.11 -4 13 -6 4.58 1.21 4 13 6 3.65 1.08 -4 -13 6 4.00 1.12 4 13 6 3.79 0.97 4 13 7 9.68 1.66 4 13 7 6.55 1.32 -4 -13 7 10.45 1.65 4 13 7 7.03 1.39 -4 -13 7 8.90 1.44 -4 -13 7 8.65 1.45 -4 13 -7 10.97 1.73 4 13 7 8.04 1.50 -4 -13 7 9.46 1.61 -4 -13 7 9.39 1.62 4 13 7 7.18 1.28 4 13 8 49.93 3.67 -4 -13 8 61.94 4.05 4 13 8 54.86 3.94 -4 -13 8 61.08 4.07 -4 13 -8 58.90 4.04 4 13 8 64.45 4.24 -4 -13 8 60.79 4.07 -4 -13 8 62.82 4.10 4 13 8 57.14 4.06 4 13 9 7.76 1.40 4 13 9 8.17 1.42 -4 -13 9 9.21 1.50 4 13 9 8.57 1.52 -4 -13 9 7.51 1.27 -4 13 -9 10.19 1.59 4 13 9 10.31 1.66 -4 -13 9 9.94 1.58 4 13 10 4.59 1.03 4 13 10 3.79 0.92 -4 -13 10 5.93 1.15 -4 -13 10 6.56 1.26 4 13 10 5.25 1.22 -4 -13 10 5.42 1.17 -4 13 -10 6.13 1.21 4 13 10 5.32 1.13 4 13 11 20.13 2.04 -4 -13 11 34.89 2.84 4 13 11 32.31 2.83 -4 -13 11 37.36 2.95 -4 13 -11 34.38 2.85 4 13 11 36.49 2.98 -4 -13 11 32.92 2.78 4 13 11 24.98 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9.67 1.48 4 14 -4 7.29 1.33 4 14 -3 2.23 0.87 -4 -14 -3 2.42 0.77 -4 -14 -3 1.68 0.61 4 14 -3 -0.64 0.34 -4 -14 -3 2.67 0.78 4 14 -3 2.92 0.95 -4 -14 -2 18.91 2.09 -4 -14 -2 19.23 2.10 4 14 -2 19.66 2.18 -4 -14 -2 22.98 2.29 4 14 -2 19.89 2.23 -4 -14 -1 73.08 4.29 -4 -14 -1 66.00 4.06 4 14 -1 71.75 4.35 -4 -14 -1 74.57 4.36 4 14 -1 76.70 4.53 4 14 0 0.09 0.55 -4 -14 0 1.17 0.61 4 14 0 0.21 0.22 -4 -14 0 0.78 0.46 -4 -14 0 0.75 0.53 4 14 0 1.34 0.69 -4 -14 1 74.39 4.39 4 14 1 61.87 3.97 4 14 1 71.07 4.34 -4 -14 1 76.72 4.43 4 14 1 76.38 4.57 -4 -14 2 20.06 2.17 4 14 2 19.16 2.14 4 14 2 21.10 2.29 -4 -14 2 22.56 2.30 4 14 2 20.62 2.30 4 14 3 3.03 0.91 -4 -14 3 1.83 0.59 -4 14 -3 2.21 0.71 4 14 3 2.13 0.76 -4 -14 3 2.71 0.92 4 14 3 1.32 0.60 4 14 4 7.31 1.30 -4 -14 4 8.25 1.42 -4 -14 4 7.77 1.39 -4 14 -4 6.34 1.25 4 14 4 8.06 1.39 -4 -14 4 7.77 1.34 4 14 4 7.10 1.27 4 14 5 1.27 0.64 -4 -14 5 0.82 0.73 4 14 5 0.18 0.23 -4 -14 5 0.25 0.64 -4 14 -5 1.31 0.63 4 14 5 0.59 0.42 -4 -14 5 0.58 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224.59 13.47 -5 -5 -1 210.80 7.96 -5 -5 -1 202.42 7.86 -5 5 1 208.22 7.93 -5 -5 -1 188.24 7.64 -5 5 0 57.87 6.53 -5 5 0 54.74 6.32 -5 -5 0 47.25 3.19 -5 5 0 42.88 3.09 5 5 0 51.79 3.39 -5 5 0 53.32 6.31 5 5 0 51.84 3.40 -5 5 0 49.61 3.32 -5 -5 0 48.25 3.28 -5 -5 0 50.70 3.36 -5 5 0 51.46 3.39 -5 -5 0 49.63 3.34 -5 -5 1 190.79 7.58 -5 5 -1 234.80 13.80 -5 5 -1 231.76 13.64 -5 -5 1 157.49 7.23 -5 5 -1 224.99 13.38 5 5 1 201.91 7.85 -5 -5 1 192.25 7.64 -5 5 -1 193.61 7.78 -5 -5 1 194.90 7.67 5 5 1 205.36 7.87 -5 -5 1 200.30 7.74 -5 5 -1 208.67 7.92 -5 -5 1 207.74 7.91 -5 -5 2 36.07 2.74 -5 5 -2 42.35 5.64 -5 5 -2 38.57 5.31 -5 -5 2 32.80 2.71 5 5 2 37.37 2.90 5 5 2 38.30 2.91 -5 -5 2 37.29 2.81 -5 5 -2 37.38 2.89 -5 -5 2 34.25 2.68 5 5 2 26.13 2.36 5 5 2 39.55 3.00 -5 -5 2 39.02 2.88 -5 5 -2 38.15 2.88 -5 -5 2 38.09 2.89 5 5 3 195.95 7.66 -5 -5 3 187.02 7.37 -5 5 -3 220.94 13.51 -5 -5 3 181.27 7.46 5 5 3 191.39 7.68 5 5 3 195.12 7.71 -5 -5 3 186.62 7.43 -5 5 -3 191.04 7.66 -5 -5 3 191.41 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5.73 1.15 -5 5 -6 3.24 1.72 5 5 7 91.53 4.99 -5 -5 7 95.50 8.42 5 5 7 82.68 4.72 -5 5 -7 90.53 4.92 -5 5 -7 103.85 9.63 -5 -5 7 88.62 4.79 -5 5 -7 71.70 4.43 -5 -5 7 90.06 4.78 -5 -5 7 95.99 5.09 -5 5 -7 88.10 4.92 -5 -5 7 90.57 4.85 -5 5 -7 85.23 4.83 -5 -5 7 91.72 4.90 -5 5 -7 91.04 5.04 5 5 7 90.40 4.99 -5 -5 7 88.74 4.83 5 5 8 213.18 8.37 -5 5 -8 208.39 8.34 -5 -5 8 201.27 13.10 5 5 8 207.14 8.28 -5 5 -8 196.72 8.10 -5 -5 8 195.25 7.98 -5 5 -8 215.93 14.60 -5 5 -8 158.05 7.42 -5 -5 8 200.48 7.98 -5 -5 8 210.90 8.39 5 5 8 176.69 7.77 -5 -5 8 198.64 8.05 -5 5 -8 192.44 7.99 -5 5 -8 202.04 8.36 -5 -5 8 202.96 8.14 5 5 9 108.56 5.58 -5 5 -9 102.96 5.49 -5 -5 9 88.24 5.06 -5 -5 9 105.02 9.46 5 5 9 102.26 5.43 -5 5 -9 104.66 5.46 -5 -5 9 102.17 5.36 -5 5 -9 100.50 9.92 -5 -5 9 103.43 5.30 -5 -5 9 112.35 5.70 5 5 9 79.55 4.83 -5 5 -9 100.80 5.32 -5 5 -9 103.92 5.57 5 5 9 100.37 9.77 -5 -5 10 56.09 3.81 5 5 10 55.87 3.93 -5 5 -10 52.07 3.79 5 5 10 56.48 3.89 -5 5 -10 50.75 3.71 -5 -5 10 51.13 3.70 -5 5 -10 48.55 7.04 -5 -5 10 52.78 3.65 -5 -5 10 54.07 3.83 -5 -5 10 42.60 6.10 -5 -5 10 48.58 3.62 -5 5 -10 47.15 3.48 -5 -5 10 54.97 3.74 5 5 10 47.06 6.58 -5 5 -10 51.76 3.85 5 5 11 60.87 4.19 -5 -5 11 57.50 3.91 -5 -5 11 53.13 3.87 -5 -5 11 55.62 7.32 5 5 11 56.68 4.00 -5 5 -11 57.61 4.02 -5 -5 11 61.07 4.12 -5 5 -11 59.49 7.75 -5 -5 11 63.18 4.02 -5 -5 11 62.71 4.13 -5 5 -11 60.94 4.18 -5 5 -11 46.34 3.51 -5 -5 11 62.33 4.03 5 5 11 46.67 6.50 -5 5 -11 55.77 4.02 -5 -5 12 112.99 5.88 -5 5 -12 121.76 6.31 -5 -5 12 111.69 6.02 -5 -5 12 109.16 10.61 5 5 12 120.57 6.25 -5 5 -12 114.12 6.08 -5 -5 12 115.55 6.10 -5 5 -12 105.88 10.91 -5 -5 12 127.15 6.14 5 5 12 130.20 6.51 -5 -5 12 116.21 5.97 -5 -5 12 120.30 6.14 -5 5 -12 108.48 6.01 -5 5 -13 42.56 6.94 -5 5 -13 40.13 3.41 -5 -5 13 38.26 3.24 5 5 13 41.59 3.55 -5 5 -13 41.18 3.54 5 5 13 44.40 3.61 -5 -5 13 40.48 3.41 -5 -5 13 37.90 6.31 -5 -5 13 40.95 3.45 -5 -5 13 40.63 3.31 -5 -5 13 39.07 3.32 -5 5 -13 40.58 3.40 -5 5 -14 33.04 6.21 -5 -5 14 34.48 3.05 -5 -5 14 39.92 3.42 -5 5 -14 43.74 3.66 5 5 14 38.57 3.45 -5 5 -14 37.45 3.31 -5 -5 14 43.01 3.51 -5 -5 14 27.99 5.58 -5 -5 14 39.81 3.37 -5 -5 14 37.71 3.32 -5 5 -14 36.15 3.25 5 5 14 41.99 3.59 -5 5 -15 27.56 5.71 -5 -5 15 33.88 3.03 -5 -5 15 37.23 3.37 5 5 15 37.52 3.46 -5 5 -15 38.62 3.48 -5 -5 15 39.96 3.31 -5 5 -15 35.22 3.26 5 5 15 38.22 3.46 -5 -5 15 40.53 3.43 -5 -5 15 24.28 5.38 -5 -5 15 36.17 3.21 -5 -5 15 36.15 3.30 -5 5 -15 33.81 3.14 -5 -5 16 280.72 10.55 -5 -5 16 282.14 10.87 5 5 16 285.81 11.13 -5 5 -16 273.85 10.91 -5 -5 16 173.79 15.59 -5 -5 16 271.61 10.36 -5 -5 16 232.49 9.83 5 5 16 279.72 10.90 -5 5 -16 142.88 14.53 -5 -5 16 292.32 10.90 -5 5 -16 251.42 10.37 -5 -5 16 279.12 10.53 -5 -5 16 267.65 10.65 -5 5 -16 226.14 9.79 -5 -5 17 66.33 4.52 -5 5 -17 67.46 4.80 -5 -5 17 65.50 4.53 5 5 17 68.23 4.81 -5 5 -17 63.29 4.52 -5 -5 17 68.77 4.73 -5 -5 17 64.15 4.47 -5 -5 17 67.03 4.69 5 5 17 69.17 4.81 -5 -5 18 9.07 1.66 5 5 18 8.61 1.65 -5 5 -18 8.60 1.75 -5 -5 18 8.33 1.50 5 5 18 8.92 1.75 -5 5 -18 6.99 1.38 -5 -5 18 9.10 1.72 -5 -5 18 6.72 1.33 -5 -5 18 7.99 1.51 5 5 19 2.85 1.03 -5 5 -19 3.00 1.14 5 5 19 2.00 0.70 -5 5 -19 1.69 0.65 -5 -5 19 2.58 0.96 -5 -5 19 1.53 0.81 -5 -5 19 0.89 0.81 -5 -5 19 2.78 0.97 -5 -5 20 14.47 2.01 -5 -5 20 13.19 1.92 5 5 20 15.07 2.17 -5 5 -20 14.10 2.11 5 5 20 16.07 2.23 -5 5 -20 12.59 1.88 -5 -5 20 13.74 2.00 -5 -5 20 15.24 2.03 -5 -5 21 19.41 2.35 5 5 21 23.66 2.71 5 5 21 20.93 2.48 -5 5 -21 20.96 2.53 -5 -5 21 21.34 2.44 -5 -5 21 22.41 2.51 -5 -5 21 19.46 2.29 -5 -5 22 11.51 1.78 -5 5 -22 12.84 1.89 -5 -5 22 10.80 1.72 5 5 22 8.69 1.59 5 5 22 9.21 1.59 -5 -5 22 10.47 1.61 -5 5 -23 5.31 1.28 -5 -5 23 5.14 1.16 5 5 23 4.52 1.19 -5 -5 23 5.19 1.12 -5 -5 23 5.28 1.08 5 5 23 3.32 0.90 -5 -5 24 15.48 1.84 -5 5 -24 15.44 1.98 -5 -5 24 16.56 1.92 5 5 24 18.49 2.14 5 5 24 11.86 1.61 5 -5 -24 14.02 1.78 -5 -5 24 15.04 1.84 -5 -5 25 29.01 2.49 -5 5 -25 30.18 2.64 -5 -5 25 27.35 2.43 5 -5 -25 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54.15 4.18 -5 -6 -20 55.31 4.26 5 6 -20 51.88 4.03 5 6 -20 53.03 3.95 -5 -6 -20 46.71 3.82 -5 6 20 55.50 4.02 -5 6 20 50.34 3.99 -5 -6 -19 104.43 6.14 -5 -6 -19 104.55 6.11 -5 6 19 100.31 5.95 5 6 -19 100.46 5.91 5 6 -19 103.31 5.87 -5 -6 -19 100.91 5.94 -5 6 19 103.76 5.80 -5 -6 -18 39.97 3.68 -5 -6 -18 38.37 3.59 -5 6 18 47.48 3.92 5 6 -18 36.31 3.42 5 6 -18 44.49 3.65 5 6 -18 39.00 3.34 -5 -6 -18 43.39 3.75 -5 6 18 42.79 3.63 -5 -6 -17 84.73 5.49 -5 -6 -17 94.06 5.76 -5 6 17 88.79 5.47 5 6 -17 90.95 5.42 -5 6 17 86.77 5.50 -5 6 17 64.21 4.61 5 6 -17 80.40 5.29 5 6 -17 90.81 5.43 5 6 -17 81.25 5.12 -5 -6 -17 91.31 5.61 -5 6 17 89.89 5.43 -5 -6 -16 55.90 4.36 -5 -6 -16 60.83 4.51 5 6 -16 58.03 4.27 -5 6 16 59.83 4.47 -5 6 16 43.98 3.70 5 6 -16 49.11 4.05 -5 6 16 57.50 4.31 5 6 -16 58.28 4.27 5 6 -16 55.23 4.14 -5 -6 -16 56.61 4.37 -5 -6 -16 46.81 3.71 -5 6 16 57.11 4.25 -5 -6 -15 122.77 6.77 -5 -6 -15 131.97 6.93 -5 6 15 126.67 6.80 -5 6 15 98.94 5.91 5 6 -15 108.40 6.34 5 6 -15 124.86 6.58 5 6 -15 120.44 6.49 -5 6 15 127.38 6.73 -5 -6 -15 136.70 6.98 -5 -6 -15 109.93 6.13 5 6 -15 130.29 6.67 -5 6 15 129.76 6.68 -5 -6 -14 47.42 3.89 -5 6 14 47.94 3.91 -5 -6 -14 46.22 3.88 -5 6 14 45.81 3.83 5 6 -14 49.19 3.82 -5 6 14 36.26 3.34 5 6 -14 42.79 3.64 5 6 -14 46.17 3.75 5 6 -14 45.15 3.75 -5 -6 -14 47.64 3.91 -5 -6 -14 43.31 3.59 -5 6 14 45.60 3.71 -5 -6 -13 43.27 3.66 -5 6 13 39.94 3.54 5 6 -13 39.61 3.36 -5 6 13 40.09 3.53 -5 6 13 33.83 3.15 5 6 -13 38.72 3.41 -5 -6 -13 41.71 3.60 -5 -6 -13 46.90 3.82 -5 -6 -13 42.71 3.53 -5 6 13 42.16 3.57 -5 -6 -12 175.77 8.02 -5 -6 -12 170.11 7.91 -5 6 12 178.38 8.08 5 6 -12 176.69 7.75 -5 6 12 147.94 7.34 -5 6 12 175.17 7.95 5 6 -12 158.87 7.59 -5 6 12 130.28 12.66 -5 -6 -12 172.62 7.92 -5 -6 -12 158.54 7.61 -5 6 12 173.81 7.89 5 6 -12 155.05 7.47 -5 -6 -11 50.38 3.88 -5 -6 -11 48.26 3.81 5 6 -11 51.62 3.78 -5 6 11 43.25 6.47 -5 6 11 42.55 3.49 5 6 -11 43.61 3.53 5 6 -11 54.37 3.89 -5 6 11 39.09 6.55 -5 -6 -11 52.37 3.91 -5 6 11 52.41 3.94 -5 -6 -11 49.06 3.81 -5 6 11 51.84 3.95 5 6 -11 45.30 3.60 -5 -6 -10 67.39 4.48 -5 -6 -10 60.98 4.26 -5 6 10 68.52 4.53 5 6 -10 68.52 4.37 -5 6 10 67.46 4.43 -5 -6 -10 59.75 4.15 -5 6 10 62.86 8.26 -5 6 10 59.26 4.14 5 6 -10 66.05 4.32 -5 6 10 59.20 7.70 -5 -6 -10 66.71 4.42 -5 -6 -10 63.92 4.36 5 6 -10 56.95 7.57 5 6 -10 64.45 4.37 -5 -6 -9 136.17 6.58 5 6 -9 119.79 6.06 -5 -6 -9 118.98 6.19 5 6 -9 131.86 6.36 -5 6 9 126.70 6.42 -5 6 9 130.66 6.41 -5 6 9 114.46 6.03 -5 6 9 115.16 6.03 -5 -6 -9 126.69 6.38 -5 6 9 125.25 11.73 5 6 -9 134.92 6.42 -5 6 9 112.19 10.75 -5 -6 -9 137.79 6.55 -5 -6 -9 129.80 6.49 5 6 -9 127.15 11.64 -5 6 9 113.02 5.86 5 6 -9 126.31 6.35 -5 -6 -8 19.27 2.22 5 6 -8 17.23 2.06 -5 6 8 15.25 1.88 5 6 -8 17.93 2.10 -5 6 8 16.91 2.11 -5 6 8 14.59 1.91 -5 6 8 16.81 2.01 -5 -6 -8 17.18 2.13 -5 -6 -8 16.54 2.03 5 6 -8 17.85 2.10 -5 6 8 16.87 4.06 -5 -6 -8 19.65 2.28 -5 -6 -8 19.10 2.25 -5 6 8 16.07 3.97 5 6 -8 17.21 4.29 5 6 -8 17.39 2.13 -5 -6 -7 104.98 5.50 -5 6 7 100.26 5.44 5 6 -7 97.74 5.23 -5 -6 -7 79.36 4.81 -5 6 7 88.19 5.06 -5 6 7 99.39 5.40 -5 -6 -7 101.70 5.52 -5 6 7 99.64 9.99 5 6 -7 105.00 5.39 -5 6 7 105.78 10.08 5 6 -7 106.48 5.49 -5 -6 -7 103.61 5.47 -5 -6 -7 103.99 5.54 -5 6 7 99.70 5.26 5 6 -7 105.96 10.44 -5 6 7 80.71 4.74 5 6 -7 97.92 5.41 -5 -6 -6 121.76 6.00 5 6 -6 115.61 5.76 -5 6 6 119.95 6.04 -5 6 6 99.44 5.46 -5 6 6 119.06 5.98 -5 -6 -6 120.47 6.08 -5 6 6 113.73 10.53 5 6 -6 125.63 5.93 -5 6 6 113.29 10.39 -5 -6 -6 121.96 6.02 -5 -6 -6 126.62 6.13 -5 6 6 123.17 5.89 5 6 -6 115.81 11.00 5 6 -6 116.27 5.97 -5 6 6 88.79 5.06 -5 -6 -5 113.67 5.70 -5 6 5 121.02 10.70 -5 6 5 114.12 5.77 -5 6 5 88.39 5.09 -5 -6 -5 114.57 5.83 5 6 -5 113.09 5.56 -5 6 5 117.32 10.44 -5 6 5 108.84 5.68 -5 -6 -5 116.53 5.76 -5 -6 -5 114.57 5.73 -5 6 5 109.99 5.54 5 6 -5 114.18 5.62 5 6 -5 120.83 11.03 5 6 -5 110.30 5.70 -5 6 5 80.83 4.77 -5 -6 -4 86.62 4.87 -5 6 4 87.08 4.97 -5 6 4 69.13 4.36 -5 -6 -4 87.96 5.01 -5 6 4 79.73 8.66 5 6 -4 89.05 4.84 -5 6 4 91.34 9.09 -5 6 4 90.61 5.04 -5 -6 -4 86.32 4.86 -5 -6 -4 86.76 4.89 -5 6 4 85.72 4.80 5 6 -4 99.88 9.81 -5 6 4 93.63 9.13 -5 -6 -3 90.46 4.94 -5 6 3 92.23 8.93 5 6 -3 90.10 4.86 -5 6 3 85.50 4.91 -5 6 3 68.86 4.38 -5 6 3 93.85 5.14 -5 -6 -3 91.65 5.08 -5 6 3 96.66 9.20 -5 6 3 107.21 9.71 -5 -6 -3 90.31 4.94 -5 -6 -3 93.55 5.01 -5 6 3 90.54 4.90 5 6 -2 69.73 4.15 -5 6 2 73.59 7.75 -5 6 2 68.73 4.20 -5 6 2 54.86 3.73 -5 6 2 70.24 4.30 -5 -6 -2 67.85 4.24 -5 -6 -2 49.52 3.53 -5 6 2 72.48 7.82 -5 6 2 69.88 4.22 5 6 -2 51.50 3.55 -5 -6 -2 71.57 4.22 -5 6 2 73.79 7.92 -5 -6 -2 66.42 4.07 -5 6 2 68.76 4.14 -5 -6 -2 62.51 3.99 5 6 -1 20.45 2.18 -5 -6 -1 23.84 2.31 -5 6 1 17.98 2.03 -5 6 1 27.43 4.80 -5 6 1 22.95 2.35 -5 -6 -1 23.75 2.46 -5 -6 -1 17.49 1.99 -5 6 1 24.51 2.39 -5 -6 -1 24.63 2.37 5 6 -1 18.95 2.02 -5 -6 -1 21.15 2.18 -5 6 1 22.56 2.28 -5 6 1 24.02 2.38 -5 6 1 22.40 4.29 -5 -6 -1 23.56 2.35 -5 -6 0 65.64 4.02 -5 6 0 65.35 4.05 -5 6 0 57.03 3.80 -5 6 0 77.62 7.95 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96.83 5.38 -5 -6 7 100.25 5.34 -5 6 -7 103.66 5.60 5 6 7 100.64 10.31 -5 -6 7 91.09 8.77 -5 -6 7 109.18 5.53 -5 -6 7 104.43 5.44 5 6 7 98.08 5.49 -5 6 -8 19.64 2.23 5 6 8 18.52 2.20 5 6 8 19.08 2.22 -5 6 -8 19.49 2.22 -5 -6 8 19.27 2.17 -5 -6 8 17.88 2.03 -5 -6 8 17.56 2.08 -5 -6 8 15.66 3.69 -5 6 -8 17.92 2.18 -5 6 -8 16.69 2.09 -5 -6 8 18.09 2.10 5 6 8 22.56 4.88 5 6 8 15.72 2.05 -5 6 -8 16.35 3.96 5 6 9 141.16 6.70 -5 6 -9 124.51 6.38 -5 -6 9 115.31 10.56 5 6 9 139.42 6.70 -5 6 -9 131.99 6.48 -5 6 -9 116.78 11.00 -5 -6 9 130.41 6.41 -5 -6 9 126.80 6.17 -5 -6 9 133.17 6.52 -5 6 -9 123.32 6.32 5 6 9 126.23 11.63 -5 6 -9 137.05 6.72 -5 -6 9 133.13 6.33 5 6 9 110.96 6.08 -5 6 -10 65.86 4.44 5 6 10 73.71 4.65 -5 -6 10 59.97 7.63 -5 6 -10 67.06 4.45 -5 6 -10 52.40 7.29 -5 -6 10 67.51 4.39 5 6 10 65.84 4.46 -5 -6 10 64.93 4.19 -5 -6 10 70.74 4.54 -5 6 -10 65.84 4.34 5 6 10 57.38 7.71 -5 6 -10 59.56 4.28 -5 -6 11 51.05 3.73 5 6 11 55.89 4.04 -5 6 -11 50.84 3.85 -5 6 -11 48.69 3.79 -5 -6 11 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43.85 3.54 -5 -7 -21 42.75 3.49 -5 7 21 38.94 3.29 5 7 -21 38.65 3.24 -5 -7 -21 44.77 3.48 5 7 -21 42.86 3.33 -5 7 21 43.19 3.35 -5 -7 -20 57.37 4.21 -5 -7 -20 56.78 4.23 -5 7 20 52.73 3.98 5 7 -20 50.74 3.88 5 7 -20 54.44 3.90 -5 -7 -20 60.04 4.21 -5 7 20 56.70 3.98 -5 -7 -19 16.74 2.23 -5 7 19 12.74 1.97 -5 -7 -19 15.39 2.19 -5 7 19 11.66 1.72 5 7 -19 16.10 2.15 5 7 -19 16.34 2.15 5 7 -19 14.60 1.92 -5 -7 -19 16.96 2.25 -5 7 19 17.75 2.23 -5 -7 -18 116.98 6.50 -5 -7 -18 120.16 6.56 -5 7 18 120.77 6.52 -5 7 18 94.01 5.60 5 7 -18 108.35 6.12 5 7 -18 114.87 6.17 5 7 -18 113.67 6.11 -5 -7 -18 124.85 6.58 -5 7 18 125.27 6.40 -5 -7 -17 34.89 3.35 -5 -7 -17 36.07 3.43 -5 7 17 33.70 3.26 -5 7 17 26.39 2.78 5 7 -17 29.06 2.98 5 7 -17 30.37 2.97 5 7 -17 30.91 3.03 -5 -7 -17 32.54 3.25 -5 -7 -17 25.32 2.65 -5 7 17 34.54 3.21 -5 -7 -16 101.35 6.01 -5 -7 -16 96.72 5.82 -5 7 16 92.05 5.67 5 7 -16 96.06 5.59 -5 7 16 100.99 5.92 -5 7 16 76.27 5.06 5 7 -16 86.24 5.42 5 7 -16 91.90 5.52 5 7 -16 92.11 5.59 -5 -7 -16 105.33 6.06 -5 -7 -16 84.64 5.24 -5 7 16 97.34 5.69 -5 -7 -15 104.66 6.18 -5 7 15 110.64 6.30 -5 -7 -15 104.90 6.18 -5 7 15 92.42 5.62 -5 7 15 99.56 5.91 5 7 -15 107.22 5.97 5 7 -15 90.39 5.62 5 7 -15 101.26 5.85 5 7 -15 101.47 5.93 -5 -7 -15 107.30 6.12 -5 -7 -15 94.21 5.64 -5 7 15 104.63 5.95 -5 -7 -14 29.04 3.15 -5 7 14 28.85 3.06 -5 7 14 26.25 2.90 5 7 -14 30.41 2.94 -5 7 14 23.36 2.68 -5 -7 -14 29.17 3.12 5 7 -14 25.67 2.79 5 7 -14 29.55 2.99 5 7 -14 26.10 2.88 -5 -7 -14 29.98 3.16 -5 -7 -14 28.60 2.97 -5 7 14 29.17 2.96 -5 -7 -13 141.66 7.26 -5 -7 -13 132.49 7.07 5 7 -13 143.33 7.04 -5 7 13 142.98 7.25 5 7 -13 118.89 6.58 -5 7 13 128.64 6.89 5 7 -13 138.39 6.98 5 7 -13 140.75 7.15 -5 7 13 121.31 6.60 -5 -7 -13 139.92 7.15 -5 -7 -13 131.49 6.90 -5 7 13 145.68 7.15 5 7 -13 124.03 6.57 -5 -7 -12 8.02 1.61 -5 -7 -12 7.94 1.55 -5 7 12 7.52 1.53 -5 7 12 8.15 1.69 -5 7 12 7.16 1.48 -5 -7 -12 7.87 1.53 5 7 -12 6.57 1.42 5 7 -12 8.71 1.65 -5 -7 -12 8.77 1.60 -5 -7 -12 8.93 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3.97 -5 -7 -8 54.79 4.10 -5 7 8 52.85 7.56 5 7 -8 57.33 3.99 -5 -7 -8 61.00 4.26 -5 -7 -8 55.43 4.07 -5 7 8 58.27 4.11 5 7 -8 47.98 7.44 -5 7 8 54.86 3.87 5 7 -8 59.15 4.21 -5 -7 -7 24.84 2.63 5 7 -7 21.31 2.37 5 7 -7 25.57 2.60 -5 7 7 23.86 2.56 -5 7 7 25.79 2.62 -5 7 7 18.97 4.53 -5 7 7 24.08 2.59 -5 -7 -7 22.50 2.55 5 7 -7 24.07 2.48 -5 -7 -7 26.06 2.70 -5 -7 -7 23.70 2.53 -5 7 7 20.45 2.31 5 7 -7 18.83 4.42 -5 7 7 21.55 2.30 5 7 -7 21.10 2.45 -5 -7 -6 120.71 6.21 5 7 -6 117.55 6.03 -5 7 6 117.37 6.13 5 7 -6 122.66 6.18 -5 7 6 112.82 5.99 -5 7 6 116.94 6.17 -5 -7 -6 112.50 6.13 -5 7 6 96.78 10.44 5 7 -6 113.75 5.88 -5 -7 -6 120.14 6.16 -5 -7 -6 119.45 6.15 -5 7 6 118.24 6.05 5 7 -6 107.49 11.24 5 7 -6 121.91 6.29 -5 -7 -5 135.34 6.56 5 7 -5 127.45 6.34 5 7 -5 126.86 6.37 -5 7 5 123.90 6.28 -5 7 5 123.82 6.44 -5 7 5 110.14 10.89 5 7 -5 127.84 6.24 -5 7 5 131.07 6.51 -5 -7 -5 131.20 6.47 -5 -7 -5 131.26 6.47 -5 7 5 130.88 6.39 5 7 -5 127.75 12.20 5 7 -5 114.80 6.25 -5 -7 -4 30.79 2.87 5 7 -4 29.74 2.75 -5 7 4 31.05 2.88 -5 7 4 29.04 2.76 -5 7 4 30.46 2.90 -5 -7 -4 30.61 2.93 -5 7 4 29.18 5.52 5 7 -4 28.48 2.68 -5 -7 -4 32.73 2.92 -5 -7 -4 30.19 2.80 -5 7 4 33.81 2.93 5 7 -4 31.65 5.75 5 7 -4 28.94 2.84 -5 7 3 326.25 11.95 -5 7 3 349.28 12.38 -5 -7 -3 355.43 12.50 -5 7 3 340.25 19.62 -5 -7 -3 350.19 12.22 -5 -7 -3 354.01 12.19 -5 7 3 354.18 12.18 5 7 -3 363.55 21.16 -5 7 3 364.59 12.45 5 7 -3 347.46 12.12 5 7 -3 350.01 12.35 -5 7 2 91.45 5.17 -5 7 2 101.74 5.54 -5 -7 -2 99.48 5.48 5 7 -2 95.01 5.21 -5 -7 -2 83.11 4.93 -5 7 2 93.95 5.27 -5 7 2 95.94 9.64 -5 -7 -2 92.09 5.17 -5 -7 -2 92.57 5.17 -5 7 2 101.42 5.38 5 7 -2 91.67 10.01 -5 7 2 95.53 5.34 -5 7 2 91.25 9.26 5 7 -2 93.28 5.30 -5 -7 -2 93.39 5.23 -5 -7 -1 1.91 0.73 -5 -7 -1 2.28 0.64 5 7 -1 3.24 0.98 -5 7 1 2.66 0.85 -5 7 1 1.82 0.59 -5 7 1 3.35 1.10 -5 -7 -1 3.35 0.99 -5 7 1 3.43 1.86 -5 -7 -1 2.96 0.91 -5 7 1 3.03 0.94 5 7 -1 2.86 0.84 -5 -7 -1 3.08 0.91 -5 -7 -1 3.46 0.95 -5 7 1 4.52 1.14 -5 7 1 1.96 1.68 5 7 -1 2.83 1.28 -5 -7 -1 4.15 1.08 5 7 -1 2.99 1.00 -5 -7 0 41.40 3.27 5 7 0 43.18 3.33 -5 7 0 42.75 3.36 -5 7 0 44.29 3.40 -5 7 0 43.31 3.43 -5 -7 0 40.05 3.30 -5 7 0 40.67 6.08 -5 -7 0 39.57 3.23 -5 -7 0 44.29 3.42 -5 7 0 42.60 3.34 -5 -7 0 40.57 3.22 5 7 0 40.01 3.17 -5 -7 0 40.57 3.26 -5 7 0 43.80 3.35 5 7 0 42.66 6.82 -5 7 0 37.17 5.69 -5 -7 0 42.53 3.33 5 7 0 41.99 3.41 -5 7 -1 2.64 0.82 -5 -7 1 1.41 0.51 5 7 1 5.21 1.09 -5 7 -1 4.37 1.04 -5 7 -1 3.45 1.06 -5 -7 1 3.10 0.93 -5 -7 1 2.71 0.80 -5 -7 1 2.24 0.65 5 -7 -1 5.88 2.25 -5 7 -1 3.09 1.02 5 7 1 2.84 0.75 -5 -7 1 3.73 0.98 -5 -7 1 3.46 1.02 -5 7 -1 1.32 1.06 -5 7 -1 3.78 1.09 -5 7 -1 2.12 1.56 5 7 1 3.00 1.82 -5 -7 1 3.34 0.94 5 7 1 3.77 1.12 5 7 2 100.01 5.34 -5 7 -2 87.68 9.20 -5 7 -2 88.39 8.98 -5 7 -2 91.60 5.11 -5 -7 2 97.12 5.24 -5 -7 2 89.57 4.97 -5 -7 2 91.41 5.21 -5 -7 2 93.55 5.25 -5 7 -2 92.21 5.25 -5 -7 2 84.03 4.82 5 7 2 92.08 5.11 -5 -7 2 89.22 5.05 -5 7 -2 95.93 5.28 5 7 2 89.40 9.78 -5 -7 2 92.31 5.19 5 7 2 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3.19 0.82 -7 5 -21 4.20 1.01 -7 -5 21 3.40 0.89 7 5 21 2.84 0.89 -7 -5 21 2.81 0.87 7 5 21 2.80 0.83 -7 -5 21 2.47 0.73 -7 5 -22 1.25 0.63 -7 -5 22 1.34 0.61 7 5 22 1.33 0.54 -7 -5 22 2.96 0.81 7 5 22 1.88 0.70 -7 -5 22 1.92 0.57 -7 5 -23 2.33 0.68 -7 -5 23 1.93 0.64 7 5 23 0.25 0.31 -7 -5 23 1.04 0.48 7 5 23 0.91 0.53 -7 -6 -23 16.82 1.70 -7 -6 -22 1.14 0.47 -7 6 22 0.56 0.49 7 -6 22 0.95 0.46 7 6 -22 0.82 0.48 -7 -6 -22 1.31 0.55 -7 6 22 1.04 0.40 -7 -6 -21 65.37 4.01 -7 6 21 66.33 4.01 7 -6 21 70.30 4.22 7 6 -21 68.74 4.00 -7 -6 -21 56.35 3.55 -7 6 21 65.35 3.83 -7 -6 -21 64.29 4.02 -7 -6 -20 3.22 0.90 -7 6 20 3.55 1.08 7 -6 20 3.84 1.02 7 6 -20 3.50 1.00 -7 -6 -20 2.13 0.66 -7 -6 -20 2.66 0.94 -7 6 20 2.58 0.74 -7 -6 -19 72.30 4.54 -7 6 19 67.02 4.36 7 -6 19 66.53 4.45 7 6 -19 73.73 4.43 -7 -6 -19 64.27 4.23 -7 6 19 70.92 4.29 -7 -6 -19 70.05 4.54 -7 -6 -18 3.59 1.06 -7 6 18 4.43 1.13 -7 6 18 3.87 1.10 7 -6 18 3.62 1.00 7 6 -18 4.47 1.16 -7 -6 -18 4.07 1.03 -7 6 18 3.52 1.03 -7 -6 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2.60 7 6 -5 255.89 10.28 -7 6 5 250.13 10.26 -7 -6 -5 266.23 10.66 -7 6 5 272.34 10.81 -7 6 5 222.35 17.46 7 6 -5 291.67 10.94 -7 -6 -5 280.64 10.97 -7 -6 -5 290.24 11.14 -7 6 5 283.62 10.79 7 6 -5 227.21 18.45 -7 6 4 65.79 8.95 7 6 -4 83.89 5.08 -7 -6 -4 90.75 5.37 -7 6 4 80.67 5.01 -7 6 4 88.19 5.34 -7 6 4 63.52 8.82 7 6 -4 96.51 5.51 -7 -6 -4 98.42 5.67 -7 -6 -4 89.97 5.49 -7 6 4 95.49 5.46 -7 -6 -3 67.81 4.54 -7 6 3 61.73 4.36 -7 6 3 62.15 8.54 -7 -6 -3 69.91 4.71 -7 -6 -3 73.12 4.83 -7 6 3 68.76 4.59 -7 6 3 51.79 7.85 7 6 -3 64.63 4.39 -7 -6 -2 70.26 4.64 7 6 -2 71.47 4.60 -7 6 2 57.81 4.04 -7 6 2 63.60 4.39 -7 6 2 56.11 8.03 -7 6 2 54.81 8.02 -7 -6 -2 74.81 4.70 -7 -6 -2 74.35 4.81 -7 6 2 72.78 4.71 -7 -6 -2 63.60 4.31 -7 6 1 42.20 3.36 -7 6 1 41.55 3.43 -7 -6 -1 42.56 3.54 -7 -6 -1 47.59 3.69 -7 -6 -1 49.49 3.83 -7 6 1 45.76 3.69 7 6 -1 43.46 3.55 -7 6 1 34.57 6.38 -7 -6 -1 44.06 3.57 -7 -6 -1 42.44 3.47 -7 -6 0 387.31 13.45 -7 6 0 328.09 12.73 -7 6 0 348.22 21.67 -7 -6 0 382.51 13.45 -7 -6 0 399.92 13.55 -7 -6 0 415.99 13.89 -7 6 0 411.70 13.80 7 6 0 380.86 13.43 -7 -6 0 362.42 13.19 -7 -6 1 43.17 3.50 7 6 1 48.56 3.77 -7 -6 1 41.43 3.44 -7 -6 1 45.42 3.61 -7 -6 1 48.12 3.78 -7 6 -1 49.83 3.86 -7 6 -1 38.87 6.67 -7 -6 1 40.75 3.47 -7 6 -2 58.74 4.09 -7 -6 2 65.60 4.38 7 6 2 71.45 4.64 -7 6 -2 52.18 7.80 -7 -6 2 56.57 4.11 -7 -6 2 72.19 4.59 -7 -6 2 70.42 4.59 -7 -6 2 72.35 4.69 -7 6 -2 70.96 4.68 -7 -6 2 64.70 4.48 -7 6 -3 60.71 4.19 -7 -6 3 62.00 4.28 -7 6 -3 54.59 8.00 -7 -6 3 60.36 4.32 -7 -6 3 67.26 4.44 -7 -6 3 65.55 4.49 7 6 3 69.46 4.60 -7 -6 3 69.84 4.61 -7 6 -3 72.24 4.71 -7 -6 3 63.64 4.46 -7 6 -4 84.82 5.13 -7 -6 4 95.53 5.39 -7 -6 4 80.25 5.13 -7 -6 4 93.77 5.38 -7 -6 4 91.27 5.40 -7 6 -4 97.74 5.58 7 6 4 96.85 5.57 -7 6 -5 248.09 10.26 7 6 5 287.78 10.99 -7 6 -5 225.68 17.28 -7 -6 5 289.89 10.76 -7 -6 5 267.42 10.61 -7 6 -5 275.49 10.77 7 6 5 237.28 18.75 -7 6 -6 16.87 2.15 7 6 6 19.68 2.52 -7 -6 6 16.71 2.19 -7 -6 6 18.59 2.48 7 6 6 14.16 1.94 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77.47 4.98 -8 6 9 76.62 4.98 8 6 -9 74.43 4.88 -8 -6 -9 66.09 4.61 8 6 -9 76.78 5.12 -8 6 9 61.27 4.36 -8 -6 -8 26.37 2.82 -8 6 8 22.54 2.65 8 6 -8 26.80 2.87 -8 6 8 22.59 2.55 8 6 -8 26.55 2.82 -8 -6 -8 24.01 2.69 8 6 -8 26.12 2.91 -8 6 7 39.92 3.42 -8 -6 -7 48.66 3.90 -8 6 7 42.19 3.72 8 6 -7 48.89 3.88 8 6 -7 48.43 3.92 -8 -6 -7 42.26 3.70 8 6 -7 46.42 3.97 -8 6 6 99.40 5.75 -8 -6 -6 111.72 6.25 -8 6 6 99.90 5.87 8 6 -6 112.83 6.19 8 6 -6 110.47 6.16 -8 -6 -6 106.87 6.15 -8 6 6 105.99 5.94 -8 -6 -6 95.81 5.95 8 6 -6 111.56 6.39 -8 6 5 41.23 3.47 -8 -6 -5 45.54 3.80 -8 6 5 34.23 3.21 -8 -6 -5 35.12 3.24 8 6 -5 40.42 3.53 -8 -6 -5 42.50 3.68 -8 6 5 39.74 3.47 -8 -6 -5 32.44 3.26 8 6 -5 39.51 3.72 -8 6 4 77.42 4.96 -8 -6 -4 90.24 5.43 -8 6 4 76.98 4.98 -8 -6 -4 73.04 4.78 8 6 -4 86.69 5.32 -8 -6 -4 86.35 5.40 -8 -6 -4 84.51 5.41 -8 6 4 80.76 5.13 -8 -6 -4 75.19 5.04 8 6 -3 34.37 3.14 -8 6 3 32.95 3.01 -8 -6 -3 43.50 3.63 -8 6 3 39.38 3.41 -8 6 3 32.26 3.08 -8 -6 -3 36.51 3.18 -8 -6 -3 41.61 3.55 8 6 -3 44.24 3.72 -8 -6 -3 40.34 3.60 -8 -6 -3 44.66 3.78 -8 6 3 42.41 3.58 -8 -6 -3 37.46 3.35 8 6 -2 40.23 3.44 -8 6 2 32.54 3.02 -8 -6 -2 37.87 3.39 8 6 -2 45.28 3.68 -8 -6 -2 42.58 3.67 -8 -6 -2 46.03 3.88 -8 6 2 39.44 3.50 -8 -6 -2 41.01 3.53 -8 6 1 5.04 1.18 -8 -6 -1 7.58 1.55 8 6 -1 7.92 1.51 -8 -6 -1 4.99 1.04 -8 -6 -1 5.77 1.37 -8 -6 -1 6.05 1.40 -8 6 1 5.83 1.39 -8 6 0 11.91 1.79 -8 -6 0 11.51 1.82 8 6 0 10.24 1.71 -8 -6 0 9.58 1.67 -8 -6 0 12.34 1.96 -8 6 0 12.44 1.95 -8 -6 1 6.32 1.39 8 6 1 7.00 1.51 -8 -6 1 4.44 1.03 -8 6 -1 6.06 1.28 -8 -6 1 8.78 1.67 -8 6 -1 7.09 1.53 -8 6 -2 34.96 3.13 -8 -6 2 41.11 3.50 8 6 2 37.58 3.40 -8 6 -2 37.80 3.34 -8 -6 2 34.37 3.17 -8 -6 2 41.05 3.55 -8 6 -2 41.64 3.61 -8 6 -3 35.23 3.15 8 6 3 42.54 3.61 -8 -6 3 39.77 3.42 -8 -6 3 40.73 3.49 -8 6 -3 43.17 3.62 -8 6 -4 73.49 4.84 8 6 4 84.76 5.31 -8 -6 4 83.28 5.12 -8 -6 4 87.90 5.35 -8 6 -4 86.98 5.40 -8 6 -5 39.01 3.41 -8 -6 5 47.71 3.87 8 6 5 45.83 3.78 -8 -6 5 36.29 3.30 -8 -6 5 42.29 3.57 -8 -6 5 45.45 3.71 -8 6 -5 43.57 3.72 -8 6 -6 100.47 5.76 -8 -6 6 113.54 6.20 8 6 6 109.07 6.14 -8 -6 6 93.06 5.60 -8 -6 6 104.98 5.82 -8 -6 6 89.86 5.27 -8 6 -6 104.22 5.94 8 6 6 110.03 6.37 -8 6 -7 45.54 3.67 -8 -6 7 50.73 4.01 8 6 7 50.60 4.03 -8 -6 7 43.35 3.67 -8 -6 7 48.44 3.80 -8 -6 7 37.83 3.23 -8 6 -7 48.36 3.88 8 6 7 43.30 3.85 -8 6 -8 24.49 2.68 -8 -6 8 26.79 2.91 8 6 8 27.31 2.92 -8 -6 8 24.10 2.71 -8 -6 8 23.13 2.58 -8 -6 8 20.69 2.31 -8 6 -8 28.67 2.96 -8 -6 8 21.68 2.34 8 6 8 24.72 2.78 -8 6 -9 69.98 4.71 -8 -6 9 77.39 4.95 8 6 9 80.20 5.16 -8 -6 9 66.33 4.67 -8 -6 9 72.91 4.68 -8 -6 9 59.76 4.14 -8 6 -9 73.78 4.86 8 6 9 59.22 4.42 -8 6 -10 41.82 3.57 -8 -6 10 48.05 3.81 8 6 10 46.62 3.87 -8 -6 10 37.52 3.45 -8 -6 10 42.73 3.50 -8 -6 10 37.49 3.18 -8 -6 10 42.04 3.51 -8 6 -10 44.99 3.71 -8 6 -11 87.96 5.41 -8 -6 11 99.62 5.61 8 6 11 105.19 5.94 -8 -6 11 91.06 5.49 -8 -6 11 80.61 4.89 -8 -6 11 88.33 5.33 -8 6 -11 96.61 5.60 -8 6 -12 47.00 3.74 -8 -6 12 45.94 3.68 8 6 12 52.25 4.03 -8 -6 12 51.33 3.92 -8 -6 12 36.44 3.08 8 6 12 36.21 3.22 -8 -6 12 43.53 3.54 -8 6 -12 49.95 3.81 -8 6 -13 34.14 3.15 -8 -6 13 36.82 3.21 8 6 13 39.08 3.42 -8 -6 13 38.63 3.38 -8 -6 13 36.16 3.23 -8 -6 13 32.20 2.83 8 6 13 27.24 2.78 -8 -6 13 32.63 2.99 -8 6 -13 36.34 3.24 -8 6 -14 33.40 3.07 8 6 14 35.83 3.21 -8 -6 14 33.44 2.93 -8 -6 14 33.29 3.06 -8 -6 14 33.61 3.07 -8 -6 14 26.37 2.49 8 6 14 25.47 2.61 -8 -6 14 29.31 2.77 -8 6 -14 31.10 2.90 -8 6 -15 101.33 5.58 -8 -6 15 117.74 5.69 8 6 15 110.88 5.88 -8 -6 15 106.64 5.52 -8 -6 15 103.22 5.59 8 6 15 118.08 6.14 -8 -6 15 113.93 5.86 -8 -6 15 82.84 4.74 -8 -6 15 94.21 5.23 8 6 15 83.33 5.09 -8 6 -15 93.82 5.27 -8 6 -16 11.73 1.69 -8 -6 16 10.96 1.61 8 6 16 10.35 1.64 -8 -6 16 10.00 1.60 -8 -6 16 10.71 1.58 8 6 16 11.86 1.80 -8 -6 16 11.45 1.73 8 6 16 9.81 1.54 -8 -6 16 7.20 1.30 -8 6 -16 11.28 1.59 -8 6 -17 50.81 3.60 -8 -6 17 54.90 3.56 -8 -6 17 56.33 3.64 -8 -6 17 44.47 3.24 8 6 17 42.40 3.26 -8 6 -17 41.66 3.07 8 6 17 56.76 3.82 -8 6 -18 36.52 2.90 -8 -6 18 43.94 3.05 8 6 18 43.97 3.23 -8 -6 18 42.35 3.00 -8 -6 18 26.28 2.32 8 6 18 30.60 2.63 -8 6 -19 13.80 1.69 -8 -6 19 14.93 1.67 -8 -6 19 15.14 1.71 8 6 19 14.23 1.72 8 6 19 10.39 1.43 -8 -6 20 37.11 2.62 -8 6 -20 35.00 2.60 8 6 20 34.98 2.65 -8 -6 20 39.37 2.67 -8 -7 -19 21.85 2.01 -8 7 19 25.21 2.16 8 7 -19 20.84 1.90 -8 -7 -19 22.22 2.08 -8 -7 -18 11.58 1.55 -8 7 18 11.13 1.51 8 -7 18 9.09 1.34 8 7 -18 12.12 1.49 -8 -7 -18 11.19 1.56 -8 7 18 8.63 1.21 -8 -7 -17 12.97 1.66 -8 7 17 11.74 1.59 8 -7 17 9.73 1.44 8 7 -17 12.68 1.61 -8 7 17 10.47 1.40 -8 -7 -17 14.30 1.85 -8 7 16 5.33 1.15 8 -7 16 4.81 1.03 8 7 -16 3.80 0.95 8 7 -16 3.30 0.84 -8 -7 -16 4.98 1.07 -8 7 16 4.65 0.99 -8 7 15 5.50 1.18 8 7 -15 6.39 1.27 -8 7 15 7.00 1.39 8 -7 15 6.35 1.21 8 7 -15 6.51 1.23 8 7 -15 6.74 1.26 -8 -7 -15 7.22 1.32 -8 7 15 5.41 1.09 -8 7 14 30.55 2.79 8 7 -14 40.04 3.20 -8 7 14 37.07 3.13 8 -7 14 30.39 2.77 8 7 -14 33.17 2.91 8 7 -14 31.40 2.87 -8 -7 -14 37.78 3.29 -8 7 14 29.70 2.62 -8 -7 -13 7.78 1.45 -8 7 13 10.53 1.63 8 7 -13 12.28 1.79 -8 7 13 9.72 1.63 8 -7 13 8.89 1.51 8 7 -13 8.81 1.51 8 7 -13 8.50 1.48 -8 -7 -13 9.98 1.70 -8 -7 -13 14.46 2.09 -8 7 13 9.04 1.43 -8 -7 -12 50.68 3.81 -8 7 12 41.64 3.42 8 7 -12 49.63 3.72 -8 7 12 49.23 3.74 8 7 -12 47.99 3.65 -8 -7 -12 51.94 3.94 -8 -7 -12 40.95 3.28 -8 7 12 41.96 3.24 8 7 -12 43.76 3.57 -8 -7 -11 105.68 5.82 -8 7 11 93.71 5.42 8 7 -11 104.15 5.70 -8 7 11 106.05 5.79 -8 -7 -11 113.61 6.10 -8 -7 -11 97.95 5.47 -8 7 11 81.09 4.86 8 7 -11 92.90 5.55 -8 -7 -10 133.07 6.69 -8 7 10 110.50 6.04 8 7 -10 127.44 6.49 -8 7 10 118.71 6.37 -8 -7 -10 111.86 6.11 8 7 -10 115.44 6.36 -8 -7 -9 252.89 10.15 -8 7 9 214.67 9.41 8 7 -9 261.25 10.16 -8 7 9 245.00 10.01 8 7 -9 255.75 10.13 -8 -7 -9 229.49 9.78 8 7 -9 243.48 10.20 -8 -7 -8 218.29 9.27 -8 7 8 203.04 8.94 8 7 -8 216.44 9.13 8 7 -8 221.14 9.23 -8 -7 -8 195.80 8.92 -8 7 8 188.78 8.56 8 7 -8 211.22 9.35 -8 7 7 41.54 3.43 -8 -7 -7 51.17 4.00 -8 7 7 47.25 3.71 -8 7 7 48.28 3.85 8 7 -7 52.42 4.04 8 7 -7 52.47 4.03 -8 -7 -7 53.77 4.13 -8 -7 -7 46.89 3.88 8 7 -7 54.29 4.21 -8 7 6 181.45 8.37 -8 -7 -6 228.61 9.42 -8 7 6 192.42 8.82 8 7 -6 221.30 9.27 -8 -7 -6 180.98 8.40 8 7 -6 230.79 9.43 -8 -7 -6 229.20 9.54 -8 -7 -6 219.37 9.41 8 7 -6 222.10 9.62 -8 7 5 237.83 10.03 -8 -7 -5 291.72 11.06 -8 7 5 242.28 10.33 8 7 -5 288.65 11.01 8 7 -5 284.25 10.97 -8 -7 -5 280.22 10.91 -8 -7 -5 280.00 11.05 -8 7 5 281.86 10.90 -8 -7 -5 238.86 10.41 8 7 -5 289.00 11.38 8 7 -4 35.91 3.24 -8 7 4 34.66 3.13 -8 -7 -4 43.60 3.63 -8 7 4 38.06 3.33 8 7 -4 46.92 3.80 -8 -7 -4 41.59 3.54 8 7 -4 44.89 3.75 -8 -7 -4 42.13 3.64 -8 -7 -4 39.64 3.57 -8 7 4 43.50 3.65 -8 -7 -4 33.10 3.18 8 7 -4 40.44 3.75 8 7 -3 67.73 4.60 -8 7 3 67.15 4.50 -8 -7 -3 79.29 5.03 -8 7 3 65.05 4.50 -8 -7 -3 74.61 4.88 8 7 -3 80.48 5.11 -8 -7 -3 79.10 5.05 -8 -7 -3 82.49 5.25 -8 7 3 78.27 5.04 8 7 -3 78.51 5.28 -8 7 2 6.61 1.31 -8 -7 -2 6.40 1.36 8 7 -2 7.65 1.50 -8 7 2 6.14 1.35 -8 -7 -2 8.13 1.49 8 7 -2 6.73 1.50 -8 -7 -2 7.23 1.51 -8 -7 -2 7.71 1.61 -8 7 2 8.23 1.74 8 7 -2 10.04 1.87 8 7 -1 33.33 3.18 -8 -7 -1 35.94 3.34 -8 -7 -1 34.37 3.23 8 7 -1 37.39 3.43 -8 -7 -1 36.48 3.35 -8 -7 -1 37.56 3.46 -8 7 1 40.24 3.53 8 7 -1 43.97 3.88 8 7 0 61.33 4.47 -8 -7 0 66.40 4.58 -8 -7 0 65.47 4.55 -8 -7 0 66.40 4.61 -8 7 0 67.24 4.69 8 7 0 67.66 4.96 -8 -7 1 38.28 3.36 8 7 1 33.88 3.22 -8 7 -1 30.70 2.89 -8 -7 1 36.59 3.29 -8 -7 1 39.26 3.47 -8 7 -1 36.75 3.40 8 7 1 37.12 3.59 -8 7 -2 5.61 1.17 8 7 2 8.70 1.65 -8 -7 2 6.58 1.37 -8 -7 2 7.20 1.44 -8 7 -2 8.28 1.72 8 7 2 7.15 1.74 8 7 3 74.51 4.93 -8 -7 3 75.76 4.87 -8 -7 3 82.18 5.13 -8 7 -3 78.96 5.08 -8 7 -3 65.22 4.47 8 7 3 80.84 5.40 8 7 4 45.57 3.75 -8 -7 4 41.87 3.50 -8 -7 4 42.50 3.62 -8 7 -4 44.89 3.86 8 7 4 41.63 3.79 8 7 5 287.39 11.18 -8 -7 5 273.27 10.71 -8 -7 5 288.78 11.04 -8 7 -5 281.59 10.99 8 7 5 287.24 11.47 -8 -7 6 225.70 9.35 8 7 6 224.79 9.41 -8 -7 6 182.14 8.56 -8 -7 6 211.57 8.91 -8 -7 6 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29.85 3.03 -8 -8 -3 29.18 2.99 -8 8 3 30.63 3.04 8 8 -3 33.01 3.30 8 8 -2 56.72 4.19 -8 -8 -2 62.63 4.41 -8 8 2 48.74 3.76 8 8 -2 61.63 4.42 -8 -8 -2 57.04 4.22 8 8 -2 63.69 4.45 -8 -8 -2 62.91 4.46 -8 -8 -2 64.60 4.56 -8 8 2 65.84 4.59 8 8 -2 61.89 4.62 8 8 -1 38.48 3.47 -8 -8 -1 38.20 3.38 8 8 -1 44.98 3.69 -8 -8 -1 39.19 3.45 8 8 -1 43.32 3.61 -8 -8 -1 44.74 3.69 -8 -8 -1 46.32 3.85 -8 8 1 43.96 3.70 8 8 -1 45.06 3.88 -8 -8 0 96.14 5.63 8 8 0 91.97 5.58 -8 -8 0 91.58 5.51 8 8 0 99.10 5.72 -8 -8 0 96.71 5.68 -8 8 0 103.90 5.88 8 8 0 101.63 6.08 -8 -8 1 41.28 3.48 8 8 1 43.13 3.60 -8 -8 1 42.81 3.62 -8 8 -1 46.32 3.79 8 8 1 43.43 3.64 8 8 1 43.68 3.89 8 8 2 63.13 4.44 -8 -8 2 58.10 4.20 -8 -8 2 58.95 4.30 -8 8 -2 61.68 4.44 8 8 2 57.18 4.46 8 8 3 29.86 2.99 -8 -8 3 28.79 2.88 -8 -8 3 27.91 2.86 -8 8 -3 25.31 2.76 8 8 3 26.96 2.99 8 8 4 14.75 2.08 -8 -8 4 12.20 1.91 -8 8 -4 13.49 2.13 8 8 4 12.74 2.05 8 8 5 68.87 4.64 -8 -8 5 52.96 3.96 -8 -8 5 67.70 4.48 -8 8 -5 65.61 4.51 8 8 5 61.27 4.58 -8 -8 6 3.20 1.01 8 8 6 3.71 1.22 -8 -8 6 3.34 0.98 -8 -8 6 2.26 0.88 -8 -8 6 3.19 1.02 -8 8 -6 4.37 1.29 8 8 6 2.97 1.04 -8 -8 7 28.23 2.87 8 8 7 30.27 3.05 -8 -8 7 24.15 2.60 -8 -8 7 27.73 2.76 -8 -8 7 23.64 2.49 -8 8 -7 28.39 2.88 8 8 7 24.11 2.70 -8 -8 8 51.06 3.82 8 8 8 51.98 4.00 -8 -8 8 40.95 3.44 -8 -8 8 44.42 3.53 -8 -8 8 39.74 3.25 -8 8 -8 47.79 3.72 8 8 8 41.03 3.47 -8 -8 9 9.93 1.64 8 8 9 10.27 1.79 -8 -8 9 9.78 1.63 -8 -8 9 8.50 1.52 -8 -8 9 9.18 1.49 -8 8 -9 10.10 1.69 8 8 9 5.88 1.27 -8 -8 10 10.07 1.65 8 8 10 12.22 1.87 -8 -8 10 9.01 1.57 -8 -8 10 6.72 1.27 -8 8 -10 8.79 1.52 -8 -8 11 27.06 2.63 -8 -8 11 23.12 2.45 -8 -8 11 20.51 2.21 8 8 11 17.48 2.05 -8 8 -11 21.17 2.34 8 8 11 25.14 2.61 -8 -8 12 11.90 1.68 8 8 12 15.85 2.06 -8 -8 12 14.03 1.87 -8 -8 12 11.10 1.55 8 8 12 9.78 1.51 -8 8 -12 12.91 1.77 -8 -8 13 32.21 2.73 8 8 13 34.72 2.97 -8 -8 13 36.43 2.93 -8 -8 13 31.34 2.82 -8 -8 13 34.63 2.93 -8 -8 13 27.76 2.46 8 8 13 25.50 2.44 -8 8 -13 28.09 2.57 -8 -8 14 16.69 1.95 8 8 14 16.17 1.96 -8 -8 14 16.55 1.91 -8 -8 14 13.97 1.78 8 8 14 16.03 2.08 -8 -8 14 16.94 1.99 -8 -8 14 14.34 1.67 8 8 14 9.59 1.44 -8 8 -14 12.06 1.59 -8 -8 15 18.72 1.98 8 8 15 19.26 2.09 -8 -8 15 19.34 2.00 -8 -8 15 14.11 1.66 8 8 15 18.55 2.16 -8 -8 15 16.98 1.93 -8 -8 15 13.16 1.52 8 8 15 10.44 1.45 -8 -8 16 0.43 0.50 8 8 16 0.33 0.36 -8 -8 16 0.51 0.33 -8 -8 16 0.46 0.44 8 8 16 1.16 0.58 -8 -8 16 0.34 0.41 -8 -8 16 0.13 0.19 8 8 16 0.31 0.27 -8 -8 17 11.26 1.41 8 8 17 10.14 1.37 -8 -8 17 11.03 1.39 8 8 17 11.60 1.57 -8 -8 17 10.89 1.42 -8 -8 18 1.37 0.49 -8 -8 18 1.23 0.56 8 8 18 0.74 0.44 -8 9 16 32.27 2.43 -8 -9 -16 34.03 2.47 -8 -9 -16 31.85 2.49 -8 -9 -15 45.40 3.02 -8 9 15 39.23 2.82 8 9 -15 33.92 2.57 -8 -9 -15 43.68 2.95 -8 -9 -15 46.19 3.15 -8 -9 -14 0.12 0.29 -8 9 14 0.05 0.37 8 9 -14 1.33 0.65 -8 -9 -14 -0.06 0.43 -8 -9 -14 0.82 0.66 8 9 -13 34.17 2.66 -8 9 13 32.38 2.61 8 9 -13 34.32 2.70 -8 -9 -13 31.55 2.62 -8 -9 -13 34.33 2.72 -8 -9 -13 34.06 2.79 -8 -9 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109.85 5.86 -8 -9 -6 114.27 6.05 -8 -9 -6 107.16 5.89 -8 -9 -6 110.97 5.98 8 9 -6 108.68 6.07 8 9 -5 12.10 1.77 -8 -9 -5 14.43 2.03 -8 9 5 10.61 1.68 8 9 -5 11.69 1.83 -8 -9 -5 12.78 1.84 8 9 -5 13.88 1.96 -8 -9 -5 14.04 2.01 -8 -9 -5 16.04 2.14 8 9 -5 15.12 2.15 -8 -9 -4 8.02 1.48 8 9 -4 7.71 1.47 -8 9 4 8.17 1.45 8 9 -4 9.82 1.64 -8 -9 -4 10.12 1.66 8 9 -4 11.64 1.79 -8 -9 -4 9.57 1.64 -8 -9 -4 9.77 1.74 8 9 -4 10.58 1.88 -8 -9 -3 14.71 2.07 8 9 -3 10.32 1.68 8 9 -3 12.77 1.82 -8 -9 -3 12.29 1.86 8 9 -3 12.60 1.88 -8 -9 -3 15.23 2.08 -8 -9 -3 15.31 2.08 8 9 -3 13.48 2.04 8 9 -2 25.32 2.66 -8 -9 -2 27.76 2.83 8 9 -2 25.08 2.63 -8 -9 -2 27.73 2.73 8 9 -2 25.78 2.69 -8 -9 -2 24.78 2.72 -8 -9 -2 31.72 3.04 8 9 -2 27.06 2.94 8 9 -1 30.49 2.97 -8 -9 -1 30.11 2.98 8 9 -1 27.70 2.77 -8 -9 -1 30.97 2.92 8 9 -1 29.90 2.92 -8 -9 -1 31.67 3.04 -8 -9 -1 32.46 3.09 8 9 -1 30.36 3.13 8 9 0 8.00 1.54 8 9 0 4.29 1.17 -8 -9 0 6.73 1.28 8 9 0 5.58 1.25 -8 -9 0 3.77 1.05 -8 9 0 7.23 1.52 8 9 0 4.50 1.29 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21.39 2.27 -10 4 -11 6.29 1.28 -10 4 -11 7.23 1.38 -10 -4 11 5.43 1.12 10 4 11 6.41 1.33 -10 -4 11 6.77 1.28 -10 -4 11 5.37 1.04 -10 -4 11 5.96 1.23 -10 4 -11 7.06 1.30 -10 4 -12 0.62 0.45 -10 -4 12 0.31 0.39 -10 -4 12 -0.36 0.38 10 4 12 -0.47 0.41 -10 -4 12 0.55 0.50 -10 -4 12 0.22 0.27 -10 -4 12 -0.73 0.54 -10 4 -12 -0.25 0.41 -10 4 -13 17.81 1.99 -10 -4 13 15.37 1.76 10 4 13 17.50 2.05 -10 -4 13 18.04 1.95 -10 -4 13 14.30 1.64 -10 -4 13 22.11 2.25 -10 -4 13 18.29 2.00 -10 4 -13 17.66 1.99 -10 4 -14 7.49 1.26 -10 -4 14 4.48 0.92 -10 -4 14 6.02 1.08 10 4 14 5.76 1.15 -10 -4 14 7.07 1.25 -10 -4 14 5.41 0.95 -10 -4 14 6.73 1.19 -10 4 -14 6.53 1.21 -10 4 -15 21.25 2.06 -10 -4 15 21.30 1.93 10 4 15 18.79 1.99 -10 -4 15 16.87 1.75 -10 -4 15 17.90 1.85 -10 -4 15 22.29 2.09 -10 -4 15 21.28 2.03 -10 4 -15 18.34 1.89 -10 4 -16 11.89 1.44 10 4 16 11.83 1.49 -10 4 -16 11.59 1.46 -10 -4 16 13.20 1.52 -10 -4 16 12.04 1.45 -10 4 -16 10.50 1.34 -10 5 15 20.37 1.88 -10 -5 -15 21.58 1.99 10 5 -15 21.34 1.95 -10 -5 -15 19.99 1.88 -10 -5 -15 20.11 1.97 -10 -5 -14 24.64 2.10 -10 5 14 32.41 2.47 10 5 -14 29.97 2.43 -10 5 14 28.56 2.30 -10 -5 -14 34.48 2.65 10 5 -14 34.56 2.62 -10 -5 -14 32.13 2.48 -10 -5 -14 32.47 2.64 -10 5 14 22.72 1.97 -10 -5 -13 0.38 0.27 -10 5 13 1.06 0.57 10 5 -13 0.58 0.46 -10 5 13 1.04 0.51 -10 -5 -13 0.89 0.64 10 5 -13 -0.13 0.33 -10 -5 -13 0.25 0.44 -10 -5 -13 0.44 0.46 -10 -5 -12 10.82 1.46 -10 5 12 10.83 1.49 10 5 -12 11.91 1.57 -10 5 12 8.51 1.29 -10 -5 -12 12.19 1.67 -10 -5 -12 12.15 1.59 -10 -5 -12 10.27 1.55 -10 5 12 6.73 1.08 -10 5 11 1.29 0.54 -10 -5 -11 3.67 0.97 -10 5 11 2.51 0.75 10 5 -11 3.32 0.94 -10 5 11 2.21 0.69 -10 -5 -11 2.68 0.82 -10 -5 -11 3.43 0.89 -10 -5 -11 2.49 0.85 -10 5 11 1.04 0.45 10 5 -11 1.69 0.65 -10 -5 -10 14.03 1.79 -10 5 10 9.12 1.35 -10 5 10 13.95 1.80 10 5 -10 13.22 1.77 -10 5 10 10.57 1.48 -10 -5 -10 12.38 1.69 -10 -5 -10 13.75 1.77 -10 -5 -10 13.69 1.84 10 5 -10 12.59 1.71 -10 5 9 10.96 1.55 -10 -5 -9 10.26 1.56 -10 5 9 10.47 1.57 10 5 -9 11.65 1.69 -10 5 9 8.42 1.35 -10 -5 -9 9.21 1.49 -10 -5 -9 11.77 1.73 -10 -5 -9 11.87 1.75 10 5 -9 9.27 1.51 -10 5 8 10.30 1.59 -10 5 8 8.27 1.38 -10 -5 -8 7.34 1.32 -10 5 8 9.39 1.53 10 5 -8 10.34 1.59 -10 -5 -8 6.92 1.32 -10 -5 -8 10.57 1.62 -10 -5 -8 7.16 1.36 10 5 -8 9.25 1.58 -10 5 7 39.92 3.19 -10 -5 -7 36.26 3.08 -10 5 7 34.08 2.88 10 5 -7 44.23 3.46 -10 -5 -7 35.19 3.04 -10 -5 -7 40.15 3.30 -10 -5 -7 32.72 2.93 10 5 -7 40.48 3.42 -10 5 6 33.71 3.00 -10 -5 -6 35.17 3.04 10 5 -6 41.28 3.36 -10 -5 -6 31.59 2.87 10 5 -6 31.32 2.77 -10 -5 -6 37.01 3.15 -10 -5 -6 30.25 2.81 10 5 -6 36.29 3.27 -10 -5 -5 11.44 1.67 -10 5 5 14.34 1.94 -10 -5 -5 12.06 1.74 10 5 -5 14.62 2.02 -10 -5 -5 12.46 1.72 10 5 -5 11.26 1.64 -10 -5 -5 13.41 1.87 10 5 -5 14.16 2.06 -10 -5 -4 9.37 1.56 -10 5 4 9.53 1.59 -10 -5 -4 10.81 1.66 10 5 -4 11.87 1.82 -10 -5 -4 8.75 1.48 10 5 -4 9.11 1.48 -10 -5 -4 10.60 1.70 -10 5 4 7.64 1.29 -10 -5 -3 8.84 1.55 -10 5 3 8.43 1.57 -10 -5 -3 8.39 1.45 -10 -5 -3 8.37 1.43 10 5 -3 6.69 1.27 -10 -5 -3 7.70 1.45 -10 5 3 9.44 1.56 -10 -5 -2 42.90 3.48 -10 5 2 49.20 3.68 -10 5 2 45.74 3.50 10 5 -2 44.27 3.46 10 -5 2 42.98 3.49 -10 -5 -2 44.24 3.54 -10 5 2 40.84 3.34 -10 -5 -1 25.90 2.69 -10 5 1 30.14 2.86 -10 5 1 27.86 2.72 10 5 -1 27.10 2.70 10 -5 1 26.92 2.69 -10 -5 -1 27.76 2.79 -10 5 1 25.71 2.63 -10 -5 0 54.73 3.97 -10 5 0 50.30 3.78 10 -5 0 48.22 3.60 10 5 0 51.64 3.85 -10 -5 0 54.10 3.94 -10 5 0 56.77 4.01 -10 -5 1 26.70 2.72 -10 5 -1 26.35 2.68 10 5 1 28.55 2.78 -10 -5 1 27.29 2.69 -10 5 -1 28.42 2.79 -10 -5 2 47.93 3.72 -10 5 -2 45.15 3.57 -10 -5 2 44.67 3.51 -10 5 -2 47.93 3.71 -10 -5 2 46.80 3.64 -10 -5 3 8.00 1.57 -10 5 -3 7.57 1.42 -10 5 -3 8.79 1.55 -10 -5 3 8.45 1.51 -10 -5 4 9.85 1.65 -10 5 -4 10.27 1.63 10 5 4 7.42 1.30 -10 5 -4 10.09 1.69 -10 -5 4 10.00 1.62 -10 -5 5 13.72 2.03 -10 5 -5 12.58 1.81 10 5 5 11.70 1.71 -10 -5 5 15.15 2.13 -10 5 -5 11.96 1.80 -10 -5 5 11.78 1.74 10 5 5 13.91 2.00 -10 5 -6 31.67 2.86 -10 -5 6 34.32 3.08 10 5 6 33.26 2.93 -10 5 -6 35.24 3.09 -10 -5 6 38.35 3.32 -10 5 -6 35.58 3.14 -10 -5 6 34.42 2.96 10 5 6 35.15 3.22 -10 5 -7 37.54 3.09 -10 -5 7 41.66 3.31 10 5 7 34.34 2.99 -10 5 -7 34.83 3.07 -10 -5 7 36.56 2.99 -10 -5 7 45.23 3.57 -10 5 -7 40.43 3.26 -10 -5 7 36.18 3.00 10 5 7 34.49 3.11 -10 5 -8 8.21 1.44 -10 -5 8 9.08 1.52 -10 5 -8 8.08 1.45 -10 -5 8 8.02 1.34 10 5 8 7.41 1.36 -10 5 -8 11.26 1.71 -10 -5 8 7.86 1.31 10 5 8 8.64 1.51 -10 5 -9 10.49 1.57 -10 -5 9 13.96 1.89 -10 5 -9 10.29 1.61 -10 -5 9 9.80 1.47 10 5 9 10.42 1.61 -10 -5 9 14.36 1.97 -10 -5 9 12.09 1.72 -10 5 -9 11.11 1.64 -10 -5 9 7.24 1.20 10 5 9 6.64 1.24 -10 5 -10 11.51 1.62 -10 5 -10 11.15 1.60 -10 -5 10 10.45 1.48 10 5 10 11.47 1.65 -10 -5 10 14.15 1.72 -10 -5 10 15.18 1.95 -10 -5 10 14.88 1.88 -10 5 -10 14.45 1.82 -10 5 -11 3.37 0.89 -10 5 -11 3.38 0.95 -10 -5 11 2.18 0.62 10 5 11 1.86 0.72 -10 -5 11 3.38 0.97 -10 -5 11 3.66 0.87 -10 -5 11 3.36 0.89 -10 5 -11 2.59 0.82 -10 5 -12 11.37 1.57 -10 5 -12 11.32 1.64 -10 -5 12 6.84 1.12 -10 -5 12 11.12 1.50 10 5 12 10.57 1.55 -10 -5 12 11.58 1.64 -10 -5 12 9.55 1.35 -10 5 -12 11.90 1.58 -10 -5 12 10.73 1.51 -10 5 -13 0.48 0.31 -10 5 -13 0.58 0.52 -10 -5 13 0.51 0.38 10 5 13 0.02 0.40 -10 -5 13 0.97 0.48 -10 -5 13 -0.10 0.33 -10 -5 13 -0.13 0.32 -10 5 -13 0.25 0.34 -10 5 -14 31.51 2.46 -10 -5 14 33.03 2.45 10 5 14 33.32 2.64 -10 5 -14 31.44 2.52 -10 -5 14 27.02 2.16 -10 -5 14 35.49 2.68 -10 -5 14 27.02 2.27 -10 5 -14 33.82 2.56 -10 5 -15 17.94 1.76 -10 -5 15 19.55 1.78 10 5 15 18.39 1.87 -10 5 -15 20.86 1.94 -10 -5 15 19.57 1.86 -10 5 -15 17.14 1.70 10 6 -14 9.60 1.26 -10 -6 -14 10.04 1.27 -10 -6 -13 5.22 0.94 10 6 -13 6.25 1.08 -10 -6 -13 3.90 0.81 10 6 -13 5.89 1.03 -10 -6 -13 5.43 1.00 -10 -6 -13 4.70 0.94 -10 -6 -12 22.84 2.06 -10 6 12 20.10 1.90 10 6 -12 24.04 2.18 -10 6 12 18.16 1.80 -10 -6 -12 19.96 1.95 10 6 -12 24.41 2.17 10 6 -12 13.60 1.60 -10 -6 -12 25.18 2.25 -10 -6 -12 21.97 2.13 -10 -6 -11 30.36 2.46 -10 6 11 23.54 2.12 10 6 -11 30.16 2.52 -10 6 11 19.67 1.94 -10 -6 -11 24.43 2.21 -10 -6 -11 28.77 2.48 -10 -6 -11 24.98 2.32 10 6 -11 16.76 1.82 -10 -6 -10 27.47 2.41 -10 6 10 23.54 2.18 10 6 -10 32.23 2.67 -10 6 10 21.12 2.03 -10 -6 -10 23.79 2.23 -10 -6 -10 29.52 2.57 -10 -6 -10 22.76 2.28 10 6 -10 23.41 2.28 -10 -6 -9 10.94 1.55 -10 6 9 7.42 1.27 10 6 -9 13.34 1.78 -10 -6 -9 9.36 1.39 -10 -6 -9 12.27 1.69 -10 -6 -9 8.99 1.40 10 6 -9 11.13 1.61 -10 -6 -8 3.53 0.92 -10 6 8 1.56 0.58 10 6 -8 3.11 0.88 -10 -6 -8 2.33 0.81 -10 -6 -8 4.07 1.01 -10 -6 -8 2.41 0.77 10 6 -8 3.45 1.03 -10 -6 -7 0.92 0.53 -10 6 7 0.23 0.28 10 6 -7 0.50 0.50 -10 -6 -7 1.48 0.64 -10 -6 -7 0.11 0.40 -10 -6 -7 1.31 0.59 10 6 -7 1.24 0.68 -10 -6 -6 48.88 3.45 -10 6 6 52.59 3.60 -10 -6 -6 58.00 3.89 -10 6 6 52.97 3.53 10 6 -6 65.94 4.14 -10 -6 -6 42.98 3.21 10 6 -6 54.22 3.67 -10 -6 -6 62.51 4.08 10 6 -6 64.22 4.25 -10 -6 -5 18.89 2.09 -10 -6 -5 20.01 2.25 -10 6 5 18.26 2.07 -10 6 5 17.79 1.98 10 6 -5 23.36 2.43 10 6 -5 20.75 2.21 -10 -6 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4.93 0.95 -11 6 -1 5.80 1.06 -11 -6 1 6.32 1.14 11 6 1 4.90 1.03 -11 -6 2 13.87 1.66 -11 6 -2 11.94 1.45 -11 -6 2 11.97 1.53 11 6 2 11.97 1.49 -11 6 -2 14.36 1.66 -11 -6 2 15.57 1.73 11 6 2 14.77 1.81 -11 -6 3 0.54 0.49 -11 6 -3 0.56 0.35 -11 -6 3 1.04 0.51 11 6 3 0.29 0.35 -11 6 -3 0.86 0.53 -11 -6 3 1.09 0.54 11 6 3 0.69 0.43 -11 -6 4 -0.11 0.30 -11 6 -4 0.38 0.34 -11 6 -4 0.25 0.30 -11 -6 4 0.37 0.35 11 6 4 0.08 0.25 -11 6 -4 0.77 0.45 -11 -6 4 -0.02 0.25 11 6 4 0.28 0.35 -11 6 -5 3.85 0.81 -11 6 -5 4.11 0.85 -11 -6 5 6.04 1.12 11 6 5 4.64 0.91 -11 -6 5 4.72 0.91 -11 6 -5 4.59 0.92 -11 -6 5 4.15 0.84 11 6 5 4.86 0.97 -11 -6 6 -0.27 0.43 11 6 6 -0.37 0.41 -11 6 -6 0.90 0.52 -11 -6 7 3.88 0.87 11 6 7 2.65 0.62 -11 6 -7 5.13 0.97 -11 -6 8 3.64 0.80 -11 6 -8 5.30 0.94 11 7 -4 7.21 1.09 -11 -7 -4 6.80 1.07 11 7 -4 6.78 1.10 11 7 -3 19.67 1.84 -11 -7 -3 17.91 1.77 11 7 -3 20.01 1.95 11 7 -2 6.86 1.10 -11 -7 -2 5.41 0.97 11 7 -2 6.71 1.14 11 7 -1 17.81 1.77 -11 -7 -1 17.26 1.73 11 7 -1 16.64 1.81 11 7 0 1.99 0.60 -11 -7 0 1.27 0.49 11 7 0 1.75 0.63 -11 -7 1 15.31 1.62 11 7 1 17.00 1.72 -11 -7 1 16.46 1.66 11 7 1 16.64 1.79 -11 -7 2 4.06 0.83 11 7 2 5.44 0.95 11 7 2 5.04 0.97 -11 -7 3 18.91 1.81 11 7 3 15.90 1.65 -11 7 -3 19.30 1.82 -11 -7 4 6.26 1.02 -11 7 -4 8.45 1.18 -12 0 0 5.48 1.03 -12 0 1 0.18 0.37 -12 0 -1 0.01 0.42 -12 0 -1 0.93 0.49 -12 0 2 39.22 2.87 -12 0 -2 40.96 2.92 -12 0 -2 35.56 2.70 -12 0 3 22.57 2.11 -12 0 -3 20.14 1.99 -12 0 -3 17.57 1.80 -12 0 4 1.41 0.69 -12 0 -4 0.84 0.46 -12 0 -4 1.09 0.38 -12 0 -5 0.28 0.36 12 0 5 0.96 0.47 -12 0 5 -0.07 0.33 -12 0 -6 0.42 0.34 -12 0 6 -0.01 0.27 12 0 6 0.00 0.40 -12 0 6 0.67 0.34 -12 0 -7 5.45 0.96 -12 0 7 5.13 0.93 12 0 7 4.46 0.91 -12 0 7 4.02 0.80 -12 0 8 15.34 1.58 12 0 8 13.92 1.54 -12 1 7 18.12 1.76 12 -1 7 16.52 1.72 -12 1 6 6.63 1.08 12 -1 6 7.71 1.21 -12 1 5 11.54 1.46 -12 -1 -5 8.63 1.23 12 -1 5 9.80 1.37 -12 1 5 10.32 1.31 -12 -1 -5 6.95 1.06 -12 1 4 2.54 0.71 -12 -1 -4 1.83 0.59 12 -1 4 2.04 0.60 -12 1 4 2.43 0.67 -12 -1 -4 3.09 0.77 -12 1 3 3.76 0.82 -12 -1 -3 4.13 0.90 12 -1 3 3.42 0.82 -12 -1 -3 3.79 0.83 -12 1 2 6.82 1.16 -12 -1 -2 4.44 0.92 12 1 -2 4.68 0.90 -12 -1 -2 6.07 1.07 -12 1 1 1.17 0.44 -12 -1 -1 0.52 0.36 12 1 -1 0.98 0.49 -12 -1 -1 -0.20 0.35 -12 -1 0 4.81 0.98 -12 1 0 5.54 1.03 -12 -1 0 5.15 1.05 -12 -1 1 -0.20 0.42 -12 1 -1 0.41 0.41 -12 -1 1 0.43 0.40 -12 -1 2 4.88 0.99 -12 1 -2 5.89 1.10 -12 -1 2 4.98 0.95 -12 -1 3 2.18 0.64 -12 1 -3 4.07 0.94 -12 1 -4 2.48 0.73 -12 1 -5 11.54 1.50 -12 -1 5 13.06 1.55 -12 1 -6 6.77 1.11 -12 -1 6 6.93 1.11 -12 -1 6 7.71 1.17 -12 1 -7 16.93 1.71 -12 1 -7 17.00 1.73 -12 -1 7 18.24 1.76 -12 -1 7 17.54 1.73 -12 2 6 17.16 1.70 12 -2 6 16.14 1.72 -12 2 5 43.52 2.83 12 -2 5 39.59 2.80 -12 -2 -5 37.26 2.59 -12 2 4 18.06 1.81 12 -2 4 16.41 1.75 -12 -2 -4 18.73 1.82 -12 2 3 91.01 4.42 12 2 -3 66.90 3.79 12 -2 3 70.95 3.98 -12 -2 -3 91.05 4.34 -12 2 2 14.76 1.67 12 2 -2 13.30 1.57 12 -2 2 13.61 1.57 -12 -2 -2 15.26 1.68 -12 2 1 74.11 3.94 12 2 -1 63.29 3.63 -12 -2 -1 70.45 3.82 -12 -2 0 -0.22 0.38 -12 2 0 0.90 0.53 -12 -2 0 1.45 0.59 -12 2 -1 71.25 3.86 -12 -2 1 72.67 3.87 -12 2 -2 13.79 1.60 -12 -2 2 15.49 1.71 -12 2 -3 90.88 4.55 -12 -2 3 90.07 4.51 -12 2 -4 18.27 1.86 -12 2 -5 47.75 3.06 -12 -2 5 43.41 2.92 -12 -2 5 51.45 3.14 -12 2 -6 19.06 1.82 -12 2 -6 16.69 1.71 -12 -2 6 15.30 1.63 -12 -2 6 18.22 1.76 -12 2 -7 33.45 2.42 -12 2 -7 31.81 2.37 -12 -2 7 34.74 2.43 -12 3 4 21.50 1.94 -12 -3 -4 23.65 2.01 12 3 -4 20.38 1.97 -12 3 3 36.15 2.56 12 3 -3 31.15 2.41 -12 -3 -3 35.22 2.52 12 3 -3 33.69 2.62 -12 3 2 14.31 1.61 12 3 -2 14.33 1.59 -12 -3 -2 14.67 1.61 12 3 -2 14.78 1.71 -12 3 1 32.78 2.48 12 3 -1 30.24 2.40 -12 -3 -1 30.25 2.37 12 3 -1 29.42 2.46 -12 3 0 25.69 2.19 12 3 0 28.12 2.29 -12 -3 0 24.67 2.13 12 3 0 24.11 2.23 -12 3 -1 30.05 2.37 -12 -3 1 30.99 2.40 12 3 1 28.35 2.42 -12 3 -2 17.09 1.75 -12 -3 2 17.08 1.74 12 3 2 14.44 1.70 -12 3 -3 37.23 2.61 -12 -3 3 34.07 2.49 12 3 3 29.43 2.43 -12 3 -4 21.53 1.94 -12 -3 4 21.16 1.90 -12 3 -5 2.32 0.64 -12 -3 5 4.04 0.82 12 4 -2 30.75 2.40 -12 -4 -1 3.84 0.81 12 4 -1 1.92 0.61 12 4 0 47.27 2.99 -12 -4 0 52.39 3.07 12 4 0 47.10 3.07 12 4 1 3.34 0.78 -12 -4 1 3.24 0.76 TITL exp_3361 in P2(1)2(1)2(1) REM P2(1)2(1)2(1) (#19 in standard setting) CELL 1.54184 10.358071 13.403916 26.168851 90.0000 90.0000 90.0000 ZERR 16.00 0.000064 0.000079 0.000171 0.0000 0.0000 0.0000 LATT -1 SYMM -x+1/2,-y, z+1/2 SYMM -x, y+1/2,-z+1/2 SYMM x+1/2,-y+1/2,-z SFAC C H N O UNIT 176.00 160.00 16.00 16.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 17715 _shelx_res_file ; REM 16SAN102, sample 4FC REM colourless square plate TITL s92_a.res in P2(1)2(1)2(1) REM Old TITL exp_3361 in P2(1)2(1)2(1) REM SHELXT solution in P2(1)2(1)2(1) REM R1 0.119, Rweak 0.029, Alpha 0.001, Orientation as input REM Flack x = 0.113 ( 0.043 ) from Parsons' quotients REM Formula found by SHELXT: C37 N3 O12 CELL 1.54184 10.3581 13.4039 26.1689 90.000 90.000 90.000 ZERR 4.000 0.0001 0.0001 0.0002 0.000 0.000 0.000 LATT -1 SYMM 1/2-X, -Y, 1/2+Z SYMM -X, 1/2+Y, 1/2-Z SYMM 1/2+X, 1/2-Y, -Z SFAC C H N O UNIT 144 220 4 60 L.S. 20 SIZE .25 .15 .05 TEMP -100 HTAB BOND $H SHEL 999 0.80 EQIV $4 x, y-1, z EQIV $3 x-1/2, -y+1/2, -z+1 EQIV $7 x-1/2, -y+3/2, -z+1 HTAB N8 O1O_$4 HTAB O42 O3O_$3 HTAB O46 O5O HTAB O6O O1O_$7 CONF ACTA BOND $H LIST 6 FMAP 2 PLAN 20 DFIX .84 .01 O46 H46 O42 H42 O6o H6o DFIX .88 .01 N8 H8 WGHT 0.080700 1.840000 FVAR 0.38758 O1 4 0.727072 0.231526 0.600032 11.00000 0.02651 0.01801 = 0.02162 0.00017 -0.00562 -0.00447 C2 1 0.688550 0.125765 0.600782 11.00000 0.02263 0.01470 = 0.02152 0.00185 -0.00278 0.00035 AFIX 13 H2 2 0.757523 0.085401 0.617738 11.00000 -1.20000 AFIX 0 C3 1 0.561647 0.113068 0.629877 11.00000 0.02781 0.01928 = 0.01976 0.00160 0.00127 -0.00135 AFIX 13 H3 2 0.548011 0.040396 0.636629 11.00000 0.01704 AFIX 0 C4 1 0.448705 0.151619 0.598563 11.00000 0.01990 0.02409 = 0.02733 -0.00022 0.00304 0.00140 AFIX 23 H4A 2 0.463191 0.222863 0.590398 11.00000 -1.20000 H4B 2 0.368804 0.146838 0.619179 11.00000 -1.20000 AFIX 0 C5 1 0.430426 0.092848 0.548443 11.00000 0.01733 0.02434 = 0.02707 -0.00048 0.00034 0.00033 AFIX 23 H5A 2 0.360258 0.043635 0.553384 11.00000 -1.20000 H5B 2 0.402492 0.139766 0.521398 11.00000 -1.20000 AFIX 0 C6 1 0.551641 0.037522 0.529895 11.00000 0.01891 0.01501 = 0.02486 0.00325 -0.00052 -0.00135 C7 1 0.551389 0.026946 0.470540 11.00000 0.01967 0.01784 = 0.02379 -0.00137 -0.00100 0.00188 AFIX 13 H7 2 0.470869 -0.009446 0.460688 11.00000 -1.20000 AFIX 0 N8 3 0.664986 -0.038993 0.456874 11.00000 0.02520 0.01792 = 0.02435 -0.00196 -0.00037 0.00168 H8 2 0.655627 -0.095083 0.473849 11.00000 0.02781 C9 1 0.790836 0.010756 0.470103 11.00000 0.01819 0.02255 = 0.02907 0.00035 0.00232 0.00270 AFIX 23 H9A 2 0.800196 0.072966 0.450051 11.00000 -1.20000 H9B 2 0.863496 -0.033994 0.461233 11.00000 -1.20000 AFIX 0 C10 1 0.794967 0.034748 0.526649 11.00000 0.01889 0.02034 = 0.02619 0.00068 -0.00164 0.00193 AFIX 23 H10A 2 0.873480 0.074289 0.534080 11.00000 -1.20000 H10B 2 0.800416 -0.028196 0.546324 11.00000 -1.20000 AFIX 0 C11 1 0.675921 0.093337 0.544013 11.00000 0.01837 0.01352 = 0.02152 0.00230 -0.00079 -0.00069 C12 1 0.664151 0.193712 0.518285 11.00000 0.01625 0.01642 = 0.02123 0.00239 0.00005 0.00125 C13 1 0.695323 0.267366 0.552303 11.00000 0.01755 0.01610 = 0.02168 0.00409 0.00117 -0.00085 C14 1 0.684005 0.367878 0.539015 11.00000 0.01766 0.01687 = 0.02436 -0.00046 -0.00002 -0.00248 C15 1 0.633854 0.387378 0.490729 11.00000 0.02114 0.01647 = 0.02773 0.00369 0.00052 0.00070 AFIX 43 H15 2 0.625398 0.454850 0.480131 11.00000 -1.20000 AFIX 0 C16 1 0.595424 0.312082 0.457180 11.00000 0.02186 0.02276 = 0.02188 0.00227 -0.00077 0.00142 AFIX 43 H16 2 0.559828 0.328867 0.424847 11.00000 0.02482 AFIX 0 C17 1 0.609304 0.211794 0.471153 11.00000 0.01863 0.01556 = 0.02179 -0.00009 0.00246 0.00224 C18 1 0.553153 0.126548 0.440949 11.00000 0.02400 0.01976 = 0.02138 -0.00210 -0.00277 0.00098 AFIX 23 H18A 2 0.604128 0.117771 0.409265 11.00000 -1.20000 H18B 2 0.463736 0.143765 0.430909 11.00000 -1.20000 AFIX 0 O19 4 0.562363 0.164567 0.677528 11.00000 0.03727 0.02832 = 0.01905 -0.00004 0.00022 0.00360 C20 1 0.627969 0.112990 0.717018 11.00000 0.04105 0.05147 = 0.02200 0.00204 -0.00195 0.01078 AFIX 23 H20A 2 0.719226 0.102337 0.707185 11.00000 -1.20000 H20B 2 0.587482 0.046944 0.722495 11.00000 -1.20000 AFIX 0 C21 1 0.621540 0.173132 0.765440 11.00000 0.03873 0.05818 = 0.02346 -0.00059 -0.00296 0.00024 AFIX 23 H21A 2 0.679743 0.143405 0.791297 11.00000 -1.20000 H21B 2 0.651303 0.242025 0.758569 11.00000 -1.20000 AFIX 0 O22 4 0.495543 0.175635 0.784572 11.00000 0.04190 0.05981 = 0.02563 -0.00239 0.00249 0.00386 C23 1 0.491164 0.238146 0.829482 11.00000 0.06003 0.06514 = 0.03293 -0.00924 -0.00697 0.00410 AFIX 23 H23A 2 0.517206 0.306826 0.820132 11.00000 -1.20000 H23B 2 0.553585 0.212808 0.855022 11.00000 -1.20000 AFIX 0 C24 1 0.363110 0.240405 0.851998 11.00000 0.07441 0.08991 = 0.03197 -0.00943 -0.00824 0.04218 AFIX 23 H24A 2 0.333111 0.170977 0.857054 11.00000 -1.20000 H24B 2 0.368659 0.272248 0.886062 11.00000 -1.20000 AFIX 0 O25 4 0.271760 0.291476 0.822758 11.00000 0.07108 0.10212 = 0.02756 -0.00707 -0.00562 0.04746 C26 1 0.192436 0.354530 0.850158 11.00000 0.05846 0.04409 = 0.03915 -0.01133 -0.00671 0.01038 AFIX 23 H26A 2 0.244657 0.409587 0.864604 11.00000 -1.20000 H26B 2 0.153467 0.317299 0.878961 11.00000 -1.20000 AFIX 0 C27 1 0.087632 0.397122 0.817698 11.00000 0.04660 0.05629 = 0.03921 -0.00364 0.00111 0.01061 AFIX 23 H27A 2 0.126945 0.431563 0.788069 11.00000 -1.20000 H27B 2 0.033679 0.341960 0.804402 11.00000 -1.20000 AFIX 0 O28 4 0.008064 0.465017 0.844236 11.00000 0.05799 0.04582 = 0.05337 -0.00531 -0.00218 0.01145 C29 1 -0.085169 0.427265 0.876384 11.00000 0.06984 0.10525 = 0.05890 0.01989 0.01638 0.02613 AFIX 23 H29A 2 -0.105671 0.479315 0.901968 11.00000 -1.20000 H29B 2 -0.046852 0.370341 0.895120 11.00000 -1.20000 AFIX 0 C30 1 -0.205632 0.393741 0.854241 11.00000 0.07422 0.10011 = 0.06714 0.03148 -0.00761 -0.01279 AFIX 23 H30A 2 -0.183051 0.346314 0.826652 11.00000 -1.20000 H30B 2 -0.250619 0.354630 0.880940 11.00000 -1.20000 AFIX 0 O31 4 -0.296957 0.460132 0.833765 11.00000 0.05382 0.06168 = 0.05678 0.00501 0.01512 0.00986 C32 1 -0.261213 0.522340 0.792598 11.00000 0.04810 0.03209 = 0.04511 -0.00587 0.00256 0.00651 AFIX 23 H32A 2 -0.172853 0.547841 0.798711 11.00000 -1.20000 H32B 2 -0.320247 0.580392 0.791565 11.00000 -1.20000 AFIX 0 C33 1 -0.264489 0.470945 0.741759 11.00000 0.03245 0.04863 = 0.04106 -0.00557 -0.00106 0.00852 AFIX 23 H33A 2 -0.345347 0.432089 0.738480 11.00000 -1.20000 H33B 2 -0.262387 0.521147 0.714023 11.00000 -1.20000 AFIX 0 C35 1 -0.152423 0.357694 0.689416 11.00000 0.03424 0.04657 = 0.02480 -0.00859 -0.00082 -0.00121 AFIX 23 H35A 2 -0.143749 0.407367 0.661630 11.00000 -1.20000 H35B 2 -0.232985 0.319511 0.683773 11.00000 -1.20000 AFIX 0 O34 4 -0.157418 0.406785 0.737365 11.00000 0.03383 0.04955 = 0.02946 -0.01140 -0.00373 0.01016 C36 1 -0.039332 0.288815 0.689120 11.00000 0.03657 0.03510 = 0.02941 -0.00804 0.00302 -0.00351 AFIX 23 H36A 2 -0.042198 0.245315 0.719673 11.00000 -1.20000 H36B 2 -0.042717 0.245810 0.658393 11.00000 -1.20000 AFIX 0 O37 4 0.077501 0.344910 0.689084 11.00000 0.02830 0.03132 = 0.03183 -0.00013 -0.00006 0.00494 C38 1 0.186269 0.280962 0.693532 11.00000 0.03797 0.03231 = 0.03146 0.00285 0.00234 0.01217 AFIX 23 H38A 2 0.190028 0.235994 0.663558 11.00000 -1.20000 H38B 2 0.177346 0.239289 0.724566 11.00000 -1.20000 AFIX 0 C39 1 0.308055 0.340098 0.696661 11.00000 0.03645 0.04065 = 0.02729 0.00124 -0.00432 0.00991 AFIX 23 H39A 2 0.299455 0.392155 0.723281 11.00000 -1.20000 H39B 2 0.380583 0.295810 0.706276 11.00000 -1.20000 AFIX 0 O40 4 0.334200 0.385584 0.648593 11.00000 0.02877 0.04891 = 0.03040 0.00524 -0.00336 -0.00035 C41 1 0.459932 0.427697 0.647741 11.00000 0.02941 0.05495 = 0.04353 0.00140 -0.00542 -0.00139 AFIX 137 H41A 2 0.467688 0.477269 0.675096 11.00000 -1.50000 H41B 2 0.474783 0.459959 0.614653 11.00000 -1.50000 H41C 2 0.524125 0.374934 0.652886 11.00000 -1.50000 AFIX 0 O42 4 0.558851 -0.060686 0.551183 11.00000 0.02642 0.01514 = 0.03037 0.00432 -0.00082 -0.00442 H42 2 0.490148 -0.090535 0.543791 11.00000 0.03472 C43 1 0.668870 -0.073735 0.401946 11.00000 0.04102 0.02311 = 0.02483 -0.00669 0.00048 0.00551 AFIX 23 H43A 2 0.689418 -0.016016 0.379787 11.00000 -1.20000 H43B 2 0.739375 -0.123033 0.398099 11.00000 -1.20000 AFIX 0 C44 1 0.545963 -0.119717 0.383977 11.00000 0.05111 0.02500 = 0.03357 -0.00616 -0.00332 -0.00647 AFIX 43 H44 2 0.504633 -0.167592 0.405164 11.00000 -1.20000 AFIX 0 C45 1 0.492570 -0.096699 0.340052 11.00000 0.05691 0.04416 = 0.04275 -0.00304 -0.01278 -0.00389 AFIX 93 H45A 2 0.532367 -0.049001 0.318307 11.00000 -1.20000 H45B 2 0.414124 -0.127736 0.330001 11.00000 -1.20000 AFIX 0 O46 4 0.720756 0.440430 0.572693 11.00000 0.03362 0.01460 = 0.03015 -0.00063 -0.00510 -0.00377 H46 2 0.702420 0.494914 0.558401 11.00000 0.04845 MOLE 2 O1O 4 0.787112 0.778186 0.492459 11.00000 0.02086 0.01699 = 0.06623 0.00616 0.00428 -0.00149 C2O 1 0.747413 0.689768 0.498071 11.00000 0.01798 0.01634 = 0.03638 0.00000 -0.00233 0.00095 O3O 4 0.811049 0.613328 0.493337 11.00000 0.02225 0.02160 = 0.09705 -0.00508 0.00673 0.00497 C4O 1 0.604957 0.676381 0.513211 11.00000 0.01892 0.01400 = 0.03194 -0.00212 -0.00097 -0.00069 O5O 4 0.572933 0.610100 0.542463 11.00000 0.02841 0.02593 = 0.04222 0.00869 0.00191 -0.00278 O6O 4 0.527509 0.739601 0.491506 11.00000 0.01740 0.02884 = 0.04824 0.01112 -0.00074 0.00567 H6O 2 0.448510 0.730135 0.498468 11.00000 0.06945 HKLF 4 REM s92_a.res in P2(1)2(1)2(1) REM R1 = 0.0476 for 6429 Fo > 4sig(Fo) and 0.0484 for all 6563 data REM 488 parameters refined using 4 restraints END WGHT 0.0802 1.8526 REM Instructions for potential hydrogen bonds HTAB C3 O42 HTAB C5 O3O_$3 HTAB C7 O3O_$3 HTAB N8 O1O_$4 HTAB N8 O6O_$4 EQIV $8 x+1/2, -y+1/2, -z+1 HTAB C9 O5O_$8 HTAB C18 O37_$8 HTAB C30 O34 HTAB C32 O28 EQIV $9 x-1, y, z HTAB C35 O1_$9 HTAB O42 O3O_$3 HTAB C43 O40_$8 HTAB C44 O6O_$4 HTAB O46 O3O HTAB O46 O5O HTAB O6O O1O_$7 HTAB O6O O3O_$7 REM Highest difference peak 0.731, deepest hole -0.428, 1-sigma level 0.063 Q1 1 -0.2212 0.4561 0.8741 11.00000 0.05 0.73 Q2 1 0.4514 0.1654 0.8347 11.00000 0.05 0.55 Q3 1 -0.1019 0.3732 0.8525 11.00000 0.05 0.50 Q4 1 0.4300 0.3029 0.8386 11.00000 0.05 0.31 Q5 1 -0.2040 0.5449 0.8281 11.00000 0.05 0.27 Q6 1 0.1255 0.4527 0.8471 11.00000 0.05 0.22 Q7 1 0.2052 0.3851 0.8886 11.00000 0.05 0.21 Q8 1 0.4382 0.1144 0.7791 11.00000 0.05 0.20 Q9 1 0.8716 0.2637 0.6051 11.00000 0.05 0.19 Q10 1 0.3626 -0.1647 0.3400 11.00000 0.05 0.19 Q11 1 0.8006 0.6230 0.5266 11.00000 0.05 0.19 Q12 1 -0.1188 0.3651 0.7768 11.00000 0.05 0.18 Q13 1 -0.2474 0.2611 0.9046 11.00000 0.05 0.18 Q14 1 0.0794 0.3970 0.7725 11.00000 0.05 0.18 Q15 1 0.6592 0.2849 0.7476 11.00000 0.05 0.18 Q16 1 -0.1106 0.4784 0.8486 11.00000 0.05 0.17 Q17 1 0.4471 0.2017 0.6857 11.00000 0.05 0.17 Q18 1 0.0648 0.1590 0.7493 11.00000 0.05 0.17 Q19 1 0.4172 0.2154 0.7500 11.00000 0.05 0.17 Q20 1 -0.0672 0.2034 0.7582 11.00000 0.05 0.17 ; _shelx_res_checksum 37661 _shelxl_version_number 2014/6 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy O O1 0.7271(2) 0.23153(15) 0.60003(8) 0.0220(4) Uani d 1 C C2 0.6886(3) 0.1258(2) 0.60078(11) 0.0196(6) Uani d 1 H H2 0.7575 0.0854 0.6177 0.024 Uiso calc 1 C C3 0.5616(3) 0.1131(2) 0.62988(11) 0.0223(6) Uani d 1 H H3 0.5480 0.0404 0.6366 0.017(8) Uiso calc 1 C C4 0.4487(3) 0.1516(2) 0.59856(12) 0.0238(6) Uani d 1 H H4A 0.4632 0.2229 0.5904 0.029 Uiso calc 1 H H4B 0.3688 0.1468 0.6192 0.029 Uiso calc 1 C C5 0.4304(3) 0.0928(2) 0.54844(11) 0.0229(6) Uani d 1 H H5A 0.3603 0.0436 0.5534 0.027 Uiso calc 1 H H5B 0.4025 0.1398 0.5214 0.027 Uiso calc 1 C C6 0.5516(3) 0.0375(2) 0.52989(11) 0.0196(6) Uani d 1 C C7 0.5514(3) 0.0269(2) 0.47054(11) 0.0204(6) Uani d 1 H H7 0.4709 -0.0094 0.4607 0.025 Uiso calc 1 N N8 0.6650(2) -0.03899(18) 0.45687(9) 0.0225(5) Uani d 1 H H8 0.656(4) -0.0951(17) 0.4738(13) 0.028(9) Uiso d 1 C C9 0.7908(3) 0.0108(2) 0.47010(12) 0.0233(6) Uani d 1 H H9A 0.8002 0.0730 0.4501 0.028 Uiso calc 1 H H9B 0.8635 -0.0340 0.4612 0.028 Uiso calc 1 C C10 0.7950(3) 0.0347(2) 0.52665(11) 0.0218(6) Uani d 1 H H10A 0.8735 0.0743 0.5341 0.026 Uiso calc 1 H H10B 0.8004 -0.0282 0.5463 0.026 Uiso calc 1 C C11 0.6759(3) 0.0933(2) 0.54401(11) 0.0178(5) Uani d 1 C C12 0.6642(3) 0.1937(2) 0.51828(10) 0.0180(5) Uani d 1 C C13 0.6953(3) 0.2674(2) 0.55230(11) 0.0184(5) Uani d 1 C C14 0.6840(3) 0.3679(2) 0.53902(11) 0.0196(5) Uani d 1 C C15 0.6339(3) 0.3874(2) 0.49073(11) 0.0218(6) Uani d 1 H H15 0.6254 0.4548 0.4801 0.026 Uiso calc 1 C C16 0.5954(3) 0.3121(2) 0.45718(11) 0.0222(6) Uani d 1 H H16 0.5598 0.3289 0.4248 0.025(9) Uiso calc 1 C C17 0.6093(3) 0.2118(2) 0.47115(11) 0.0187(5) Uani d 1 C C18 0.5532(3) 0.1265(2) 0.44095(11) 0.0217(6) Uani d 1 H H18A 0.6041 0.1178 0.4093 0.026 Uiso calc 1 H H18B 0.4637 0.1438 0.4309 0.026 Uiso calc 1 O O19 0.5624(2) 0.16457(16) 0.67753(8) 0.0282(5) Uani d 1 C C20 0.6280(4) 0.1130(3) 0.71702(12) 0.0382(8) Uani d 1 H H20A 0.7192 0.1023 0.7072 0.046 Uiso calc 1 H H20B 0.5875 0.0469 0.7225 0.046 Uiso calc 1 C C21 0.6215(4) 0.1731(3) 0.76544(13) 0.0401(8) Uani d 1 H H21A 0.6797 0.1434 0.7913 0.048 Uiso calc 1 H H21B 0.6513 0.2420 0.7586 0.048 Uiso calc 1 O O22 0.4955(3) 0.1756(2) 0.78457(9) 0.0424(6) Uani d 1 C C23 0.4912(5) 0.2381(4) 0.82948(15) 0.0527(11) Uani d 1 H H23A 0.5172 0.3068 0.8201 0.063 Uiso calc 1 H H23B 0.5536 0.2128 0.8550 0.063 Uiso calc 1 C C24 0.3631(5) 0.2404(5) 0.85200(16) 0.0654(15) Uani d 1 H H24A 0.3331 0.1710 0.8571 0.079 Uiso calc 1 H H24B 0.3687 0.2722 0.8861 0.079 Uiso calc 1 O O25 0.2718(3) 0.2915(3) 0.82276(11) 0.0669(11) Uani d 1 C C26 0.1924(5) 0.3545(3) 0.85016(16) 0.0472(10) Uani d 1 H H26A 0.2447 0.4096 0.8646 0.057 Uiso calc 1 H H26B 0.1535 0.3173 0.8790 0.057 Uiso calc 1 C C27 0.0876(4) 0.3971(4) 0.81770(16) 0.0474(9) Uani d 1 H H27A 0.1269 0.4316 0.7881 0.057 Uiso calc 1 H H27B 0.0337 0.3420 0.8044 0.057 Uiso calc 1 O O28 0.0081(3) 0.4650(2) 0.84424(12) 0.0524(7) Uani d 1 C C29 -0.0852(6) 0.4273(6) 0.8764(2) 0.0780(17) Uani d 1 H H29A -0.1057 0.4793 0.9020 0.094 Uiso calc 1 H H29B -0.0469 0.3703 0.8951 0.094 Uiso calc 1 C C30 -0.2056(6) 0.3937(5) 0.8542(2) 0.0805(18) Uani d 1 H H30A -0.1831 0.3463 0.8267 0.097 Uiso calc 1 H H30B -0.2506 0.3546 0.8809 0.097 Uiso calc 1 O O31 -0.2970(3) 0.4601(3) 0.83377(12) 0.0574(8) Uani d 1 C C32 -0.2612(4) 0.5223(3) 0.79260(15) 0.0418(8) Uani d 1 H H32A -0.1729 0.5478 0.7987 0.050 Uiso calc 1 H H32B -0.3202 0.5804 0.7916 0.050 Uiso calc 1 C C33 -0.2645(4) 0.4709(3) 0.74176(15) 0.0407(8) Uani d 1 H H33A -0.3453 0.4321 0.7385 0.049 Uiso calc 1 H H33B -0.2624 0.5211 0.7140 0.049 Uiso calc 1 C C35 -0.1524(4) 0.3577(3) 0.68942(13) 0.0352(8) Uani d 1 H H35A -0.1437 0.4074 0.6616 0.042 Uiso calc 1 H H35B -0.2330 0.3195 0.6838 0.042 Uiso calc 1 O O34 -0.1574(2) 0.4068(2) 0.73736(9) 0.0376(6) Uani d 1 C C36 -0.0393(3) 0.2888(3) 0.68912(13) 0.0337(7) Uani d 1 H H36A -0.0422 0.2453 0.7197 0.040 Uiso calc 1 H H36B -0.0427 0.2458 0.6584 0.040 Uiso calc 1 O O37 0.0775(2) 0.34491(17) 0.68908(9) 0.0305(5) Uani d 1 C C38 0.1863(4) 0.2810(3) 0.69353(13) 0.0339(7) Uani d 1 H H38A 0.1900 0.2360 0.6636 0.041 Uiso calc 1 H H38B 0.1773 0.2393 0.7246 0.041 Uiso calc 1 C C39 0.3081(4) 0.3401(3) 0.69666(13) 0.0348(8) Uani d 1 H H39A 0.2995 0.3922 0.7233 0.042 Uiso calc 1 H H39B 0.3806 0.2958 0.7063 0.042 Uiso calc 1 O O40 0.3342(2) 0.3856(2) 0.64859(9) 0.0360(5) Uani d 1 C C41 0.4599(4) 0.4277(3) 0.64774(16) 0.0426(9) Uani d 1 H H41A 0.4677 0.4773 0.6751 0.064 Uiso calc 1 H H41B 0.4748 0.4600 0.6147 0.064 Uiso calc 1 H H41C 0.5241 0.3749 0.6529 0.064 Uiso calc 1 O O42 0.5589(2) -0.06069(15) 0.55118(8) 0.0240(4) Uani d 1 H H42 0.490(2) -0.091(3) 0.5438(15) 0.035(11) Uiso d 1 C C43 0.6689(3) -0.0737(2) 0.40195(12) 0.0297(7) Uani d 1 H H43A 0.6894 -0.0160 0.3798 0.036 Uiso calc 1 H H43B 0.7394 -0.1230 0.3981 0.036 Uiso calc 1 C C44 0.5460(4) -0.1197(3) 0.38398(14) 0.0366(8) Uani d 1 H H44 0.5046 -0.1676 0.4052 0.044 Uiso calc 1 C C45 0.4926(5) -0.0967(3) 0.34005(16) 0.0479(10) Uani d 1 H H45A 0.5324 -0.0490 0.3183 0.058 Uiso calc 1 H H45B 0.4141 -0.1277 0.3300 0.058 Uiso calc 1 O O46 0.7208(2) 0.44043(15) 0.57269(8) 0.0261(5) Uani d 1 H H46 0.702(5) 0.495(2) 0.5584(16) 0.048(13) Uiso d 1 O O1O 0.7871(2) 0.77819(16) 0.49246(11) 0.0347(6) Uani d 1 C C2O 0.7474(3) 0.6898(2) 0.49807(13) 0.0236(6) Uani d 1 O O3O 0.8110(2) 0.61333(17) 0.49334(13) 0.0470(7) Uani d 1 C C4O 0.6050(3) 0.6764(2) 0.51321(12) 0.0216(6) Uani d 1 O O5O 0.5729(2) 0.61010(17) 0.54246(9) 0.0322(5) Uani d 1 O O6O 0.5275(2) 0.73960(17) 0.49151(10) 0.0315(5) Uani d 1 H H6O 0.449(2) 0.730(4) 0.498(2) 0.069(16) Uiso d 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 O1 0.0265(10) 0.0180(10) 0.0216(9) -0.0045(8) -0.0056(8) 0.0002(8) C2 0.0226(13) 0.0147(13) 0.0215(13) 0.0003(11) -0.0028(11) 0.0019(10) C3 0.0278(15) 0.0193(13) 0.0198(14) -0.0014(12) 0.0013(11) 0.0016(10) C4 0.0199(13) 0.0241(14) 0.0273(14) 0.0014(12) 0.0030(12) -0.0002(12) C5 0.0173(13) 0.0243(14) 0.0271(14) 0.0003(11) 0.0003(11) -0.0005(12) C6 0.0189(13) 0.0150(12) 0.0249(14) -0.0013(11) -0.0005(11) 0.0032(11) C7 0.0197(13) 0.0178(13) 0.0238(14) 0.0019(11) -0.0010(11) -0.0014(11) N8 0.0252(12) 0.0179(12) 0.0243(12) 0.0017(10) -0.0004(10) -0.0020(10) C9 0.0182(13) 0.0226(13) 0.0291(15) 0.0027(11) 0.0023(11) 0.0004(12) C10 0.0189(13) 0.0203(13) 0.0262(14) 0.0019(11) -0.0016(11) 0.0007(11) C11 0.0184(13) 0.0135(12) 0.0215(13) -0.0007(10) -0.0008(10) 0.0023(10) C12 0.0163(12) 0.0164(12) 0.0212(13) 0.0012(10) 0.0001(10) 0.0024(10) C13 0.0176(12) 0.0161(13) 0.0217(13) -0.0008(10) 0.0012(10) 0.0041(10) C14 0.0177(12) 0.0169(13) 0.0244(14) -0.0025(10) 0.0000(11) -0.0005(11) C15 0.0211(13) 0.0165(12) 0.0277(14) 0.0007(11) 0.0005(11) 0.0037(11) C16 0.0219(13) 0.0228(14) 0.0219(14) 0.0014(11) -0.0008(11) 0.0023(11) C17 0.0186(12) 0.0156(12) 0.0218(13) 0.0022(10) 0.0025(11) -0.0001(11) C18 0.0240(13) 0.0198(13) 0.0214(13) 0.0010(11) -0.0028(11) -0.0021(11) O19 0.0373(13) 0.0283(11) 0.0191(10) 0.0036(10) 0.0002(9) 0.0000(8) C20 0.041(2) 0.051(2) 0.0220(16) 0.0108(17) -0.0020(14) 0.0020(15) C21 0.0387(19) 0.058(2) 0.0235(16) 0.0002(17) -0.0030(14) -0.0006(16) O22 0.0419(14) 0.0598(17) 0.0256(11) 0.0039(13) 0.0025(10) -0.0024(11) C23 0.060(3) 0.065(3) 0.0329(18) 0.004(2) -0.0070(18) -0.0092(19) C24 0.074(3) 0.090(4) 0.032(2) 0.042(3) -0.008(2) -0.009(2) O25 0.071(2) 0.102(3) 0.0276(13) 0.047(2) -0.0056(14) -0.0071(15) C26 0.058(2) 0.044(2) 0.039(2) 0.0104(19) -0.0067(18) -0.0113(17) C27 0.047(2) 0.056(2) 0.039(2) 0.0106(19) 0.0011(17) -0.0036(18) O28 0.0580(17) 0.0458(16) 0.0534(17) 0.0114(14) -0.0022(14) -0.0053(13) C29 0.070(3) 0.105(5) 0.059(3) 0.026(3) 0.016(3) 0.020(3) C30 0.074(4) 0.100(5) 0.067(3) -0.013(3) -0.008(3) 0.031(3) O31 0.0538(18) 0.0617(19) 0.0568(18) 0.0099(15) 0.0151(14) 0.0050(15) C32 0.048(2) 0.0321(18) 0.045(2) 0.0065(17) 0.0026(17) -0.0059(15) C33 0.0324(18) 0.049(2) 0.0411(19) 0.0085(17) -0.0011(15) -0.0056(16) C35 0.0342(18) 0.047(2) 0.0248(16) -0.0012(16) -0.0008(13) -0.0086(14) O34 0.0338(12) 0.0496(14) 0.0295(12) 0.0102(11) -0.0037(10) -0.0114(11) C36 0.0366(18) 0.0351(18) 0.0294(16) -0.0035(15) 0.0030(14) -0.0080(14) O37 0.0283(11) 0.0313(12) 0.0318(12) 0.0049(10) -0.0001(9) -0.0001(9) C38 0.0380(18) 0.0323(17) 0.0315(16) 0.0122(15) 0.0023(14) 0.0029(13) C39 0.0365(18) 0.0407(19) 0.0273(16) 0.0099(15) -0.0043(14) 0.0012(14) O40 0.0288(12) 0.0489(14) 0.0304(12) -0.0003(11) -0.0034(9) 0.0052(11) C41 0.0294(17) 0.055(2) 0.044(2) -0.0014(17) -0.0054(15) 0.0014(17) O42 0.0264(11) 0.0151(9) 0.0304(11) -0.0044(8) -0.0008(9) 0.0043(8) C43 0.0410(18) 0.0231(15) 0.0248(15) 0.0055(14) 0.0005(14) -0.0067(12) C44 0.051(2) 0.0250(16) 0.0336(17) -0.0065(15) -0.0033(16) -0.0062(13) C45 0.057(2) 0.044(2) 0.043(2) -0.0039(19) -0.0128(19) -0.0030(17) O46 0.0336(12) 0.0146(10) 0.0302(11) -0.0038(9) -0.0051(9) -0.0006(8) O1O 0.0209(10) 0.0170(10) 0.0662(16) -0.0015(8) 0.0043(10) 0.0062(10) C2O 0.0180(13) 0.0163(13) 0.0364(16) 0.0010(11) -0.0023(12) 0.0000(12) O3O 0.0223(11) 0.0216(11) 0.097(2) 0.0050(9) 0.0067(13) -0.0051(13) C4O 0.0189(13) 0.0140(12) 0.0319(15) -0.0007(10) -0.0010(11) -0.0021(11) O5O 0.0284(11) 0.0259(11) 0.0422(13) -0.0028(9) 0.0019(10) 0.0087(10) O6O 0.0174(10) 0.0288(11) 0.0482(14) 0.0057(9) -0.0007(10) 0.0111(10) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle C13 O1 C2 106.4(2) O1 C2 C3 110.3(2) O1 C2 C11 106.2(2) C3 C2 C11 111.9(2) O1 C2 H2 109.5 C3 C2 H2 109.5 C11 C2 H2 109.5 O19 C3 C4 108.1(2) O19 C3 C2 112.2(2) C4 C3 C2 110.8(2) O19 C3 H3 108.5 C4 C3 H3 108.5 C2 C3 H3 108.5 C3 C4 C5 112.3(2) C3 C4 H4A 109.1 C5 C4 H4A 109.1 C3 C4 H4B 109.1 C5 C4 H4B 109.1 H4A C4 H4B 107.9 C6 C5 C4 114.5(2) C6 C5 H5A 108.6 C4 C5 H5A 108.6 C6 C5 H5B 108.6 C4 C5 H5B 108.6 H5A C5 H5B 107.6 O42 C6 C11 108.1(2) O42 C6 C5 111.3(2) C11 C6 C5 112.0(2) O42 C6 C7 107.7(2) C11 C6 C7 106.6(2) C5 C6 C7 110.9(2) N8 C7 C18 112.2(2) N8 C7 C6 106.7(2) C18 C7 C6 114.9(2) N8 C7 H7 107.6 C18 C7 H7 107.6 C6 C7 H7 107.6 C9 N8 C43 109.4(2) C9 N8 C7 111.1(2) C43 N8 C7 115.2(2) C9 N8 H8 111(3) C43 N8 H8 103(3) C7 N8 H8 107(3) N8 C9 C10 110.1(2) N8 C9 H9A 109.6 C10 C9 H9A 109.6 N8 C9 H9B 109.6 C10 C9 H9B 109.6 H9A C9 H9B 108.2 C9 C10 C11 112.1(2) C9 C10 H10A 109.2 C11 C10 H10A 109.2 C9 C10 H10B 109.2 C11 C10 H10B 109.2 H10A C10 H10B 107.9 C12 C11 C10 112.9(2) C12 C11 C6 105.0(2) C10 C11 C6 110.7(2) C12 C11 C2 100.6(2) C10 C11 C2 111.1(2) C6 C11 C2 115.9(2) C13 C12 C17 123.5(3) C13 C12 C11 109.5(2) C17 C12 C11 126.1(2) C12 C13 O1 113.2(2) C12 C13 C14 121.0(3) O1 C13 C14 125.6(3) O46 C14 C15 123.8(2) O46 C14 C13 120.2(3) C15 C14 C13 116.0(3) C14 C15 C16 122.8(3) C14 C15 H15 118.6 C16 C15 H15 118.6 C15 C16 C17 120.0(3) C15 C16 H16 120.0 C17 C16 H16 120.0 C12 C17 C16 116.4(3) C12 C17 C18 119.7(2) C16 C17 C18 123.5(3) C17 C18 C7 113.4(2) C17 C18 H18A 108.9 C7 C18 H18A 108.9 C17 C18 H18B 108.9 C7 C18 H18B 108.9 H18A C18 H18B 107.7 C20 O19 C3 113.8(2) O19 C20 C21 109.4(3) O19 C20 H20A 109.8 C21 C20 H20A 109.8 O19 C20 H20B 109.8 C21 C20 H20B 109.8 H20A C20 H20B 108.2 O22 C21 C20 110.9(3) O22 C21 H21A 109.5 C20 C21 H21A 109.5 O22 C21 H21B 109.5 C20 C21 H21B 109.5 H21A C21 H21B 108.1 C21 O22 C23 109.6(3) O22 C23 C24 111.8(4) O22 C23 H23A 109.3 C24 C23 H23A 109.3 O22 C23 H23B 109.3 C24 C23 H23B 109.3 H23A C23 H23B 107.9 O25 C24 C23 114.0(4) O25 C24 H24A 108.7 C23 C24 H24A 108.7 O25 C24 H24B 108.7 C23 C24 H24B 108.7 H24A C24 H24B 107.6 C26 O25 C24 114.8(3) O25 C26 C27 111.8(3) O25 C26 H26A 109.3 C27 C26 H26A 109.3 O25 C26 H26B 109.3 C27 C26 H26B 109.3 H26A C26 H26B 107.9 O28 C27 C26 113.1(3) O28 C27 H27A 109.0 C26 C27 H27A 109.0 O28 C27 H27B 109.0 C26 C27 H27B 109.0 H27A C27 H27B 107.8 C29 O28 C27 118.3(4) O28 C29 C30 118.3(5) O28 C29 H29A 107.7 C30 C29 H29A 107.7 O28 C29 H29B 107.7 C30 C29 H29B 107.7 H29A C29 H29B 107.1 O31 C30 C29 122.4(6) O31 C30 H30A 106.7 C29 C30 H30A 106.7 O31 C30 H30B 106.7 C29 C30 H30B 106.7 H30A C30 H30B 106.6 C30 O31 C32 119.2(4) O31 C32 C33 113.6(3) O31 C32 H32A 108.8 C33 C32 H32A 108.8 O31 C32 H32B 108.8 C33 C32 H32B 108.8 H32A C32 H32B 107.7 O34 C33 C32 109.6(3) O34 C33 H33A 109.8 C32 C33 H33A 109.8 O34 C33 H33B 109.8 C32 C33 H33B 109.8 H33A C33 H33B 108.2 O34 C35 C36 108.7(3) O34 C35 H35A 110.0 C36 C35 H35A 110.0 O34 C35 H35B 110.0 C36 C35 H35B 110.0 H35A C35 H35B 108.3 C33 O34 C35 112.6(3) O37 C36 C35 109.9(3) O37 C36 H36A 109.7 C35 C36 H36A 109.7 O37 C36 H36B 109.7 C35 C36 H36B 109.7 H36A C36 H36B 108.2 C38 O37 C36 110.8(3) O37 C38 C39 110.8(3) O37 C38 H38A 109.5 C39 C38 H38A 109.5 O37 C38 H38B 109.5 C39 C38 H38B 109.5 H38A C38 H38B 108.1 O40 C39 C38 109.9(3) O40 C39 H39A 109.7 C38 C39 H39A 109.7 O40 C39 H39B 109.7 C38 C39 H39B 109.7 H39A C39 H39B 108.2 C41 O40 C39 111.0(3) O40 C41 H41A 109.5 O40 C41 H41B 109.5 H41A C41 H41B 109.5 O40 C41 H41C 109.5 H41A C41 H41C 109.5 H41B C41 H41C 109.5 C6 O42 H42 108(3) C44 C43 N8 113.9(3) C44 C43 H43A 108.8 N8 C43 H43A 108.8 C44 C43 H43B 108.8 N8 C43 H43B 108.8 H43A C43 H43B 107.7 C45 C44 C43 122.6(4) C45 C44 H44 118.7 C43 C44 H44 118.7 C44 C45 H45A 120.0 C44 C45 H45B 120.0 H45A C45 H45B 120.0 C14 O46 H46 106(3) O3O C2O O1O 126.7(3) O3O C2O C4O 116.4(3) O1O C2O C4O 116.9(2) O5O C4O O6O 125.6(3) O5O C4O C2O 120.5(3) O6O C4O C2O 113.8(3) C4O O6O H6O 114(4) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance O1 C13 1.378(3) O1 C2 1.473(3) C2 C3 1.529(4) C2 C11 1.553(4) C2 H2 1.0000 C3 O19 1.425(4) C3 C4 1.519(4) C3 H3 1.0000 C4 C5 1.542(4) C4 H4A 0.9900 C4 H4B 0.9900 C5 C6 1.537(4) C5 H5A 0.9900 C5 H5B 0.9900 C6 O42 1.431(3) C6 C11 1.534(4) C6 C7 1.560(4) C7 N8 1.514(4) C7 C18 1.543(4) C7 H7 1.0000 N8 C9 1.505(4) N8 C43 1.512(4) N8 H8 0.879(14) C9 C10 1.515(4) C9 H9A 0.9900 C9 H9B 0.9900 C10 C11 1.531(4) C10 H10A 0.9900 C10 H10B 0.9900 C11 C12 1.509(4) C12 C13 1.368(4) C12 C17 1.379(4) C13 C14 1.396(4) C14 O46 1.367(3) C14 C15 1.391(4) C15 C16 1.396(4) C15 H15 0.9500 C16 C17 1.400(4) C16 H16 0.9500 C17 C18 1.506(4) C18 H18A 0.9900 C18 H18B 0.9900 O19 C20 1.417(4) C20 C21 1.503(5) C20 H20A 0.9900 C20 H20B 0.9900 C21 O22 1.398(5) C21 H21A 0.9900 C21 H21B 0.9900 O22 C23 1.444(5) C23 C24 1.452(7) C23 H23A 0.9900 C23 H23B 0.9900 C24 O25 1.396(5) C24 H24A 0.9900 C24 H24B 0.9900 O25 C26 1.380(5) C26 C27 1.492(6) C26 H26A 0.9900 C26 H26B 0.9900 C27 O28 1.411(5) C27 H27A 0.9900 C27 H27B 0.9900 O28 C29 1.377(7) C29 C30 1.447(9) C29 H29A 0.9900 C29 H29B 0.9900 C30 O31 1.405(7) C30 H30A 0.9900 C30 H30B 0.9900 O31 C32 1.412(5) C32 C33 1.499(5) C32 H32A 0.9900 C32 H32B 0.9900 C33 O34 1.408(4) C33 H33A 0.9900 C33 H33B 0.9900 C35 O34 1.418(4) C35 C36 1.492(5) C35 H35A 0.9900 C35 H35B 0.9900 C36 O37 1.425(4) C36 H36A 0.9900 C36 H36B 0.9900 O37 C38 1.420(4) C38 C39 1.492(5) C38 H38A 0.9900 C38 H38B 0.9900 C39 O40 1.424(4) C39 H39A 0.9900 C39 H39B 0.9900 O40 C41 1.420(5) C41 H41A 0.9800 C41 H41B 0.9800 C41 H41C 0.9800 O42 H42 0.839(14) C43 C44 1.491(5) C43 H43A 0.9900 C43 H43B 0.9900 C44 C45 1.312(6) C44 H44 0.9500 C45 H45A 0.9500 C45 H45B 0.9500 O46 H46 0.842(14) O1O C2O 1.263(4) C2O O3O 1.225(4) C2O C4O 1.538(4) C4O O5O 1.219(4) C4O O6O 1.298(4) O6O H6O 0.848(14) loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA N8 H8 O1O 1_545 0.879(14) 2.23(3) 2.911(3) 134(3) O42 H42 O3O 4_456 0.839(14) 2.12(2) 2.906(3) 157(4) O46 H46 O5O . 0.842(14) 2.09(3) 2.853(3) 151(5) O6O H6O O1O 4_466 0.848(14) 1.692(16) 2.536(3) 173(6) loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_publ_flag C13 O1 C2 C3 -102.0(2) ? C13 O1 C2 C11 19.4(3) ? O1 C2 C3 O19 -47.5(3) ? C11 C2 C3 O19 -165.5(2) ? O1 C2 C3 C4 73.5(3) ? C11 C2 C3 C4 -44.5(3) ? O19 C3 C4 C5 -173.9(2) ? C2 C3 C4 C5 62.7(3) ? C3 C4 C5 C6 -22.0(3) ? C4 C5 C6 O42 88.8(3) ? C4 C5 C6 C11 -32.4(3) ? C4 C5 C6 C7 -151.3(2) ? O42 C6 C7 N8 -51.1(3) ? C11 C6 C7 N8 64.7(3) ? C5 C6 C7 N8 -173.2(2) ? O42 C6 C7 C18 -176.1(2) ? C11 C6 C7 C18 -60.3(3) ? C5 C6 C7 C18 61.9(3) ? C18 C7 N8 C9 61.4(3) ? C6 C7 N8 C9 -65.2(3) ? C18 C7 N8 C43 -63.7(3) ? C6 C7 N8 C43 169.7(2) ? C43 N8 C9 C10 -173.1(2) ? C7 N8 C9 C10 58.6(3) ? N8 C9 C10 C11 -52.4(3) ? C9 C10 C11 C12 -62.4(3) ? C9 C10 C11 C6 55.1(3) ? C9 C10 C11 C2 -174.6(2) ? O42 C6 C11 C12 177.3(2) ? C5 C6 C11 C12 -59.7(3) ? C7 C6 C11 C12 61.8(3) ? O42 C6 C11 C10 55.1(3) ? C5 C6 C11 C10 178.1(2) ? C7 C6 C11 C10 -60.4(3) ? O42 C6 C11 C2 -72.6(3) ? C5 C6 C11 C2 50.4(3) ? C7 C6 C11 C2 171.8(2) ? O1 C2 C11 C12 -18.8(3) ? C3 C2 C11 C12 101.6(3) ? O1 C2 C11 C10 101.0(3) ? C3 C2 C11 C10 -138.6(2) ? O1 C2 C11 C6 -131.4(2) ? C3 C2 C11 C6 -11.0(3) ? C10 C11 C12 C13 -106.3(3) ? C6 C11 C12 C13 132.9(2) ? C2 C11 C12 C13 12.2(3) ? C10 C11 C12 C17 84.4(3) ? C6 C11 C12 C17 -36.4(4) ? C2 C11 C12 C17 -157.2(3) ? C17 C12 C13 O1 169.0(2) ? C11 C12 C13 O1 -0.7(3) ? C17 C12 C13 C14 -6.1(4) ? C11 C12 C13 C14 -175.8(3) ? C2 O1 C13 C12 -12.2(3) ? C2 O1 C13 C14 162.7(3) ? C12 C13 C14 O46 -177.2(3) ? O1 C13 C14 O46 8.3(4) ? C12 C13 C14 C15 3.0(4) ? O1 C13 C14 C15 -171.5(3) ? O46 C14 C15 C16 -179.2(3) ? C13 C14 C15 C16 0.6(4) ? C14 C15 C16 C17 -1.4(4) ? C13 C12 C17 C16 5.0(4) ? C11 C12 C17 C16 173.0(3) ? C13 C12 C17 C18 -167.3(3) ? C11 C12 C17 C18 0.6(4) ? C15 C16 C17 C12 -1.3(4) ? C15 C16 C17 C18 170.8(3) ? C12 C17 C18 C7 6.4(4) ? C16 C17 C18 C7 -165.4(3) ? N8 C7 C18 C17 -97.9(3) ? C6 C7 C18 C17 24.1(3) ? C4 C3 O19 C20 157.5(3) ? C2 C3 O19 C20 -80.0(3) ? C3 O19 C20 C21 -179.4(3) yes O19 C20 C21 O22 69.0(4) yes C20 C21 O22 C23 -177.0(3) yes C21 O22 C23 C24 -177.9(4) yes O22 C23 C24 O25 -69.9(6) yes C23 C24 O25 C26 -136.1(5) yes C24 O25 C26 C27 -173.2(5) yes O25 C26 C27 O28 -177.6(4) yes C26 C27 O28 C29 -78.4(5) yes C27 O28 C29 C30 -81.2(7) yes O28 C29 C30 O31 -70.5(8) yes C29 C30 O31 C32 60.2(8) yes C30 O31 C32 C33 80.4(5) yes O31 C32 C33 O34 -74.8(4) yes C32 C33 O34 C35 -178.3(3) yes C36 C35 O34 C33 -177.8(3) yes O34 C35 C36 O37 -68.8(4) yes C35 C36 O37 C38 174.7(3) yes C36 O37 C38 C39 -176.6(3) yes O37 C38 C39 O40 -70.0(3) yes C38 C39 O40 C41 -169.8(3) yes C9 N8 C43 C44 -177.1(3) ? C7 N8 C43 C44 -51.1(3) ? N8 C43 C44 C45 133.6(4) ? O3O C2O C4O O5O 35.8(5) ? O1O C2O C4O O5O -143.3(3) ? O3O C2O C4O O6O -143.1(3) ? O1O C2O C4O O6O 37.8(4) ? _cod_database_fobs_code 2242426