#------------------------------------------------------------------------------ #$Date: 2018-03-14 09:11:19 +0200 (Wed, 14 Mar 2018) $ #$Revision: 206944 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/24/2242428.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2242428 _cell_angle_alpha 90.000 _cell_angle_beta 105.326 _cell_angle_gamma 90.000 _cell_length_a 12.0263 _cell_length_b 12.3999 _cell_length_c 21.9164 _exptl_crystal_F_000 1420.00 _reflns_d_resolution_high 0.6489 _cod_data_source_file vm22092sup3.hkl _cod_data_source_block 2 _shelx_title ' BO60_0m in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 235.06 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 -19 0 283.90 272.02 26.81 o 0 -18 0 120.32 118.40 20.82 o 1 -18 0 135.14 113.60 17.21 o 2 -18 0 182.85 189.21 24.03 o 3 -18 0 29.36 46.37 21.13 o 4 -18 0 11.36 77.98 32.28 o 5 -18 0 51.47 40.38 32.63 o 1 -17 0 302.67 248.28 21.79 o 2 -17 0 120.60 165.97 28.82 o 3 -17 0 73.64 72.73 19.08 o 4 -17 0 10.15 5.80 24.24 o 5 -17 0 120.09 127.54 32.52 o 6 -17 0 11.13 13.28 30.23 o 7 -17 0 6.63 54.95 31.70 o 1 -16 0 7.18 5.23 21.15 o 2 -16 0 1016.37 1079.73 45.52 o 3 -16 0 216.97 191.63 18.74 o 4 -16 0 102.35 66.30 23.31 o 5 -16 0 7.85 -5.66 13.59 o 6 -16 0 61.51 73.59 28.26 o 7 -16 0 37.98 29.99 26.87 o 8 -16 0 32.45 8.46 30.25 o 9 -16 0 281.58 332.71 44.50 o 1 -15 0 850.70 847.92 48.32 o 2 -15 0 131.56 106.11 16.15 o 3 -15 0 745.62 748.06 28.41 o 4 -15 0 193.46 164.11 19.48 o 5 -15 0 262.94 232.37 20.87 o 6 -15 0 579.73 631.79 30.08 o 7 -15 0 116.63 91.41 29.25 o 8 -15 0 348.70 453.23 53.51 o 9 -15 0 245.40 228.38 35.01 o 10 -15 0 265.31 273.39 40.97 o 0 -14 0 1105.24 1206.32 65.60 o 1 -14 0 35.42 24.59 18.48 o 2 -14 0 148.46 145.22 15.82 o 3 -14 0 195.43 215.44 22.34 o 4 -14 0 142.01 154.62 11.94 o 5 -14 0 275.31 287.08 19.20 o 6 -14 0 228.13 214.10 17.25 o 7 -14 0 81.93 89.10 25.72 o 8 -14 0 234.35 225.77 32.46 o 9 -14 0 249.24 210.10 34.34 o 10 -14 0 40.17 66.91 31.05 o 11 -14 0 98.82 96.65 35.04 o 1 -13 0 246.37 236.86 14.03 o 2 -13 0 24.11 12.46 7.94 o 3 -13 0 202.33 174.18 15.93 o 4 -13 0 49.70 42.07 7.79 o 5 -13 0 118.16 117.07 12.93 o 6 -13 0 66.43 61.73 7.69 o 7 -13 0 53.69 59.56 12.10 o 8 -13 0 103.17 95.53 14.53 o 9 -13 0 28.77 -1.32 23.42 o 10 -13 0 116.95 111.15 30.38 o 11 -13 0 26.75 70.05 31.20 o 12 -13 0 66.99 44.55 33.41 o 0 -12 0 1055.88 971.34 37.55 o 1 -12 0 20.25 36.69 7.89 o 2 -12 0 545.71 556.67 17.42 o 3 -12 0 9.86 27.56 7.20 o 4 -12 0 212.43 201.69 11.27 o 5 -12 0 325.05 323.80 14.09 o 6 -12 0 193.12 193.46 8.89 o 7 -12 0 489.36 441.01 22.26 o 8 -12 0 32.07 23.39 12.02 o 9 -12 0 92.26 97.51 15.77 o 10 -12 0 36.21 26.65 23.81 o 11 -12 0 154.75 174.33 31.25 o 12 -12 0 67.87 84.33 31.70 o 13 -12 0 103.26 86.96 37.84 o 1 -11 0 1533.88 1566.35 37.03 o 2 -11 0 408.48 411.11 14.46 o 3 -11 0 1647.92 1748.17 37.13 o 4 -11 0 158.18 150.30 8.93 o 5 -11 0 307.77 319.61 10.34 o 6 -11 0 104.68 85.57 5.43 o 7 -11 0 499.90 461.41 22.92 o 8 -11 0 1297.63 1298.26 41.97 o 9 -11 0 117.06 88.97 14.65 o 10 -11 0 405.61 470.60 32.71 o 11 -11 0 225.27 181.05 31.87 o 12 -11 0 236.51 305.56 38.28 o 13 -11 0 192.80 169.06 36.61 o 14 -11 0 194.18 173.56 38.70 o 0 -10 0 848.20 867.66 32.03 o 1 -10 0 68.92 71.37 6.89 o 2 -10 0 571.22 550.40 17.07 o 3 -10 0 634.08 676.83 17.88 o 4 -10 0 887.69 992.59 22.77 o 5 -10 0 1623.09 1693.46 31.44 o 6 -10 0 1252.18 1252.25 24.50 o 7 -10 0 2245.26 2325.70 55.44 o 8 -10 0 557.02 573.72 24.01 o 9 -10 0 1916.72 2025.74 56.81 o 10 -10 0 203.69 238.43 25.49 o 11 -10 0 361.05 332.85 30.94 o 12 -10 0 44.87 23.65 26.22 o 13 -10 0 568.17 557.32 59.83 o 14 -10 0 116.46 85.80 33.12 o 1 -9 0 881.09 816.09 20.97 o 2 -9 0 483.89 460.05 14.65 o 3 -9 0 1266.67 1241.67 25.20 o 4 -9 0 306.55 291.65 10.09 o 5 -9 0 441.73 442.22 11.15 o 6 -9 0 837.46 782.91 22.29 o 7 -9 0 465.16 441.17 17.24 o 8 -9 0 523.40 569.08 20.22 o 9 -9 0 582.19 567.45 24.33 o 10 -9 0 659.98 695.68 28.15 o 11 -9 0 3.41 16.01 26.59 o 12 -9 0 624.84 678.33 54.10 o 13 -9 0 22.77 20.23 25.82 o 14 -9 0 623.51 610.55 62.67 o 15 -9 0 4.36 -10.53 30.87 o 0 -8 0 261.26 238.72 14.07 o 1 -8 0 369.53 345.22 12.87 o 2 -8 0 114.42 125.41 7.20 o 3 -8 0 219.36 228.82 9.07 o 4 -8 0 438.08 516.50 13.19 o 5 -8 0 588.03 549.28 12.25 o 6 -8 0 260.40 227.30 12.60 o 7 -8 0 325.31 286.28 14.21 o 8 -8 0 431.65 437.44 17.45 o 9 -8 0 208.88 218.58 15.76 o 10 -8 0 300.50 313.22 28.60 o 11 -8 0 47.84 19.10 12.22 o 12 -8 0 139.34 143.93 18.92 o 13 -8 0 55.36 60.35 28.06 o 14 -8 0 81.65 54.22 28.96 o 15 -8 0 128.19 86.92 34.57 o 1 -7 0 374.83 346.94 11.26 o 2 -7 0 149.78 132.52 6.52 o 3 -7 0 1771.27 1899.61 36.34 o 4 -7 0 202.68 216.87 7.94 o 5 -7 0 213.97 234.93 7.07 o 6 -7 0 285.67 288.34 12.70 o 7 -7 0 383.88 353.49 14.56 o 8 -7 0 52.50 47.13 7.55 o 9 -7 0 490.48 511.05 18.85 o 10 -7 0 2.83 8.07 8.69 o 11 -7 0 173.17 183.29 17.30 o 12 -7 0 164.89 123.49 17.40 o 13 -7 0 16.61 22.47 17.50 o 14 -7 0 25.75 12.76 26.29 o 15 -7 0 24.28 57.12 32.01 o 16 -7 0 37.85 43.93 35.43 o 0 -6 0 9990.67 10082.76 293.28 o 1 -6 0 2412.33 2419.46 51.46 o 2 -6 0 7336.24 7476.78 154.84 o 3 -6 0 3168.88 3139.14 59.08 o 4 -6 0 4967.68 5088.39 94.34 o 5 -6 0 1761.23 1711.78 38.54 o 6 -6 0 1737.42 1753.48 58.74 o 7 -6 0 3264.92 3327.62 83.36 o 8 -6 0 1689.50 1764.00 47.91 o 9 -6 0 1793.65 1843.54 50.26 o 10 -6 0 227.98 246.49 18.64 o 11 -6 0 879.40 889.33 27.76 o 12 -6 0 61.98 64.68 16.71 o 13 -6 0 561.85 553.24 56.97 o 14 -6 0 17.43 -14.58 18.30 o 15 -6 0 433.11 396.42 56.98 o 16 -6 0 14.14 32.88 33.74 o 1 -5 0 14184.16 13034.00 307.23 o 2 -5 0 1180.13 1089.63 21.93 o 3 -5 0 10480.61 10191.15 185.33 o 4 -5 0 1448.59 1598.20 31.52 o 5 -5 0 412.26 340.72 14.23 o 6 -5 0 1692.92 1656.10 43.67 o 7 -5 0 3655.84 3886.19 97.86 o 8 -5 0 3796.86 3798.43 92.79 o 9 -5 0 1242.27 1305.98 38.46 o 10 -5 0 1425.81 1431.58 41.20 o 11 -5 0 131.50 113.46 12.38 o 12 -5 0 1055.68 1014.51 37.84 o 13 -5 0 9.80 -6.03 15.82 o 14 -5 0 270.03 246.12 23.04 o 15 -5 0 41.40 25.91 29.42 o 16 -5 0 328.56 362.17 31.71 o 17 -5 0 119.14 138.89 25.40 o 0 -4 0 2358.08 2270.94 67.38 o 1 -4 0 6645.65 6358.36 130.68 o 2 -4 0 3654.13 3475.08 63.91 o 3 -4 0 215.08 243.97 7.66 o 4 -4 0 3937.77 3964.20 97.73 o 5 -4 0 3952.31 4379.92 102.99 o 6 -4 0 2187.85 2160.69 55.10 o 7 -4 0 4269.20 4344.03 125.20 o 8 -4 0 1953.40 1999.36 52.72 o 9 -4 0 2730.96 2798.47 70.18 o 10 -4 0 258.44 212.47 14.43 o 11 -4 0 481.59 466.89 22.34 o 12 -4 0 144.13 127.68 13.24 o 13 -4 0 553.75 574.23 33.46 o 14 -4 0 168.81 186.81 21.30 o 15 -4 0 249.53 249.74 25.62 o 16 -4 0 127.08 111.78 20.80 o 17 -4 0 213.41 177.60 43.55 o 1 -3 0 4103.40 4004.13 81.00 o 2 -3 0 2591.40 2479.17 52.33 o 3 -3 0 2600.90 2553.79 62.03 o 4 -3 0 2250.72 2479.63 60.36 o 5 -3 0 368.03 425.88 14.22 o 6 -3 0 722.42 780.74 22.31 o 7 -3 0 217.34 147.66 11.92 o 8 -3 0 1862.10 1742.55 63.14 o 9 -3 0 401.26 381.52 17.76 o 10 -3 0 1434.73 1383.43 40.40 o 11 -3 0 251.05 204.10 15.04 o 12 -3 0 73.65 61.95 11.30 o 13 -3 0 74.01 78.98 15.61 o 14 -3 0 64.06 45.42 16.55 o 15 -3 0 37.57 16.77 13.61 o 16 -3 0 0.66 -2.65 17.23 o 17 -3 0 35.74 23.95 34.51 o 0 -2 0 5639.72 5040.01 146.18 o 1 -2 0 1074.24 1114.54 27.14 o 2 -2 0 1832.75 1782.62 50.67 o 3 -2 0 4.95 5.77 3.52 o 4 -2 0 1645.83 2051.09 50.31 o 5 -2 0 453.07 405.35 13.66 o 6 -2 0 3698.04 3778.70 90.19 o 7 -2 0 580.52 624.06 19.30 o 8 -2 0 3318.76 3429.30 84.82 o 9 -2 0 1166.34 1151.89 39.31 o 10 -2 0 1162.07 1213.68 35.00 o 11 -2 0 1002.84 1051.95 32.72 o 12 -2 0 642.64 661.85 25.64 o 13 -2 0 39.82 36.13 16.90 o 14 -2 0 38.68 36.43 14.86 o 15 -2 0 52.14 51.79 13.64 o 16 -2 0 104.33 106.40 16.35 o 17 -2 0 47.67 81.51 35.99 o 2 -1 0 9477.58 9430.94 269.22 o 3 -1 0 7637.18 7316.48 179.12 o 4 -1 0 952.54 947.56 23.74 o 5 -1 0 2428.99 2610.18 65.83 o 6 -1 0 6695.82 6729.13 162.14 o 7 -1 0 524.49 509.31 17.97 o 8 -1 0 156.48 165.58 11.45 o 9 -1 0 381.40 410.76 17.48 o 10 -1 0 455.14 471.33 18.24 o 11 -1 0 546.48 539.78 23.11 o 12 -1 0 257.75 279.48 17.83 o 13 -1 0 38.26 31.85 12.93 o 14 -1 0 48.68 42.34 10.25 o 15 -1 0 44.61 44.97 14.19 o 16 -1 0 228.72 254.30 21.13 o 17 -1 0 157.60 137.92 36.50 o 3 0 0 126.32 138.75 7.35 o 4 0 0 6069.92 5523.94 131.54 o 5 0 0 7905.42 7989.84 189.95 o 6 0 0 11346.50 11292.74 268.04 o 7 0 0 44.07 34.73 5.39 o 8 0 0 532.80 596.00 19.05 o 9 0 0 287.94 272.40 13.56 o 10 0 0 33.72 31.28 8.20 o 11 0 0 3671.64 3758.44 93.94 o 12 0 0 230.50 228.63 17.21 o 13 0 0 1493.28 1604.27 44.12 o 14 0 0 17.95 30.77 9.15 o 15 0 0 297.87 325.76 29.66 o 16 0 0 75.00 59.66 20.93 o 17 0 0 897.57 1008.65 56.60 o 2 1 0 9146.13 9027.10 380.24 o 3 1 0 8340.83 7948.17 277.15 o 4 1 0 876.43 877.28 23.38 o 5 1 0 2629.53 2791.22 65.71 o 6 1 0 6830.73 6842.42 162.01 o 7 1 0 651.79 628.98 18.26 o 8 1 0 167.14 167.44 10.30 o 9 1 0 451.43 501.49 16.96 o 10 1 0 330.27 354.02 16.70 o 11 1 0 525.77 537.28 20.76 o 12 1 0 295.34 324.69 13.79 o 13 1 0 35.70 40.41 7.55 o 14 1 0 63.87 58.20 8.94 o 15 1 0 29.95 23.64 10.69 o 16 1 0 221.55 221.55 34.96 o 17 1 0 167.69 177.49 27.60 o 2 2 0 1648.80 1608.91 50.56 o 3 2 0 9.58 1.23 5.70 o 4 2 0 1679.91 2038.30 49.74 o 5 2 0 430.71 386.84 12.28 o 6 2 0 3568.79 3636.35 89.57 o 7 2 0 516.21 576.63 17.97 o 8 2 0 3335.03 3441.20 84.22 o 9 2 0 1071.14 1043.23 25.39 o 10 2 0 1148.59 1197.98 28.49 o 11 2 0 1008.03 1035.60 25.85 o 12 2 0 599.76 611.28 19.94 o 13 2 0 60.44 60.22 6.63 o 14 2 0 43.89 50.74 8.49 o 15 2 0 41.85 52.75 26.66 o 16 2 0 123.03 151.03 23.76 o 17 2 0 43.28 36.86 56.19 o 1 3 0 4252.14 3819.74 308.26 o 2 3 0 2702.32 2639.60 105.38 o 3 3 0 2568.21 2542.90 61.97 o 4 3 0 2256.49 2430.93 73.94 o 5 3 0 324.78 379.99 17.73 o 6 3 0 639.27 710.78 27.46 o 7 3 0 222.99 167.53 16.73 o 8 3 0 1944.59 1922.16 59.01 o 9 3 0 415.09 409.87 11.16 o 10 3 0 1540.34 1471.97 38.69 o 11 3 0 220.46 196.64 25.06 o 12 3 0 66.02 42.14 19.63 o 13 3 0 57.92 32.76 20.43 o 14 3 0 46.73 78.09 25.36 o 15 3 0 50.42 42.56 25.33 o 16 3 0 3.26 2.85 20.39 o 17 3 0 26.96 -6.69 23.42 o 1 4 0 6646.64 6372.28 185.33 o 2 4 0 3568.85 3348.13 101.38 o 3 4 0 161.15 201.46 16.76 o 4 4 0 4103.65 4162.45 119.89 o 5 4 0 3758.43 4044.76 125.89 o 6 4 0 2183.90 2215.44 68.00 o 7 4 0 3899.96 3982.47 124.93 o 8 4 0 2039.09 2062.61 65.01 o 9 4 0 2666.65 2663.61 86.31 o 10 4 0 303.91 274.86 22.66 o 11 4 0 542.51 513.44 28.85 o 12 4 0 163.77 118.58 22.63 o 13 4 0 546.21 577.18 47.48 o 14 4 0 160.48 171.77 29.28 o 15 4 0 257.83 275.36 35.00 o 16 4 0 149.36 123.38 34.57 o 17 4 0 258.97 287.73 37.70 o 1 5 0 14225.73 12832.54 532.53 o 2 5 0 1277.87 1199.33 50.07 o 3 5 0 9871.34 9560.80 414.18 o 4 5 0 1677.58 1828.50 72.67 o 5 5 0 434.84 372.46 23.74 o 6 5 0 1744.44 1690.41 53.52 o 7 5 0 3957.52 4108.77 120.23 o 8 5 0 3603.64 3624.51 113.68 o 9 5 0 1336.76 1389.83 47.85 o 10 5 0 1443.45 1406.63 51.23 o 11 5 0 124.15 80.15 20.57 o 12 5 0 1014.58 1022.18 60.29 o 13 5 0 10.21 5.22 22.62 o 14 5 0 250.16 251.81 32.05 o 15 5 0 54.23 78.82 27.80 o 16 5 0 266.17 274.60 27.05 o 17 5 0 139.87 123.22 27.82 o 2 6 0 7668.59 7703.00 311.07 o 3 6 0 3178.46 3125.79 132.81 o 4 6 0 4970.44 5086.42 212.54 o 5 6 0 1819.48 1765.31 77.09 o 6 6 0 1949.37 2010.33 83.01 o 7 6 0 3253.49 3357.71 143.91 o 8 6 0 1696.92 1777.42 58.61 o 9 6 0 1816.45 1835.18 61.69 o 10 6 0 238.33 235.24 19.80 o 11 6 0 971.86 1004.97 55.57 o 12 6 0 61.63 82.85 22.39 o 13 6 0 569.92 440.71 58.68 o 14 6 0 23.36 16.01 22.78 o 15 6 0 447.30 461.20 53.49 o 16 6 0 20.46 35.77 21.36 o 2 7 0 149.72 132.39 16.49 o 3 7 0 1600.58 1699.52 81.79 o 4 7 0 199.61 211.32 20.41 o 5 7 0 169.53 181.69 21.26 o 6 7 0 298.15 284.42 25.14 o 7 7 0 355.35 293.55 28.67 o 8 7 0 34.46 13.32 14.05 o 9 7 0 442.80 427.72 36.01 o 10 7 0 7.59 36.95 16.96 o 11 7 0 146.43 130.17 22.05 o 12 7 0 201.20 162.85 25.82 o 13 7 0 9.29 -1.44 20.87 o 14 7 0 25.71 -8.32 23.60 o 15 7 0 26.55 39.14 18.67 o 16 7 0 46.32 53.58 21.99 o 2 8 0 127.64 158.41 18.76 o 3 8 0 233.65 254.36 21.70 o 4 8 0 458.36 549.96 31.88 o 5 8 0 541.98 539.27 33.53 o 6 8 0 271.16 213.30 24.96 o 7 8 0 343.77 312.55 28.82 o 8 8 0 470.64 479.61 34.31 o 9 8 0 248.70 246.80 30.27 o 10 8 0 276.18 291.77 34.34 o 11 8 0 48.03 32.98 19.18 o 12 8 0 151.89 155.12 26.53 o 13 8 0 61.33 42.95 22.80 o 14 8 0 70.76 62.19 18.71 o 15 8 0 132.92 133.49 22.97 o 16 8 0 25.20 24.07 23.28 o 3 9 0 1040.11 1010.23 57.10 o 4 9 0 288.01 272.23 26.00 o 5 9 0 488.66 442.47 31.23 o 6 9 0 749.40 761.12 43.97 o 7 9 0 418.81 383.62 33.65 o 8 9 0 506.78 514.57 39.15 o 9 9 0 595.09 553.89 41.95 o 10 9 0 623.02 654.64 47.41 o 11 9 0 3.88 -17.72 18.10 o 12 9 0 579.45 606.63 52.55 o 13 9 0 19.19 44.31 25.17 o 14 9 0 584.51 602.16 40.38 o 15 9 0 1.26 -10.04 36.86 o 3 10 0 707.66 751.42 31.14 o 4 10 0 976.90 1081.50 52.98 o 5 10 0 1643.97 1689.07 79.81 o 6 10 0 1319.41 1346.56 64.21 o 7 10 0 2372.49 2396.36 107.07 o 8 10 0 545.32 605.15 42.06 o 9 10 0 1966.47 2144.08 99.85 o 10 10 0 215.75 262.28 35.86 o 11 10 0 351.06 275.37 37.13 o 12 10 0 42.94 31.34 15.40 o 13 10 0 562.57 587.19 37.25 o 14 10 0 112.27 101.87 21.50 o 15 10 0 248.11 231.98 27.56 o 4 11 0 113.93 120.67 12.65 o 5 11 0 239.33 268.97 17.20 o 6 11 0 132.89 105.27 19.57 o 7 11 0 472.29 470.64 38.22 o 8 11 0 1306.30 1456.67 75.63 o 9 11 0 117.67 117.29 22.09 o 10 11 0 451.94 482.32 29.17 o 11 11 0 221.04 214.18 19.67 o 12 11 0 244.01 240.11 21.76 o 13 11 0 187.98 195.80 21.73 o 14 11 0 204.70 192.09 24.08 o 5 12 0 346.22 375.31 20.93 o 6 12 0 206.56 197.40 15.12 o 7 12 0 515.45 520.62 24.92 o 8 12 0 27.66 43.27 11.42 o 9 12 0 101.28 100.09 14.11 o 10 12 0 46.25 28.50 13.52 o 11 12 0 164.94 151.78 20.66 o 12 12 0 80.99 99.14 20.89 o 13 12 0 102.92 100.96 20.41 o 6 13 0 66.58 65.58 10.34 o 7 13 0 49.64 40.11 10.26 o 8 13 0 117.52 128.97 24.16 o 9 13 0 26.31 8.99 12.08 o 10 13 0 128.27 100.78 15.49 o 11 13 0 20.20 26.33 15.08 o 12 13 0 68.24 68.85 17.93 o 13 13 0 66.39 41.45 31.50 o 7 14 0 77.53 102.05 12.11 o 8 14 0 264.00 257.20 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