#------------------------------------------------------------------------------ #$Date: 2019-07-13 13:00:45 +0300 (Sat, 13 Jul 2019) $ #$Revision: 217009 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/24/30/2243016.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2243016 loop_ _publ_author_name 'Rayni, Ibtissam' 'El Bakri, Youness' 'Lai, Chin-Hung' 'Sebhaoui, Jihad' 'Essassi, El Mokhtar' 'Mague, Joel T.' _publ_section_title ; Crystal structure, DFT study and Hirshfeld surface analysis of 1-nonyl-2,3-dihydro-1H-indole-2,3-dione ; _journal_coeditor_code VM2219 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first 1140 _journal_page_last 1144 _journal_paper_doi 10.1107/S2056989019009691 _journal_volume 75 _journal_year 2019 _chemical_formula_iupac 'C17 H23 N O2' _chemical_formula_moiety 'C17 H23 N O2' _chemical_formula_sum 'C17 H23 N O2' _chemical_formula_weight 273.36 _chemical_name_systematic ; 1-Nonyl-2,3-dihydro-1H-indole-2,3-dione ; _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _atom_sites_solution_hydrogens difmap _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2018/1 _cell_angle_alpha 90 _cell_angle_beta 106.6400(10) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 16.2512(4) _cell_length_b 7.6859(2) _cell_length_c 13.0989(3) _cell_measurement_reflns_used 9962 _cell_measurement_temperature 150(2) _cell_measurement_theta_max 74.3744 _cell_measurement_theta_min 5.1207 _cell_volume 1567.60(7) _computing_cell_refinement ; SAINT (Bruker, 2016) ; _computing_data_collection ; APEX3 (Bruker, 2016) ; _computing_data_reduction ; SAINT (Bruker, 2016) ; _computing_molecular_graphics ; DIAMOND (Brandenburg & Putz, 2012) ; _computing_publication_material ; SHELXTL (Sheldrick, 2008) ; _computing_structure_refinement ; SHELXL2018 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT (Sheldrick, 2015a) ; _diffrn_ambient_temperature 150(2) _diffrn_detector_area_resol_mean 10.4167 _diffrn_measured_fraction_theta_full 0.990 _diffrn_measured_fraction_theta_max 0.977 _diffrn_measurement_device_type 'Bruker D8 VENTURE PHOTON 100 CMOS' _diffrn_measurement_method '\w scans' _diffrn_radiation_monochromator mirror _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_reflns_av_R_equivalents 0.0291 _diffrn_reflns_av_unetI/netI 0.0269 _diffrn_reflns_limit_h_max 19 _diffrn_reflns_limit_h_min -18 _diffrn_reflns_limit_k_max 8 _diffrn_reflns_limit_k_min -9 _diffrn_reflns_limit_l_max 15 _diffrn_reflns_limit_l_min -16 _diffrn_reflns_number 11594 _diffrn_reflns_theta_full 70.500 _diffrn_reflns_theta_max 74.367 _diffrn_reflns_theta_min 6.422 _diffrn_source 'INCOATEC I\mS micro--focus source' _exptl_absorpt_coefficient_mu 0.593 _exptl_absorpt_correction_T_max 0.92 _exptl_absorpt_correction_T_min 0.82 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Krause et al., 2015) ; _exptl_crystal_colour orange-red _exptl_crystal_density_diffrn 1.158 _exptl_crystal_density_method 'not measured' _exptl_crystal_description block _exptl_crystal_F_000 592 _exptl_crystal_size_max 0.242 _exptl_crystal_size_mid 0.195 _exptl_crystal_size_min 0.136 _refine_diff_density_max 0.222 _refine_diff_density_min -0.136 _refine_ls_extinction_coef 0.0114(9) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method ; SHELXL2018 (Sheldrick, 2015b) ; _refine_ls_goodness_of_fit_ref 1.046 _refine_ls_hydrogen_treatment refall _refine_ls_matrix_type full _refine_ls_number_parameters 274 _refine_ls_number_reflns 3128 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.046 _refine_ls_R_factor_all 0.0377 _refine_ls_R_factor_gt 0.0351 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0474P)^2^+0.2775P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0935 _refine_ls_wR_factor_ref 0.0960 _reflns_number_gt 2879 _reflns_number_total 3128 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file vm2219sup1.cif _cod_data_source_block I _cod_database_code 2243016 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.870 _shelx_estimated_absorpt_t_max 0.924 _shelx_hkl_file ; 0 0 2 1456.05 51.29 0 0 -2 1361.06 51.29 0 0 -3 0.60 0.20 0 0 3 1.00 0.30 0 0 4 2408.96 85.89 0 0 -4 2320.17 86.09 0 0 5 0.30 0.20 0 0 -5 0.20 0.20 0 0 -6 748.53 27.70 0 0 6 768.02 27.70 0 0 -7 -0.10 0.50 0 0 -8 351.86 14.30 0 0 8 388.46 14.20 0 0 8 392.36 14.30 0 0 -9 0.10 0.90 0 0 9 0.80 1.20 0 0 9 4.00 1.30 0 0 9 0.40 0.70 0 0 10 72.69 3.50 0 0 11 0.10 0.70 0 0 -11 0.30 0.80 0 0 12 353.36 13.60 0 0 -12 355.76 13.60 0 0 -13 0.20 0.60 0 0 13 0.30 0.60 0 0 -13 1.50 0.80 0 0 -14 16.90 1.20 0 0 14 16.60 1.30 0 0 -14 15.40 1.40 0 0 -15 0.20 0.60 0 0 15 -0.80 0.50 0 1 1 2015.60 73.09 0 1 -1 1901.41 73.59 0 -1 1 1955.10 73.59 0 -1 -1 2191.18 73.09 0 1 2 129.99 4.70 0 1 2 133.79 4.80 0 -1 2 126.09 4.90 0 1 -3 5.20 0.50 0 -1 4 1.20 0.50 0 1 -5 1025.00 38.10 0 -1 5 1063.39 38.10 0 1 -6 1079.79 40.20 0 -1 6 1120.09 40.30 0 1 7 16.80 1.40 0 1 -7 18.30 1.70 0 -1 7 15.30 2.00 0 1 8 220.78 8.70 0 -1 8 222.18 8.70 0 -1 8 223.68 8.70 0 1 9 400.66 14.50 0 -1 9 399.66 14.50 0 -1 9 384.06 14.40 0 -1 -9 361.26 14.50 0 -1 9 360.86 14.50 0 1 10 251.17 9.60 0 1 -10 238.88 9.70 0 -1 10 245.28 9.80 0 -1 -10 235.58 9.80 0 -1 10 253.67 9.60 0 1 11 260.07 9.90 0 1 -11 248.18 10.00 0 -1 11 260.37 10.00 0 -1 -11 242.38 10.00 0 1 -12 167.08 6.90 0 1 12 168.88 6.80 0 -1 12 171.78 6.90 0 -1 -12 163.48 6.90 0 1 13 114.89 4.70 0 1 -13 109.29 4.70 0 -1 -13 111.39 4.70 0 -1 13 112.69 4.70 0 -1 -13 100.49 4.90 0 1 14 208.18 8.10 0 1 -14 216.78 8.30 0 1 -14 205.28 8.20 0 -1 -14 215.48 8.30 0 -1 14 216.58 8.20 0 1 -15 15.40 1.20 0 1 -15 14.40 1.10 0 -1 -15 14.00 1.20 0 -1 15 14.30 1.00 0 2 1 583.74 21.70 0 2 -1 585.04 21.80 0 -2 -1 614.84 21.80 0 -2 1 605.24 21.90 0 2 -2 819.92 30.70 0 2 2 836.72 30.50 0 -2 2 795.62 30.70 0 -2 -2 917.41 30.70 0 2 -3 268.27 10.60 0 2 3 275.37 10.20 0 2 3 300.47 10.30 0 -2 3 280.47 10.70 0 2 -4 7.70 0.80 0 -2 4 4.70 0.90 0 2 -5 76.09 3.40 0 2 5 71.79 3.10 0 -2 5 72.49 3.50 0 2 6 137.19 5.40 0 2 -6 132.79 5.80 0 2 7 239.38 9.00 0 2 -7 235.08 9.70 0 -2 7 230.38 9.10 0 2 8 53.39 3.50 0 2 8 56.19 2.70 0 -2 8 60.59 2.80 0 -2 8 50.89 3.10 0 -2 8 53.39 3.00 0 2 9 69.49 3.40 0 2 9 71.49 3.20 0 2 9 62.29 3.80 0 -2 9 67.69 3.30 0 -2 9 65.89 3.50 0 -2 9 69.39 3.30 0 2 -10 1.80 0.70 0 -2 10 2.20 0.70 0 -2 10 2.20 1.20 0 2 -11 11.80 1.40 0 2 11 12.20 1.50 0 -2 11 12.70 1.40 0 -2 11 8.30 2.20 0 -2 -11 13.60 1.40 0 2 -12 1.50 0.70 0 2 12 4.80 1.30 0 -2 -12 2.30 0.70 0 -2 12 0.50 0.60 0 2 13 36.60 2.00 0 2 -13 33.60 2.00 0 2 -13 34.70 2.00 0 -2 13 35.70 2.00 0 -2 -13 34.90 2.00 0 2 -14 62.99 3.10 0 2 -14 53.89 2.80 0 -2 14 56.39 2.70 0 -2 -14 69.39 3.50 0 2 -15 17.10 1.10 0 -2 15 18.30 1.10 0 -2 -15 18.20 1.00 0 3 0 0.10 0.30 0 -3 0 0.30 0.30 0 3 1 707.53 25.80 0 3 -1 680.73 25.90 0 -3 1 694.53 26.00 0 -3 -1 740.23 25.90 0 3 2 1.80 0.60 0 3 -2 2.10 0.70 0 3 2 0.80 0.40 0 -3 -2 1.40 0.60 0 3 3 321.97 12.20 0 3 -3 337.37 12.60 0 3 3 334.27 12.10 0 -3 3 316.77 12.60 0 3 -4 4.00 1.00 0 3 4 4.10 0.70 0 3 -5 457.95 18.10 0 3 5 489.65 17.60 0 3 -6 51.09 3.70 0 3 6 45.90 2.30 0 -3 6 43.20 2.40 0 3 7 163.28 7.00 0 3 7 176.38 6.80 0 -3 7 164.68 6.80 0 -3 7 174.68 6.80 0 3 8 0.20 1.10 0 3 8 0.30 0.60 0 3 8 -0.70 1.00 0 -3 8 0.50 0.90 0 -3 8 0.10 0.60 0 -3 8 0.40 1.30 0 3 9 79.89 4.20 0 3 9 87.29 3.80 0 -3 9 80.99 3.90 0 -3 9 83.99 3.80 0 -3 -9 81.29 3.80 0 -3 9 83.29 4.30 0 3 -10 5.70 1.50 0 3 10 4.00 1.50 0 3 10 8.90 1.70 0 -3 -10 3.90 1.20 0 -3 10 6.60 1.80 0 -3 10 4.20 1.10 0 3 -11 123.39 5.30 0 3 11 124.79 5.20 0 -3 -11 123.59 5.20 0 -3 11 115.89 5.30 0 -3 11 124.59 5.30 0 3 12 43.90 2.50 0 -3 -12 45.90 3.10 0 3 -13 127.69 5.20 0 -3 13 119.89 5.00 0 -3 -13 120.29 5.00 0 3 -14 278.57 10.70 0 -3 -14 277.77 10.70 0 -3 14 296.57 10.70 0 4 0 4694.23 162.08 0 4 0 4353.66 160.38 0 -4 0 4295.37 160.78 0 4 1 83.89 3.50 0 4 1 83.89 3.70 0 4 -1 83.79 3.80 0 4 -1 78.39 3.50 0 -4 -1 78.89 3.90 0 -4 1 84.09 5.20 0 4 -2 888.81 33.50 0 4 2 929.71 33.70 0 4 2 922.51 33.50 0 4 -2 936.31 34.00 0 -4 -2 914.51 33.80 0 4 -3 1094.19 38.50 0 4 -3 996.70 37.70 0 4 3 1019.60 37.80 0 4 3 1025.70 37.80 0 -4 -3 1039.50 38.20 0 4 4 48.60 2.30 0 4 5 324.27 12.40 0 4 5 329.97 12.40 0 -4 5 320.67 12.30 0 4 6 22.60 1.50 0 4 6 20.40 1.90 0 -4 6 18.00 1.70 0 -4 -6 21.10 2.10 0 -4 6 22.80 1.60 0 4 7 69.09 3.50 0 4 7 71.99 3.60 0 4 7 76.69 3.40 0 -4 -7 68.99 3.50 0 -4 7 73.99 3.40 0 -4 7 72.69 3.40 0 4 8 70.09 3.90 0 4 8 68.09 3.20 0 4 8 68.89 3.50 0 -4 8 67.79 3.30 0 -4 8 66.19 3.20 0 -4 -8 70.19 3.40 0 4 9 133.49 5.70 0 4 9 129.69 5.70 0 -4 -9 137.49 5.70 0 -4 9 134.89 5.70 0 -4 9 133.99 5.60 0 4 10 5.30 1.20 0 4 -10 5.50 1.30 0 -4 10 4.70 1.60 0 -4 10 5.60 1.10 0 -4 -10 9.00 1.30 0 4 -11 17.40 1.60 0 -4 11 16.80 1.70 0 -4 -11 17.10 1.60 0 -4 11 19.80 1.90 0 4 -12 1.60 0.60 0 -4 12 0.70 0.50 0 -4 -12 0.20 0.50 0 4 -13 0.90 0.50 0 -4 -13 1.30 0.50 0 -4 13 0.70 0.40 0 4 -14 2.30 0.50 0 -4 14 3.40 0.60 0 -4 -14 2.90 0.80 0 5 0 -0.30 1.20 0 5 0 1.40 0.60 0 5 1 165.18 7.80 0 5 1 179.18 6.90 0 5 -1 178.48 6.90 0 5 2 5.30 0.90 0 5 -2 6.00 1.10 0 -5 2 5.50 1.20 0 5 3 80.29 3.70 0 5 3 82.79 3.60 0 5 -3 81.69 3.70 0 -5 3 81.79 3.70 0 5 4 36.80 2.10 0 5 4 38.70 2.20 0 -5 4 38.60 2.20 0 5 5 295.07 11.00 0 5 5 274.47 10.90 0 -5 5 274.77 10.90 0 -5 5 287.97 10.90 0 5 6 121.69 5.50 0 5 6 126.29 5.30 0 -5 6 124.19 5.20 0 -5 6 129.39 5.30 0 5 7 476.35 17.00 0 5 7 439.06 16.90 0 -5 -7 434.96 16.80 0 -5 7 450.65 17.00 0 -5 7 438.26 16.80 0 5 -8 588.74 21.40 0 5 8 558.04 21.40 0 5 8 574.14 21.30 0 -5 -8 584.74 21.30 0 -5 8 567.34 21.30 0 -5 8 557.84 21.30 0 5 -9 49.90 2.70 0 5 9 46.70 2.60 0 5 9 50.29 2.70 0 -5 -9 51.99 2.60 0 -5 9 46.50 2.60 0 -5 9 52.39 2.70 0 5 10 110.19 4.90 0 5 -10 112.19 4.90 0 -5 -10 117.09 4.80 0 -5 10 122.99 4.90 0 5 11 1.70 1.20 0 5 -11 2.20 0.60 0 -5 -11 3.20 1.10 0 -5 11 2.80 0.90 0 -5 11 4.10 0.80 0 5 -12 55.49 2.60 0 -5 12 55.99 2.60 0 -5 -12 60.69 3.20 0 5 -13 63.59 2.70 0 6 0 172.68 6.80 0 6 0 163.98 6.80 0 6 1 417.46 16.00 0 6 -1 436.66 16.10 0 6 1 438.66 16.10 0 -6 1 407.16 16.20 0 6 -2 57.59 2.90 0 6 2 57.49 2.90 0 -6 2 55.59 2.80 0 6 3 15.50 1.30 0 -6 3 17.20 1.50 0 6 4 1.30 0.60 0 -6 4 0.90 0.70 0 -6 4 1.80 0.70 0 6 5 207.28 8.10 0 -6 5 191.28 8.40 0 -6 5 196.98 7.80 0 6 6 52.19 2.80 0 -6 6 57.69 2.80 0 -6 6 51.99 2.70 0 6 7 79.99 3.90 0 6 -7 82.09 3.90 0 -6 7 86.99 3.80 0 -6 7 83.99 3.80 0 6 8 57.09 3.00 0 6 -8 63.19 3.00 0 -6 8 60.09 2.90 0 -6 8 59.69 2.90 0 6 9 23.00 1.70 0 6 -9 23.10 1.70 0 -6 9 24.60 1.50 0 -6 9 24.50 1.60 0 6 -10 8.70 1.20 0 6 10 7.20 1.20 0 -6 10 6.60 1.10 0 -6 10 5.90 0.90 0 6 -11 29.70 1.60 0 -6 11 26.40 1.50 0 7 0 0.30 0.70 0 -7 0 -0.50 0.60 0 7 1 202.48 8.20 0 7 -1 199.78 8.20 0 -7 1 200.28 8.20 0 -7 -1 217.78 8.40 0 7 2 22.90 1.70 0 -7 2 25.40 1.70 0 7 3 111.59 5.00 0 -7 3 116.39 4.80 0 -7 3 116.89 4.90 0 7 4 184.08 7.80 0 -7 4 193.78 7.60 0 -7 4 199.28 7.70 0 7 5 43.00 2.40 0 -7 5 43.70 2.30 0 -7 5 45.20 2.30 0 7 6 9.90 1.20 0 -7 6 8.40 1.10 0 7 7 177.48 7.30 0 -7 7 182.18 7.10 0 -7 7 177.68 7.00 0 7 8 29.90 1.80 0 -7 8 28.70 1.60 0 -7 8 26.00 1.60 0 -7 -8 27.10 1.70 0 7 9 27.30 1.70 0 -7 9 25.90 1.40 0 -7 9 27.80 1.50 0 -7 10 13.00 1.00 0 8 0 321.07 12.50 0 -8 0 329.07 12.40 0 8 1 21.70 1.70 0 -8 1 20.60 1.50 0 -8 -1 24.10 1.50 0 8 2 18.90 1.50 0 -8 -2 20.30 1.40 0 -8 2 19.00 1.30 0 8 3 73.99 3.50 0 -8 3 73.29 3.30 0 -8 -3 75.69 3.30 0 -8 -4 1.60 0.50 0 -8 4 1.30 0.50 0 8 5 26.00 1.60 0 -8 5 22.60 1.40 0 -8 -5 25.40 1.50 0 8 6 35.60 2.00 0 -8 -6 33.50 1.80 0 -8 6 35.90 1.80 0 8 7 12.70 1.20 0 -8 7 11.10 0.90 0 -8 8 0.90 0.50 0 -9 0 -0.70 0.40 0 -9 -1 45.50 2.20 0 -9 -2 8.50 0.80 0 -9 2 9.40 1.00 0 -9 -3 3.00 0.70 0 -9 3 3.00 0.60 0 -9 4 19.30 1.10 0 -9 -4 18.30 1.10 0 -9 5 0.40 0.40 1 0 -15 0.30 0.80 -1 0 15 -0.40 0.60 1 0 -15 -0.10 0.50 -1 0 14 115.89 4.70 1 0 -14 112.19 4.70 1 0 -14 110.09 4.70 -1 0 13 0.30 1.00 1 0 -13 0.40 0.60 1 0 -12 1271.17 47.40 -1 0 12 1317.47 47.40 1 0 -11 -0.90 0.80 -1 0 11 0.30 0.70 -1 0 10 555.04 20.10 1 0 -10 514.75 20.00 1 0 -9 -0.80 0.90 -1 0 9 -1.10 0.80 -1 0 8 185.28 7.30 1 0 -7 0.10 0.50 -1 0 7 0.70 0.60 -1 0 6 52.79 2.40 1 0 -6 48.70 2.40 1 0 -5 0.00 0.20 -1 0 5 0.40 0.20 -1 0 4 37.80 1.70 1 0 -4 39.20 1.70 1 0 -3 0.70 0.30 -1 0 3 1.00 0.30 1 0 -2 3218.88 119.59 -1 0 2 3370.06 119.59 -1 0 1 0.10 0.10 1 0 -1 0.00 0.10 1 0 1 0.60 0.10 1 0 2 527.05 18.90 -1 0 -2 514.15 18.90 1 0 3 -0.10 0.10 -1 0 -3 0.00 0.10 1 0 4 1283.07 45.80 -1 0 -4 1241.48 45.70 -1 0 -5 -0.10 0.20 1 0 5 0.00 0.30 1 0 6 1829.22 66.99 -1 0 -6 1876.51 67.09 -1 0 -7 -0.20 0.60 1 0 8 118.89 5.10 1 0 8 118.19 5.10 1 0 8 124.89 5.60 1 0 9 0.60 0.70 1 0 9 0.30 0.70 1 0 9 0.50 1.00 -1 0 -9 1.00 0.90 1 0 10 0.20 0.70 -1 0 -10 0.60 0.90 -1 0 -11 -0.50 0.80 1 0 11 2.60 1.20 1 0 11 -1.10 0.60 -1 0 -12 197.98 7.90 1 0 12 191.48 7.80 1 0 13 -0.30 0.50 -1 0 -13 -0.80 0.70 1 0 14 73.99 3.10 -1 0 -14 69.09 3.30 -1 0 -14 71.09 3.30 1 0 15 0.60 0.50 -1 0 -15 0.00 0.40 1 1 -15 1.40 0.60 1 1 -15 1.40 0.60 1 -1 -15 0.50 0.50 -1 -1 15 1.10 0.50 1 1 -14 -0.40 0.60 -1 1 14 -0.30 0.70 1 1 -14 0.40 0.60 -1 1 13 60.89 2.90 1 1 -13 60.69 2.90 1 -1 -13 58.79 3.10 1 -1 -13 60.09 3.20 1 1 -12 37.00 2.30 -1 1 12 39.20 2.30 1 -1 -12 36.00 2.20 1 -1 -12 35.80 2.50 -1 -1 12 39.80 2.30 -1 1 11 330.97 12.60 1 1 -11 333.77 12.70 1 -1 -11 320.47 12.60 -1 -1 11 322.97 12.60 -1 1 10 761.52 27.40 1 1 -10 751.52 27.60 -1 -1 10 727.23 27.50 1 -1 -10 718.53 27.40 -1 1 9 81.19 3.70 1 1 -9 78.99 3.70 1 -1 -9 72.49 3.80 -1 -1 9 79.79 3.60 -1 -1 9 82.39 3.60 -1 1 8 106.49 4.30 1 1 -8 99.69 5.10 -1 -1 8 103.69 4.40 -1 -1 8 99.69 4.40 1 1 -7 0.90 0.60 -1 -1 7 5.40 1.70 1 1 -6 274.67 10.60 -1 1 6 264.07 10.40 -1 1 6 289.77 10.20 -1 -1 6 276.67 10.60 1 1 -5 677.33 25.80 -1 1 5 700.83 25.50 -1 -1 5 729.53 25.80 1 1 -4 681.83 24.70 -1 1 4 739.53 24.50 -1 -1 4 602.04 24.90 -1 1 3 80.89 3.00 -1 1 3 79.79 3.00 1 1 -3 71.89 3.10 -1 -1 3 78.99 3.20 -1 1 2 314.27 11.80 1 1 -2 317.97 11.90 -1 -1 2 341.27 12.00 1 1 -1 3633.54 139.49 -1 1 1 3844.12 139.19 1 -1 -1 3884.71 139.29 -1 -1 1 4008.30 139.59 -1 1 0 1704.83 63.79 1 1 0 1708.43 63.69 1 -1 0 1759.32 63.79 -1 -1 0 1811.72 63.49 -1 1 -1 850.31 32.50 1 1 1 848.82 32.20 -1 -1 -1 936.21 32.20 1 -1 1 907.61 32.60 -1 1 -3 117.69 4.80 1 -1 3 130.09 4.80 -1 1 -4 1009.20 33.90 1 -1 4 848.52 34.00 -1 1 -5 699.23 26.10 1 -1 5 722.43 26.10 -1 1 -6 648.94 24.00 1 -1 6 649.74 24.10 -1 1 -7 43.40 2.70 1 1 8 55.19 3.10 1 1 8 51.69 2.70 1 1 8 50.29 2.70 1 -1 8 47.60 2.60 1 -1 8 53.79 2.70 1 -1 8 49.80 2.90 1 1 9 204.88 7.90 1 1 9 197.18 8.10 1 -1 9 200.38 7.90 -1 -1 -9 180.08 8.00 1 -1 9 199.68 8.00 1 -1 9 206.48 7.90 1 1 10 95.59 4.10 -1 1 -10 90.49 4.20 1 1 10 84.09 4.40 -1 -1 -10 83.89 4.30 1 -1 10 95.69 4.10 1 -1 10 93.39 4.40 1 -1 10 93.59 4.20 -1 1 -11 7.20 1.40 1 1 11 9.50 2.10 1 1 11 7.60 1.40 1 -1 11 7.70 1.30 1 -1 11 9.80 2.10 -1 -1 -11 8.70 2.00 -1 1 -12 3.70 0.90 1 1 12 2.70 0.70 1 -1 12 3.30 1.00 -1 -1 -12 3.60 1.20 -1 1 -13 222.38 8.70 1 1 13 219.18 8.60 -1 -1 -13 219.78 8.70 1 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68.49 3.20 5 6 2 65.99 3.40 5 6 2 68.39 3.40 5 -6 2 66.69 3.20 5 -6 2 67.09 3.30 5 6 3 8.70 1.30 5 6 3 7.90 1.20 5 6 3 8.90 1.10 5 -6 3 11.80 1.60 5 -6 3 9.30 1.20 5 6 4 77.89 3.90 5 6 4 85.09 3.90 5 6 4 83.19 3.80 5 -6 4 92.19 4.20 5 -6 4 86.49 3.90 5 6 5 1.30 0.70 5 6 5 1.00 0.60 5 6 5 0.80 0.60 5 -6 5 0.50 0.60 5 6 6 80.99 3.90 5 6 6 87.09 3.90 5 6 6 86.99 3.80 5 -6 6 86.89 3.80 5 6 7 49.80 2.40 5 6 7 44.10 2.30 5 6 7 50.49 2.60 5 -6 7 45.10 2.40 5 6 8 83.89 3.80 5 6 8 85.59 3.60 5 6 8 81.89 3.50 5 -6 8 86.79 4.20 5 6 9 79.09 3.20 -5 6 -9 76.69 3.30 5 -6 9 75.79 3.30 -5 6 -10 24.90 1.30 5 -6 10 22.90 1.30 -5 -7 11 26.70 1.30 -5 7 10 10.90 1.10 -5 -7 10 11.10 0.80 -5 7 9 7.40 1.00 -5 -7 9 6.40 0.80 -5 7 8 13.70 1.40 -5 -7 8 12.00 1.00 -5 -7 7 1.30 0.50 -5 -7 7 1.10 0.70 -5 7 6 1.30 0.70 -5 -7 6 1.90 0.70 -5 -7 6 4.00 0.90 -5 7 5 57.09 3.00 -5 -7 5 65.79 2.90 -5 7 4 63.89 3.10 5 7 -4 60.89 3.20 5 -7 -4 65.99 3.20 -5 -7 4 69.69 3.10 5 7 -3 49.10 2.80 -5 7 3 50.99 2.70 -5 -7 3 57.19 2.70 5 -7 -3 51.59 2.60 -5 7 2 330.17 12.90 5 7 -2 312.47 13.00 5 7 -2 352.46 12.80 -5 -7 2 349.47 12.90 5 -7 -2 339.57 12.80 5 7 -1 95.29 4.50 5 7 -1 103.89 4.30 5 -7 -1 104.69 4.40 5 7 0 1.10 0.60 5 7 0 2.20 0.80 5 -7 0 0.10 0.60 5 7 1 9.80 1.10 5 7 1 9.90 1.20 5 -7 1 9.10 1.20 5 7 2 14.00 1.20 5 7 2 11.70 1.20 5 -7 2 11.90 1.20 5 7 3 2.70 0.90 5 7 3 4.70 1.30 5 -7 3 4.60 0.90 5 7 4 7.10 1.10 5 7 4 6.20 1.00 5 -7 4 6.70 1.50 5 7 5 0.80 0.70 5 7 5 1.20 0.60 5 -7 5 1.20 0.60 5 7 6 7.10 1.00 5 7 6 8.70 1.10 -5 7 -6 6.70 1.60 5 -7 6 7.50 1.00 -5 7 -7 65.99 3.00 5 7 7 56.89 2.80 5 7 7 58.39 2.60 5 -7 7 58.19 2.70 5 -7 8 4.00 0.80 -5 -8 8 9.20 0.80 -5 8 7 17.10 1.30 -5 -8 7 14.90 1.00 -5 8 6 102.29 4.30 -5 -8 6 103.59 4.10 -5 -8 6 101.59 4.10 -5 8 5 5.30 1.10 -5 -8 5 4.90 0.80 -5 -8 5 5.40 0.90 -5 8 4 27.60 1.90 -5 -8 4 28.50 1.60 5 8 -3 132.49 5.60 5 -8 -3 132.09 5.30 -5 -8 3 131.49 5.30 5 8 -2 40.10 2.40 5 -8 -2 45.90 2.20 -5 -8 2 45.20 2.20 5 8 -1 30.40 2.00 -5 -8 1 30.80 1.70 5 -8 -1 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3 11 100.09 4.10 6 3 11 96.89 4.10 -6 -3 -11 97.19 4.00 6 -3 11 96.59 4.10 6 -3 11 93.59 4.00 6 3 12 4.40 1.00 6 3 12 3.20 0.80 -6 3 -12 5.30 1.20 6 -3 12 3.40 0.70 6 -3 12 4.60 0.90 -6 -3 -12 2.80 1.00 6 -4 -14 45.60 2.10 6 4 -13 10.40 1.10 -6 4 13 9.40 1.40 6 -4 -13 7.60 0.90 -6 -4 13 9.40 0.90 6 4 -12 0.50 0.60 -6 4 12 0.10 0.70 6 -4 -12 0.20 0.50 -6 -4 12 0.50 0.50 -6 4 11 10.90 1.20 6 4 -11 13.20 1.50 6 -4 -11 11.70 1.20 -6 -4 11 13.00 1.20 6 4 -10 195.78 7.70 -6 4 10 180.28 7.60 -6 -4 10 183.38 7.50 6 -4 -10 188.48 7.60 6 4 -9 19.20 1.90 -6 4 9 20.80 2.10 -6 -4 9 16.90 1.50 6 -4 -9 18.90 1.60 6 4 -8 174.68 7.30 -6 4 8 180.38 7.30 6 4 -8 179.28 7.30 6 -4 -8 177.78 7.20 6 4 -7 48.60 2.80 -6 4 7 49.50 2.60 6 4 -7 47.50 3.10 6 -4 -7 49.90 2.60 -6 4 6 227.68 9.00 6 4 -6 226.08 8.90 6 -4 -6 216.78 8.70 6 4 -5 3.40 1.10 6 4 -5 5.40 1.00 -6 4 5 5.80 0.90 6 -4 -5 8.20 1.30 6 4 -4 52.29 2.60 6 4 -4 50.69 2.50 -6 4 4 50.29 2.50 6 -4 -4 49.70 2.60 6 4 -3 912.61 33.10 -6 4 3 907.31 33.00 6 4 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6 30.90 2.00 6 4 7 153.58 6.40 6 4 7 154.88 6.30 6 4 7 138.49 6.30 6 -4 7 151.38 6.40 6 -4 7 147.59 6.20 6 -4 7 165.68 7.10 6 -4 7 150.88 6.20 6 4 8 20.00 1.60 6 4 8 20.20 1.50 6 -4 8 19.70 1.60 6 -4 8 20.20 1.60 6 -4 8 23.00 1.60 6 4 9 130.89 5.30 6 4 9 130.09 5.40 6 -4 9 125.59 5.30 6 -4 9 127.59 5.20 -6 -4 -9 124.49 5.60 6 -4 9 136.39 5.40 6 4 10 50.19 2.40 6 4 10 48.30 2.30 6 -4 10 47.60 2.30 6 -4 10 48.10 2.40 6 -4 10 51.49 2.30 6 4 11 30.90 1.50 -6 4 -11 31.50 2.10 6 -4 11 29.90 1.60 6 -4 11 26.40 1.70 -6 4 -12 46.00 2.00 6 5 -13 4.70 1.10 -6 -5 13 2.50 0.70 -6 5 12 2.70 1.00 -6 -5 12 2.60 0.80 6 -5 -12 2.70 0.80 6 5 -11 13.70 1.50 -6 5 11 15.80 1.30 6 -5 -11 17.00 1.20 -6 -5 11 14.40 1.20 6 5 -10 0.00 0.80 -6 5 10 0.60 0.60 -6 -5 10 0.20 0.50 6 -5 -10 0.20 0.60 6 5 -9 140.59 5.90 -6 5 9 133.59 5.90 6 -5 -9 147.19 5.80 -6 -5 9 141.19 5.80 -6 5 8 11.40 1.20 -6 -5 8 12.70 1.30 6 -5 -8 14.90 1.40 -6 5 7 24.60 1.70 6 5 -7 27.30 2.10 6 -5 -7 22.80 1.70 -6 5 6 80.69 3.70 6 5 -6 84.19 3.90 6 -5 -6 84.49 3.70 -6 -5 6 71.89 3.80 6 5 -5 763.42 27.50 6 5 -5 787.52 27.80 -6 5 5 760.62 27.80 6 -5 -5 670.33 27.90 -6 -5 5 742.93 27.50 -6 5 4 877.81 31.50 6 5 -4 895.51 31.60 6 5 -4 814.52 31.90 6 -5 -4 824.22 31.30 6 5 -3 0.40 0.50 -6 5 3 1.00 0.60 6 -5 -3 0.40 0.80 6 -5 -3 -1.00 1.10 6 5 -2 561.94 20.80 6 5 -2 565.74 21.00 -6 5 2 579.64 20.80 6 -5 -2 532.95 20.70 6 -5 -2 558.44 20.80 -6 5 1 0.90 0.80 6 5 -1 2.20 0.70 6 5 -1 0.60 0.50 6 5 -1 1.50 0.70 6 -5 -1 0.80 0.90 6 -5 -1 0.80 0.80 6 -5 -1 -0.20 0.80 6 5 0 66.99 3.20 6 5 0 70.59 3.40 6 5 0 66.79 3.20 6 -5 0 66.29 3.20 6 -5 0 67.89 3.30 6 -5 0 65.49 3.30 6 5 1 37.60 2.10 6 5 1 39.30 2.20 6 5 1 37.30 2.20 6 -5 1 36.50 2.30 6 -5 1 36.90 2.20 6 -5 1 37.00 2.20 6 5 2 30.90 1.90 6 5 2 25.60 1.70 6 5 2 27.50 1.90 6 -5 2 26.60 1.80 6 -5 2 27.70 2.00 6 -5 2 21.40 1.90 6 5 3 21.60 1.70 6 5 3 18.40 1.60 6 5 3 22.90 1.60 6 -5 3 19.70 1.80 6 -5 3 20.70 1.70 6 -5 3 21.80 1.70 6 5 4 5.00 1.10 6 5 4 7.70 1.20 6 5 4 8.30 1.20 6 -5 4 9.20 1.70 6 -5 4 6.30 1.30 6 -5 4 6.60 1.20 6 5 5 138.89 5.90 6 5 5 137.19 5.80 6 5 5 142.09 5.90 6 -5 5 132.39 5.70 6 -5 5 141.49 5.80 6 -5 5 140.09 5.80 6 5 6 41.90 2.50 6 5 6 46.20 2.40 6 5 6 45.40 2.50 6 -5 6 45.20 2.40 6 -5 6 44.40 2.40 6 -5 6 41.20 2.40 6 5 7 14.60 1.30 6 5 7 17.80 1.40 6 5 7 13.70 1.60 6 -5 7 14.80 1.30 6 -5 7 11.30 1.60 6 5 8 37.60 2.00 6 5 8 34.10 1.90 6 -5 8 32.60 2.00 6 -5 8 37.40 2.10 6 -5 8 35.20 2.30 6 5 9 194.18 7.20 6 5 9 189.48 7.10 6 -5 9 171.68 7.30 6 -5 9 176.08 7.00 6 5 10 55.19 2.50 6 5 10 48.30 2.20 -6 5 -10 46.10 2.40 6 -5 10 47.90 2.20 6 -5 10 48.40 2.30 -6 5 -11 80.99 3.20 6 -5 11 75.49 3.20 -6 -6 12 3.70 0.60 6 -6 -12 3.30 0.80 -6 6 11 0.90 0.60 -6 -6 11 0.70 0.40 6 -6 -11 0.70 0.50 -6 6 10 8.30 1.20 -6 -6 10 7.20 0.90 6 -6 -10 7.40 0.90 -6 6 9 5.10 0.90 6 -6 -9 3.80 0.90 -6 -6 9 5.70 0.80 -6 6 8 1.10 0.60 6 -6 -8 0.50 0.70 -6 6 7 38.40 2.20 6 -6 -7 42.40 2.20 -6 -6 7 37.20 2.40 6 6 -6 194.58 7.80 -6 6 6 181.58 7.60 6 -6 -6 188.68 7.50 -6 -6 6 187.68 7.50 6 6 -5 74.89 3.70 -6 6 5 71.39 3.50 6 -6 -5 76.59 3.40 -6 -6 5 75.29 3.50 6 6 -4 5.30 1.40 -6 6 4 7.30 1.70 6 6 -4 4.80 1.00 6 -6 -4 6.50 1.40 -6 -6 4 4.70 1.40 6 6 -3 1286.07 46.30 -6 6 3 1316.77 46.10 6 6 -3 1245.28 46.00 6 -6 -3 1246.58 45.90 6 -6 -3 1202.08 45.90 6 6 -2 17.30 1.40 6 6 -2 15.00 1.40 -6 6 2 15.50 1.50 6 -6 -2 15.10 1.60 6 -6 -2 14.80 1.70 6 6 -1 22.40 1.60 6 6 -1 20.90 1.60 6 -6 -1 21.30 1.90 6 -6 -1 23.10 1.80 6 6 0 273.47 10.50 6 6 0 266.27 10.20 6 -6 0 251.27 10.10 6 -6 0 263.47 10.20 6 6 1 3.50 0.90 6 6 1 3.20 1.00 6 -6 1 1.40 1.00 6 -6 1 4.70 1.10 6 -6 1 3.90 1.10 6 6 2 41.70 2.50 6 6 2 45.10 2.40 6 6 2 47.50 2.40 6 -6 2 44.00 2.50 6 -6 2 44.20 2.40 6 6 3 70.09 3.30 6 6 3 70.39 3.50 6 6 3 73.99 3.40 6 -6 3 72.69 3.40 6 -6 3 71.99 3.40 6 6 4 40.70 2.40 6 6 4 49.90 3.10 6 6 4 39.90 2.20 6 -6 4 41.70 2.30 6 -6 4 43.90 2.40 6 6 5 3.90 1.10 6 6 5 4.30 1.00 6 6 5 3.70 0.90 6 -6 5 3.70 1.00 6 6 6 27.50 1.60 6 6 6 26.00 1.60 6 6 6 24.90 1.80 6 -6 6 26.10 1.60 6 6 7 0.10 0.40 6 6 7 -0.70 0.90 6 6 7 0.00 0.80 6 -6 7 0.50 0.40 6 6 8 4.60 0.80 6 6 8 3.80 0.80 6 -6 8 3.80 0.90 -6 6 -9 72.99 3.10 6 6 9 72.19 3.00 6 -6 9 74.99 3.10 -6 -7 11 123.09 4.70 -6 7 10 0.20 1.00 -6 -7 10 1.10 0.40 -6 7 9 1.50 0.60 -6 -7 9 0.90 0.40 -6 7 8 21.90 1.50 -6 -7 8 21.80 1.30 -6 7 7 35.10 2.00 -6 -7 7 33.50 2.00 -6 -7 7 36.80 2.10 -6 7 6 1.40 0.60 -6 -7 6 0.50 0.70 -6 7 5 499.35 18.70 6 7 -5 491.45 18.80 -6 -7 5 504.75 18.60 -6 7 4 24.40 1.70 6 7 -4 23.20 1.80 -6 -7 4 25.40 1.60 6 7 -3 5.90 1.10 -6 7 3 4.90 1.20 6 -7 -3 4.20 1.50 -6 -7 3 5.70 1.10 6 7 -2 77.39 3.80 6 7 -2 84.19 3.60 -6 -7 2 84.19 3.70 6 -7 -2 80.99 3.60 6 7 -1 3.60 1.00 6 7 -1 3.80 0.90 6 -7 -1 2.20 0.70 6 7 0 31.50 2.10 6 7 0 32.80 1.90 6 -7 0 36.50 2.00 6 7 1 17.70 1.50 6 7 1 18.80 1.40 6 -7 1 22.10 1.50 6 7 2 22.40 1.50 6 7 2 19.10 1.60 6 -7 2 22.10 1.70 6 7 3 6.00 0.90 6 7 3 5.00 1.00 6 -7 3 6.10 0.90 6 7 4 13.30 1.10 6 7 4 11.90 1.20 6 -7 4 12.90 1.10 6 7 5 45.80 2.10 6 7 5 44.70 2.40 6 -7 5 41.00 2.10 6 7 6 14.30 1.40 -6 7 -6 13.90 1.40 6 7 6 16.00 1.10 6 -7 6 15.20 1.10 6 7 7 0.60 0.60 -6 7 -7 1.00 1.00 6 -7 7 1.00 0.40 6 -7 8 82.29 3.30 -6 -8 8 0.30 0.40 -6 -8 7 3.60 0.60 -6 8 6 27.60 1.80 -6 -8 6 28.40 1.70 -6 -8 6 31.30 1.50 -6 8 5 26.00 1.80 -6 -8 5 24.10 1.40 -6 -8 5 25.40 1.50 -6 -8 4 3.60 0.90 6 8 -3 11.50 1.60 -6 -8 3 9.60 1.00 6 8 -2 81.89 3.70 -6 -8 2 83.49 3.50 6 -8 -2 78.99 3.40 6 8 -1 0.70 0.70 -6 -8 1 3.20 0.80 6 -8 -1 1.30 0.60 6 8 0 21.30 1.60 6 -8 0 21.80 1.40 -6 -8 0 20.90 1.40 6 8 1 0.10 0.40 6 8 1 0.30 0.70 6 -8 1 0.20 0.50 -6 -8 -1 0.40 0.40 6 8 2 22.20 1.50 6 8 2 19.90 1.20 6 -8 2 21.30 1.30 6 8 3 0.60 0.60 6 8 3 -0.50 0.70 6 -8 3 -0.10 0.40 6 8 4 29.40 1.50 6 8 4 29.70 1.80 6 -8 4 29.00 1.50 6 -8 5 21.10 1.20 -6 -9 3 0.30 0.40 -6 -9 2 97.59 3.80 -6 -9 1 11.80 0.90 -6 -9 0 -0.10 0.40 -6 -9 -1 1.60 0.40 7 0 -16 53.89 2.40 7 0 -15 1.20 0.80 7 0 -15 -0.20 1.00 7 0 -14 128.59 5.30 7 0 -14 124.79 5.10 7 0 -13 0.80 0.60 7 0 -13 -0.30 0.70 -7 0 12 1000.10 38.00 7 0 -12 1057.69 38.00 7 0 -12 1046.50 38.50 7 0 -11 0.50 0.60 7 0 -11 0.20 0.60 -7 0 11 0.40 0.90 7 0 -10 386.66 14.70 7 0 -10 379.56 15.00 7 0 -9 0.60 0.80 7 0 -9 -0.40 0.90 7 0 -8 2024.50 73.09 7 0 -8 2018.00 73.29 7 0 -8 2000.70 73.19 7 0 -7 0.90 0.70 7 0 -7 0.20 0.60 7 0 -6 1098.79 40.20 7 0 -5 0.00 0.50 -7 0 4 11.50 1.50 7 0 -4 12.70 1.10 -7 0 2 22.50 1.60 7 0 -2 23.60 1.50 -7 0 2 28.40 1.90 -7 0 1 -0.10 0.40 -7 0 1 0.60 0.40 -7 0 0 195.18 7.70 -7 0 0 187.58 7.60 -7 0 -1 0.20 0.40 -7 0 -1 -0.20 0.50 -7 0 -2 229.98 9.10 -7 0 -2 224.78 8.80 -7 0 -3 5.10 1.20 7 0 4 215.38 8.60 7 0 4 239.38 9.20 7 0 4 214.08 8.70 7 0 5 0.20 0.80 7 0 5 0.80 0.70 7 0 5 -0.80 1.10 7 0 5 0.10 0.70 7 0 6 1.00 0.70 7 0 6 -0.40 0.60 7 0 6 0.30 1.00 7 0 7 0.40 0.70 7 0 7 0.50 0.60 7 0 7 0.10 0.60 7 0 8 69.39 3.40 7 0 8 71.79 3.40 7 0 8 71.39 3.50 7 0 9 0.50 1.20 7 0 9 -0.10 0.70 7 0 9 -0.80 0.60 -7 0 -10 17.60 2.00 7 0 10 20.90 1.50 7 0 10 19.90 1.50 7 0 10 19.10 1.50 7 0 11 -0.30 0.60 7 0 11 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39.80 2.30 -7 -7 3 43.90 2.30 7 7 -2 11.90 1.30 7 7 -2 13.30 1.10 -7 -7 2 12.10 1.30 7 -7 -2 11.10 1.40 7 7 -1 372.36 12.90 7 7 -1 329.87 13.20 7 -7 -1 316.47 13.60 7 7 0 34.10 1.90 7 7 0 33.10 2.10 7 -7 0 35.80 2.20 7 7 1 1.00 0.60 7 -7 1 -0.50 0.50 7 7 2 43.00 2.40 7 7 2 43.40 2.20 7 -7 2 46.90 2.30 7 7 3 3.20 0.80 7 7 3 3.50 0.90 7 -7 3 1.90 0.60 7 7 4 10.00 1.20 7 7 4 9.60 0.90 7 -7 4 8.90 1.00 7 7 5 2.70 0.80 7 7 5 4.00 0.70 7 -7 5 3.10 0.70 -7 7 -6 12.70 1.30 7 7 6 11.90 1.00 7 -7 6 13.50 1.00 7 -7 7 19.70 1.20 -7 -8 8 18.30 1.00 -7 -8 7 0.20 0.30 -7 -8 6 9.50 0.80 -7 -8 5 4.60 0.70 -7 -8 5 6.70 1.10 -7 -8 4 0.10 0.60 7 8 -3 131.79 5.50 -7 -8 3 133.39 5.20 7 8 -2 60.79 3.00 -7 -8 2 62.29 2.70 7 8 -1 0.10 0.60 -7 -8 1 0.40 0.50 7 -8 -1 0.60 0.60 7 8 0 204.68 8.30 7 -8 0 213.98 8.00 -7 -8 0 213.88 8.10 7 8 1 21.30 1.30 7 8 1 23.50 1.50 7 -8 1 21.20 1.40 -7 -8 -1 24.00 1.40 7 8 2 0.10 0.70 7 8 2 0.20 0.40 -7 -8 -2 0.40 0.40 7 -8 2 1.00 0.50 7 8 3 10.20 1.10 7 8 3 10.10 0.80 7 -8 3 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2273.87 77.89 8 2 2 3196.78 110.39 8 2 2 3101.09 110.49 8 2 2 2969.40 110.49 8 -2 2 3066.39 110.39 8 -2 2 2957.20 110.39 8 -2 2 3033.80 110.39 8 2 3 47.60 2.90 8 2 3 49.60 2.80 8 2 3 55.89 2.70 8 -2 3 52.09 2.60 8 -2 3 51.49 2.70 8 -2 3 53.89 2.60 8 2 4 284.57 11.40 8 2 4 294.07 11.50 8 2 4 300.07 11.40 8 -2 4 300.67 11.40 8 -2 4 293.47 11.40 8 -2 4 299.67 11.30 8 -2 4 303.77 11.50 8 2 5 2.40 1.00 8 -2 5 0.60 1.00 8 -2 5 -0.30 1.00 8 2 6 30.70 2.00 8 2 6 31.40 2.10 8 2 6 26.10 2.20 8 -2 6 31.70 2.00 8 -2 6 28.90 2.00 8 -2 6 29.60 1.90 8 -2 6 32.60 2.20 8 2 7 5.20 1.40 8 2 7 6.40 1.10 8 2 7 6.40 1.30 8 -2 7 5.50 1.30 8 -2 7 4.40 1.30 8 -2 7 3.90 1.10 8 -2 7 4.20 1.20 8 2 8 88.39 4.10 8 2 8 92.49 4.00 8 -2 8 90.39 4.00 8 -2 8 85.09 4.00 8 -2 8 89.79 4.10 8 2 9 22.40 2.10 8 2 9 16.80 1.50 8 -2 9 19.60 1.80 8 -2 9 16.10 1.60 8 -2 9 18.40 1.40 8 2 10 107.59 4.60 8 -2 10 114.29 4.60 8 -2 10 114.29 4.70 8 -2 10 113.69 4.80 8 2 11 2.30 0.80 8 2 11 1.00 0.40 -8 2 -11 1.10 0.60 8 -2 11 0.20 0.50 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187.38 7.20 -8 4 9 164.08 7.20 8 -4 -9 168.38 7.10 8 -4 -9 173.98 7.00 -8 -4 9 178.68 7.10 8 4 -8 55.19 2.90 -8 4 8 53.69 2.80 8 4 -8 50.59 3.10 8 -4 -8 42.60 2.90 8 -4 -8 52.39 2.70 8 4 -7 81.99 3.90 -8 4 7 83.59 3.80 8 -4 -7 72.39 3.90 8 -4 -7 81.89 3.80 8 4 -6 15.60 1.50 -8 4 6 16.90 1.40 8 -4 -6 15.70 2.00 8 -4 -6 14.30 1.50 8 4 -5 12.00 1.30 -8 4 5 14.50 1.20 8 4 -5 11.70 1.30 8 -4 -5 10.70 1.30 8 -4 -5 10.30 1.80 8 4 -4 13.50 1.30 8 4 -4 14.10 1.30 -8 4 4 15.20 1.20 8 -4 -4 14.30 1.40 8 -4 -4 16.40 1.90 8 4 -3 97.29 4.40 8 4 -3 99.59 4.30 -8 4 3 107.69 4.30 8 -4 -3 97.29 4.20 8 -4 -3 90.89 4.30 -8 4 2 39.10 2.20 8 4 -2 36.80 2.40 8 4 -2 41.90 2.20 8 4 -2 43.10 2.40 8 -4 -2 36.90 2.40 8 -4 -2 43.50 2.20 8 4 -1 143.89 5.90 8 4 -1 134.69 5.80 8 4 -1 145.89 5.70 8 -4 -1 135.49 5.70 8 -4 -1 131.29 5.80 8 -4 -1 142.69 5.70 8 4 0 128.79 5.20 8 4 0 117.19 5.10 8 4 0 118.89 5.00 8 -4 0 119.89 5.00 8 -4 0 115.39 5.10 8 -4 0 116.59 5.10 8 4 1 918.81 33.60 8 4 1 907.91 33.50 8 4 1 948.61 33.50 8 -4 1 895.61 33.40 8 -4 1 873.21 33.40 8 -4 1 917.51 33.40 8 4 2 96.79 4.20 8 4 2 87.69 4.60 8 -4 2 93.39 4.60 8 -4 2 95.59 4.20 8 -4 2 95.09 4.10 8 4 3 46.40 2.60 8 4 3 48.50 2.50 8 4 3 48.70 2.60 8 -4 3 46.20 2.40 8 -4 3 49.10 2.60 8 -4 3 45.70 2.50 8 4 4 0.30 0.60 8 4 4 0.20 0.60 8 4 4 0.80 0.60 8 -4 4 -0.20 0.60 8 -4 4 -0.40 0.60 8 4 5 12.50 1.30 8 4 5 10.90 1.40 8 4 5 12.00 1.40 8 -4 5 11.90 1.30 8 -4 5 12.90 1.30 8 -4 5 11.40 1.30 8 4 6 8.60 1.30 8 4 6 6.80 1.10 8 -4 6 6.30 1.10 8 -4 6 6.80 1.60 8 -4 6 8.10 1.10 8 4 7 189.18 7.50 8 4 7 182.98 7.50 8 -4 7 191.38 7.50 8 -4 7 188.28 7.50 8 -4 7 197.08 7.40 8 -4 7 172.28 7.40 8 4 8 24.90 1.60 8 4 8 25.90 1.60 8 -4 8 25.80 1.60 8 -4 8 21.80 1.70 8 -4 8 23.50 2.10 8 4 9 11.20 1.10 8 4 9 11.50 1.00 8 -4 9 11.00 1.10 8 -4 9 7.30 1.20 8 -4 9 9.90 1.00 -8 4 -10 12.40 1.00 8 4 10 11.30 0.90 8 4 10 10.90 0.90 8 -4 10 11.60 1.00 8 -4 10 11.90 1.00 -8 -5 13 101.89 4.10 8 -5 -13 106.19 4.10 8 5 -12 51.19 2.70 -8 5 12 57.39 2.70 8 -5 -12 57.39 2.50 -8 -5 12 56.79 2.50 8 5 -11 0.90 1.00 -8 5 11 0.10 0.60 8 -5 -11 0.60 0.50 -8 -5 11 -0.50 0.50 -8 5 10 67.59 3.20 -8 -5 10 62.09 3.00 8 -5 -10 62.69 2.90 -8 5 9 41.10 2.40 -8 -5 9 47.20 2.40 8 -5 -9 45.00 2.30 8 5 -8 61.89 3.40 -8 5 8 61.49 3.10 8 -5 -8 68.59 3.20 8 5 -7 247.88 10.00 -8 5 7 242.68 9.80 8 -5 -7 254.77 9.70 8 5 -6 52.99 2.90 -8 5 6 55.39 2.80 8 -5 -6 52.49 2.70 8 5 -5 96.49 4.20 -8 5 5 104.29 4.40 8 5 -5 102.19 4.50 8 -5 -5 88.79 4.40 8 -5 -5 94.89 4.20 -8 5 4 239.08 9.00 8 5 -4 226.48 9.00 8 5 -4 235.78 9.30 8 -5 -4 206.38 8.90 8 -5 -4 236.48 9.00 8 5 -3 315.47 12.00 -8 5 3 333.17 12.10 8 5 -3 323.27 12.30 8 -5 -3 326.07 12.00 8 -5 -3 271.47 12.00 8 5 -2 23.00 1.70 8 5 -2 26.00 1.80 -8 5 2 26.40 1.80 8 -5 -2 23.30 1.70 8 -5 -2 22.40 2.10 8 5 -1 28.80 2.00 8 5 -1 32.20 1.90 8 5 -1 28.90 1.90 8 -5 -1 27.20 2.10 8 -5 -1 28.30 1.80 8 5 0 12.20 1.30 8 5 0 11.40 1.20 8 5 0 11.40 1.40 8 -5 0 11.60 1.50 8 -5 0 13.60 1.30 8 -5 0 14.20 1.50 8 5 1 34.50 2.20 8 5 1 37.50 2.10 8 5 1 38.50 2.20 8 -5 1 35.10 2.10 8 -5 1 36.70 2.20 8 -5 1 37.40 2.20 8 5 2 740.13 26.80 8 5 2 708.33 26.60 8 5 2 697.23 26.60 8 -5 2 714.53 26.50 8 -5 2 722.93 26.60 8 -5 2 726.63 26.60 8 5 3 18.80 1.50 8 5 3 18.00 1.50 8 5 3 16.80 1.50 8 -5 3 18.50 1.60 8 -5 3 21.20 1.60 8 -5 3 21.00 1.80 8 5 4 39.30 2.30 8 5 4 40.00 2.20 8 -5 4 41.20 2.30 8 -5 4 39.30 2.30 8 -5 4 38.50 2.30 8 5 5 5.30 1.00 8 5 5 7.20 1.10 8 5 5 7.20 1.20 8 -5 5 6.30 1.00 8 -5 5 4.10 1.10 8 -5 5 6.60 1.10 8 5 6 108.59 5.00 8 5 6 120.49 5.20 8 5 6 101.59 4.90 8 -5 6 133.99 5.70 8 -5 6 113.79 5.60 8 -5 6 111.29 4.70 8 5 7 23.80 1.50 8 5 7 23.20 1.50 8 -5 7 25.10 1.50 8 -5 7 23.30 1.80 8 5 8 0.00 0.40 8 5 8 0.30 0.40 8 -5 8 0.40 0.50 8 -5 8 0.00 0.70 8 5 9 6.40 0.80 8 5 9 6.70 0.70 8 -5 9 6.30 0.80 -8 5 -10 2.00 0.70 8 5 10 0.70 0.40 8 -5 10 0.60 0.40 -8 -6 12 4.90 0.70 8 -6 -12 4.70 0.80 -8 6 11 16.30 1.30 -8 -6 11 18.40 1.10 8 -6 -11 18.30 1.10 -8 6 10 11.50 1.10 8 -6 -10 14.00 1.00 -8 -6 10 11.80 1.00 -8 6 9 38.40 2.20 8 -6 -9 37.40 1.90 -8 -6 9 38.70 2.00 -8 6 8 19.60 1.50 8 -6 -8 20.90 1.40 -8 -6 8 21.00 1.40 8 6 -7 130.89 5.90 -8 6 7 132.39 5.80 8 -6 -7 150.28 5.60 8 6 -6 6.70 1.40 -8 6 6 10.10 1.10 8 -6 -6 7.70 1.10 8 6 -5 22.40 1.70 -8 6 5 20.40 1.50 -8 -6 5 18.30 1.80 8 -6 -5 22.20 1.60 -8 6 4 5.00 1.10 8 6 -4 4.00 1.10 8 6 -4 4.10 1.00 8 -6 -4 6.50 1.10 -8 -6 4 5.70 1.50 -8 6 3 248.78 9.60 8 6 -3 252.37 9.60 8 6 -3 225.78 9.80 8 -6 -3 250.57 9.50 8 6 -2 218.78 9.60 8 6 -2 241.08 9.90 8 -6 -2 245.18 9.40 8 -6 -2 240.68 9.30 8 -6 -2 250.77 9.30 8 6 -1 246.78 9.60 8 6 -1 216.68 9.30 8 -6 -1 232.68 8.90 8 -6 -1 230.28 9.00 8 -6 -1 226.88 9.00 8 6 0 36.00 2.30 8 6 0 35.80 2.10 8 -6 0 37.70 2.20 8 -6 0 39.80 2.30 8 -6 0 36.70 2.20 8 6 1 521.75 19.70 8 6 1 486.25 20.00 8 6 1 544.75 19.80 8 -6 1 528.85 19.60 8 -6 1 539.95 19.70 8 -6 1 547.15 19.70 8 6 2 2.00 0.70 8 6 2 2.60 0.90 8 6 2 2.70 0.80 8 -6 2 4.20 1.30 8 -6 2 5.00 1.30 8 -6 2 3.00 0.80 8 6 3 73.59 3.40 8 6 3 75.89 3.40 8 6 3 69.69 3.60 8 -6 3 80.39 3.50 8 -6 3 75.29 3.40 8 -6 3 74.09 3.40 8 6 4 2.30 0.80 8 6 4 1.40 0.60 8 -6 4 1.70 0.50 8 -6 4 4.10 1.20 8 -6 4 3.30 1.00 8 6 5 11.50 1.00 8 6 5 9.00 1.00 8 6 5 11.00 1.30 8 -6 5 10.20 1.10 8 -6 5 13.20 1.40 8 6 6 0.70 0.40 8 6 6 -0.20 0.40 8 6 6 1.80 1.10 8 -6 6 0.60 0.50 8 6 7 -0.50 0.40 8 6 7 0.50 0.40 8 -6 7 0.00 0.40 -8 6 -8 11.90 0.90 8 6 8 10.30 0.80 8 6 8 10.30 0.90 8 -6 8 11.80 0.90 -8 -7 10 16.40 1.00 -8 7 9 2.70 1.00 8 -7 -9 1.50 0.70 -8 -7 9 2.70 0.60 -8 7 8 1.00 0.70 -8 -7 8 2.10 0.70 8 -7 -8 0.90 0.90 -8 7 7 55.99 2.70 8 -7 -7 53.39 2.50 -8 -7 7 54.29 2.50 8 7 -6 141.29 5.80 -8 7 6 121.89 5.90 8 -7 -6 137.69 5.30 -8 7 5 52.69 2.60 8 7 -5 49.00 2.70 -8 -7 5 54.89 2.60 8 -7 -5 49.20 2.50 -8 7 4 24.70 1.90 8 7 -4 27.10 1.80 -8 -7 4 24.90 1.70 8 -7 -4 25.00 1.70 8 7 -3 136.69 6.10 8 -7 -3 140.49 5.70 -8 -7 3 150.38 5.80 8 7 -2 3.90 1.00 8 7 -2 5.70 1.00 -8 -7 2 2.90 0.70 8 -7 -2 3.50 0.90 8 -7 -2 3.00 0.90 8 7 -1 136.49 5.60 8 7 -1 129.39 5.70 8 -7 -1 136.29 5.40 8 7 0 47.60 2.30 8 7 0 45.10 2.50 8 -7 0 47.00 2.40 8 7 1 0.20 0.40 8 7 1 0.60 0.60 8 -7 1 0.60 0.60 8 7 2 2.60 0.90 8 7 2 2.20 0.70 8 -7 2 2.80 1.00 8 7 3 19.60 1.70 8 7 3 17.20 1.20 8 -7 3 21.20 1.30 8 7 4 3.20 0.70 8 7 4 5.10 1.10 8 -7 4 5.80 0.80 8 7 5 1.00 0.90 8 -7 5 1.30 0.80 8 7 6 0.70 0.40 8 -7 6 0.60 0.40 -8 -8 7 1.80 0.50 -8 -8 6 2.60 0.60 -8 -8 5 25.80 1.40 -8 -8 4 9.70 1.20 8 8 -3 4.90 1.30 -8 -8 3 6.30 1.00 8 8 -2 18.00 1.50 -8 -8 2 20.30 1.30 8 8 -1 1.30 0.80 -8 -8 1 0.50 0.50 8 8 0 4.30 1.00 -8 -8 0 3.00 0.80 8 -8 0 1.90 0.70 8 8 1 24.80 1.60 8 8 1 22.60 1.30 -8 -8 -1 24.50 1.30 8 -8 1 23.20 1.40 8 8 2 0.10 0.70 8 8 2 -0.50 0.40 8 -8 2 -0.70 0.50 -8 -8 -2 0.60 0.70 -8 -8 -3 0.50 0.40 8 -8 4 9.60 0.90 -8 -8 -4 11.00 0.80 9 0 -16 4.40 0.80 9 0 -15 0.50 0.50 9 0 -14 1.00 0.70 9 0 -14 0.60 0.60 9 0 -13 0.20 0.70 -9 0 13 0.00 1.10 -9 0 12 339.47 13.50 9 0 -12 359.66 13.50 9 0 -12 349.57 13.20 9 0 -11 1.00 0.90 9 0 -11 0.40 0.70 9 0 -10 135.29 5.70 9 0 -10 141.79 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1 952.70 34.90 9 -3 1 947.71 34.90 9 -3 1 907.31 34.90 9 3 2 1016.10 36.00 9 3 2 962.50 35.90 9 3 2 993.90 35.90 9 -3 2 966.30 35.90 9 -3 2 954.50 35.80 9 -3 2 968.90 35.90 9 3 3 177.68 7.10 9 3 3 178.78 7.30 9 3 3 175.58 7.00 9 -3 3 168.38 7.00 9 -3 3 162.88 6.90 9 3 4 42.80 2.50 9 3 4 43.50 2.50 9 3 4 42.30 2.40 9 -3 4 43.10 2.60 9 -3 4 43.40 2.40 9 -3 4 44.00 2.50 9 3 5 8.70 1.40 9 3 5 10.30 1.30 9 -3 5 8.80 1.40 9 -3 5 10.20 1.30 9 -3 5 9.70 1.40 9 3 6 162.28 6.70 9 3 6 167.48 6.70 9 -3 6 161.18 6.70 9 -3 6 158.78 6.60 9 -3 6 164.48 6.80 9 -3 6 158.78 6.60 9 3 7 44.60 2.50 9 3 7 44.50 2.40 9 -3 7 44.20 2.40 9 -3 7 42.80 2.60 9 -3 7 48.00 2.70 9 -3 7 43.20 2.40 9 3 8 156.88 6.30 9 3 8 147.39 6.20 9 -3 8 156.68 6.10 9 -3 8 143.89 6.10 9 -3 8 157.48 6.30 9 3 9 110.09 4.50 9 3 9 102.99 4.40 9 -3 9 106.69 4.50 9 -3 9 99.49 4.30 9 -3 9 108.19 4.30 -9 3 -10 4.70 0.90 9 3 10 5.70 0.80 9 3 10 5.10 0.70 9 -3 10 6.20 1.00 9 -3 10 5.70 0.80 9 -3 10 5.20 0.80 -9 3 -11 5.00 1.30 9 3 11 6.10 0.60 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9 4 8 1.60 0.50 9 4 8 1.10 0.60 9 -4 8 0.80 0.50 9 4 9 16.40 1.10 9 4 9 17.20 1.10 9 -4 9 16.50 1.10 9 -4 9 16.30 1.10 9 4 10 2.40 0.60 9 4 10 1.60 0.40 -9 4 -10 2.40 0.70 -9 -5 13 5.50 1.00 9 -5 -13 6.70 0.70 -9 5 12 125.89 5.00 9 -5 -12 117.49 4.80 -9 -5 12 120.59 4.80 -9 5 11 20.60 1.50 -9 -5 11 22.80 1.40 9 -5 -11 20.60 1.30 -9 5 10 45.90 2.50 9 -5 -10 45.90 2.30 -9 -5 10 48.10 2.30 -9 5 9 54.39 3.00 9 5 -9 56.79 3.30 9 -5 -9 69.89 3.10 -9 -5 9 63.79 2.90 9 5 -8 72.49 3.70 -9 5 8 69.69 3.50 9 -5 -8 79.19 3.70 -9 5 7 75.09 3.60 9 5 -7 77.29 3.80 9 -5 -7 75.99 3.90 -9 5 6 17.40 1.40 9 5 -6 18.10 1.60 9 -5 -6 20.80 2.00 9 5 -5 7.80 1.10 -9 5 5 7.40 1.10 9 -5 -5 5.50 1.60 9 -5 -5 5.10 1.10 9 5 -4 39.80 2.40 -9 5 4 38.10 2.10 9 5 -4 37.80 2.10 9 -5 -4 36.40 2.40 9 -5 -4 37.60 2.10 -9 5 3 3.20 0.90 9 5 -3 2.80 0.90 9 -5 -3 3.50 1.10 9 -5 -3 4.20 1.40 9 5 -2 0.20 0.60 9 5 -2 0.50 0.60 9 -5 -2 0.30 0.70 9 -5 -2 0.70 0.80 9 5 -1 21.30 1.70 9 5 -1 22.20 1.70 9 5 -1 21.10 1.50 9 -5 -1 17.90 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1.20 9 -7 3 21.80 1.30 9 7 4 7.40 1.20 9 7 4 5.50 0.70 9 -7 4 6.80 0.90 9 7 5 32.80 1.50 9 -7 5 33.20 1.60 9 -7 6 12.80 0.90 -9 -8 7 0.60 0.30 -9 -8 6 11.50 0.80 -9 -8 5 5.40 0.70 -9 -8 3 29.50 1.70 9 8 -2 80.69 3.60 -9 -8 2 85.09 3.40 9 8 -1 9.30 1.20 -9 -8 1 9.50 1.10 9 8 0 28.20 1.70 -9 -8 0 29.40 1.60 -9 -8 -1 45.70 2.00 -9 -8 -2 6.10 0.80 -9 -8 -3 1.80 0.60 10 0 -15 -0.40 0.50 10 0 -14 1.10 0.60 10 0 -13 0.20 0.70 -10 0 13 -0.50 1.00 10 0 -13 0.20 0.70 -10 0 12 65.69 3.40 10 0 -12 65.99 3.20 10 0 -12 74.79 3.40 10 0 -11 -0.20 0.90 10 0 -10 2898.71 104.29 10 0 -10 2854.01 104.09 10 0 -9 1.20 0.90 10 0 -9 0.10 0.80 10 0 -8 25.50 2.10 10 0 -8 26.20 1.90 10 0 -8 23.90 2.00 10 0 -7 0.80 0.90 10 0 -7 -0.20 1.00 10 0 -7 -0.60 0.60 10 0 -6 2.50 1.20 10 0 -6 1.60 1.00 10 0 -6 2.90 0.80 10 0 -5 -1.20 1.00 10 0 -5 0.70 0.70 10 0 -4 206.88 7.90 10 0 -4 183.78 7.70 10 0 -3 1.10 0.60 10 0 -2 552.94 20.60 -10 0 2 549.85 21.40 10 0 -1 0.80 0.70 -10 0 1 2.20 1.10 10 0 0 4.90 1.60 10 0 0 3.10 1.20 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44.60 2.50 10 1 1 35.20 2.60 10 1 1 34.80 2.50 10 1 1 37.60 2.30 10 -1 1 33.90 2.60 10 -1 1 39.30 2.10 10 -1 1 39.30 2.20 10 1 2 1087.69 40.10 10 1 2 1098.29 40.30 10 1 2 1111.49 40.20 10 -1 2 1088.59 40.20 10 -1 2 1121.89 40.10 10 -1 2 1083.09 40.20 10 1 3 9.20 1.50 10 1 3 12.10 1.60 10 1 3 10.80 1.70 10 -1 3 11.80 1.60 10 -1 3 12.10 1.30 10 -1 3 9.80 1.50 10 1 4 499.75 18.80 10 1 4 508.15 18.90 10 1 4 479.15 18.80 10 -1 4 504.45 18.80 10 -1 4 500.35 18.90 10 -1 4 511.65 18.80 10 -1 4 505.65 18.80 10 1 5 4.50 1.20 10 1 5 3.20 0.90 10 1 5 3.10 0.80 10 -1 5 5.30 1.20 10 -1 5 4.30 1.40 10 -1 5 4.90 1.40 10 -1 5 3.70 1.10 10 1 6 134.49 5.60 10 1 6 127.79 5.40 10 1 6 128.09 5.50 10 -1 6 133.69 5.80 10 -1 6 130.79 5.50 10 -1 6 133.69 5.70 10 -1 6 126.29 5.50 10 1 7 24.10 1.70 10 1 7 27.20 1.80 10 1 7 25.80 1.80 10 -1 7 24.10 1.80 10 -1 7 26.60 2.00 10 -1 7 24.10 1.70 10 1 8 1.20 0.50 10 1 8 1.40 0.70 10 -1 8 1.60 0.70 10 -1 8 1.00 0.60 10 1 9 1.10 0.50 10 1 9 1.30 0.60 10 -1 9 -0.30 0.50 10 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75.49 3.80 10 2 -5 75.79 4.10 10 2 -5 86.19 3.80 10 -2 -5 83.79 3.60 10 -2 -5 80.89 3.70 10 2 -4 70.09 3.40 10 2 -4 71.89 3.40 10 -2 -4 66.49 3.20 10 -2 -4 69.49 3.30 10 2 -3 14.60 1.30 10 2 -3 13.70 1.80 10 -2 -3 10.90 1.60 10 -2 -3 13.20 1.40 10 2 -2 6.70 1.00 10 -2 -2 4.70 1.30 10 -2 -2 5.40 1.20 10 2 -1 71.59 3.40 10 2 -1 75.69 3.40 -10 -2 1 64.99 4.80 10 -2 -1 75.49 3.40 10 -2 -1 72.59 3.30 10 2 0 103.09 5.00 10 2 0 114.29 4.80 10 2 0 120.19 4.90 10 -2 0 116.29 4.70 10 -2 0 108.09 4.80 10 2 1 52.39 2.70 10 2 1 51.69 2.70 10 2 1 46.90 2.90 10 -2 1 52.89 2.70 10 -2 1 52.29 2.60 10 2 2 1.80 0.80 10 2 2 -0.30 0.70 10 2 2 0.50 0.80 10 -2 2 -0.10 0.60 10 -2 2 -0.20 0.60 10 -2 2 -1.40 0.90 10 2 3 324.37 13.90 10 2 3 359.26 13.50 10 -2 3 353.76 13.30 10 -2 3 366.26 13.40 10 2 4 507.15 18.80 10 2 4 492.25 18.90 10 -2 4 498.95 18.80 10 -2 4 508.35 18.80 10 -2 4 503.45 18.90 10 2 5 4.80 1.10 10 2 5 6.80 1.30 10 2 5 6.00 1.20 10 -2 5 3.00 1.10 10 -2 5 4.70 1.30 10 -2 5 3.20 1.10 10 -2 5 4.20 1.20 10 2 6 36.60 2.10 10 2 6 34.70 2.30 10 2 6 38.50 2.30 10 -2 6 34.10 2.30 10 -2 6 37.30 2.20 10 -2 6 37.50 2.20 10 -2 6 37.10 2.10 10 2 7 20.00 1.60 10 2 7 19.30 2.20 10 2 7 16.70 1.40 10 -2 7 20.20 1.40 10 -2 7 16.40 1.50 10 -2 7 14.20 1.90 10 -2 7 19.80 2.00 10 2 8 0.30 0.60 10 2 8 0.10 0.50 10 -2 8 0.10 0.60 10 -2 8 0.70 0.70 10 -2 8 0.20 0.50 10 2 9 0.50 0.50 10 2 9 0.80 0.50 10 -2 9 -1.00 0.60 10 -2 9 0.20 0.50 10 -2 9 -0.50 0.80 10 2 10 7.50 0.80 10 2 10 6.70 0.70 -10 2 -10 6.00 1.10 -10 -2 -10 6.60 1.10 10 -2 10 7.80 1.00 10 -2 10 7.00 0.80 10 -2 10 6.70 0.80 10 3 -15 2.70 0.80 10 -3 -15 3.30 0.60 10 3 -14 1.70 0.50 10 3 -13 45.30 2.20 -10 3 13 46.10 2.30 10 -3 -13 41.80 2.30 10 -3 -13 42.90 2.10 10 3 -12 1.40 0.70 -10 3 12 -0.20 0.60 10 -3 -12 0.30 0.50 10 -3 -12 0.10 0.70 -10 -3 12 0.30 0.90 10 3 -11 34.60 2.20 -10 3 11 34.00 2.10 10 -3 -11 37.50 2.00 10 -3 -11 37.90 2.20 10 3 -10 79.99 4.10 10 3 -10 91.39 4.00 -10 3 10 81.79 4.00 10 -3 -10 84.79 3.90 -10 -3 10 87.19 3.90 10 -3 -10 83.39 3.80 10 3 -9 120.99 5.60 -10 3 9 123.09 5.50 10 3 -9 130.79 5.50 -10 -3 9 128.79 5.40 10 -3 -9 125.49 5.30 10 -3 -9 130.19 5.40 10 3 -8 0.90 0.80 10 3 -8 -0.30 1.00 -10 3 8 0.40 0.70 10 -3 -8 0.30 0.80 10 -3 -8 0.90 0.60 10 3 -7 52.69 2.90 10 3 -7 50.99 3.40 -10 3 7 51.79 2.80 10 -3 -7 49.40 2.80 10 -3 -7 50.69 2.60 10 3 -6 11.30 1.30 -10 3 6 11.50 1.30 10 3 -6 13.40 1.50 10 -3 -6 11.40 1.30 10 -3 -6 11.00 2.40 10 3 -5 38.90 2.30 10 3 -5 39.20 2.20 -10 3 5 37.50 2.20 10 -3 -5 38.00 2.30 10 -3 -5 37.50 2.10 10 3 -4 55.39 2.80 -10 3 4 56.29 2.80 10 3 -4 54.69 2.90 10 -3 -4 58.19 2.80 10 -3 -4 56.29 2.90 10 3 -3 85.49 3.90 -10 3 3 87.69 3.80 10 3 -3 84.89 3.70 10 -3 -3 82.49 3.80 10 -3 -3 80.09 3.70 10 3 -2 93.09 4.00 10 3 -2 90.89 4.10 -10 3 2 84.49 3.90 10 -3 -2 90.39 4.00 10 -3 -2 90.29 3.90 10 3 -1 92.59 4.10 10 3 -1 89.89 3.90 10 3 -1 83.09 4.20 10 -3 -1 87.69 3.90 10 -3 -1 87.59 3.80 10 3 0 115.39 4.70 10 3 0 106.99 4.80 10 3 0 109.99 4.80 10 -3 0 109.49 4.60 10 -3 0 110.99 4.70 10 -3 0 105.39 4.80 10 3 1 13.30 1.40 10 3 1 13.30 1.40 10 3 1 15.40 1.60 10 -3 1 15.90 1.40 10 -3 1 15.70 1.70 10 -3 1 14.40 1.70 10 3 2 146.09 5.90 10 3 2 134.59 5.80 10 3 2 141.79 5.80 10 -3 2 139.29 5.80 10 -3 2 128.59 5.70 10 -3 2 141.99 5.80 10 3 3 802.62 29.00 10 3 3 812.32 29.10 10 3 3 779.92 28.90 10 -3 3 764.02 28.90 10 -3 3 770.82 28.90 10 -3 3 766.32 28.80 10 3 4 847.82 31.30 10 3 4 867.81 31.40 10 -3 4 841.32 31.30 10 -3 4 852.91 31.20 10 -3 4 830.02 31.30 10 3 5 5.50 1.30 10 3 5 5.70 1.10 10 -3 5 6.90 1.20 10 -3 5 5.00 1.30 10 -3 5 6.00 1.10 10 3 6 23.50 1.70 10 3 6 23.50 1.60 10 -3 6 21.80 1.60 10 -3 6 22.60 1.60 10 -3 6 24.40 1.80 10 3 7 34.70 2.00 10 3 7 30.30 1.80 10 -3 7 29.50 1.80 10 -3 7 30.50 1.90 10 -3 7 30.00 1.80 10 3 8 2.90 0.90 10 3 8 2.50 0.80 10 -3 8 3.20 0.80 10 -3 8 2.90 0.80 10 3 9 0.00 0.40 10 3 9 0.70 0.70 10 -3 9 0.10 0.50 10 -3 9 0.80 0.60 -10 3 -10 18.10 1.20 10 3 10 17.10 1.00 10 3 10 18.30 1.10 10 -3 10 16.40 1.10 10 -4 -14 3.00 0.50 10 4 -13 29.90 1.60 -10 4 13 24.10 1.70 -10 -4 13 24.50 2.30 10 -4 -13 26.30 1.40 10 4 -12 1.10 0.80 -10 4 12 2.20 0.70 -10 -4 12 0.90 0.60 10 -4 -12 1.50 0.50 -10 4 11 21.80 1.50 10 4 -11 21.80 1.80 10 -4 -11 23.30 1.40 10 -4 -11 16.20 1.80 -10 -4 11 21.80 1.50 10 4 -10 214.48 8.30 10 4 -10 202.88 8.50 -10 4 10 204.08 8.60 10 -4 -10 186.08 8.30 -10 -4 10 233.08 8.40 10 -4 -10 218.18 8.30 10 4 -9 35.40 2.50 -10 4 9 30.40 2.00 10 4 -9 30.00 2.20 10 -4 -9 32.40 2.10 -10 -4 9 29.80 2.00 10 -4 -9 31.20 1.90 10 4 -8 12.40 1.50 -10 4 8 12.30 1.30 10 -4 -8 13.70 1.70 10 -4 -8 13.20 1.90 -10 4 7 81.19 4.80 10 -4 -7 100.69 4.20 10 -4 -7 100.49 4.30 10 4 -6 11.30 1.30 -10 4 6 12.00 1.20 10 -4 -6 13.10 1.30 10 -4 -6 11.40 1.60 10 4 -5 240.38 9.30 -10 4 5 239.28 9.40 10 -4 -5 239.48 9.40 10 -4 -5 237.58 9.30 -10 4 4 22.20 1.60 10 4 -4 21.10 1.60 10 4 -4 20.60 1.70 10 -4 -4 21.50 1.70 10 -4 -4 20.80 1.60 -10 4 3 406.06 15.10 10 4 -3 397.66 15.00 10 4 -3 405.26 15.40 10 -4 -3 381.06 15.10 10 -4 -3 401.96 15.10 10 4 -2 1.30 0.60 10 4 -2 1.30 1.00 10 4 -2 1.90 0.70 10 -4 -2 1.40 0.70 10 4 -1 78.59 3.50 10 4 -1 79.79 3.80 10 4 -1 72.39 3.70 10 -4 -1 80.09 3.60 10 -4 -1 77.79 3.50 10 4 0 24.30 1.60 10 4 0 20.60 1.70 10 4 0 22.10 1.80 10 -4 0 20.90 1.60 10 -4 0 24.70 1.90 10 -4 0 22.80 1.60 10 4 1 29.70 2.00 10 4 1 28.30 1.90 10 4 1 32.30 2.00 10 -4 1 29.10 1.80 10 -4 1 26.80 1.90 10 -4 1 32.20 2.10 10 4 2 1.80 0.80 10 4 2 5.10 1.10 10 4 2 3.10 1.10 10 -4 2 3.90 1.10 10 -4 2 2.40 0.70 10 -4 2 3.00 1.00 10 4 3 28.50 2.00 10 4 3 31.50 2.00 10 4 3 31.10 1.90 10 -4 3 31.90 1.90 10 -4 3 30.40 2.00 10 -4 3 31.70 2.00 10 4 4 181.08 7.00 10 4 4 177.48 7.30 10 4 4 154.08 7.10 10 -4 4 172.48 7.00 10 -4 4 175.68 7.10 10 -4 4 177.98 6.90 10 4 5 93.49 4.20 10 4 5 94.09 4.20 10 -4 5 95.09 4.20 10 -4 5 96.29 4.10 10 -4 5 93.79 4.20 10 4 6 30.90 1.80 10 4 6 30.60 1.80 10 -4 6 32.20 1.90 10 -4 6 30.50 1.80 10 -4 6 28.10 1.70 10 4 7 38.30 2.10 10 4 7 36.80 1.90 10 -4 7 38.10 2.10 10 -4 7 38.60 1.90 10 4 8 2.30 0.70 10 4 8 2.40 0.70 10 -4 8 2.10 0.50 10 4 9 16.20 1.10 10 4 9 16.90 1.00 10 -4 9 16.20 1.20 10 -4 9 15.00 1.00 10 -5 -13 0.80 0.40 -10 5 12 28.60 1.70 -10 -5 12 29.60 1.50 10 -5 -12 30.30 1.50 -10 5 11 4.90 0.90 10 -5 -11 5.00 0.70 -10 -5 11 5.50 0.90 -10 5 10 12.40 1.20 10 -5 -10 13.20 1.10 -10 -5 10 11.30 1.10 10 5 -9 2.80 1.20 -10 5 9 3.80 0.90 -10 -5 9 1.20 0.50 10 -5 -9 1.90 0.50 10 5 -8 1.00 0.90 -10 5 8 -0.40 0.70 10 -5 -8 0.00 0.50 10 5 -7 3.10 1.20 -10 5 7 2.40 0.90 10 -5 -7 3.50 0.90 10 -5 -7 5.30 1.50 -10 5 6 0.70 0.60 10 5 -6 0.50 0.80 10 -5 -6 0.20 0.90 10 -5 -6 -0.30 0.60 -10 5 5 10.50 1.20 10 5 -5 12.20 1.30 10 5 -5 12.90 1.20 10 -5 -5 10.90 1.60 10 -5 -5 13.70 1.20 -10 5 4 39.50 2.20 10 5 -4 35.10 2.30 10 5 -4 35.10 2.10 10 -5 -4 37.30 2.10 10 -5 -4 39.30 2.30 10 5 -3 12.80 1.30 -10 5 3 10.70 2.00 10 5 -3 13.80 1.30 10 -5 -3 12.40 1.30 10 -5 -3 13.60 1.50 10 5 -2 32.50 2.10 10 5 -2 35.60 2.00 10 -5 -2 36.60 2.00 10 -5 -2 33.70 2.10 10 5 -1 24.10 1.60 10 5 -1 22.90 1.70 10 5 -1 23.50 1.80 10 -5 -1 25.80 1.70 10 -5 -1 25.90 1.70 10 5 0 54.49 2.70 10 5 0 50.69 2.90 10 5 0 54.19 2.70 10 -5 0 52.89 2.80 10 -5 0 52.39 2.70 10 -5 0 55.29 2.70 10 5 1 0.20 0.70 10 5 1 -0.40 0.50 10 5 1 -0.40 0.60 10 -5 1 0.50 0.60 10 -5 1 0.00 0.60 10 -5 1 -1.30 0.70 10 5 2 -0.10 0.50 10 5 2 -0.10 0.60 10 5 2 0.70 0.70 10 -5 2 0.30 0.60 10 -5 2 0.30 0.60 10 -5 2 1.30 0.60 10 5 3 301.67 11.50 10 5 3 276.17 11.60 10 5 3 298.27 11.50 10 -5 3 296.07 11.50 10 -5 3 306.67 11.40 10 -5 3 314.67 11.60 10 5 4 0.20 0.90 10 5 4 1.60 0.50 10 -5 4 1.00 0.80 10 -5 4 0.50 0.60 10 -5 4 1.30 0.90 10 5 5 0.60 0.50 10 5 5 0.30 0.40 10 -5 5 0.70 0.50 10 -5 5 0.70 0.60 10 -5 5 0.50 0.50 10 5 6 2.50 0.80 10 5 6 1.80 0.50 10 -5 6 3.70 0.90 10 -5 6 2.50 0.60 10 5 7 9.70 0.90 10 5 7 9.40 0.80 10 -5 7 9.90 0.90 10 -5 7 9.10 0.90 10 5 8 0.00 0.30 10 5 8 0.10 0.40 10 -5 8 0.60 0.40 10 -5 8 1.00 0.60 -10 -6 11 31.90 1.50 10 -6 -11 31.90 1.50 -10 6 10 -0.80 0.70 -10 -6 10 0.20 0.40 10 -6 -10 0.10 0.40 -10 6 9 6.40 1.00 -10 -6 9 9.20 0.90 10 -6 -9 9.30 0.90 10 6 -8 123.19 5.40 -10 6 8 127.89 5.30 10 -6 -8 125.49 5.00 -10 -6 8 123.59 5.10 -10 6 7 7.70 1.10 10 6 -7 8.90 1.40 10 -6 -7 7.80 1.00 -10 6 6 3.80 1.00 10 6 -6 2.70 0.80 10 -6 -6 3.90 0.80 10 6 -5 15.20 1.50 -10 6 5 17.60 1.50 10 -6 -5 19.00 1.30 10 6 -4 1.90 0.50 10 6 -4 1.50 0.70 -10 6 4 1.20 1.10 10 -6 -4 1.10 0.50 10 -6 -4 1.70 1.00 10 6 -3 1.80 0.50 10 6 -3 2.80 1.00 10 -6 -3 2.30 0.90 10 -6 -3 1.50 0.60 10 6 -2 0.40 0.60 10 6 -2 0.20 0.50 10 -6 -2 -1.00 0.50 10 -6 -2 1.20 0.70 10 6 -1 39.30 2.00 10 6 -1 33.70 2.20 10 -6 -1 36.00 2.10 10 -6 -1 39.50 2.00 10 6 0 16.70 1.30 10 6 0 16.00 1.50 10 -6 0 17.20 1.50 10 -6 0 15.40 1.60 10 -6 0 15.10 1.30 10 6 1 3.80 1.00 10 -6 1 4.80 1.00 10 -6 1 4.40 0.70 10 -6 1 4.60 1.20 10 6 2 5.90 1.10 10 6 2 5.90 1.00 10 6 2 6.40 0.80 10 -6 2 7.70 1.00 10 -6 2 4.40 1.10 10 -6 2 5.20 1.10 10 6 3 21.50 1.60 10 6 3 22.80 1.40 10 6 3 22.90 1.40 10 -6 3 22.10 1.40 10 -6 3 23.50 1.50 10 -6 3 22.00 1.40 10 6 4 65.69 3.20 10 6 4 63.29 2.90 10 6 4 67.79 3.10 10 -6 4 67.39 3.00 10 -6 4 64.19 3.00 10 -6 4 65.29 2.80 10 6 5 7.10 1.00 10 6 5 5.90 0.70 10 -6 5 5.30 0.90 10 -6 5 3.50 0.80 10 6 6 6.70 0.70 10 6 6 6.80 0.70 10 6 7 1.90 0.50 10 -6 7 0.30 0.40 -10 -7 9 -0.30 0.40 -10 -7 8 1.10 0.40 10 -7 -8 0.70 0.50 -10 7 7 0.10 1.10 10 -7 -7 3.60 1.00 -10 -7 7 2.60 0.60 10 7 -6 67.99 3.30 10 -7 -6 64.69 2.80 10 7 -5 16.40 1.50 10 -7 -5 15.10 1.10 10 7 -4 28.40 1.90 10 -7 -4 28.50 1.60 10 7 -3 1.20 1.00 10 -7 -3 1.30 0.60 -10 -7 3 0.30 0.70 10 7 -2 49.60 2.60 10 7 -2 48.60 2.30 10 -7 -2 49.99 2.30 -10 -7 2 52.59 2.40 10 7 -1 23.90 2.10 10 7 -1 19.80 1.30 10 -7 -1 18.60 1.40 10 7 0 22.60 1.30 10 7 0 22.00 1.50 10 -7 0 19.50 1.60 10 7 1 19.80 1.50 10 7 1 18.40 1.20 10 -7 1 17.60 1.40 10 7 2 1.00 0.40 10 7 2 1.60 0.70 10 -7 2 2.00 1.10 10 7 3 30.90 1.60 10 7 3 33.30 2.10 10 -7 3 36.20 1.70 10 7 4 -0.20 0.30 10 -7 4 0.40 0.50 10 7 5 58.29 2.40 -10 -8 6 16.60 0.90 -10 -8 5 95.89 3.80 -10 -8 1 57.59 2.40 -10 -8 0 10.30 1.00 -10 -8 -1 23.80 1.30 11 0 -14 3.80 0.90 11 0 -13 1.00 0.60 -11 0 13 -1.10 1.00 11 0 -12 123.49 5.20 11 0 -12 135.39 5.50 -11 0 12 125.79 5.50 11 0 -11 0.20 0.80 11 0 -11 1.10 0.80 11 0 -10 721.03 26.40 11 0 -10 695.83 26.10 11 0 -9 1.20 0.90 11 0 -9 -0.40 0.80 11 0 -8 638.94 23.70 11 0 -8 607.54 23.20 11 0 -8 637.04 23.50 11 0 -7 0.80 1.00 11 0 -7 1.10 0.90 11 0 -7 1.90 0.70 11 0 -6 138.79 5.80 11 0 -6 136.79 5.90 11 0 -6 134.69 5.70 11 0 -5 0.90 0.80 11 0 -5 2.20 1.10 11 0 -5 0.10 0.70 11 0 -4 146.19 6.00 11 0 -4 140.99 5.90 11 0 -4 148.79 6.10 11 0 -3 -2.10 1.10 11 0 -3 0.90 0.70 11 0 -3 -0.70 0.80 11 0 -2 1113.39 41.10 11 0 -2 1159.08 41.20 11 0 -2 1096.19 40.90 11 0 -1 0.70 1.00 11 0 -1 -1.50 0.90 11 0 -1 0.40 0.80 11 0 0 11.20 1.80 11 0 0 13.50 1.60 11 0 0 8.90 1.70 11 0 2 37.20 2.40 11 0 2 38.80 2.20 11 0 2 39.80 2.50 11 0 2 39.60 2.60 11 0 3 3.90 1.30 11 0 3 1.50 0.90 11 0 4 418.16 16.20 11 0 4 432.46 16.20 11 0 4 434.26 16.20 11 0 4 438.96 16.40 11 0 5 -0.90 0.70 11 0 5 0.70 0.70 11 0 5 0.50 1.00 11 0 5 1.60 0.70 11 0 6 913.71 33.90 11 0 6 892.91 33.70 11 0 6 947.61 33.70 11 0 7 -0.20 0.60 11 0 7 -0.90 0.60 11 0 7 -1.60 0.70 11 0 8 22.70 1.50 11 0 8 23.80 1.50 11 0 8 23.30 1.60 11 0 9 -0.10 0.50 11 0 9 0.10 0.50 11 0 9 0.10 0.50 11 0 10 47.20 2.10 11 1 -15 1.10 0.50 11 -1 -15 0.70 0.50 -11 1 14 6.10 2.10 11 -1 -14 -0.50 0.60 11 1 -13 18.90 1.60 -11 1 13 14.20 1.80 11 -1 -13 17.90 1.40 -11 -1 13 20.40 1.90 11 -1 -13 17.10 1.30 11 1 -12 29.10 1.90 -11 1 12 26.90 1.90 11 -1 -12 29.10 1.90 11 -1 -12 27.10 1.70 -11 1 11 483.25 19.30 11 1 -11 516.95 19.10 11 -1 -11 519.85 19.20 11 -1 -11 511.55 18.90 11 1 -10 418.06 15.70 11 1 -10 385.36 15.80 11 -1 -10 419.16 16.00 11 -1 -10 420.86 15.50 11 1 -9 9.30 1.70 11 1 -9 8.90 1.40 11 -1 -9 10.20 1.40 11 -1 -9 11.20 1.60 11 1 -8 3187.18 114.79 11 1 -8 3168.58 115.09 11 -1 -8 3175.38 114.79 11 -1 -8 3140.89 114.59 11 1 -7 94.59 4.30 11 1 -7 103.79 4.50 11 -1 -7 83.69 4.60 11 -1 -7 91.39 4.10 11 1 -6 0.20 0.70 11 1 -6 1.20 1.00 11 -1 -6 0.70 0.90 11 -1 -6 1.00 0.80 11 -1 -6 -0.80 0.70 11 1 -5 452.85 17.50 11 1 -5 455.75 17.30 11 -1 -5 476.65 17.50 11 -1 -5 460.95 17.20 11 -1 -5 453.25 17.30 11 1 -4 146.49 6.30 11 1 -4 157.48 6.40 11 -1 -4 151.58 6.10 11 -1 -4 147.49 6.20 11 -1 -4 154.18 6.30 11 1 -3 68.09 3.50 11 1 -3 75.29 3.50 11 -1 -3 70.49 3.30 11 -1 -3 68.19 3.40 11 -1 -3 75.49 3.50 11 1 -2 51.79 2.70 11 1 -2 47.80 3.00 11 -1 -2 52.09 2.60 11 -1 -2 53.69 2.80 11 -1 -2 52.69 2.70 11 1 -1 34.50 3.70 11 1 -1 38.80 2.30 11 -1 -1 42.30 2.20 11 -1 -1 41.90 2.30 11 -1 -1 41.40 2.50 11 1 0 18.60 2.10 11 1 0 19.60 1.80 11 -1 0 18.90 1.70 11 -1 0 16.40 1.50 11 1 1 9.30 1.60 11 1 1 15.40 1.70 11 1 1 12.70 1.80 11 -1 1 13.10 1.40 11 -1 1 12.00 1.50 11 1 2 141.19 5.70 11 1 2 130.49 5.60 11 1 2 134.39 5.80 11 -1 2 131.09 5.60 11 -1 2 144.49 5.80 11 -1 2 136.79 5.70 11 1 3 59.59 3.10 11 1 3 59.69 3.00 11 1 3 58.89 2.90 11 -1 3 60.59 3.00 11 -1 3 59.29 3.00 11 -1 3 59.59 3.10 11 1 4 99.09 4.30 11 1 4 103.09 4.40 11 1 4 102.79 4.50 11 -1 4 102.69 4.40 11 -1 4 100.29 4.40 11 -1 4 98.69 4.40 11 -1 4 94.89 4.50 11 1 5 0.30 0.70 11 1 5 0.00 0.80 11 1 5 0.50 0.70 11 -1 5 0.20 0.90 11 -1 5 0.30 0.80 11 -1 5 0.70 0.70 11 -1 5 -0.60 0.60 11 1 6 253.17 9.60 11 1 6 248.58 9.70 11 1 6 246.08 9.50 11 -1 6 241.68 9.70 11 -1 6 239.28 9.50 11 -1 6 242.88 9.50 11 -1 6 244.38 9.50 11 1 7 20.60 1.60 11 1 7 20.80 1.70 11 1 7 18.80 1.70 11 -1 7 22.40 1.80 11 -1 7 18.10 1.50 11 -1 7 19.30 1.90 11 1 8 2.50 0.80 11 1 8 4.10 1.10 11 1 8 2.60 0.70 11 -1 8 2.90 0.90 11 -1 8 2.40 0.70 11 -1 8 4.40 1.00 11 1 9 21.70 1.80 11 1 9 15.50 1.10 11 -1 9 17.20 1.30 11 -1 9 16.40 1.20 11 -1 9 17.20 1.20 11 1 10 0.40 0.40 11 1 10 0.30 0.40 11 -1 10 0.20 0.40 11 -1 10 0.50 0.60 11 2 -15 31.10 1.50 11 2 -14 1.20 0.50 11 -2 -14 1.30 0.50 11 -2 -14 0.20 0.50 -11 2 13 7.50 1.10 11 2 -13 8.30 1.10 11 -2 -13 7.50 0.90 11 -2 -13 6.80 1.00 11 2 -12 10.40 1.30 -11 2 12 7.20 1.10 11 -2 -12 8.90 1.00 11 -2 -12 10.50 1.20 11 2 -11 27.70 2.00 -11 2 11 24.30 1.80 11 -2 -11 25.00 1.80 11 -2 -11 27.80 1.70 11 2 -10 7.60 1.30 11 2 -10 11.00 1.60 -11 2 10 9.40 1.30 11 -2 -10 8.70 1.20 11 -2 -10 8.50 1.40 11 2 -9 58.89 3.00 -11 2 9 52.89 3.00 11 2 -9 45.20 3.90 11 -2 -9 57.09 2.80 11 -2 -9 56.49 2.90 11 2 -8 138.29 5.90 11 2 -8 139.69 6.10 11 -2 -8 136.99 5.70 11 -2 -8 135.09 5.80 11 2 -7 178.58 7.20 11 2 -7 172.48 7.30 11 -2 -7 172.58 7.10 11 -2 -7 173.58 7.00 11 2 -6 28.80 2.00 11 2 -6 32.70 2.50 11 -2 -6 29.30 1.90 11 -2 -6 28.50 2.20 11 2 -5 46.80 2.60 11 2 -5 46.50 3.00 11 -2 -5 45.70 2.40 11 -2 -5 45.60 2.50 11 2 -4 21.70 1.60 11 -2 -4 15.80 1.70 11 -2 -4 19.10 1.50 11 2 -3 47.50 2.60 11 2 -3 47.50 2.60 11 -2 -3 45.60 2.40 11 -2 -3 47.80 2.50 11 2 -2 33.10 2.00 11 2 -2 30.90 2.20 11 -2 -2 34.20 2.00 11 -2 -2 32.40 2.10 11 2 -1 42.30 2.30 11 2 -1 40.90 2.40 11 -2 -1 44.10 2.30 11 -2 -1 39.50 2.30 11 2 0 13.80 1.40 11 2 0 10.10 1.60 11 2 0 12.00 2.00 11 -2 0 11.80 1.40 11 -2 0 13.50 1.30 11 2 1 13.90 1.50 11 2 1 10.60 1.80 11 2 1 12.70 1.50 11 -2 1 10.30 1.80 11 -2 1 10.00 2.00 11 2 2 816.52 30.60 11 2 2 864.51 30.60 11 2 2 835.92 30.70 11 -2 2 817.72 30.60 11 -2 2 803.52 30.60 11 -2 2 839.12 30.50 11 2 3 7.10 1.50 11 2 3 8.60 1.30 11 -2 3 7.80 1.40 11 -2 3 8.30 1.50 11 -2 3 7.30 1.10 11 2 4 328.07 12.70 11 2 4 334.57 12.60 11 -2 4 332.07 12.60 11 -2 4 326.67 12.60 11 -2 4 316.47 12.50 11 2 5 97.19 4.30 11 2 5 95.29 4.40 11 2 5 94.79 4.40 11 -2 5 99.59 4.40 11 -2 5 95.99 4.20 11 -2 5 100.69 4.30 11 2 6 201.48 8.20 11 2 6 210.28 8.30 11 -2 6 212.08 8.40 11 -2 6 204.38 8.20 11 -2 6 202.98 8.30 11 2 7 13.80 1.20 11 2 7 14.20 1.30 11 -2 7 14.50 1.40 11 -2 7 15.60 1.50 11 -2 7 14.10 1.20 11 2 8 176.18 6.90 11 2 8 182.18 7.00 11 -2 8 176.88 7.00 11 -2 8 176.28 6.90 11 -2 8 169.78 6.80 11 2 9 3.10 0.70 11 2 9 3.30 0.70 11 -2 9 4.20 0.70 11 -2 9 3.40 0.80 11 2 10 172.88 6.60 11 2 10 171.78 6.60 11 -2 10 178.78 6.70 11 3 -14 0.90 0.50 11 -3 -14 0.50 0.40 -11 3 13 4.20 1.00 11 3 -13 4.80 1.00 11 -3 -13 4.30 0.70 11 -3 -13 3.70 1.20 -11 3 12 22.50 1.60 11 3 -12 23.60 1.60 11 -3 -12 21.90 1.50 11 -3 -12 22.50 1.60 -11 3 11 0.00 0.70 11 3 -11 -0.10 0.80 11 -3 -11 0.80 0.60 11 -3 -11 0.50 0.70 -11 3 10 14.10 1.40 11 3 -10 14.80 1.60 11 3 -10 16.30 1.70 11 -3 -10 15.90 1.50 -11 -3 10 12.90 1.60 11 -3 -10 16.10 1.30 11 3 -9 5.80 1.40 11 3 -9 9.70 1.80 -11 3 9 9.00 1.20 -11 -3 9 8.80 1.60 11 -3 -9 7.20 1.40 11 -3 -9 9.30 1.40 -11 3 8 1187.78 44.50 11 3 -8 1235.68 44.30 11 3 -8 1166.18 44.60 11 -3 -8 1243.18 44.20 11 -3 -8 1209.38 44.30 11 3 -7 60.89 3.30 11 3 -7 55.59 3.40 -11 3 7 60.79 3.40 11 -3 -7 54.49 2.80 11 -3 -7 57.19 3.00 11 3 -6 187.48 7.90 -11 3 6 189.58 7.70 11 -3 -6 190.18 7.60 11 -3 -6 184.88 7.50 -11 3 5 51.29 2.70 11 3 -5 52.59 2.80 11 3 -5 42.10 2.80 11 -3 -5 47.60 2.70 11 -3 -5 48.20 2.50 -11 3 4 18.90 1.60 11 3 -4 19.90 1.60 11 3 -4 20.30 1.60 11 -3 -4 18.00 1.70 11 -3 -4 19.90 1.50 11 3 -3 8.10 1.10 11 3 -3 7.10 1.30 -11 3 3 5.20 1.30 11 -3 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1.50 11 -3 8 10.20 0.90 11 3 9 34.70 1.70 11 -3 9 27.50 2.00 11 -3 9 33.60 1.60 11 4 -13 31.40 1.90 11 -4 -13 36.70 1.60 -11 4 12 11.30 1.10 11 4 -12 13.40 1.90 -11 -4 12 5.40 1.50 11 -4 -12 8.40 0.90 11 4 -11 7.40 1.40 -11 4 11 6.60 1.00 11 -4 -11 6.10 1.40 11 -4 -11 7.00 0.90 -11 -4 11 5.40 1.10 11 4 -10 178.98 7.00 11 4 -10 175.28 7.30 -11 4 10 178.38 7.20 -11 -4 10 174.98 7.00 11 -4 -10 173.18 7.00 11 -4 -10 175.28 7.00 -11 4 9 1.10 0.60 11 4 -9 1.10 0.90 -11 -4 9 0.00 0.70 11 -4 -9 1.20 0.80 11 -4 -9 0.40 0.50 -11 4 8 39.90 2.40 11 4 -8 41.40 2.60 11 -4 -8 46.30 2.30 11 -4 -8 43.10 2.40 -11 4 7 6.50 1.10 11 4 -7 7.90 1.30 11 -4 -7 9.70 1.10 11 -4 -7 7.90 1.40 -11 4 6 17.60 1.40 11 4 -6 15.00 1.50 11 -4 -6 17.40 1.40 11 -4 -6 16.60 1.70 -11 4 5 468.15 17.10 11 4 -5 441.46 16.90 11 4 -5 451.85 17.40 11 -4 -5 432.46 16.90 11 -4 -5 458.35 17.00 11 4 -4 22.50 1.60 -11 4 4 23.00 1.70 11 4 -4 24.80 1.80 11 -4 -4 24.10 1.60 11 -4 -4 22.30 1.80 11 4 -3 576.04 21.30 11 4 -3 559.44 20.90 -11 4 3 572.84 20.90 11 -4 -3 537.75 20.90 11 -4 -3 559.34 20.90 11 4 -2 54.59 2.60 11 4 -2 53.59 2.90 11 -4 -2 47.30 2.70 11 -4 -2 53.19 2.60 11 4 -1 77.29 3.80 11 4 -1 83.89 3.70 11 4 -1 81.79 3.90 11 -4 -1 82.19 3.80 11 -4 -1 81.89 3.70 11 4 0 108.89 4.80 11 4 0 113.99 5.20 11 4 0 112.49 4.80 11 -4 0 121.89 4.90 11 -4 0 109.09 4.80 11 4 1 57.79 2.90 11 4 1 56.49 3.00 11 4 1 55.49 2.80 11 -4 1 57.39 2.90 11 -4 1 57.49 3.00 11 -4 1 54.49 2.70 11 4 2 12.20 1.30 11 4 2 11.90 1.40 11 4 2 15.20 1.50 11 -4 2 13.40 1.70 11 -4 2 13.70 1.30 11 -4 2 10.90 1.50 11 4 3 518.85 18.90 11 4 3 468.25 19.00 11 4 3 508.15 19.00 11 -4 3 509.55 18.90 11 -4 3 503.15 18.80 11 -4 3 514.55 18.90 11 4 4 225.98 9.30 11 4 4 239.48 9.40 11 -4 4 241.08 9.30 11 -4 4 241.98 9.30 11 -4 4 245.48 9.40 11 4 5 8.00 0.90 11 4 5 7.00 1.10 11 -4 5 7.60 1.10 11 -4 5 7.70 1.00 11 -4 5 6.60 0.90 11 4 6 34.00 2.00 11 4 6 31.70 1.80 11 -4 6 32.80 1.80 11 -4 6 33.80 1.80 11 -4 6 35.90 1.90 11 4 7 0.20 0.40 11 4 7 0.10 0.40 11 -4 7 0.30 0.50 11 -4 7 0.30 0.60 11 4 8 1.20 0.40 11 -4 8 0.50 0.60 11 -4 8 -0.10 0.50 11 -5 -12 22.20 1.50 -11 5 11 8.20 1.00 -11 -5 11 7.10 0.90 11 -5 -11 6.60 0.70 -11 5 10 78.79 3.60 -11 -5 10 80.39 3.40 11 -5 -10 75.49 3.30 11 5 -9 227.58 9.10 -11 5 9 221.28 8.70 -11 -5 9 223.18 8.60 11 -5 -9 212.98 8.50 -11 5 8 0.50 0.70 11 5 -8 1.50 1.00 11 -5 -8 -0.50 0.80 11 5 -7 26.20 1.90 -11 5 7 23.50 1.70 11 -5 -7 25.30 2.40 11 -5 -7 27.10 1.60 -11 5 6 11.50 1.30 11 5 -6 13.50 1.40 11 -5 -6 13.40 1.50 11 -5 -6 12.20 1.20 11 5 -5 50.49 2.50 11 5 -5 48.70 2.90 -11 5 5 49.70 2.60 11 -5 -5 49.90 2.50 11 -5 -5 53.49 2.70 11 5 -4 99.59 4.30 11 5 -4 105.09 5.10 -11 5 4 88.99 4.30 11 -5 -4 102.19 4.30 11 -5 -4 100.59 4.30 11 5 -3 28.90 2.00 11 5 -3 31.90 1.90 11 -5 -3 29.40 1.80 11 -5 -3 34.30 2.10 11 5 -2 152.78 6.80 11 5 -2 164.38 6.60 11 -5 -2 168.08 6.80 11 -5 -2 164.18 6.60 11 5 -1 59.29 3.40 11 5 -1 60.59 2.90 11 5 -1 59.99 2.90 11 -5 -1 61.99 3.00 11 -5 -1 57.89 2.80 11 5 0 8.70 1.10 11 5 0 7.20 1.20 11 5 0 11.80 1.40 11 -5 0 9.10 1.20 11 -5 0 8.80 1.60 11 -5 0 11.00 1.10 11 5 1 125.79 5.20 11 5 1 128.79 5.20 11 5 1 115.19 5.40 11 -5 1 122.69 5.10 11 -5 1 129.49 5.20 11 -5 1 125.49 5.20 11 5 2 11.40 1.30 11 5 2 8.70 1.00 11 5 2 10.70 1.30 11 -5 2 10.40 1.10 11 -5 2 8.70 1.10 11 5 3 7.10 1.30 11 5 3 7.90 1.00 11 5 3 5.90 1.10 11 -5 3 7.70 1.20 11 -5 3 8.60 1.10 11 -5 3 4.90 1.10 11 5 4 8.40 1.80 11 5 4 11.70 1.20 11 5 4 10.60 1.00 11 -5 4 12.80 1.20 11 -5 4 10.50 1.00 11 -5 4 9.10 1.00 11 5 5 13.80 1.10 11 5 5 12.30 1.00 11 -5 5 13.20 1.10 11 -5 5 14.70 1.10 11 -5 5 13.80 1.20 11 5 6 0.30 0.40 11 5 6 -0.10 0.90 11 -5 6 0.60 0.50 11 -5 6 -0.60 0.40 11 5 7 12.10 1.00 11 -5 7 12.50 1.00 11 -5 7 12.90 1.00 11 -6 -11 1.50 0.40 -11 -6 11 1.40 0.50 -11 6 10 61.19 2.90 -11 -6 10 60.59 2.60 11 -6 -10 64.59 2.70 -11 6 9 61.79 2.90 11 -6 -9 60.19 2.60 -11 -6 9 62.79 2.70 -11 6 8 11.60 1.20 11 6 -8 11.20 1.70 -11 -6 8 11.50 1.00 11 -6 -8 9.50 0.90 -11 6 7 1.50 0.70 11 6 -7 0.10 1.00 11 -6 -7 0.80 0.50 -11 6 6 8.60 1.30 11 6 -6 7.30 1.20 11 -6 -6 8.60 1.00 -11 6 5 8.90 1.60 11 6 -5 12.60 1.40 11 -6 -5 13.30 1.10 11 6 -4 4.20 1.00 11 6 -4 3.60 0.80 11 -6 -4 6.00 1.40 11 -6 -4 5.40 0.90 11 6 -3 12.80 1.30 11 6 -3 11.50 1.20 11 -6 -3 10.10 1.30 11 -6 -3 11.10 1.00 11 6 -2 6.90 1.10 11 6 -2 7.40 1.30 11 -6 -2 8.00 1.20 11 -6 -2 8.80 1.00 11 6 -1 83.89 3.60 11 6 -1 79.29 3.90 11 -6 -1 83.19 3.50 11 -6 -1 84.09 3.60 11 6 0 2.00 0.70 11 6 0 2.70 0.70 11 -6 0 4.40 0.90 11 -6 0 2.80 1.00 11 6 1 11.60 1.30 11 6 1 13.00 1.10 11 -6 1 12.90 1.10 11 -6 1 14.80 1.20 11 -6 1 13.40 1.50 11 6 2 13.80 1.40 11 6 2 14.30 1.10 11 -6 2 13.60 1.10 11 -6 2 15.70 1.10 11 -6 2 13.90 1.40 11 6 3 34.20 2.10 11 6 3 32.00 1.70 11 6 3 31.60 1.70 11 -6 3 34.40 1.80 11 -6 3 33.60 1.70 11 -6 3 33.10 1.70 11 6 4 1.70 0.60 11 -6 4 4.60 0.90 11 -6 4 2.60 0.90 11 -6 4 2.30 0.70 11 6 5 8.70 0.70 11 -6 5 9.90 0.90 11 -6 5 5.80 1.10 11 6 6 0.00 0.30 11 -6 6 0.50 0.40 -11 -7 9 47.90 2.00 11 -7 -8 33.00 1.60 -11 -7 8 34.60 1.60 11 -7 -7 1.20 0.50 -11 -7 7 1.40 0.40 11 7 -6 114.69 5.00 11 -7 -6 116.69 4.80 11 7 -5 7.20 1.20 11 -7 -5 4.20 0.80 11 7 -4 36.20 2.10 11 -7 -4 32.90 1.70 11 7 -3 12.10 1.30 11 -7 -3 12.60 1.10 11 7 -2 3.10 0.80 11 7 -2 3.90 0.70 11 -7 -2 1.70 0.60 -11 -7 2 3.20 0.90 11 7 -1 2.90 1.00 11 7 -1 2.00 0.60 11 -7 -1 1.40 0.60 -11 -7 1 1.70 0.60 11 7 0 4.40 0.60 11 7 0 2.50 0.80 11 -7 0 5.30 1.10 11 7 1 94.19 3.90 11 7 1 98.69 4.20 11 7 2 14.60 1.00 11 7 3 -0.30 0.30 -11 -8 4 97.89 3.80 12 0 -15 0.20 0.40 12 0 -14 0.50 0.70 12 0 -13 0.60 0.50 -12 0 13 -1.20 0.90 -12 0 12 24.30 1.80 12 0 -12 18.40 1.70 12 0 -11 -0.20 0.70 12 0 -10 88.09 4.10 12 0 -10 94.79 4.20 12 0 -9 0.20 1.00 12 0 -9 -0.40 0.80 12 0 -8 243.98 9.60 12 0 -8 230.48 9.30 12 0 -8 249.18 9.80 12 0 -7 0.10 1.10 12 0 -7 1.10 0.80 12 0 -7 0.10 1.00 12 0 -6 2858.41 108.09 12 0 -6 3121.49 108.59 12 0 -5 2.90 1.00 12 0 -5 -0.30 0.70 12 0 -5 -0.10 0.70 12 0 -4 220.78 8.70 12 0 -4 218.88 8.50 12 0 -4 206.88 8.40 12 0 -3 3.50 1.10 12 0 -3 -0.20 0.80 12 0 -3 -0.40 0.80 12 0 -2 616.64 23.70 12 0 -2 647.54 23.80 12 0 -2 663.73 24.00 12 0 -1 1.90 0.90 12 0 -1 1.00 0.90 12 0 -1 0.60 1.00 12 0 0 91.49 4.10 12 0 0 94.49 4.20 12 0 1 1.10 0.90 12 0 1 -0.10 1.20 12 0 2 208.98 8.10 12 0 2 202.48 8.20 12 0 2 208.98 8.30 12 0 3 -0.50 0.80 12 0 3 -0.20 1.00 12 0 3 -0.30 0.70 12 0 3 -0.30 0.90 12 0 4 105.89 4.50 12 0 4 108.89 4.70 12 0 4 105.59 4.60 12 0 4 101.89 4.70 12 0 5 0.70 0.60 12 0 5 0.50 0.70 12 0 5 -1.00 0.70 12 0 6 65.09 3.40 12 0 6 59.09 2.90 12 0 6 54.79 2.80 12 0 7 0.10 0.60 12 0 7 -0.50 0.60 12 0 7 0.00 0.60 12 0 8 2.40 0.60 12 0 8 4.50 0.90 12 0 8 3.50 0.90 12 0 9 0.20 0.50 12 0 9 0.50 0.50 12 1 -15 9.30 0.80 12 -1 -15 9.40 0.90 12 1 -14 15.60 1.10 12 -1 -14 15.00 1.10 12 1 -13 18.00 1.40 -12 1 13 19.30 1.50 -12 -1 13 16.40 1.80 12 -1 -13 18.30 1.30 12 -1 -13 18.50 1.30 12 1 -12 18.60 1.50 -12 1 12 19.80 1.60 12 -1 -12 18.60 1.40 12 -1 -12 18.70 1.40 -12 1 11 172.28 7.50 12 1 -11 186.88 7.40 12 -1 -11 183.78 7.30 12 -1 -11 176.78 7.10 12 1 -10 254.87 9.90 12 -1 -10 251.27 9.90 12 -1 -10 244.58 9.70 12 1 -9 52.99 3.00 12 1 -9 56.69 3.00 12 -1 -9 52.49 2.70 12 -1 -9 51.89 2.90 12 1 -8 94.49 4.50 12 1 -8 99.59 4.40 12 -1 -8 93.19 4.40 12 -1 -8 94.99 4.20 12 1 -7 164.68 6.70 12 1 -7 162.78 6.90 12 -1 -7 154.08 6.60 12 -1 -7 154.28 6.40 12 1 -6 220.98 8.60 12 -1 -6 221.88 8.50 12 -1 -6 176.08 8.30 12 -1 -6 205.98 8.30 12 1 -5 241.58 9.60 12 1 -5 250.27 9.90 12 -1 -5 253.17 9.90 12 -1 -5 246.28 9.70 12 -1 -5 237.98 9.50 12 1 -4 325.77 12.60 12 1 -4 335.37 12.90 12 -1 -4 338.17 12.80 12 -1 -4 330.97 12.50 12 -1 -4 319.67 12.60 12 1 -3 9.00 1.30 12 1 -3 10.40 1.90 12 -1 -3 9.30 1.40 12 -1 -3 9.50 1.40 12 -1 -3 12.90 1.50 12 1 -2 36.20 2.60 12 1 -2 36.50 2.20 12 -1 -2 38.20 2.40 12 -1 -2 38.10 2.30 12 -1 -2 36.00 2.20 12 1 -1 7.40 2.20 12 1 -1 4.20 1.20 12 -1 -1 2.30 0.70 12 -1 -1 4.30 1.30 12 1 0 11.20 1.60 12 -1 0 14.30 1.40 12 -1 0 12.10 1.60 12 1 1 43.80 2.60 12 -1 1 37.80 2.70 12 -1 1 41.50 2.40 12 -1 1 41.30 2.20 12 1 2 1.50 1.00 12 -1 2 1.90 0.90 12 -1 2 4.00 1.30 12 -1 2 4.40 0.80 12 1 3 27.40 2.00 12 1 3 26.50 2.00 12 1 3 24.50 1.90 12 -1 3 27.00 2.00 12 -1 3 27.00 1.80 12 -1 3 30.70 1.90 12 1 4 322.97 12.20 12 1 4 310.97 12.00 12 1 4 318.77 12.10 12 -1 4 315.37 12.10 12 -1 4 309.57 12.20 12 -1 4 313.27 12.10 12 1 5 37.30 2.10 12 1 5 35.00 2.10 12 1 5 36.80 2.20 12 -1 5 35.50 2.20 12 -1 5 34.00 2.00 12 -1 5 36.20 2.20 12 -1 5 37.50 2.30 12 1 6 407.66 15.20 12 -1 6 396.86 15.10 12 -1 6 406.26 15.10 12 1 7 11.90 1.10 12 1 7 12.30 1.20 12 1 7 11.50 1.30 12 -1 7 8.90 1.20 12 -1 7 12.00 1.40 12 -1 7 12.80 1.10 12 1 8 128.89 5.20 12 -1 8 143.19 5.70 12 -1 8 129.39 5.40 12 -1 8 120.29 5.40 12 1 9 30.00 1.50 12 1 9 29.60 1.50 12 -1 9 25.00 1.70 12 -1 9 30.50 1.70 12 2 -14 2.70 0.80 12 -2 -14 3.00 0.70 12 -2 -14 1.60 0.60 -12 2 13 6.20 1.10 12 2 -13 5.10 0.90 12 -2 -13 5.90 0.90 12 -2 -13 6.70 0.90 12 2 -12 1.30 0.70 -12 2 12 2.90 1.00 12 -2 -12 4.30 0.90 12 -2 -12 2.30 0.60 -12 2 11 33.40 2.20 12 -2 -11 29.70 2.50 12 -2 -11 36.20 2.10 12 2 -10 0.20 0.80 12 2 -10 1.30 0.80 -12 2 10 0.50 0.70 12 -2 -10 -0.50 0.70 12 -2 -10 -0.20 0.60 12 2 -9 7.80 1.60 12 2 -9 4.70 1.20 -12 2 9 4.60 1.20 12 -2 -9 4.10 1.30 12 -2 -9 4.90 1.10 12 2 -8 81.49 3.70 12 2 -8 66.59 4.90 12 -2 -8 77.29 3.50 12 -2 -8 75.29 3.60 12 2 -7 2.60 1.10 12 2 -7 3.90 1.30 12 -2 -7 1.90 0.60 12 -2 -7 4.80 1.40 12 2 -6 1002.40 36.40 12 2 -6 982.40 36.10 12 -2 -6 978.60 36.00 12 -2 -6 962.30 36.10 12 2 -5 41.50 2.70 12 2 -5 37.70 2.40 12 -2 -5 38.20 2.30 12 -2 -5 40.40 2.20 12 2 -4 35.50 2.20 12 -2 -4 34.30 2.20 12 -2 -4 34.70 2.10 12 2 -3 63.19 3.30 12 -2 -3 63.29 3.50 12 2 -2 101.79 4.60 12 2 -2 113.69 4.90 12 -2 -2 102.09 4.80 12 -2 -2 114.89 5.20 12 2 -1 19.90 1.70 12 2 -1 18.80 1.80 12 -2 -1 20.60 1.50 12 -2 -1 21.70 1.70 12 2 0 26.90 1.90 12 2 0 27.20 1.90 12 -2 0 25.00 1.70 12 -2 0 23.60 1.80 12 2 1 13.10 1.70 12 2 1 13.00 1.80 12 2 1 13.30 1.60 12 -2 1 15.40 1.90 12 -2 1 13.30 1.30 12 -2 1 13.90 1.40 12 2 2 515.05 19.20 12 2 2 511.65 19.30 12 -2 2 506.35 19.20 12 -2 2 518.15 19.20 12 2 3 5.60 1.20 12 2 3 7.00 1.40 12 -2 3 4.90 1.20 12 -2 3 3.70 0.90 12 -2 3 5.50 1.10 12 2 4 24.20 1.70 12 2 4 22.50 1.80 12 -2 4 23.70 1.60 12 -2 4 23.00 1.70 12 -2 4 23.90 1.70 12 2 5 0.00 0.60 12 2 5 1.40 0.60 12 -2 5 1.90 0.70 12 -2 5 1.30 0.60 12 -2 5 1.00 0.60 12 2 6 126.49 5.20 12 2 6 128.29 5.30 12 -2 6 126.39 5.20 12 -2 6 126.89 5.20 12 -2 6 130.49 5.40 12 2 7 0.20 0.50 12 2 7 0.50 0.50 12 -2 7 -0.20 0.50 12 -2 7 0.20 0.50 12 2 8 199.88 7.60 12 2 8 184.28 7.50 12 -2 8 196.28 7.50 12 -2 8 202.98 7.60 12 2 9 3.20 0.60 12 2 9 4.00 0.70 12 -2 9 2.50 0.80 12 -2 9 3.70 0.70 12 3 -14 12.00 1.00 12 -3 -14 13.10 0.80 -12 3 13 3.30 0.90 12 3 -13 4.80 1.00 12 -3 -13 3.60 0.70 -12 3 12 32.00 1.90 12 3 -12 31.70 1.90 12 -3 -12 31.70 1.70 12 -3 -12 33.70 1.80 -12 3 11 1.80 0.70 12 3 -11 -0.30 0.70 12 -3 -11 0.90 0.50 12 -3 -11 -0.20 0.60 12 3 -10 24.60 1.90 -12 3 10 28.30 2.20 12 3 -10 26.50 2.00 12 -3 -10 29.60 1.70 12 -3 -10 30.20 1.90 12 3 -9 10.40 1.60 -12 3 9 8.40 1.20 12 3 -9 8.80 1.40 12 -3 -9 10.30 1.40 12 -3 -9 9.30 1.20 -12 -3 9 10.10 1.90 -12 3 8 34.10 2.20 12 3 -8 38.30 2.60 12 3 -8 33.80 2.30 12 -3 -8 34.40 2.00 12 -3 -8 36.70 2.20 -12 3 7 36.00 2.20 12 3 -7 36.10 2.30 12 3 -7 39.50 2.70 12 -3 -7 32.20 2.00 12 -3 -7 36.90 2.30 -12 3 6 11.70 1.30 12 3 -6 10.20 1.30 12 -3 -6 7.20 1.40 12 -3 -6 8.90 1.20 -12 3 5 10.30 1.30 12 3 -5 11.50 1.50 12 3 -5 9.10 1.50 12 -3 -5 12.50 1.20 12 -3 -5 8.00 1.40 12 3 -4 4.90 0.90 -12 3 4 8.50 1.30 12 3 -4 8.50 1.20 12 -3 -4 6.10 1.10 12 -3 -4 5.40 1.30 -12 3 3 3.50 1.00 12 3 -3 1.80 0.70 12 3 -3 4.70 1.30 12 -3 -3 3.20 0.80 12 -3 -3 5.30 1.10 12 3 -2 9.20 1.30 12 3 -2 9.30 1.20 12 -3 -2 9.20 1.20 12 -3 -2 9.10 1.30 12 3 -1 0.10 0.60 12 3 -1 1.70 0.70 12 -3 -1 0.80 0.70 12 -3 -1 1.20 0.60 12 3 0 7.50 1.30 12 3 0 6.40 1.20 12 3 0 5.70 1.80 12 -3 0 7.90 1.30 12 -3 0 9.50 1.20 12 3 1 339.17 12.90 12 3 1 340.87 12.90 12 -3 1 333.37 12.90 12 -3 1 343.77 13.00 12 -3 1 334.57 13.00 12 3 2 180.38 7.20 12 3 2 176.18 7.10 12 3 2 171.18 7.30 12 -3 2 176.38 7.20 12 -3 2 175.98 7.10 12 -3 2 187.38 7.20 12 3 3 104.09 4.50 12 3 3 104.99 4.60 12 -3 3 100.59 4.50 12 -3 3 105.49 4.60 12 -3 3 100.79 4.40 12 3 4 128.49 5.70 12 3 4 136.89 5.60 12 -3 4 136.89 5.60 12 -3 4 140.39 5.60 12 -3 4 138.49 5.70 12 3 5 5.50 1.00 12 3 5 6.50 1.00 12 -3 5 4.70 0.90 12 -3 5 5.50 1.10 12 -3 5 5.40 0.90 12 3 6 141.99 5.70 12 3 6 145.69 6.00 12 -3 6 145.49 5.80 12 -3 6 144.29 5.80 12 -3 6 138.19 5.70 12 3 7 53.69 2.60 12 3 7 58.49 3.30 12 -3 7 48.20 2.50 12 -3 7 52.49 2.50 12 3 8 0.20 0.50 12 3 8 0.40 0.40 12 -3 8 0.80 0.40 12 -3 8 0.10 0.60 12 -4 -13 23.20 1.20 -12 4 12 21.40 1.40 12 -4 -12 18.60 1.10 -12 4 11 4.90 0.90 12 -4 -11 4.20 1.30 12 -4 -11 4.90 0.70 -12 4 10 2.40 0.90 12 4 -10 4.20 1.40 -12 -4 10 1.50 0.70 12 -4 -10 2.70 0.70 12 -4 -10 3.50 1.20 -12 4 9 45.90 2.50 12 4 -9 46.80 2.70 12 -4 -9 47.70 2.40 -12 -4 9 49.30 2.40 -12 4 8 0.00 0.60 12 4 -8 1.40 0.90 12 -4 -8 1.10 0.50 12 -4 -8 4.00 1.20 12 4 -7 0.20 0.70 -12 4 7 -0.20 0.70 12 -4 -7 1.50 0.80 12 -4 -7 0.70 0.50 12 4 -6 202.28 8.80 -12 4 6 211.28 8.60 12 -4 -6 224.18 8.50 12 -4 -6 218.48 8.50 12 4 -5 383.76 14.60 -12 4 5 380.36 14.70 12 4 -5 367.46 15.00 12 -4 -5 398.56 14.70 12 -4 -5 401.86 14.70 12 4 -4 26.70 2.00 -12 4 4 29.20 2.00 12 4 -4 32.00 1.90 12 -4 -4 29.10 2.00 12 -4 -4 32.70 2.00 12 4 -3 346.57 14.20 12 4 -3 371.36 13.80 12 -4 -3 371.66 13.90 12 -4 -3 370.96 13.80 12 4 -2 66.39 3.10 12 4 -2 59.89 3.20 12 -4 -2 65.99 3.30 12 -4 -2 63.19 3.00 12 4 -1 18.50 1.60 12 4 -1 17.40 1.40 12 4 -1 21.10 1.90 12 -4 -1 17.80 1.40 12 -4 -1 17.50 1.60 12 4 0 27.90 2.00 12 4 0 30.10 1.80 12 4 0 25.70 2.10 12 -4 0 29.40 1.90 12 -4 0 29.60 1.80 12 4 1 4.70 1.00 12 4 1 5.00 1.20 12 4 1 2.80 0.80 12 -4 1 1.50 1.00 12 -4 1 2.30 0.70 12 -4 1 3.90 1.10 12 4 2 14.50 1.30 12 4 2 14.80 1.50 12 4 2 16.30 1.60 12 -4 2 16.00 1.40 12 -4 2 15.20 1.70 12 -4 2 18.00 1.30 12 4 3 273.07 11.30 12 4 3 294.87 11.40 12 4 3 297.17 11.20 12 -4 3 304.37 11.20 12 -4 3 302.77 11.10 12 -4 3 269.77 11.60 12 4 4 23.70 1.60 12 4 4 23.70 1.50 12 -4 4 23.10 1.50 12 -4 4 24.20 1.60 12 -4 4 25.00 1.60 12 4 5 7.90 1.00 12 4 5 9.60 1.00 12 -4 5 10.10 1.10 12 -4 5 8.10 1.30 12 -4 5 8.60 0.90 12 4 6 63.49 2.80 12 -4 6 65.69 2.80 12 -4 6 62.29 2.90 12 -4 6 64.59 2.90 12 4 7 42.80 2.00 12 4 7 44.80 2.00 12 -4 7 43.80 2.00 12 4 8 0.00 0.50 12 4 8 -0.20 0.30 12 -4 8 -0.50 0.40 12 -5 -12 0.60 0.30 -12 5 11 2.40 0.70 -12 -5 11 1.30 0.70 12 -5 -11 2.10 0.60 -12 5 10 67.69 3.00 -12 -5 10 64.49 2.80 12 -5 -10 59.89 2.90 12 5 -9 33.30 2.20 -12 5 9 28.50 2.30 12 -5 -9 33.30 1.70 -12 -5 9 33.90 1.80 12 -5 -9 33.50 2.00 -12 5 8 114.99 4.80 12 5 -8 112.59 4.90 12 -5 -8 106.49 4.50 12 -5 -8 108.09 4.60 -12 5 7 13.10 1.20 12 5 -7 12.30 1.60 12 -5 -7 11.60 1.10 12 -5 -7 10.00 1.40 12 5 -6 93.79 4.50 -12 5 6 96.09 4.20 12 -5 -6 100.99 4.20 -12 5 5 18.80 1.70 12 5 -5 19.00 1.40 12 5 -5 18.10 1.60 12 -5 -5 20.80 1.40 12 -5 -5 19.20 1.50 12 5 -4 7.80 1.20 12 5 -4 8.10 1.00 12 -5 -4 9.40 1.00 12 -5 -4 11.60 1.30 12 5 -3 24.00 1.80 12 5 -3 25.40 1.60 12 -5 -3 27.50 1.70 12 -5 -3 27.20 1.70 12 5 -2 48.00 2.80 12 5 -2 53.39 2.60 12 -5 -2 52.39 2.50 12 -5 -2 53.49 2.60 12 5 -1 4.80 1.10 12 5 -1 2.90 0.90 12 -5 -1 2.50 1.00 12 5 0 41.90 2.10 12 5 0 35.00 2.10 12 5 0 36.70 2.30 12 -5 0 39.60 2.00 12 -5 0 40.70 2.10 12 5 1 81.59 3.60 12 5 1 81.99 3.90 12 -5 1 79.79 3.70 12 5 2 26.60 1.60 12 5 2 26.50 1.90 12 5 2 26.30 1.60 12 -5 2 26.30 1.60 12 -5 2 24.30 1.90 12 -5 2 28.10 1.60 12 5 3 8.20 0.90 12 5 3 8.50 1.00 12 5 3 9.30 1.70 12 -5 3 8.60 1.00 12 -5 3 8.40 1.20 12 -5 3 9.40 1.00 12 5 4 5.30 0.80 12 5 4 3.60 0.70 12 -5 4 3.80 0.80 12 -5 4 4.60 1.00 12 -5 4 3.40 0.70 12 5 5 0.50 0.30 12 5 5 0.30 0.40 12 -5 5 -0.30 0.40 12 -5 5 0.10 0.50 12 -5 5 -0.30 0.50 12 5 6 45.60 2.00 12 5 6 40.10 2.20 12 -5 6 47.20 2.10 -12 -6 10 0.50 0.50 12 -6 -10 -0.10 0.30 12 -6 -9 0.10 0.40 -12 -6 9 0.50 0.60 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1.80 12 7 -4 16.80 1.40 12 -7 -4 16.30 1.10 12 7 -3 17.30 1.40 12 -7 -3 17.50 1.10 12 7 -2 -0.70 0.70 12 -7 -2 -1.10 0.50 12 7 -1 16.10 1.00 12 7 -1 18.40 1.40 12 -7 -1 17.70 1.20 12 7 0 4.20 1.20 12 7 0 3.40 0.50 -12 -7 0 2.40 0.70 12 -7 0 1.70 0.70 12 7 1 5.20 0.60 -12 -7 -1 6.70 1.00 12 7 2 13.20 0.80 -12 -7 -2 10.70 1.10 13 0 -15 0.60 0.40 13 0 -14 29.50 1.60 -13 0 13 1.80 0.90 -13 0 12 3.70 1.10 13 0 -12 3.40 1.00 13 0 -11 -0.50 0.70 13 0 -10 4.00 0.80 13 0 -9 0.20 0.90 13 0 -8 53.39 2.80 13 0 -8 51.59 3.00 13 0 -7 0.10 0.80 13 0 -7 0.30 0.70 13 0 -6 928.81 34.00 13 0 -6 898.21 33.70 13 0 -5 -0.80 0.70 13 0 -5 0.60 0.80 13 0 -4 218.08 8.50 13 0 -4 217.48 8.70 13 0 -4 205.58 8.40 13 0 -3 -0.90 0.80 13 0 -3 0.40 0.80 13 0 -3 0.80 0.90 13 0 -2 2.40 1.00 13 0 -2 3.10 0.90 13 0 -2 0.30 1.00 13 0 -1 0.90 0.90 13 0 -1 0.40 1.10 13 0 -1 -0.60 0.90 13 0 0 128.09 5.30 13 0 0 131.39 5.50 13 0 1 3.20 0.90 13 0 1 -0.20 0.80 13 0 1 -0.20 1.10 13 0 2 57.29 3.10 13 0 2 57.49 2.80 13 0 2 57.89 3.00 13 0 3 0.00 0.80 13 0 3 0.50 0.70 13 0 3 1.50 0.90 13 0 4 93.29 4.20 13 0 4 89.39 4.00 13 0 4 92.19 4.00 13 0 5 0.20 0.60 13 0 5 -0.80 0.70 13 0 5 0.80 0.80 13 0 6 145.79 6.00 13 0 6 145.79 5.80 13 0 6 146.59 5.80 13 0 7 0.10 0.50 13 0 7 0.30 0.60 13 0 7 0.80 0.60 13 0 8 248.98 9.20 13 0 8 235.28 9.00 13 0 9 0.20 0.40 13 1 -14 10.60 0.90 13 -1 -14 10.20 0.90 -13 1 13 18.10 1.50 13 1 -13 18.80 1.30 -13 -1 13 15.50 1.70 13 -1 -13 18.50 1.20 13 -1 -13 17.50 1.40 13 1 -12 -0.40 0.60 -13 1 12 1.00 0.80 13 -1 -12 0.70 0.60 13 -1 -12 0.00 0.60 -13 1 11 0.10 0.70 13 1 -11 1.10 0.80 13 -1 -11 0.50 0.60 13 1 -10 22.00 1.70 13 -1 -10 18.50 1.60 13 -1 -10 20.40 1.50 13 1 -9 198.18 7.90 13 1 -9 180.78 8.10 13 -1 -9 194.68 7.70 13 -1 -9 203.18 7.90 13 1 -8 228.98 9.90 13 1 -8 253.27 9.60 13 -1 -8 242.08 9.60 13 -1 -8 246.08 9.40 13 1 -7 0.60 0.80 13 1 -7 1.50 0.80 13 -1 -7 -0.50 0.70 13 -1 -7 0.40 0.60 13 1 -6 215.68 8.70 13 1 -6 224.58 9.00 13 -1 -6 211.68 8.50 13 -1 -6 219.78 8.70 13 1 -5 41.70 2.50 13 1 -5 41.70 2.60 13 -1 -5 42.80 2.50 13 -1 -5 42.80 2.40 13 -1 -5 47.20 2.60 13 1 -4 678.43 24.20 13 1 -4 632.54 23.90 13 -1 -4 631.34 23.90 13 -1 -4 653.13 24.10 13 -1 -4 622.24 23.80 13 1 -3 118.69 5.60 13 1 -3 120.29 5.20 13 -1 -3 113.19 4.90 13 -1 -3 120.99 5.20 13 -1 -3 115.89 5.10 13 1 -2 77.29 3.70 13 -1 -2 74.29 3.60 13 -1 -2 76.19 3.70 13 -1 -2 78.79 3.50 13 1 -1 37.60 2.40 13 -1 -1 34.70 2.20 13 -1 -1 35.20 2.10 13 1 0 41.60 2.70 13 -1 0 43.70 2.40 13 -1 0 43.10 2.30 13 1 1 40.20 2.60 13 1 1 37.00 2.40 13 -1 1 33.60 3.30 13 -1 1 36.90 2.20 13 1 2 9.50 1.50 13 1 2 7.90 1.60 13 1 2 9.60 1.70 13 -1 2 8.80 1.70 13 -1 2 5.80 1.30 13 -1 2 5.90 1.30 13 1 3 0.50 0.80 13 1 3 1.40 0.80 13 1 3 1.60 0.90 13 -1 3 2.20 0.90 13 -1 3 0.40 0.70 13 -1 3 1.50 0.60 13 1 4 1.30 0.80 13 1 4 1.00 0.80 13 1 4 0.90 0.70 13 -1 4 3.80 1.30 13 -1 4 0.00 0.60 13 -1 4 -0.50 0.70 13 1 5 3.00 0.70 13 1 5 0.70 0.80 13 1 5 2.60 0.80 13 -1 5 2.30 0.60 13 -1 5 1.30 0.70 13 -1 5 4.10 1.20 13 1 6 38.10 2.10 13 1 6 38.80 2.10 13 1 6 38.50 2.00 13 -1 6 41.20 2.10 13 -1 6 38.70 2.00 13 1 7 15.70 1.20 13 1 7 12.90 1.10 13 -1 7 16.00 1.10 13 -1 7 16.10 1.20 13 1 8 131.89 5.10 13 1 8 137.59 5.30 13 -1 8 131.79 5.50 13 -1 8 132.69 5.30 13 2 -14 2.70 0.80 13 -2 -14 0.10 0.50 -13 2 13 0.60 0.70 13 -2 -13 1.10 0.50 13 -2 -13 1.00 0.50 13 2 -12 5.00 1.00 -13 2 12 3.40 1.00 13 -2 -12 2.50 0.60 13 -2 -12 2.60 0.80 -13 2 11 53.09 2.90 13 2 -11 54.29 2.70 13 -2 -11 51.29 2.60 13 -2 -11 52.89 2.50 13 2 -10 126.99 5.10 13 2 -10 109.19 5.20 -13 2 10 109.59 5.20 13 -2 -10 123.29 4.90 13 -2 -10 122.09 5.10 13 2 -9 169.78 6.70 13 2 -9 156.48 7.00 -13 2 9 153.08 6.90 13 -2 -9 163.28 6.80 13 -2 -9 172.18 6.60 13 2 -8 2.30 0.90 13 2 -8 1.70 0.90 13 -2 -8 0.80 0.70 13 -2 -8 1.30 0.60 13 2 -7 13.40 1.80 13 2 -7 11.80 1.50 13 -2 -7 13.10 1.50 13 -2 -7 12.40 1.30 13 2 -6 1087.09 40.10 13 2 -6 1128.99 40.60 13 -2 -6 1067.69 40.10 13 -2 -6 1098.39 40.20 13 2 -5 3.70 1.10 13 2 -5 2.90 1.20 13 -2 -5 0.90 0.60 13 -2 -5 2.10 0.80 13 2 -4 199.48 8.10 13 -2 -4 192.18 7.80 13 -2 -4 190.98 7.70 13 2 -3 10.50 1.30 13 -2 -3 9.20 1.30 13 -2 -3 8.50 1.30 13 2 -2 35.70 2.20 13 -2 -2 36.00 2.10 13 -2 -2 32.80 2.00 13 2 -1 2.60 0.90 13 2 -1 4.70 1.20 13 -2 -1 3.20 0.90 13 -2 -1 3.60 0.80 13 2 0 67.69 3.40 13 2 0 64.69 3.20 13 -2 0 63.69 3.20 13 -2 0 66.19 3.10 13 2 1 7.20 1.70 13 2 1 8.60 1.40 13 -2 1 9.00 1.20 13 -2 1 9.80 1.20 13 2 2 124.19 5.20 13 2 2 121.99 5.10 13 -2 2 122.49 5.20 13 -2 2 122.89 5.20 13 -2 2 118.19 5.10 13 2 3 1.90 0.80 13 2 3 -0.10 0.60 13 -2 3 1.90 0.70 13 -2 3 1.40 0.60 13 -2 3 1.30 0.80 13 2 4 23.80 1.70 13 2 4 21.10 1.70 13 -2 4 22.50 1.50 13 -2 4 20.80 1.60 13 2 5 0.70 0.50 13 2 5 0.50 0.60 13 -2 5 0.60 0.50 13 -2 5 -1.00 0.60 13 -2 5 -0.40 0.50 13 2 6 62.79 3.00 13 2 6 66.19 2.90 13 -2 6 64.19 2.90 13 -2 6 67.79 3.00 13 -2 6 66.49 2.90 13 2 7 34.40 1.70 13 2 7 34.20 1.80 13 -2 7 33.60 1.70 13 -2 7 36.30 1.80 13 2 8 1.30 0.40 13 2 8 2.60 0.70 13 -2 8 1.20 0.40 13 -2 8 2.60 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16.30 1.30 13 -5 -2 16.80 1.60 13 5 -1 2.70 0.80 13 5 -1 2.80 0.80 13 -5 -1 4.10 0.90 13 -5 -1 3.90 0.80 13 5 0 1.80 0.50 13 5 0 0.10 0.70 13 -5 0 1.40 0.50 13 -5 0 1.50 0.50 13 5 1 10.70 1.20 13 5 1 13.00 1.10 13 -5 1 12.50 1.00 13 -5 1 15.50 1.40 13 5 2 2.80 0.90 13 5 2 2.90 0.70 13 5 2 2.90 1.10 13 -5 2 2.50 0.80 13 -5 2 3.50 0.80 13 5 3 1.20 0.40 13 5 3 1.30 0.50 13 -5 3 1.30 0.40 13 5 4 -0.50 0.40 13 5 4 0.40 0.50 13 -5 4 0.10 0.40 13 -5 4 1.00 0.40 13 -5 4 0.40 0.70 13 5 5 3.50 0.50 13 5 5 3.40 0.70 13 -5 5 2.70 0.70 13 -5 5 3.60 0.70 13 -6 -9 20.50 1.10 -13 -6 9 20.30 1.20 13 -6 -8 4.00 0.70 -13 -6 8 5.20 0.80 13 6 -7 53.39 2.70 13 -6 -7 51.49 2.30 -13 -6 7 54.59 2.40 13 6 -6 6.80 1.20 13 -6 -6 5.10 0.80 13 6 -5 1.80 0.80 13 -6 -5 2.70 0.70 13 -6 -5 0.70 0.70 13 6 -4 0.90 0.60 13 -6 -4 1.30 0.50 13 -6 -4 3.80 1.00 13 6 -3 22.60 1.30 13 6 -3 26.40 1.70 13 -6 -3 23.80 1.40 13 -6 -3 21.70 1.30 13 6 -2 6.00 0.70 13 6 -2 5.50 1.10 13 -6 -2 5.90 0.80 13 -6 -2 4.90 0.90 13 6 -1 4.30 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248.08 9.40 14 -2 -10 250.87 9.60 14 2 -9 171.98 7.60 -14 2 9 171.18 7.50 14 -2 -9 194.38 7.40 14 -2 -9 191.08 7.40 14 2 -8 180.18 8.30 14 2 -8 210.38 8.00 14 -2 -8 210.18 8.10 14 -2 -8 203.98 7.90 14 2 -7 0.50 0.80 14 2 -7 0.40 0.80 14 -2 -7 1.20 0.70 14 -2 -7 0.50 0.60 14 2 -6 213.58 8.20 14 2 -6 194.08 8.40 14 -2 -6 202.78 8.20 14 -2 -6 206.68 8.10 14 2 -5 101.59 4.80 14 2 -5 93.29 4.80 14 -2 -5 105.19 4.60 14 -2 -5 107.89 4.40 14 2 -4 1.50 0.80 14 -2 -4 1.50 0.70 14 -2 -4 1.10 0.70 14 2 -3 132.39 5.80 14 -2 -3 136.69 5.60 14 -2 -3 130.39 5.50 14 2 -2 53.39 3.00 14 -2 -2 57.09 3.00 14 -2 -2 49.80 2.80 14 2 -1 0.00 0.90 14 -2 -1 1.90 0.70 14 -2 -1 0.10 0.60 14 2 0 6.10 1.40 14 2 0 6.00 1.70 14 -2 0 4.70 1.10 14 -2 0 5.70 1.10 14 2 1 21.30 1.60 14 2 1 20.30 2.00 14 -2 1 20.60 1.50 14 -2 1 20.50 1.60 14 2 2 3.50 0.70 14 2 2 3.00 0.90 14 -2 2 4.30 1.10 14 -2 2 4.10 1.10 14 2 3 5.30 1.10 14 2 3 8.50 1.30 14 -2 3 5.30 1.00 14 -2 3 6.20 1.40 14 2 4 1.20 0.60 14 2 4 1.70 0.60 14 -2 4 1.70 0.60 14 -2 4 1.20 0.70 14 -2 4 1.70 0.60 14 2 5 0.80 0.50 14 2 5 0.60 0.60 14 -2 5 1.30 0.60 14 -2 5 1.20 0.50 14 -2 5 0.80 0.50 14 2 6 25.60 1.40 14 2 6 26.80 1.50 14 -2 6 27.40 1.50 14 -2 6 24.10 1.40 14 2 7 3.10 0.80 14 2 7 3.20 0.80 14 -2 7 3.50 0.80 14 -3 -13 5.10 0.90 14 -3 -13 3.00 0.70 -14 3 12 1.30 0.60 14 3 -12 0.50 0.70 14 -3 -12 -0.40 0.50 14 3 -11 0.50 0.70 -14 3 11 1.10 0.70 14 -3 -11 1.20 0.50 14 -3 -11 0.60 0.40 14 3 -10 10.30 1.30 -14 3 10 13.00 1.20 14 3 -10 11.60 1.40 14 -3 -10 13.10 1.00 14 -3 -10 12.60 1.10 14 3 -9 58.39 3.20 -14 3 9 63.09 3.10 14 3 -9 59.39 3.00 14 -3 -9 65.19 2.90 14 -3 -9 66.09 2.90 14 3 -8 7.40 1.30 -14 3 8 6.80 1.20 14 -3 -8 8.90 1.00 14 -3 -8 10.40 1.20 14 3 -7 14.10 1.50 -14 3 7 13.50 1.40 14 -3 -7 14.80 1.40 14 -3 -7 15.50 1.30 -14 3 6 8.90 1.30 14 3 -6 9.80 1.40 14 -3 -6 8.40 1.30 14 -3 -6 9.20 1.10 -14 3 5 29.80 2.00 14 3 -5 30.30 2.10 14 -3 -5 31.70 1.90 14 -3 -5 33.40 2.00 14 3 -4 675.63 25.10 -14 3 4 662.73 25.30 14 3 -4 658.43 25.70 14 -3 -4 702.83 25.20 14 -3 -4 701.53 25.30 14 3 -3 401.96 16.10 14 3 -3 422.06 15.70 14 -3 -3 419.86 15.70 14 -3 -3 429.16 15.90 14 3 -2 99.69 4.20 14 3 -2 91.19 4.50 14 -3 -2 100.39 4.30 14 -3 -2 100.39 4.30 14 3 -1 80.29 3.90 14 3 -1 80.59 3.60 14 -3 -1 82.19 3.70 14 -3 -1 83.29 3.70 14 3 0 42.40 2.60 14 3 0 44.90 2.30 14 -3 0 45.50 2.30 14 -3 0 46.60 2.40 14 3 1 27.60 1.80 14 3 1 19.70 1.90 14 -3 1 25.40 1.60 14 -3 1 25.10 1.50 14 3 2 54.69 2.60 14 3 2 54.59 2.50 14 -3 2 49.60 3.00 14 -3 2 49.30 2.80 14 3 3 36.30 1.90 14 3 3 37.40 2.00 14 -3 3 36.20 1.90 14 -3 3 34.80 1.90 14 -3 3 32.70 2.10 14 3 4 166.68 6.60 14 3 4 168.88 6.70 14 -3 4 169.88 6.70 14 -3 4 173.48 6.70 14 -3 4 170.18 6.60 14 3 5 0.20 0.40 14 3 5 0.80 0.50 14 -3 5 0.50 0.50 14 -3 5 0.80 0.60 14 -3 5 0.00 0.60 14 3 6 32.70 1.60 14 3 6 33.40 1.60 14 -3 6 33.90 1.70 14 -3 6 35.90 1.70 14 3 7 10.30 0.90 14 -4 -12 0.30 0.40 -14 4 11 6.60 1.00 14 -4 -11 7.90 1.00 14 -4 -11 6.50 0.70 -14 4 10 0.70 0.70 14 4 -10 0.80 0.90 14 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143.59 5.50 16 -5 -8 10.20 0.70 16 -5 -7 0.30 0.40 16 -5 -7 -0.10 0.40 16 5 -6 3.80 1.20 16 -5 -6 0.20 0.40 16 5 -5 1.70 0.80 16 -5 -5 1.00 0.40 16 -5 -5 1.10 0.40 16 5 -4 11.50 1.30 16 -5 -4 12.80 0.90 16 5 -3 18.10 1.60 16 -5 -3 17.80 1.10 16 -5 -3 15.70 1.10 16 -5 -2 0.30 0.40 16 -5 -2 -0.30 0.40 16 -5 -1 42.30 2.10 16 -5 -1 39.40 1.80 16 5 0 -0.70 0.70 16 -5 0 1.10 0.40 16 -5 0 0.70 0.40 16 -5 1 23.40 1.20 16 -5 1 22.60 1.10 17 0 -12 23.00 1.30 17 0 -11 -0.10 0.40 -17 0 11 -1.30 0.70 17 0 -10 11.20 1.00 17 0 -9 0.90 0.50 17 0 -8 4.40 1.00 17 0 -7 0.20 0.60 17 0 -6 3.80 1.00 17 0 -5 -0.30 0.60 17 0 -4 43.70 2.30 17 0 -2 22.90 1.60 17 0 -1 1.60 0.80 17 -1 -12 44.20 2.00 -17 1 11 35.80 2.00 17 -1 -11 36.10 1.70 17 1 -10 37.00 1.80 -17 1 10 38.50 2.00 17 -1 -10 33.40 1.90 -17 1 9 31.00 1.90 17 1 -9 31.30 1.70 17 -1 -9 34.30 1.90 17 1 -8 16.20 1.30 17 -1 -8 16.30 1.40 17 1 -7 -0.30 0.60 17 -1 -7 -0.10 0.50 17 1 -6 49.20 2.70 17 1 -6 47.50 2.40 17 -1 -6 48.50 2.40 17 -1 -6 47.70 2.30 17 1 -5 16.00 1.60 17 1 -5 15.30 1.60 17 -1 -5 19.50 1.40 17 -1 -5 17.40 1.30 17 1 -4 13.70 1.70 17 -1 -4 13.80 1.40 17 -1 -4 16.30 1.30 17 -1 -3 5.50 1.10 17 -1 -3 7.50 1.10 17 -1 -2 1.10 0.70 17 -1 -2 0.20 0.50 17 -1 -1 26.60 1.60 17 -1 -1 24.80 1.60 17 -1 0 10.90 1.20 17 -1 0 12.40 1.10 17 -1 1 6.40 1.00 17 -1 1 5.60 1.10 17 -1 2 3.10 1.10 17 -1 3 19.50 1.30 17 -2 -11 16.60 1.00 -17 2 10 1.90 0.70 -17 2 9 2.60 0.80 17 -2 -9 1.30 0.60 17 -2 -9 4.10 1.00 -17 2 8 76.49 3.50 17 2 -8 74.59 3.50 17 -2 -8 77.39 3.20 17 -2 -8 72.99 3.30 17 2 -7 16.40 1.50 -17 2 7 17.70 1.60 17 -2 -7 16.80 1.20 17 -2 -7 19.10 1.50 -17 2 6 10.90 1.70 17 2 -6 12.10 1.40 17 -2 -6 13.20 1.10 17 -2 -6 13.00 1.10 17 2 -5 0.00 0.90 17 -2 -5 -0.20 0.50 17 -2 -5 -0.30 0.50 17 2 -4 0.50 1.50 17 -2 -4 0.80 0.60 17 -2 -4 0.60 0.50 17 2 -3 9.20 1.70 17 -2 -3 7.70 1.00 17 -2 -3 8.60 1.10 17 -2 -2 22.20 1.30 17 -2 -2 20.60 1.40 17 -2 -1 0.50 0.50 17 -2 -1 0.10 0.50 17 -2 0 30.20 1.60 17 -2 0 29.60 1.60 17 -2 1 30.90 1.70 17 -2 1 34.00 1.70 17 -2 2 4.30 0.90 17 -2 2 4.00 0.90 17 -2 3 77.29 3.10 17 -3 -10 8.30 0.80 17 -3 -10 8.20 0.90 17 -3 -9 45.10 2.00 17 -3 -9 43.80 2.00 17 3 -8 150.68 6.00 17 -3 -8 139.99 5.60 17 -3 -8 144.89 5.80 17 3 -7 3.20 0.90 17 -3 -7 2.00 0.50 17 -3 -7 2.80 0.70 17 3 -6 2.80 0.80 17 -3 -6 2.70 0.80 17 -3 -6 3.40 0.80 17 3 -5 36.10 2.10 17 -3 -5 32.90 1.80 17 -3 -5 31.50 1.70 17 3 -4 1.40 0.90 17 -3 -4 -0.30 0.50 17 -3 -4 0.10 0.40 17 3 -3 16.60 1.70 17 -3 -3 14.80 1.10 17 -3 -3 14.70 1.10 17 -3 -2 0.70 0.40 17 -3 -2 0.90 0.50 17 -3 -1 0.40 0.40 17 -3 -1 1.10 0.60 17 -3 0 11.20 0.90 17 -3 0 10.50 0.90 17 -3 1 21.70 1.20 17 -3 1 21.80 1.30 17 -3 2 3.70 0.70 17 -3 2 4.70 0.70 17 -3 3 12.80 0.80 17 -4 -9 31.60 1.50 17 -4 -9 34.80 1.50 17 -4 -8 0.10 0.40 17 -4 -8 0.50 0.40 17 4 -7 22.80 1.60 17 -4 -7 20.40 1.30 17 -4 -7 18.40 1.20 17 4 -6 5.40 1.10 17 -4 -6 5.50 0.70 17 -4 -6 5.90 0.70 17 4 -5 3.90 1.20 17 -4 -5 3.40 0.70 17 -4 -5 5.40 0.70 17 4 -4 2.00 1.10 17 -4 -4 2.50 0.60 17 -4 -4 3.00 1.00 17 -4 -3 21.30 1.20 17 -4 -3 23.10 1.30 17 -4 -2 -0.10 0.50 17 -4 -2 0.20 0.30 17 -4 -1 4.70 0.70 17 -4 -1 5.60 0.90 17 -4 0 7.40 0.80 17 -4 0 9.40 0.70 17 -4 1 55.89 2.30 17 -5 -6 0.70 0.30 17 -5 -6 1.10 0.50 17 -5 -5 4.80 0.60 17 -5 -5 4.30 0.70 17 -5 -4 2.10 0.50 17 -5 -4 1.80 0.60 17 -5 -3 2.10 0.60 17 -5 -3 1.80 0.60 17 -5 -2 1.20 0.40 17 -5 -2 1.50 0.40 18 0 -11 0.90 0.50 18 0 -10 55.09 2.40 18 0 -9 -0.40 0.50 18 0 -8 28.40 1.60 18 0 -7 0.40 0.50 18 0 -6 3.70 1.00 18 0 -5 0.50 0.60 18 0 -4 9.70 1.10 18 0 -3 -0.70 0.70 18 -1 -11 2.20 0.70 18 -1 -10 1.90 0.70 -18 1 9 97.59 4.10 18 1 -9 94.99 3.90 18 -1 -9 99.79 3.90 18 1 -8 31.80 1.70 -18 1 8 29.90 1.90 18 -1 -8 30.50 1.60 18 1 -7 1.30 1.20 -18 1 7 1.30 1.00 18 -1 -7 2.90 0.80 -18 1 6 97.99 4.40 18 -1 -6 102.89 4.10 18 -1 -5 7.80 1.00 18 -1 -4 1.50 0.60 18 -1 -3 26.60 1.50 18 -1 -2 1.40 0.60 18 -1 -1 44.00 2.20 18 -1 -1 46.20 2.30 18 -1 0 14.20 1.30 18 -2 -10 9.50 0.80 18 -2 -9 155.38 6.00 18 -2 -8 123.89 5.00 18 -2 -7 5.00 0.90 18 2 -6 45.40 2.50 18 -2 -6 48.10 2.30 18 2 -5 2.00 1.00 18 -2 -5 4.70 1.30 18 -2 -5 2.50 0.60 18 2 -4 46.40 2.70 18 -2 -4 45.80 2.10 18 -2 -4 44.60 2.10 18 -2 -3 7.80 1.00 18 -2 -3 9.00 0.90 18 -2 -2 54.69 2.40 18 -2 -2 52.39 2.40 18 -2 -1 21.10 1.30 18 -2 0 88.69 3.60 18 -2 0 88.19 3.50 18 -2 1 1.50 0.60 18 -3 -9 9.20 0.80 18 -3 -8 20.10 1.20 18 -3 -8 22.30 1.20 18 -3 -7 11.70 1.00 18 -3 -7 10.00 0.90 18 3 -6 11.10 1.50 18 -3 -6 8.30 1.00 18 -3 -6 9.70 0.80 18 -3 -5 18.10 1.10 18 -3 -5 18.60 1.30 18 -3 -4 19.50 1.20 18 -3 -4 18.10 1.10 18 -3 -3 56.19 2.50 18 -3 -3 58.09 2.50 18 -3 -2 -0.40 0.60 18 -3 -1 8.70 0.80 18 -3 -1 8.60 0.90 18 -3 0 41.50 1.80 18 -3 0 39.30 1.80 18 -4 -7 7.90 0.70 18 -4 -6 2.00 0.60 18 -4 -6 0.90 0.40 18 -4 -5 0.00 0.40 18 -4 -4 5.70 0.60 18 -4 -4 4.30 0.60 18 -4 -3 -0.50 0.40 18 -4 -3 -0.10 0.40 18 -4 -2 4.20 0.60 19 0 -9 -0.60 0.50 19 0 -8 21.10 1.30 19 0 -7 0.60 0.60 19 0 -6 0.10 0.60 19 0 -5 0.60 0.60 19 -1 -9 4.70 0.70 19 -1 -8 70.49 2.90 19 -1 -7 23.90 1.30 19 -1 -6 36.70 2.20 19 -1 -5 2.20 0.80 19 -1 -4 8.80 0.90 19 -1 -3 38.30 1.80 19 -1 -2 2.30 0.70 19 -2 -8 68.19 2.80 19 -2 -7 10.20 0.90 19 -2 -6 52.89 2.30 19 -2 -5 5.20 0.70 19 -2 -4 50.89 2.20 19 -2 -3 7.10 0.80 19 -2 -2 100.59 3.90 19 -3 -6 -0.10 0.30 19 -3 -5 -0.10 0.40 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 45756 _shelx_res_file ; TITL JTM1123_0ma_a.res in P2(1)/c JTM1123_0ma_a.res created by SHELXL-2018/1 at 16:05:42 on 10-Apr-2019 REM Old TITL JTM1123_0ma in P2(1)/c REM SHELXT solution in P2(1)/c REM R1 0.136, Rweak 0.004, Alpha 0.023, Orientation as input REM Formula found by SHELXT: C17 N O2 CELL 1.54178 16.2512 7.6859 13.0989 90.000 106.640 90.000 ZERR 4.000 0.0004 0.0002 0.0003 0.000 0.001 0.000 LATT 1 SYMM -X, 1/2+Y, 1/2-Z SFAC C H N O UNIT 68 92 4 8 TEMP -123 SIZE 0.136 0.195 0.242 L.S. 5 BOND $H LIST 4 FMAP 2 PLAN 5 CONF EQIV $1 x, -y+3/2, z-1/2 HTAB C2 O2_$1 HTAB C9 O1_$1 ACTA 141 MPLA N1 > C8 WGHT 0.047400 0.277500 EXTI 0.011433 FVAR 1.03437 O1 4 0.080321 0.559406 0.772935 11.00000 0.05779 0.05545 = 0.02499 0.00279 0.01694 0.00344 O2 4 0.176194 0.857735 0.724526 11.00000 0.07395 0.04833 = 0.04268 -0.01799 0.01907 -0.01243 N1 3 0.166641 0.698945 0.572099 11.00000 0.03832 0.03313 = 0.02720 -0.00162 0.01097 -0.00272 C1 1 0.132898 0.534695 0.533017 11.00000 0.02994 0.03268 = 0.02538 -0.00032 0.00723 0.00140 C2 1 0.133010 0.458916 0.437498 11.00000 0.03604 0.04302 = 0.02862 -0.00410 0.01285 -0.00060 H2 2 0.157030 0.519956 0.385734 11.00000 0.04520 C3 1 0.097072 0.293904 0.417009 11.00000 0.04210 0.04677 = 0.03845 -0.01406 0.01479 -0.00158 H3 2 0.095410 0.235048 0.348603 11.00000 0.05168 C4 1 0.061879 0.208832 0.487975 11.00000 0.04766 0.03653 = 0.05101 -0.00958 0.01777 -0.00677 H4 2 0.037182 0.094138 0.468819 11.00000 0.05946 C5 1 0.059855 0.287805 0.582443 11.00000 0.04177 0.03761 = 0.03943 0.00292 0.01488 -0.00192 H5 2 0.032950 0.231672 0.631945 11.00000 0.05211 C6 1 0.095760 0.452109 0.604331 11.00000 0.03382 0.03529 = 0.02508 0.00158 0.00862 0.00211 C7 1 0.104013 0.571371 0.693447 11.00000 0.03853 0.04078 = 0.02222 0.00202 0.00757 0.00387 C8 1 0.153389 0.731507 0.668247 11.00000 0.04260 0.03896 = 0.02703 -0.00352 0.00828 0.00059 C9 1 0.215914 0.808315 0.519708 11.00000 0.03936 0.03407 = 0.03595 0.00576 0.01132 -0.00140 H9A 2 0.219158 0.923270 0.554647 11.00000 0.04585 H9B 2 0.182481 0.820088 0.443547 11.00000 0.03871 C10 1 0.304167 0.732233 0.528136 11.00000 0.03652 0.03902 = 0.03573 0.00717 0.00922 -0.00101 H10A 2 0.340583 0.737403 0.604413 11.00000 0.05112 H10B 2 0.297904 0.604424 0.510665 11.00000 0.04439 C11 1 0.348129 0.821870 0.454445 11.00000 0.03749 0.03933 = 0.03809 0.00802 0.00952 -0.00220 H11A 2 0.357770 0.945669 0.475101 11.00000 0.05148 H11B 2 0.309353 0.819936 0.381200 11.00000 0.04555 C12 1 0.431660 0.734370 0.452969 11.00000 0.03673 0.04219 = 0.03873 0.00681 0.00941 -0.00157 H12A 2 0.473457 0.735711 0.525794 11.00000 0.05179 H12B 2 0.420651 0.610575 0.437232 11.00000 0.05217 C13 1 0.473447 0.812846 0.373724 11.00000 0.03710 0.04615 = 0.03702 0.00705 0.00861 -0.00109 H13A 2 0.483365 0.940457 0.389844 11.00000 0.05639 H13B 2 0.432278 0.805259 0.300987 11.00000 0.04949 C14 1 0.555969 0.722746 0.371275 11.00000 0.03675 0.04566 = 0.03780 0.00579 0.00883 -0.00143 H14A 2 0.599136 0.730331 0.443711 11.00000 0.05569 H14B 2 0.544771 0.595423 0.357531 11.00000 0.05736 C15 1 0.596150 0.795075 0.289025 11.00000 0.03837 0.04496 = 0.03640 0.00519 0.00903 -0.00156 H15A 2 0.605554 0.920912 0.301762 11.00000 0.05905 H15B 2 0.554214 0.786067 0.216512 11.00000 0.04772 C16 1 0.678446 0.704875 0.286618 11.00000 0.03876 0.05228 = 0.04352 0.00656 0.01179 -0.00064 H16A 2 0.721680 0.724741 0.356725 11.00000 0.06431 H16B 2 0.668791 0.574876 0.280838 11.00000 0.06793 C17 1 0.713352 0.767286 0.197619 11.00000 0.04961 0.05413 = 0.04862 -0.00011 0.02049 -0.00667 H17A 2 0.669541 0.753259 0.129069 11.00000 0.07045 H17B 2 0.727196 0.892098 0.205062 11.00000 0.08130 H17C 2 0.768659 0.698783 0.195163 11.00000 0.07638 HKLF 4 REM JTM1123_0ma_a.res in P2(1)/c REM R1 = 0.0351 for 2879 Fo > 4sig(Fo) and 0.0377 for all 3128 data REM 274 parameters refined using 0 restraints END WGHT 0.0474 0.2775 REM Highest difference peak 0.222, deepest hole -0.136, 1-sigma level 0.030 Q1 1 0.1084 0.4911 0.5679 11.00000 0.05 0.22 Q2 1 0.0974 0.4895 0.6455 11.00000 0.05 0.20 Q3 1 0.1235 0.6655 0.6795 11.00000 0.05 0.20 Q4 1 0.0665 0.3960 0.5845 11.00000 0.05 0.17 Q5 1 0.1224 0.5136 0.4825 11.00000 0.05 0.16 ; _shelx_res_checksum 70627 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy O O1 0.08032(5) 0.55941(11) 0.77294(5) 0.0450(2) Uani d 1 O O2 0.17619(6) 0.85773(11) 0.72453(7) 0.0545(3) Uani d 1 N N1 0.16664(5) 0.69895(11) 0.57210(6) 0.0326(2) Uani d 1 C C1 0.13290(6) 0.53470(13) 0.53302(7) 0.0295(2) Uani d 1 C C2 0.13301(6) 0.45892(14) 0.43750(8) 0.0351(2) Uani d 1 H H2 0.1570(8) 0.5200(17) 0.3857(10) 0.045(3) Uiso d 1 C C3 0.09707(7) 0.29390(15) 0.41701(9) 0.0418(3) Uani d 1 H H3 0.0954(9) 0.2350(19) 0.3486(11) 0.052(4) Uiso d 1 C C4 0.06188(8) 0.20883(15) 0.48797(10) 0.0443(3) Uani d 1 H H4 0.0372(9) 0.094(2) 0.4688(11) 0.059(4) Uiso d 1 C C5 0.05985(7) 0.28781(14) 0.58244(9) 0.0389(3) Uani d 1 H H5 0.0330(9) 0.2317(19) 0.6319(11) 0.052(4) Uiso d 1 C C6 0.09576(6) 0.45211(13) 0.60433(7) 0.0314(2) Uani d 1 C C7 0.10401(6) 0.57137(14) 0.69345(7) 0.0341(2) Uani d 1 C C8 0.15339(7) 0.73151(14) 0.66825(8) 0.0365(2) Uani d 1 C C9 0.21591(7) 0.80831(14) 0.51971(9) 0.0363(2) Uani d 1 H H9A 0.2192(8) 0.9233(18) 0.5546(10) 0.046(3) Uiso d 1 H H9B 0.1825(8) 0.8201(16) 0.4435(10) 0.039(3) Uiso d 1 C C10 0.30417(7) 0.73223(15) 0.52814(9) 0.0373(2) Uani d 1 H H10A 0.3406(9) 0.7374(18) 0.6044(12) 0.051(4) Uiso d 1 H H10B 0.2979(8) 0.6044(19) 0.5107(10) 0.044(3) Uiso d 1 C C11 0.34813(7) 0.82187(15) 0.45444(9) 0.0386(3) Uani d 1 H H11A 0.3578(9) 0.946(2) 0.4751(11) 0.051(4) Uiso d 1 H H11B 0.3094(8) 0.8199(17) 0.3812(11) 0.046(3) Uiso d 1 C C12 0.43166(7) 0.73437(15) 0.45297(9) 0.0395(3) Uani d 1 H H12A 0.4735(9) 0.7357(19) 0.5258(11) 0.052(4) Uiso d 1 H H12B 0.4207(9) 0.611(2) 0.4372(11) 0.052(4) Uiso d 1 C C13 0.47345(7) 0.81285(16) 0.37372(9) 0.0405(3) Uani d 1 H H13A 0.4834(9) 0.940(2) 0.3898(11) 0.056(4) Uiso d 1 H H13B 0.4323(9) 0.8053(17) 0.3010(11) 0.049(4) Uiso d 1 C C14 0.55597(7) 0.72275(16) 0.37127(9) 0.0405(3) Uani d 1 H H14A 0.5991(9) 0.7303(19) 0.4437(12) 0.056(4) Uiso d 1 H H14B 0.5448(9) 0.595(2) 0.3575(12) 0.057(4) Uiso d 1 C C15 0.59615(7) 0.79507(16) 0.28902(9) 0.0403(3) Uani d 1 H H15A 0.6056(9) 0.921(2) 0.3018(11) 0.059(4) Uiso d 1 H H15B 0.5542(9) 0.7861(17) 0.2165(11) 0.048(3) Uiso d 1 C C16 0.67845(8) 0.70487(17) 0.28662(10) 0.0448(3) Uani d 1 H H16A 0.7217(10) 0.725(2) 0.3567(13) 0.064(4) Uiso d 1 H H16B 0.6688(10) 0.575(2) 0.2808(13) 0.068(4) Uiso d 1 C C17 0.71335(9) 0.76729(19) 0.19762(11) 0.0494(3) Uani d 1 H H17A 0.6695(11) 0.753(2) 0.1291(14) 0.070(5) Uiso d 1 H H17B 0.7272(12) 0.892(3) 0.2051(14) 0.081(5) Uiso d 1 H H17C 0.7687(12) 0.699(2) 0.1952(14) 0.076(5) Uiso d 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 O1 0.0578(5) 0.0554(5) 0.0250(4) 0.0034(4) 0.0169(3) 0.0028(3) O2 0.0739(6) 0.0483(5) 0.0427(5) -0.0124(4) 0.0191(4) -0.0180(4) N1 0.0383(5) 0.0331(4) 0.0272(4) -0.0027(3) 0.0110(3) -0.0016(3) C1 0.0299(5) 0.0327(5) 0.0254(4) 0.0014(4) 0.0072(3) -0.0003(3) C2 0.0360(5) 0.0430(6) 0.0286(5) -0.0006(4) 0.0129(4) -0.0041(4) C3 0.0421(6) 0.0468(6) 0.0384(6) -0.0016(5) 0.0148(4) -0.0141(5) C4 0.0477(6) 0.0365(6) 0.0510(7) -0.0068(5) 0.0178(5) -0.0096(5) C5 0.0418(6) 0.0376(6) 0.0394(6) -0.0019(4) 0.0149(4) 0.0029(4) C6 0.0338(5) 0.0353(5) 0.0251(4) 0.0021(4) 0.0086(3) 0.0016(4) C7 0.0385(5) 0.0408(5) 0.0222(4) 0.0039(4) 0.0076(4) 0.0020(4) C8 0.0426(6) 0.0390(5) 0.0270(5) 0.0006(4) 0.0083(4) -0.0035(4) C9 0.0394(6) 0.0341(5) 0.0360(5) -0.0014(4) 0.0113(4) 0.0058(4) C10 0.0365(5) 0.0390(6) 0.0357(5) -0.0010(4) 0.0092(4) 0.0072(4) C11 0.0375(5) 0.0393(6) 0.0381(5) -0.0022(4) 0.0095(4) 0.0080(4) C12 0.0367(6) 0.0422(6) 0.0387(6) -0.0016(4) 0.0094(4) 0.0068(4) C13 0.0371(6) 0.0461(6) 0.0370(6) -0.0011(4) 0.0086(4) 0.0070(5) C14 0.0368(6) 0.0457(6) 0.0378(6) -0.0014(4) 0.0088(4) 0.0058(4) C15 0.0384(6) 0.0450(6) 0.0364(5) -0.0016(4) 0.0090(4) 0.0052(4) C16 0.0388(6) 0.0523(7) 0.0435(6) -0.0006(5) 0.0118(5) 0.0066(5) C17 0.0496(7) 0.0541(7) 0.0486(7) -0.0067(6) 0.0205(6) -0.0001(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle C8 N1 C1 110.61(8) C8 N1 C9 125.63(9) C1 N1 C9 123.52(8) C2 C1 C6 121.72(9) C2 C1 N1 127.18(9) C6 C1 N1 111.09(8) C1 C2 C3 116.77(9) C1 C2 H2 121.5(8) C3 C2 H2 121.7(8) C4 C3 C2 122.14(10) C4 C3 H3 118.6(8) C2 C3 H3 119.3(8) C3 C4 C5 120.75(10) C3 C4 H4 118.3(8) C5 C4 H4 120.9(8) C6 C5 C4 117.84(10) C6 C5 H5 120.4(8) C4 C5 H5 121.8(9) C5 C6 C1 120.73(9) C5 C6 C7 132.39(9) C1 C6 C7 106.87(8) O1 C7 C6 131.29(10) O1 C7 C8 123.52(9) C6 C7 C8 105.19(8) O2 C8 N1 127.53(10) O2 C8 C7 126.26(9) N1 C8 C7 106.20(8) N1 C9 C10 112.12(8) N1 C9 H9A 105.1(8) C10 C9 H9A 112.6(8) N1 C9 H9B 108.0(7) C10 C9 H9B 109.9(7) H9A C9 H9B 108.9(10) C11 C10 C9 112.57(9) C11 C10 H10A 111.3(8) C9 C10 H10A 109.3(8) C11 C10 H10B 109.4(7) C9 C10 H10B 109.0(7) H10A C10 H10B 104.9(11) C12 C11 C10 113.04(9) C12 C11 H11A 110.9(8) C10 C11 H11A 109.2(8) C12 C11 H11B 107.8(8) C10 C11 H11B 109.0(8) H11A C11 H11B 106.7(11) C13 C12 C11 114.13(9) C13 C12 H12A 109.5(8) C11 C12 H12A 110.4(8) C13 C12 H12B 109.4(8) C11 C12 H12B 108.8(8) H12A C12 H12B 104.1(12) C14 C13 C12 113.83(9) C14 C13 H13A 111.1(8) C12 C13 H13A 108.6(8) C14 C13 H13B 108.0(8) C12 C13 H13B 108.7(8) H13A C13 H13B 106.3(11) C15 C14 C13 114.24(9) C15 C14 H14A 108.8(8) C13 C14 H14A 109.6(8) C15 C14 H14B 108.9(8) C13 C14 H14B 109.5(8) H14A C14 H14B 105.5(12) C16 C15 C14 114.17(10) C16 C15 H15A 110.9(9) C14 C15 H15A 108.5(8) C16 C15 H15B 108.3(8) C14 C15 H15B 109.5(8) H15A C15 H15B 105.0(11) C17 C16 C15 113.51(10) C17 C16 H16A 109.9(9) C15 C16 H16A 107.7(9) C17 C16 H16B 109.9(9) C15 C16 H16B 109.6(9) H16A C16 H16B 105.9(13) C16 C17 H17A 109.7(10) C16 C17 H17B 111.0(10) H17A C17 H17B 106.5(15) C16 C17 H17C 112.2(9) H17A C17 H17C 108.7(14) H17B C17 H17C 108.6(14) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance O1 C7 1.2126(12) O2 C8 1.2106(13) N1 C8 1.3603(13) N1 C1 1.4127(13) N1 C9 1.4606(13) C1 C2 1.3806(13) C1 C6 1.4009(13) C2 C3 1.3899(16) C2 H2 0.992(13) C3 C4 1.3868(16) C3 H3 0.997(14) C4 C5 1.3871(16) C4 H4 0.971(16) C5 C6 1.3862(15) C5 H5 0.980(14) C6 C7 1.4599(13) C7 C8 1.5554(15) C9 C10 1.5233(15) C9 H9A 0.989(14) C9 H9B 0.994(13) C10 C11 1.5204(14) C10 H10A 1.006(15) C10 H10B 1.007(14) C11 C12 1.5200(16) C11 H11A 0.989(15) C11 H11B 0.986(14) C12 C13 1.5186(15) C12 H12A 1.000(14) C12 H12B 0.979(16) C13 C14 1.5178(16) C13 H13A 1.007(16) C13 H13B 0.997(14) C14 C15 1.5163(15) C14 H14A 1.007(15) C14 H14B 1.002(16) C15 C16 1.5147(17) C15 H15A 0.986(17) C15 H15B 1.000(14) C16 C17 1.5132(16) C16 H16A 0.995(17) C16 H16B 1.011(18) C17 H17A 0.979(18) C17 H17B 0.98(2) C17 H17C 1.050(18) loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag C2 H2 O2 4_575 0.992(13) 2.412(13) 3.3737(13) 163.3(10) yes C3 H3 O1 4_565 0.997(14) 2.454(15) 3.2734(14) 139.0(11) yes C9 H9B O1 4_575 0.994(13) 2.546(13) 3.5012(13) 161.0(10) yes C17 H17B O2 3_676 0.98(2) 2.49(2) 3.3941(17) 153.3(15) yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion C8 N1 C1 C2 178.81(10) C9 N1 C1 C2 -6.62(15) C8 N1 C1 C6 -0.19(11) C9 N1 C1 C6 174.37(9) C6 C1 C2 C3 -2.13(15) N1 C1 C2 C3 178.96(9) C1 C2 C3 C4 0.59(16) C2 C3 C4 C5 1.19(18) C3 C4 C5 C6 -1.41(17) C4 C5 C6 C1 -0.11(15) C4 C5 C6 C7 179.33(11) C2 C1 C6 C5 1.95(15) N1 C1 C6 C5 -178.98(9) C2 C1 C6 C7 -177.62(9) N1 C1 C6 C7 1.45(11) C5 C6 C7 O1 -1.08(19) C1 C6 C7 O1 178.42(11) C5 C6 C7 C8 178.52(11) C1 C6 C7 C8 -1.98(10) C1 N1 C8 O2 177.89(11) C9 N1 C8 O2 3.47(18) C1 N1 C8 C7 -1.07(11) C9 N1 C8 C7 -175.49(9) O1 C7 C8 O2 2.55(17) C6 C7 C8 O2 -177.09(11) O1 C7 C8 N1 -178.47(10) C6 C7 C8 N1 1.89(11) C8 N1 C9 C10 103.80(12) C1 N1 C9 C10 -69.94(12) N1 C9 C10 C11 167.45(9) C9 C10 C11 C12 -173.60(9) C10 C11 C12 C13 175.57(9) C11 C12 C13 C14 -178.95(10) C12 C13 C14 C15 177.47(10) C13 C14 C15 C16 -179.94(10) C14 C15 C16 C17 174.71(10) _cod_database_fobs_code 2243016