Crystallography Open Database

Information card for entry 4001289

Preview

Coordinates	4001289.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H112 Ge36 N10 O92
Calculated formula	C30 H112 Ge36 N10 O92
Title of publication	Synthesis and Characterization of a Novel Germanate Material Containing 16-Ring Channels and Templated by a Simple Primary Amine
Authors of publication	Attfield, Martin P.; Al-Ebini, Yousef; Pritchard, Robin G.; Andrews, Ellen M.; Charlesworth, Richard J.; Hung, Wan; Masheder, Ben J.; Royal, Drew S.
Journal of publication	Chemistry of Materials
Year of publication	2007
Journal volume	19
Journal issue	2
Pages of publication	316
a	24.9728 ± 0.0006 Å
b	24.9728 ± 0.0006 Å
c	9.8957 ± 0.0002 Å
α	90°
β	90°
γ	90°
Cell volume	6171.4 ± 0.2 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	5
Space group number	108
Hermann-Mauguin space group symbol	I 4 c m
Hall space group symbol	I 4 -2c
Residual factor for all reflections	0.0347
Residual factor for significantly intense reflections	0.027
Weighted residual factors for significantly intense reflections	0.0577
Weighted residual factors for all reflections included in the refinement	0.0598
Goodness-of-fit parameter for all reflections included in the refinement	0.973
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178377 (current)	2016-03-21	cif/4/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/00.	4001289.cif
120073	2014-07-11	Adding DOIs to range 4/00 structures.	4001289.cif
45158	2012-03-20	../uploads/cif-deposit/cod/cif Adding structures of 4001289 via cif-deposit CGI script.	4001289.cif