Crystallography Open Database

Information card for entry 4024584

Preview

Coordinates	4024584.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C13 H19 Br N2 O2
Calculated formula	C13 H19 Br N2 O2
Title of publication	Diastereoselective Synthesis of 2,3,6-Trisubstituted Piperidines
Authors of publication	John M. Humphrey; Eric P. Arnold; Thomas A. Chappie; John B. Feltenberger; Arthur Nagel; Wendy Simon; Melani Suarez-Contreras; Norma J. Tom; Brian T. O'Neill
Journal of publication	Journal of Organic Chemistry
Year of publication	2009
Journal volume	74
Pages of publication	4525 - 4536
a	9.696 ± 0.003 Å
b	11.925 ± 0.003 Å
c	13.189 ± 0.004 Å
α	90°
β	110.928 ± 0.005°
γ	90°
Cell volume	1424.37 Å³
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4024584.cif
120074	2014-07-11	Adding DOIs to range 4/02 structures.	4024584.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4024584.cif
966	2010-01-30	cif/ Adding _cod_database_code tags to all COD entries. Adding tag description to the cif_cod.dic dictionary so that COD entries can be validated.	4024584.cif
948	2010-01-19	cif/ Adding CIFs for the Acta-Cryst-B-2009_06/ Acta-Cryst-C-2009_12/ Acta-Cryst-E-2009_12/ J-Appl-Cryst-2009_06/ J-Org-Chem-2009/ deposition.	4024584.cif