#------------------------------------------------------------------------------ #$Date: 2022-05-22 15:40:35 +0300 (Sun, 22 May 2022) $ #$Revision: 275610 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/4/03/89/4038996.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4038996 _cell_angle_alpha 90.000 _cell_angle_beta 102.164 _cell_angle_gamma 90.000 _cell_length_a 6.1658 _cell_length_b 17.1862 _cell_length_c 8.8111 _exptl_crystal_F_000 432.00 _reflns_d_resolution_high 0.8101 _cod_data_source_file bent35.fcf _cod_data_source_block bent35 _shelx_title ' bent35_a.res in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 119.82 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 5848.89 4155.39 68.09 o 2 0 0 873.21 883.20 14.60 o 3 0 0 507.26 519.14 8.69 o 4 0 0 960.60 1071.16 17.85 o 5 0 0 0.71 0.85 0.22 o 6 0 0 20.71 21.10 0.79 o 7 0 0 51.47 51.21 1.94 o 1 1 0 1.47 3.07 0.17 o 2 1 0 157.32 137.98 1.67 o 3 1 0 8.42 7.52 0.19 o 4 1 0 23.61 27.55 0.48 o 5 1 0 0.09 0.13 0.16 o 6 1 0 0.03 0.20 0.15 o 7 1 0 4.45 3.98 0.29 o 0 2 0 14357.51 9513.71 292.03 o 1 2 0 50.26 44.97 0.74 o 2 2 0 1091.15 1180.80 14.29 o 3 2 0 114.25 103.15 1.33 o 4 2 0 857.26 967.87 13.52 o 5 2 0 249.85 247.88 4.36 o 6 2 0 100.74 108.07 1.97 o 7 2 0 5.74 5.86 0.32 o 1 3 0 1606.24 1613.55 26.53 o 2 3 0 1273.70 1336.32 15.58 o 3 3 0 41.29 40.94 0.62 o 4 3 0 77.49 79.93 1.31 o 5 3 0 12.37 11.88 0.55 o 6 3 0 52.80 51.88 1.46 o 7 3 0 1.95 1.55 0.23 o 0 4 0 0.19 0.17 0.07 o 1 4 0 264.01 210.19 2.68 o 2 4 0 15.96 17.46 0.27 o 3 4 0 7.27 8.77 0.23 o 4 4 0 126.35 134.07 2.07 o 5 4 0 34.18 33.64 0.87 o 6 4 0 458.17 478.86 7.66 o 7 4 0 94.31 90.04 1.98 o 1 5 0 0.91 1.38 0.10 o 2 5 0 171.88 159.48 2.19 o 3 5 0 77.34 70.35 1.06 o 4 5 0 212.61 207.50 3.25 o 5 5 0 70.41 72.49 1.55 o 6 5 0 18.37 20.95 0.65 o 7 5 0 4.94 4.35 0.27 o 0 6 0 440.13 451.46 11.48 o 1 6 0 1157.97 1294.16 21.31 o 2 6 0 390.64 443.24 6.19 o 3 6 0 558.45 607.35 8.97 o 4 6 0 143.82 139.83 2.29 o 5 6 0 0.00 0.03 0.18 o 6 6 0 67.02 69.38 1.44 o 7 6 0 87.09 87.74 2.12 o 1 7 0 4.61 6.55 0.27 o 2 7 0 537.77 596.95 9.94 o 3 7 0 15.90 17.10 0.42 o 4 7 0 64.01 61.76 1.00 o 5 7 0 3.28 3.16 0.30 o 6 7 0 6.98 6.42 0.53 o 7 7 0 32.51 29.97 0.97 o 0 8 0 944.75 1094.29 24.43 o 1 8 0 564.62 630.83 10.49 o 2 8 0 833.82 939.25 14.56 o 3 8 0 0.31 0.62 0.12 o 4 8 0 306.85 283.27 3.97 o 5 8 0 46.56 46.57 1.10 o 6 8 0 35.77 37.16 1.04 o 1 9 0 152.74 174.46 3.02 o 2 9 0 46.39 40.36 0.78 o 3 9 0 98.87 106.78 2.34 o 4 9 0 32.70 27.09 0.76 o 5 9 0 75.93 74.16 1.67 o 6 9 0 9.51 9.75 0.48 o 0 10 0 27.26 25.73 0.94 o 1 10 0 8.10 9.13 0.30 o 2 10 0 239.13 222.70 3.86 o 3 10 0 0.30 0.18 0.14 o 4 10 0 326.94 314.08 5.51 o 5 10 0 205.21 217.98 4.22 o 6 10 0 22.82 23.89 1.30 o 1 11 0 17.64 19.65 0.53 o 2 11 0 11.97 9.41 0.40 o 3 11 0 228.50 208.77 3.13 o 4 11 0 48.27 46.99 1.30 o 5 11 0 106.17 106.43 2.20 o 6 11 0 0.48 -0.07 0.20 o 0 12 0 2.10 2.79 0.37 o 1 12 0 35.77 32.84 0.78 o 2 12 0 389.07 339.56 4.49 o 3 12 0 0.58 0.57 0.27 o 4 12 0 1.56 0.93 0.24 o 5 12 0 1.28 0.45 0.21 o 6 12 0 57.61 47.43 1.47 o 1 13 0 94.15 89.89 1.27 o 2 13 0 146.35 135.00 1.95 o 3 13 0 86.55 83.62 2.26 o 4 13 0 6.24 5.32 0.45 o 5 13 0 25.08 25.60 0.86 o 0 14 0 93.36 81.80 1.67 o 1 14 0 422.62 434.68 6.25 o 2 14 0 410.38 414.93 6.69 o 3 14 0 0.55 0.16 0.21 o 4 14 0 17.14 17.34 0.77 o 5 14 0 0.03 0.00 0.21 o 1 15 0 58.63 56.78 1.30 o 2 15 0 993.33 1052.53 24.12 o 3 15 0 20.11 20.71 0.85 o 4 15 0 12.21 11.94 0.60 o 5 15 0 47.34 45.55 2.32 o 0 16 0 131.73 138.69 3.54 o 1 16 0 4.48 4.35 0.36 o 2 16 0 12.20 8.04 0.61 o 3 16 0 55.32 52.51 2.00 o 4 16 0 10.47 10.30 0.51 o 1 17 0 1.31 0.56 0.23 o 2 17 0 5.49 3.47 0.36 o 3 17 0 0.94 2.11 0.30 o 4 17 0 1.03 0.41 0.21 o 0 18 0 56.16 57.54 1.95 o 1 18 0 11.29 12.10 0.54 o 2 18 0 29.22 31.29 0.82 o 3 18 0 9.33 8.85 0.47 o 1 19 0 25.17 26.00 1.00 o 2 19 0 54.10 60.55 1.30 o 3 19 0 0.04 -0.12 0.16 o 0 20 0 63.79 85.58 2.47 o 1 20 0 39.22 47.87 1.05 o 2 20 0 22.65 20.33 0.65 o 1 21 0 28.86 29.96 1.21 o -7 1 1 19.36 18.78 0.70 o -6 1 1 1.60 1.01 0.21 o -5 1 1 3.29 3.57 0.19 o -4 1 1 0.55 1.87 0.13 o -3 1 1 1620.48 2004.25 23.37 o -2 1 1 90.41 105.95 1.70 o -1 1 1 1176.83 1163.44 16.86 o 0 1 1 60.66 49.06 1.11 o 1 1 1 9.45 7.27 0.20 o 2 1 1 1137.81 1244.00 15.67 o 3 1 1 215.10 211.45 3.39 o 4 1 1 467.19 496.46 9.97 o 5 1 1 0.00 0.11 0.17 o 6 1 1 0.18 0.45 0.18 o 7 1 1 0.49 0.07 0.24 o -7 2 1 0.23 0.06 0.16 o -6 2 1 25.28 25.99 0.81 o -5 2 1 73.84 70.29 0.94 o -4 2 1 25.89 25.81 0.46 o -3 2 1 20.38 26.14 0.54 o -2 2 1 2203.66 2376.57 42.57 o -1 2 1 5067.15 4073.04 66.33 o 0 2 1 21.85 20.60 0.44 o 1 2 1 113.84 123.60 2.19 o 2 2 1 1450.55 1522.73 19.17 o 3 2 1 733.66 747.77 11.63 o 4 2 1 36.71 36.12 0.90 o 5 2 1 5.59 4.63 0.36 o 6 2 1 24.32 25.44 0.68 o 7 2 1 27.71 26.71 0.91 o -7 3 1 380.50 397.86 7.27 o -6 3 1 507.66 571.98 10.58 o -5 3 1 0.20 0.38 0.16 o -4 3 1 104.54 115.04 1.51 o -3 3 1 759.00 883.07 10.37 o -2 3 1 0.17 0.22 0.05 o -1 3 1 14.77 10.45 0.22 o 0 3 1 15.68 16.41 0.31 o 1 3 1 55.14 43.80 0.69 o 2 3 1 114.27 102.09 1.43 o 3 3 1 37.18 35.97 0.69 o 4 3 1 322.54 342.87 6.37 o 5 3 1 19.08 17.43 0.74 o 6 3 1 11.34 11.35 0.47 o 7 3 1 196.34 174.91 4.58 o -7 4 1 9.74 10.19 0.56 o -6 4 1 8.08 8.09 0.48 o -5 4 1 46.94 43.86 1.13 o -4 4 1 71.67 61.74 0.93 o -3 4 1 92.67 99.02 1.27 o -2 4 1 11.71 12.81 0.26 o 0 4 1 4625.01 4113.62 72.94 o 1 4 1 3754.70 3589.07 55.10 o 2 4 1 35.62 34.80 0.58 o 3 4 1 8.47 8.76 0.28 o 4 4 1 22.85 25.52 0.79 o 5 4 1 50.23 45.48 1.02 o 6 4 1 17.65 19.10 0.55 o 7 4 1 46.09 39.76 1.57 o -7 5 1 219.99 223.21 4.58 o -6 5 1 292.26 302.30 6.31 o -5 5 1 0.84 0.73 0.23 o -4 5 1 239.33 222.47 3.45 o -3 5 1 558.47 618.28 7.30 o -2 5 1 1081.40 1215.75 16.77 o -1 5 1 126.25 135.20 2.02 o 0 5 1 204.57 181.84 2.86 o 1 5 1 44.42 38.50 0.99 o 2 5 1 67.63 69.48 1.19 o 3 5 1 570.87 590.93 10.67 o 4 5 1 154.56 157.53 2.21 o 5 5 1 46.19 44.88 1.00 o 6 5 1 1.59 1.18 0.21 o 7 5 1 109.43 100.75 2.72 o -7 6 1 2.32 2.03 0.21 o -6 6 1 24.53 26.65 0.88 o -5 6 1 109.30 110.28 2.53 o -4 6 1 142.56 137.83 2.24 o -3 6 1 8.11 6.41 0.26 o -2 6 1 31.83 29.64 0.51 o -1 6 1 14.15 17.83 0.36 o 0 6 1 5.02 6.84 0.19 o 1 6 1 30.08 36.49 0.74 o 2 6 1 30.44 32.24 0.62 o 3 6 1 92.83 84.86 1.59 o 4 6 1 5.22 5.73 0.28 o 5 6 1 77.56 75.27 1.59 o 6 6 1 47.50 48.12 1.06 o -7 7 1 26.76 26.45 0.71 o -6 7 1 12.64 12.31 0.63 o -5 7 1 0.84 0.66 0.22 o -4 7 1 0.94 1.16 0.15 o -3 7 1 407.47 434.30 5.84 o -2 7 1 647.80 748.74 11.63 o -1 7 1 559.28 575.85 8.44 o 0 7 1 1224.27 1434.65 22.14 o 1 7 1 1164.13 1325.08 20.45 o 2 7 1 269.46 271.04 4.31 o 3 7 1 201.65 208.22 3.92 o 4 7 1 219.78 221.14 3.14 o 5 7 1 0.19 0.46 0.23 o 6 7 1 5.36 5.68 0.64 o -7 8 1 15.62 14.19 1.04 o -6 8 1 31.49 32.16 0.95 o -5 8 1 0.20 0.15 0.19 o -4 8 1 6.05 4.45 0.22 o -3 8 1 42.82 33.18 0.66 o -2 8 1 223.98 227.36 3.96 o -1 8 1 179.34 187.83 2.84 o 0 8 1 168.23 183.32 2.94 o 1 8 1 0.68 1.42 0.27 o 2 8 1 48.37 52.22 1.07 o 3 8 1 170.97 173.80 3.66 o 4 8 1 0.68 0.09 0.22 o 5 8 1 17.22 19.04 0.69 o 6 8 1 3.40 3.31 0.32 o -6 9 1 0.01 0.06 0.19 o -5 9 1 480.38 465.12 7.95 o -4 9 1 389.60 351.00 5.65 o -3 9 1 111.16 101.02 2.02 o -2 9 1 245.69 232.26 3.98 o -1 9 1 367.94 379.40 5.63 o 0 9 1 763.92 864.76 14.34 o 1 9 1 717.83 817.02 12.71 o 2 9 1 283.87 302.04 5.16 o 3 9 1 148.34 132.41 2.28 o 4 9 1 100.72 101.27 2.41 o 5 9 1 258.05 275.09 5.79 o 6 9 1 218.97 232.09 4.79 o -6 10 1 3.85 3.22 0.33 o -5 10 1 100.70 97.87 2.07 o -4 10 1 300.36 270.48 4.76 o -3 10 1 88.30 78.01 1.46 o -2 10 1 251.60 223.75 4.20 o -1 10 1 120.68 138.71 2.48 o 0 10 1 51.00 36.13 0.78 o 1 10 1 83.67 72.95 1.30 o 2 10 1 39.10 43.47 1.01 o 3 10 1 65.85 55.00 0.91 o 4 10 1 61.06 62.14 1.50 o 5 10 1 64.75 74.27 1.84 o 6 10 1 0.46 0.75 0.24 o -6 11 1 10.10 12.21 0.50 o -5 11 1 806.00 794.06 14.41 o -4 11 1 241.27 216.16 5.64 o -3 11 1 290.82 244.14 3.97 o -2 11 1 169.80 164.32 3.17 o -1 11 1 1.53 1.16 0.16 o 0 11 1 192.93 218.21 3.56 o 1 11 1 152.17 170.46 2.83 o 2 11 1 0.13 0.57 0.23 o 3 11 1 107.93 100.22 1.85 o 4 11 1 132.45 126.94 2.63 o 5 11 1 235.59 247.82 5.17 o 6 11 1 372.28 371.08 8.30 o -6 12 1 0.04 0.00 0.61 o -5 12 1 10.59 9.86 0.45 o -4 12 1 1.78 1.01 0.23 o -3 12 1 18.24 14.85 0.63 o -2 12 1 9.49 8.67 0.34 o -1 12 1 7.28 7.36 0.46 o 0 12 1 19.27 13.79 0.48 o 1 12 1 10.52 13.75 0.47 o 2 12 1 0.03 0.04 0.12 o 3 12 1 7.86 7.09 0.45 o 4 12 1 5.45 5.30 0.36 o 5 12 1 17.81 17.71 0.66 o -5 13 1 109.82 93.17 2.08 o -4 13 1 211.85 190.68 4.03 o -3 13 1 647.69 611.72 12.25 o -2 13 1 198.59 182.49 2.64 o -1 13 1 542.60 530.84 6.36 o 0 13 1 1141.61 1184.06 13.96 o 1 13 1 1184.90 1216.17 13.86 o 2 13 1 305.29 310.69 6.19 o 3 13 1 120.97 120.51 3.22 o 4 13 1 285.72 301.06 5.25 o 5 13 1 76.64 75.45 1.73 o -5 14 1 0.42 0.06 0.26 o -4 14 1 264.24 250.08 5.79 o -3 14 1 9.32 8.18 0.74 o -2 14 1 188.47 182.37 3.33 o -1 14 1 23.02 19.81 0.54 o 0 14 1 5.40 5.95 0.28 o 1 14 1 108.36 106.84 1.97 o 2 14 1 106.60 110.94 2.02 o 3 14 1 219.48 240.14 5.08 o 4 14 1 16.25 16.52 0.87 o 5 14 1 176.78 173.51 4.04 o -5 15 1 0.92 0.12 0.37 o -4 15 1 1.35 0.61 0.24 o -3 15 1 38.14 33.49 1.12 o -2 15 1 169.19 148.46 2.77 o -1 15 1 497.29 506.08 8.11 o 0 15 1 303.49 309.78 5.12 o 1 15 1 230.01 238.92 4.01 o 2 15 1 463.58 483.19 8.59 o 3 15 1 60.66 57.31 1.46 o 4 15 1 20.99 21.62 0.69 o 5 15 1 1.57 1.74 0.26 o -4 16 1 35.43 33.89 1.42 o -3 16 1 12.61 11.32 0.62 o -2 16 1 3.39 3.48 0.30 o -1 16 1 438.82 418.14 6.74 o 0 16 1 142.51 145.07 2.57 o 1 16 1 110.81 115.32 2.16 o 2 16 1 182.46 177.05 3.04 o 3 16 1 14.39 14.87 0.61 o 4 16 1 9.25 9.53 0.53 o -4 17 1 28.28 29.10 2.13 o -3 17 1 1.71 2.24 0.29 o -2 17 1 26.88 22.25 0.65 o -1 17 1 56.97 56.16 1.18 o 0 17 1 0.26 0.45 0.19 o 1 17 1 7.00 7.15 0.40 o 2 17 1 158.32 161.60 2.94 o 3 17 1 16.76 16.59 0.60 o 4 17 1 0.14 0.40 0.18 o -4 18 1 10.65 11.21 0.97 o -3 18 1 11.69 11.73 0.52 o -2 18 1 34.68 36.54 0.91 o -1 18 1 217.72 214.02 3.61 o 0 18 1 26.90 27.11 0.68 o 1 18 1 20.58 20.09 0.57 o 2 18 1 135.40 136.52 3.07 o 3 18 1 11.21 10.37 0.50 o -3 19 1 13.90 16.76 0.82 o -2 19 1 8.42 7.49 0.44 o -1 19 1 9.72 10.93 0.44 o 0 19 1 12.65 12.92 0.49 o 1 19 1 5.64 5.09 0.31 o 2 19 1 11.84 12.80 0.53 o 3 19 1 12.11 12.06 0.44 o -2 20 1 12.46 18.08 0.70 o -1 20 1 10.38 9.82 0.52 o 0 20 1 11.78 13.45 0.46 o 1 20 1 14.12 14.35 0.46 o 2 20 1 2.75 1.92 0.19 o 0 21 1 18.34 18.50 0.61 o -7 0 2 11.36 12.84 0.58 o -6 0 2 98.28 106.46 2.86 o -5 0 2 79.40 82.60 1.44 o -4 0 2 0.00 3.67 0.40 o -3 0 2 2062.75 2607.20 56.76 o -2 0 2 1410.47 1554.84 33.85 o -1 0 2 1964.33 1865.86 75.55 o 0 0 2 8034.35 6427.91 179.24 o 2 0 2 812.12 936.72 23.70 o 3 0 2 104.42 104.65 2.92 o 4 0 2 45.24 39.94 1.10 o 5 0 2 252.80 240.94 6.67 o 6 0 2 0.46 0.28 0.28 o 7 0 2 4.20 5.24 0.73 o -7 1 2 33.59 33.69 0.74 o -6 1 2 36.60 38.10 0.93 o -5 1 2 3.40 2.32 0.16 o -4 1 2 10.12 8.76 0.28 o -3 1 2 48.25 58.78 1.03 o -2 1 2 26.54 23.59 0.42 o -1 1 2 6.30 3.24 0.24 o 0 1 2 176.57 174.68 3.15 o 1 1 2 3657.92 3802.44 58.36 o 2 1 2 0.21 0.87 0.13 o 3 1 2 101.45 97.19 1.66 o 4 1 2 9.09 6.56 0.34 o 5 1 2 73.94 77.70 1.66 o 6 1 2 0.37 0.03 0.17 o 7 1 2 0.59 0.81 0.38 o -7 2 2 2.66 2.90 0.22 o -6 2 2 13.82 13.05 0.57 o -5 2 2 142.51 143.66 1.62 o -4 2 2 671.76 770.33 9.14 o -3 2 2 1376.72 1764.19 27.20 o -2 2 2 181.70 176.94 2.81 o -1 2 2 1092.25 1132.50 17.44 o 0 2 2 9.31 9.13 0.24 o 1 2 2 6852.18 6586.06 111.22 o 2 2 2 36.01 40.84 0.74 o 3 2 2 347.62 362.17 5.53 o 4 2 2 19.82 17.24 0.45 o 5 2 2 321.26 324.75 5.33 o 6 2 2 54.36 56.89 1.65 o -7 3 2 0.15 0.27 0.16 o -6 3 2 14.37 14.46 0.59 o -5 3 2 321.72 314.76 4.07 o -4 3 2 191.19 227.25 2.82 o -3 3 2 322.28 379.09 5.96 o -2 3 2 63.97 65.47 1.05 o -1 3 2 1992.28 2036.64 35.35 o 0 3 2 1903.63 1935.75 31.23 o 1 3 2 2.30 2.72 0.16 o 2 3 2 282.52 281.98 4.46 o 3 3 2 227.99 228.49 3.69 o 4 3 2 5.85 4.54 0.24 o 5 3 2 2.83 3.12 0.45 o 6 3 2 0.25 0.41 0.23 o -7 4 2 42.94 41.24 1.05 o -6 4 2 236.94 254.34 6.05 o -5 4 2 798.74 828.94 13.11 o -4 4 2 57.70 64.62 0.93 o -3 4 2 213.56 244.02 4.40 o -2 4 2 38.92 32.62 0.57 o -1 4 2 79.56 63.68 1.06 o 0 4 2 44.53 30.68 0.56 o 1 4 2 0.23 0.43 0.07 o 2 4 2 155.59 144.90 2.35 o 3 4 2 71.02 72.07 1.39 o 4 4 2 0.78 1.00 0.15 o 5 4 2 55.03 59.53 1.34 o 6 4 2 9.28 10.28 0.45 o -7 5 2 61.56 61.12 1.43 o -6 5 2 3.88 4.41 0.43 o -5 5 2 0.65 0.58 0.24 o -4 5 2 134.44 137.59 2.11 o -3 5 2 260.59 260.30 3.53 o -2 5 2 9.88 6.73 0.19 o -1 5 2 290.23 277.13 4.10 o 0 5 2 13.05 16.20 0.32 o 1 5 2 5.37 4.22 0.16 o 2 5 2 1.26 1.39 0.13 o 3 5 2 33.22 34.16 0.70 o 4 5 2 78.18 73.49 1.11 o 5 5 2 88.65 96.96 1.96 o 6 5 2 27.32 29.79 0.74 o -7 6 2 28.91 27.45 0.75 o -6 6 2 149.95 163.56 3.61 o -5 6 2 121.92 119.25 2.77 o -4 6 2 1.63 1.54 0.17 o -3 6 2 620.40 624.14 9.74 o -2 6 2 897.55 975.75 13.51 o -1 6 2 689.11 830.30 12.84 o 0 6 2 831.50 861.66 14.25 o 1 6 2 269.72 263.73 4.16 o 2 6 2 443.36 440.58 6.91 o 3 6 2 100.52 109.49 1.88 o 4 6 2 177.31 176.45 3.00 o 5 6 2 13.40 14.18 0.68 o 6 6 2 0.76 0.76 0.18 o -7 7 2 1.04 0.76 0.17 o -6 7 2 122.41 126.70 2.83 o -5 7 2 2.99 2.40 0.45 o -4 7 2 0.03 0.01 0.11 o -3 7 2 129.79 139.11 2.46 o -2 7 2 1.18 1.26 0.09 o -1 7 2 298.92 334.11 5.26 o 0 7 2 79.12 74.74 1.26 o 1 7 2 30.42 30.32 0.60 o 2 7 2 87.34 86.08 1.77 o 3 7 2 325.35 327.49 5.93 o 4 7 2 21.57 22.12 0.75 o 5 7 2 12.80 13.22 0.63 o 6 7 2 6.28 6.21 0.44 o -7 8 2 1.65 1.41 0.24 o -6 8 2 1.51 1.88 0.28 o -5 8 2 78.95 73.84 1.75 o -4 8 2 44.49 40.16 0.70 o -3 8 2 554.53 508.59 7.16 o -2 8 2 5.95 7.17 0.30 o -1 8 2 1067.00 1260.58 19.50 o 0 8 2 415.54 467.84 7.33 o 1 8 2 558.16 599.73 9.37 o 2 8 2 298.56 311.65 5.31 o 3 8 2 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