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Information card for entry 4075197
Preview
| Coordinates | 4075197.cif |
|---|---|
| Original paper (by DOI) | HTML |
| External links | PubChem |
| Chemical name | NOTE: This is compound 1 |
|---|---|
| Formula | C30 H42 Ge2 |
| Calculated formula | C30 H42 Ge2 |
| SMILES | [Ge]([Ge](CCCC)(CCCC)CCCC)(c1ccccc1)(c1ccccc1)c1ccccc1 |
| Title of publication | Preparation of Oligogermanes via the Hydrogermolysis Reaction |
| Authors of publication | Subashi, Esla; Rheingold, Arnold L.; Weinert, Charles S. |
| Journal of publication | Organometallics |
| Year of publication | 2006 |
| Journal volume | 25 |
| Journal issue | 13 |
| Pages of publication | 3211 |
| a | 10.051 ± 0.003 Å |
| b | 15.141 ± 0.004 Å |
| c | 20.97 ± 0.006 Å |
| α | 109.043 ± 0.004° |
| β | 100.239 ± 0.004° |
| γ | 98.645 ± 0.004° |
| Cell volume | 2893.2 ± 1.4 Å3 |
| Cell temperature | 215 ± 2 K |
| Ambient diffraction temperature | 215 ± 2 K |
| Number of distinct elements | 3 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0832 |
| Residual factor for significantly intense reflections | 0.0485 |
| Weighted residual factors for significantly intense reflections | 0.1199 |
| Weighted residual factors for all reflections included in the refinement | 0.14 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.004 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 301830 (current) | 2025-08-20 | Add cross-references to PubChem compounds in COD range 4/07/ Each referenced PubChem compound corresponds to the full crystal structure. |
4075197.cif |
| 178640 | 2016-03-21 | cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/51. |
4075197.cif |
| 120075 | 2014-07-11 | Adding DOIs to range 4/07 structures. | 4075197.cif |
| 49114 | 2012-03-27 | ../uploads/cif-deposit/cod/cif Adding structures of 4075197, 4075198 via cif-deposit CGI script. |
4075197.cif |
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Users of the data should acknowledge the original authors of the
structural data.