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Information card for entry 4077692
Preview
| Coordinates | 4077692.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C33 H68 O14 S Sn6 |
|---|---|
| Calculated formula | C33 H67 O14 S Sn6 |
| Title of publication | Reaction of Butyltin Hydroxide Oxide withp-Toluenesulfonic Acid: Synthesis, X-ray Crystal Analysis, and Multinuclear NMR Characterization of {(BuSn)12O14(OH)6}(4-CH3C6H4SO3)2 |
| Authors of publication | Eychenne-Baron, Christophe; Ribot, François; Steunou, Nathalie; Sanchez, Clément; Fayon, Franck; Biesemans, Monique; Martins, José C.; Willem, Rudolph |
| Journal of publication | Organometallics |
| Year of publication | 2000 |
| Journal volume | 19 |
| Journal issue | 10 |
| Pages of publication | 1940 |
| a | 12.722 Å |
| b | 14.07 Å |
| c | 16.014 Å |
| α | 114.003° |
| β | 96.616° |
| γ | 104.237° |
| Cell volume | 2462.03 Å3 |
| Cell temperature | 298 K |
| Ambient diffraction temperature | 298 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for significantly intense reflections | 0.0326 |
| Weighted residual factors for significantly intense reflections | 0.034 |
| Goodness-of-fit parameter for significantly intense reflections | 2.1619 |
| Diffraction radiation wavelength | 0.71069 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 211332 (current) | 2018-10-05 | cif/ Fixing enumeration values for CIF data items _atom_sites_solution_* using cif_fix_values. Data item relocations and exclusion of CIF comment lines might have occurred due to the usage of cif_filter. |
4077692.cif |
| 176467 | 2016-02-16 | cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4. |
4077692.cif |
| 131566 | 2015-02-08 | cif/ Changing empty string values "' '" into "." in range 4. In case of "_symmetry_cell_setting" tag values were added after consulting the original papers. |
4077692.cif |
| 91935 | 2013-12-29 | cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs. |
4077692.cif |
| 54672 | 2012-04-28 | cif/ Adding structures of 4077692 via cif-deposit CGI script. |
4077692.cif |
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Users of the data should acknowledge the original authors of the
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