#------------------------------------------------------------------------------ #$Date: 2016-03-21 15:20:55 +0200 (Mon, 21 Mar 2016) $ #$Revision: 178744 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/08/55/4085533.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4085533 loop_ _publ_author_name 'Evans, Daniel A.' 'Lee, Lucia Myongwon' 'Vargas-Baca, Ignacio' 'Cowley, Alan H.' _publ_section_title ; Aggregation-Induced Emission of Bis(imino)acenaphthene Zinc Complexes: Photophysical Tuning via Methylation of the Flanking Aryl Substituents ; _journal_issue 11 _journal_name_full Organometallics _journal_page_first 2422 _journal_paper_doi 10.1021/om501191c _journal_volume 34 _journal_year 2015 _chemical_formula_moiety 'C28 H24 Cl2 N2 Zn' _chemical_formula_sum 'C28 H24 Cl2 N2 Zn' _chemical_formula_weight 524.76 _chemical_name_systematic ; ? ; _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _atom_sites_solution_hydrogens mixed _audit_creation_method SHELXL-2013 _cell_angle_alpha 70.205(3) _cell_angle_beta 75.906(3) _cell_angle_gamma 88.921(3) _cell_formula_units_Z 4 _cell_length_a 11.4539(4) _cell_length_b 13.9416(4) _cell_length_c 17.0847(5) _cell_measurement_temperature 100(2) _cell_volume 2483.64(15) _computing_cell_refinement 'CrysAlisPro V 1.171.37.31, Agilent Technologies' _computing_data_collection 'CrysAlisPro V 1.171.37.31, Agilent Technologies' _computing_data_reduction 'CrysAlisPro V 1.171.37.31, Agilent Technologies' _computing_molecular_graphics 'XP SHELXTL/PC, Siemens Analytical' _computing_publication_material 'XL SHELXTL/PC, Siemens Analytical' _computing_structure_refinement 'Shelxl-2013, Sheldrick, G. M.' _computing_structure_solution ; SUPERFLIP. Palatinus, L. and Chapuis, G., J. Appl. Cryst. 40, 786-790. ; _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.973 _diffrn_measurement_device_type 'Agilent SuperNova with AtlasS2 detector' _diffrn_measurement_method \w-scans _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0240 _diffrn_reflns_av_unetI/netI 0.0325 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.973 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 20 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_number 19816 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.973 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 74.153 _diffrn_reflns_theta_min 3.377 _diffrn_source 'sealed X-ray source' _exptl_absorpt_coefficient_mu 3.487 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.89050 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro, Agilent Technologies, Version 1.171.37.31 (release 14-01-2014 CrysAlis171 .NET) (compiled Jan 14 2014,18:38:05) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 1.403 _exptl_crystal_description chunk _exptl_crystal_F_000 1080 _exptl_crystal_size_max 0.270 _exptl_crystal_size_mid 0.100 _exptl_crystal_size_min 0.063 _refine_diff_density_max 0.539 _refine_diff_density_min -0.366 _refine_diff_density_rms 0.057 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.028 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 602 _refine_ls_number_reflns 9840 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.028 _refine_ls_R_factor_all 0.0396 _refine_ls_R_factor_gt 0.0322 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0457P)^2^+0.9132P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0843 _refine_ls_wR_factor_ref 0.0892 _reflns_Friedel_coverage 0.000 _reflns_number_gt 8443 _reflns_number_total 9840 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file om501191c_si_002.cif _cod_data_source_block shelx _cod_depositor_comments 'Adding full bibliography for 4085532--4085543.cif.' _cod_original_cell_volume 2483.64(14) _cod_database_code 4085533 #BEGIN Tags that were not found in dictionaries: _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.453 _shelx_estimated_absorpt_t_max 0.810 _shelxl_version_number 2013-4 _shelx_res_file ; TITL CELL 1.54184 11.4539 13.9416 17.0847 70.205 75.906 88.921 ZERR 4.00 0.0004 0.0004 0.0005 0.003 0.003 0.003 LATT 1 SFAC C H CL N ZN UNIT 112 96 8 8 4 MERG 2 FMAP 2 PLAN 20 SIZE 0.063 0.100 0.270 ACTA BOND $H CONF L.S. 20 TEMP -173.00 WGHT 0.045700 0.913200 FVAR 3.64308 C1 1 0.014034 0.178662 0.037277 11.00000 0.01955 0.02037 = 0.02048 -0.00683 -0.00410 0.00182 C2 1 0.021240 0.173678 -0.048583 11.00000 0.02499 0.02194 = 0.02231 -0.01004 -0.00507 0.00278 C3 1 0.103677 0.210343 -0.127844 11.00000 0.02974 0.02802 = 0.02407 -0.01245 0.00081 -0.00231 AFIX 43 H3 2 0.176672 0.247306 -0.135092 11.00000 -1.20000 AFIX 0 C4 1 0.076071 0.191149 -0.198074 11.00000 0.04243 0.02874 = 0.02152 -0.01208 0.00028 0.00068 AFIX 43 H4 2 0.131401 0.217143 -0.253012 11.00000 -1.20000 AFIX 0 C5 1 -0.027289 0.136585 -0.189669 11.00000 0.04176 0.03062 = 0.02378 -0.01606 -0.00831 0.00465 AFIX 43 H5 2 -0.042346 0.125982 -0.238511 11.00000 -1.20000 AFIX 0 C6 1 -0.112336 0.095629 -0.108401 11.00000 0.03117 0.02412 = 0.02402 -0.01281 -0.00767 0.00494 C7 1 -0.085093 0.116801 -0.039728 11.00000 0.02356 0.02067 = 0.02359 -0.00990 -0.00644 0.00430 C8 1 -0.221751 0.036503 -0.089431 11.00000 0.03393 0.03359 = 0.03214 -0.02053 -0.01283 0.00341 AFIX 43 H8 2 -0.245191 0.021820 -0.134049 11.00000 -1.20000 AFIX 0 C9 1 -0.293992 0.000357 -0.007085 11.00000 0.02706 0.03431 = 0.03840 -0.02147 -0.00841 -0.00128 AFIX 43 H9 2 -0.365758 -0.040363 0.004038 11.00000 -1.20000 AFIX 0 C10 1 -0.265657 0.021417 0.061710 11.00000 0.02281 0.02789 = 0.02814 -0.01440 -0.00433 0.00109 AFIX 43 H10 2 -0.316760 -0.004983 0.118225 11.00000 -1.20000 AFIX 0 C11 1 -0.161749 0.081366 0.044556 11.00000 0.02123 0.02249 = 0.02222 -0.01085 -0.00628 0.00327 C12 1 -0.103636 0.121401 0.096026 11.00000 0.01710 0.01990 = 0.02185 -0.00715 -0.00448 0.00161 C13 1 0.196192 0.269506 0.020049 11.00000 0.02149 0.02526 = 0.01922 -0.01188 -0.00128 -0.00392 C14 1 0.299353 0.228049 0.043090 11.00000 0.02239 0.02680 = 0.01984 -0.01131 -0.00315 -0.00157 AFIX 43 H14 2 0.292663 0.168525 0.092444 11.00000 -1.20000 AFIX 0 C15 1 0.412316 0.274033 -0.006368 11.00000 0.02335 0.03507 = 0.02541 -0.01780 -0.00242 -0.00199 C16 1 0.418723 0.364500 -0.075613 11.00000 0.02646 0.03516 = 0.02576 -0.01452 0.00485 -0.00803 AFIX 43 H16 2 0.495726 0.396615 -0.109270 11.00000 -1.20000 AFIX 0 C17 1 0.316158 0.409038 -0.096863 11.00000 0.03519 0.02878 = 0.01874 -0.01102 0.00155 -0.00545 C18 1 0.203225 0.360330 -0.048431 11.00000 0.02893 0.02800 = 0.02190 -0.01156 -0.00507 -0.00019 AFIX 43 H18 2 0.131773 0.389024 -0.062165 11.00000 -1.20000 AFIX 0 C19 1 0.525391 0.226038 0.013241 11.00000 0.02350 0.05192 = 0.03626 -0.01805 -0.00278 0.00067 AFIX 137 H19A 2 0.503997 0.166099 0.065980 11.00000 -1.50000 H19B 2 0.576765 0.275712 0.021083 11.00000 -1.50000 H19C 2 0.569054 0.205044 -0.034568 11.00000 -1.50000 AFIX 0 C20 1 0.325981 0.507206 -0.172308 11.00000 0.04793 0.03522 = 0.02779 -0.00526 0.00216 -0.00338 AFIX 137 H20A 2 0.376042 0.559207 -0.166253 11.00000 -1.50000 H20B 2 0.245288 0.531182 -0.173738 11.00000 -1.50000 H20C 2 0.362980 0.494837 -0.225817 11.00000 -1.50000 AFIX 0 C21 1 -0.238597 0.061307 0.233025 11.00000 0.02009 0.02287 = 0.01652 -0.00985 -0.00245 -0.00172 C22 1 -0.227815 -0.029742 0.296500 11.00000 0.02128 0.02446 = 0.02012 -0.01096 -0.00578 0.00344 AFIX 43 H22 2 -0.150262 -0.051371 0.302322 11.00000 -1.20000 AFIX 0 C23 1 -0.331162 -0.089195 0.351576 11.00000 0.02725 0.02110 = 0.02249 -0.00950 -0.00674 0.00063 C24 1 -0.443401 -0.053292 0.343953 11.00000 0.02193 0.02440 = 0.02098 -0.00720 -0.00150 -0.00328 AFIX 43 H24 2 -0.514174 -0.093111 0.381862 11.00000 -1.20000 AFIX 0 C25 1 -0.454840 0.039639 0.282122 11.00000 0.02100 0.02235 = 0.02327 -0.00973 -0.00423 0.00039 C26 1 -0.350539 0.097312 0.226244 11.00000 0.02243 0.02169 = 0.01956 -0.00562 -0.00549 0.00046 AFIX 43 H26 2 -0.356262 0.160930 0.183775 11.00000 -1.20000 AFIX 0 C27 1 -0.321352 -0.191838 0.416454 11.00000 0.03372 0.02743 = 0.03626 -0.00120 -0.00985 0.00093 AFIX 137 H27A 2 -0.351409 -0.245917 0.400286 11.00000 -1.50000 H27B 2 -0.369535 -0.195534 0.473435 11.00000 -1.50000 H27C 2 -0.236729 -0.200838 0.417846 11.00000 -1.50000 AFIX 0 C28 1 -0.577885 0.073553 0.274282 11.00000 0.02119 0.03216 = 0.03859 -0.00479 -0.00529 0.00215 AFIX 137 H28A 2 -0.569902 0.136653 0.224700 11.00000 -1.50000 H28B 2 -0.620797 0.085996 0.326668 11.00000 -1.50000 H28C 2 -0.623316 0.020158 0.266358 11.00000 -1.50000 AFIX 0 C29 1 0.149118 0.633933 0.332874 11.00000 0.02160 0.02128 = 0.02070 -0.01014 -0.00686 0.00190 C30 1 0.024970 0.591450 0.353167 11.00000 0.02258 0.02028 = 0.01927 -0.00622 -0.00632 0.00157 C31 1 -0.034397 0.534640 0.320780 11.00000 0.02434 0.02623 = 0.02505 -0.01051 -0.00732 -0.00136 AFIX 43 H31 2 0.006571 0.516221 0.273032 11.00000 -1.20000 AFIX 0 C32 1 -0.158100 0.504368 0.360467 11.00000 0.02651 0.02967 = 0.03022 -0.00882 -0.01218 -0.00383 AFIX 43 H32 2 -0.199953 0.465993 0.337967 11.00000 -1.20000 AFIX 0 C33 1 -0.219871 0.528489 0.430397 11.00000 0.01989 0.02616 = 0.03024 -0.00397 -0.00858 -0.00138 AFIX 43 H33 2 -0.303173 0.507663 0.454555 11.00000 -1.20000 AFIX 0 C34 1 -0.160025 0.584228 0.466647 11.00000 0.01957 0.02066 = 0.02148 -0.00228 -0.00668 0.00212 C35 1 -0.038412 0.615832 0.425756 11.00000 0.02074 0.01901 = 0.01876 -0.00496 -0.00618 0.00232 C36 1 -0.210041 0.610662 0.540485 11.00000 0.02036 0.02576 = 0.02327 -0.00250 -0.00225 0.00197 AFIX 43 H36 2 -0.292278 0.591307 0.570328 11.00000 -1.20000 AFIX 0 C37 1 -0.140475 0.664129 0.569309 11.00000 0.02837 0.02824 = 0.01953 -0.00697 -0.00016 0.00192 AFIX 43 H37 2 -0.176121 0.680157 0.619315 11.00000 -1.20000 AFIX 0 C38 1 -0.018136 0.696041 0.527344 11.00000 0.02532 0.02758 = 0.02145 -0.01020 -0.00272 -0.00072 AFIX 43 H38 2 0.027947 0.732924 0.548492 11.00000 -1.20000 AFIX 0 C39 1 0.032790 0.672251 0.454766 11.00000 0.02083 0.02131 = 0.01926 -0.00721 -0.00449 0.00070 C40 1 0.154228 0.686131 0.397420 11.00000 0.02170 0.02104 = 0.01737 -0.00786 -0.00470 0.00063 C41 1 0.253194 0.580231 0.218896 11.00000 0.01849 0.02670 = 0.02010 -0.01271 -0.00034 -0.00437 C42 1 0.204038 0.619685 0.148796 11.00000 0.02645 0.02806 = 0.02999 -0.01499 -0.01014 0.00664 AFIX 43 H42 2 0.163929 0.681254 0.140584 11.00000 -1.20000 AFIX 0 C43 1 0.213940 0.568301 0.090490 11.00000 0.02768 0.03188 = 0.02555 -0.01466 -0.01018 0.00377 C44 1 0.271295 0.477723 0.104875 11.00000 0.02963 0.02982 = 0.02474 -0.01712 -0.00788 0.00211 AFIX 43 H44 2 0.277268 0.441974 0.065732 11.00000 -1.20000 AFIX 0 C45 1 0.320296 0.438013 0.175351 11.00000 0.03038 0.02343 = 0.02600 -0.01138 -0.00791 0.00221 C46 1 0.313524 0.491703 0.231363 11.00000 0.02505 0.02584 = 0.01866 -0.00781 -0.00623 -0.00190 AFIX 43 H46 2 0.350234 0.467639 0.278056 11.00000 -1.20000 AFIX 0 C47 1 0.163236 0.609709 0.012815 11.00000 0.06013 0.05161 = 0.04118 -0.02944 -0.03173 0.02616 AFIX 3 H47A 2 0.136431 0.552814 -0.001500 11.00000 -1.50000 H47B 2 0.225759 0.653390 -0.035974 11.00000 -1.50000 H47C 2 0.094577 0.649824 0.025456 11.00000 -1.50000 AFIX 0 C48 1 0.376383 0.336759 0.192538 11.00000 0.06853 0.03607 = 0.04941 -0.02434 -0.03591 0.02208 AFIX 137 H48A 2 0.313943 0.282114 0.206920 11.00000 -1.50000 H48B 2 0.413550 0.324486 0.240712 11.00000 -1.50000 H48C 2 0.438148 0.337796 0.141166 11.00000 -1.50000 AFIX 0 C49 1 0.269078 0.774745 0.452585 11.00000 0.02108 0.02719 = 0.01647 -0.01113 0.00087 -0.00704 C50 1 0.214496 0.865550 0.448552 11.00000 0.02203 0.02887 = 0.01852 -0.00996 -0.00401 -0.00170 AFIX 43 H50 2 0.166755 0.892861 0.408827 11.00000 -1.20000 AFIX 0 C51 1 0.230396 0.916197 0.503279 11.00000 0.02928 0.02756 = 0.01949 -0.01096 -0.00194 -0.00299 C52 1 0.299865 0.873115 0.561415 11.00000 0.03481 0.02950 = 0.01810 -0.01208 -0.00669 -0.00282 AFIX 43 H52 2 0.310302 0.907033 0.599250 11.00000 -1.20000 AFIX 0 C53 1 0.354396 0.782089 0.565832 11.00000 0.03166 0.02733 = 0.01790 -0.00656 -0.00648 -0.00345 C54 1 0.340721 0.733866 0.508903 11.00000 0.02655 0.02112 = 0.01851 -0.00603 -0.00363 -0.00305 AFIX 43 H54 2 0.380253 0.673393 0.508729 11.00000 -1.20000 AFIX 0 C55 1 0.172825 1.015173 0.499685 11.00000 0.04446 0.03728 = 0.03255 -0.02148 -0.01395 0.00952 AFIX 137 H55A 2 0.137685 1.038565 0.450086 11.00000 -1.50000 H55B 2 0.234074 1.066870 0.494083 11.00000 -1.50000 H55C 2 0.109274 1.004451 0.552551 11.00000 -1.50000 AFIX 0 C56 1 0.426697 0.736738 0.630904 11.00000 0.05442 0.03593 = 0.02861 -0.01189 -0.02204 0.00535 AFIX 137 H56A 2 0.489400 0.787601 0.624636 11.00000 -1.50000 H56B 2 0.464467 0.676627 0.621378 11.00000 -1.50000 H56C 2 0.373210 0.716515 0.688984 11.00000 -1.50000 AFIX 0 CL1 3 0.103563 0.068604 0.277801 11.00000 0.03156 0.05557 = 0.02807 -0.00892 -0.01384 0.00624 CL2 3 -0.044433 0.328389 0.228422 11.00000 0.05680 0.04985 = 0.07817 -0.04485 0.00131 -0.00222 CL3 3 0.501682 0.576617 0.362195 11.00000 0.03075 0.05688 = 0.04351 -0.02497 -0.01530 0.01235 CL4 3 0.470857 0.839929 0.190854 11.00000 0.05092 0.04847 = 0.03143 -0.01440 0.00194 -0.02121 N1 4 0.082644 0.216192 0.070331 11.00000 0.01839 0.02372 = 0.01967 -0.00699 -0.00325 -0.00139 N2 4 -0.129680 0.116760 0.174568 11.00000 0.01823 0.02378 = 0.01927 -0.00764 -0.00473 -0.00026 N3 4 0.247922 0.631880 0.279102 11.00000 0.02088 0.02674 = 0.02199 -0.01374 -0.00488 -0.00029 N4 4 0.256756 0.723945 0.394401 11.00000 0.02156 0.02679 = 0.01938 -0.01276 -0.00334 -0.00128 ZN1 5 0.006141 0.188544 0.202541 11.00000 0.02025 0.03241 = 0.02051 -0.01181 -0.00412 -0.00265 ZN2 5 0.396481 0.699675 0.298503 11.00000 0.01901 0.03640 = 0.02439 -0.01770 -0.00243 -0.00295 HKLF 4 REM REM R1 = 0.0322 for 8443 Fo > 4sig(Fo) and 0.0396 for all 9840 data REM 602 parameters refined using 0 restraints END WGHT 0.0454 0.9319 REM Highest difference peak 0.539, deepest hole -0.366, 1-sigma level 0.057 Q1 1 0.4419 0.6363 0.3292 11.00000 0.05 0.54 Q2 1 0.5291 0.8033 0.2114 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168417. 3928.51 1 0 6 8 162618. 3769.76 4 0 6 9 62829.0 1986.58 2 0 6 9 61593.7 1920.66 1 0 6 9 60475.7 1805.03 4 0 6 10 37724.9 1461.58 1 0 6 10 37306.9 1361.53 4 0 6 10 37999.6 1518.40 2 0 6 11 93959.2 2768.23 1 0 6 11 94571.0 2844.68 2 0 6 11 89576.7 2603.26 4 0 6 12 3862.13 487.649 1 0 6 12 3687.86 437.263 4 0 6 12 3801.27 310.718 18 0 6 12 4043.28 514.449 2 0 -6 -12 3919.69 292.148 8 0 6 13 24702.1 888.485 18 0 -6 -13 23363.8 826.999 8 0 6 13 22803.0 1301.35 2 0 6 13 21554.0 1152.96 4 0 6 13 23863.9 1284.42 1 0 6 14 452.734 246.496 4 0 6 14 308.643 150.091 18 0 -6 -14 706.150 164.677 8 0 6 15 11324.8 574.338 18 0 -6 -15 10583.6 533.492 8 0 6 16 5686.35 403.820 18 0 -6 -16 5325.01 368.157 8 0 6 17 2458.30 262.541 18 0 -6 -17 2457.21 256.312 8 0 6 18 5077.85 319.429 18 0 -6 -18 5128.12 327.147 8 0 6 19 2991.26 220.379 18 0 -6 -19 3347.02 244.760 8 0 -6 -20 3406.36 202.692 8 0 7 -14 8054.54 376.027 15 0 7 -13 2283.50 236.608 15 0 7 -12 760.320 195.177 15 0 7 -11 1901.05 264.450 15 0 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20570.2 824.010 1 0 8 6 21530.9 898.810 6 0 8 6 22156.9 935.259 2 0 8 7 16127.5 755.706 1 0 8 7 16306.7 752.923 6 0 8 7 16879.7 849.699 2 0 8 8 10616.2 684.772 2 0 8 8 9613.93 607.980 1 0 8 9 16609.1 928.078 2 0 8 9 14997.8 832.865 1 0 8 10 43692.4 1641.12 1 0 8 10 43756.0 1273.27 18 0 8 10 45412.0 1745.87 2 0 8 11 11008.8 799.933 1 0 8 11 12290.1 879.825 2 0 8 11 12475.0 588.674 18 0 8 12 55250.9 2072.55 1 0 8 12 58232.1 1607.87 18 0 8 12 57030.8 2188.18 2 0 8 13 148.053 256.476 1 0 8 13 221.266 286.540 2 0 8 13 150.043 144.418 18 0 8 14 263.460 173.521 18 0 8 15 24.1188 143.633 18 0 -8 -16 704.276 152.103 8 0 8 16 623.528 178.938 18 0 -8 -17-73.4384 119.395 8 0 8 17 114.320 142.370 18 0 8 18 15209.2 591.075 18 0 -8 -18 14419.2 527.935 8 0 8 19 3525.46 239.367 18 0 -8 -19 3079.57 201.526 8 0 8 20 9071.06 324.558 18 0 9 -12 150.882 100.989 15 0 9 -11 13.5313 108.808 15 0 9 -10 3096.08 283.807 15 0 9 -9 6364.68 397.916 9 0 9 -9 6290.01 405.955 15 0 9 -8 210.295 155.513 10 0 9 -8-25.9688 136.106 9 0 9 -8 100.916 149.017 15 0 9 -7 4788.65 365.239 9 0 9 -7 4264.70 338.360 10 0 9 -7 4349.64 362.364 15 0 9 -6 13606.0 621.321 10 0 9 -6 15502.6 656.173 9 0 9 -5 6868.64 404.214 11 0 9 -5 6974.00 417.744 10 0 9 -5 7020.80 655.473 6 0 9 -5 7233.34 435.143 9 0 9 -4 3088.34 287.022 10 0 9 -4 4038.34 309.072 11 0 9 -4 3618.84 483.146 6 0 9 -4 3379.51 289.411 9 0 9 -3 1914.84 219.307 11 0 9 -3 1716.20 356.550 6 0 9 -3 1583.94 202.135 10 0 9 -3 2046.36 255.523 9 0 9 -2-39.1701 120.345 9 0 9 -2 91.8780 117.658 11 0 9 -2 4.84967 190.430 6 0 9 -1 98.7788 164.354 6 0 9 0 4948.11 506.745 6 0 9 1 1358.55 288.145 6 0 9 2 61005.5 2001.53 6 0 9 3 42700.9 1557.71 6 0 9 4 38584.2 1444.70 6 0 9 5 20173.1 956.995 6 0 9 6 1487.62 267.494 6 0 9 6 1890.86 279.245 2 0 9 7 2288.08 336.090 2 0 9 7 2146.40 290.146 6 0 9 8 192.802 191.110 2 0 9 9 3343.95 428.396 2 0 9 9 3025.54 276.494 18 0 9 10 7404.54 669.434 2 0 9 10 7030.25 385.037 16 0 9 10 7504.93 450.142 18 0 9 10 7445.83 620.277 1 0 9 11 6688.50 657.900 2 0 9 11 8227.54 472.714 18 0 9 11 8152.15 668.248 1 0 9 12 3917.01 508.287 1 0 9 12 5593.83 401.926 18 0 9 12 4491.62 547.070 2 0 9 13 4672.87 374.877 18 0 9 14 35242.1 1163.50 18 0 9 15 7566.26 467.584 18 0 9 16 45999.5 1349.02 18 0 9 17 755.353 176.985 18 0 9 18 1350.14 191.946 18 0 9 19 1803.25 177.099 18 0 10 -11 12045.6 424.798 15 0 10 -10 6191.14 329.351 15 0 10 -9 668.370 158.080 15 0 10 -9 920.189 172.439 9 0 10 -8 1560.91 220.398 9 0 10 -8 1558.77 221.433 15 0 10 -7-7.80230 149.486 15 0 10 -7 26.4075 138.066 9 0 10 -7 29.6780 129.716 10 0 10 -6 472.907 151.674 15 0 10 -6 384.186 167.035 9 0 10 -6 464.948 152.541 10 0 10 -5 13.7634 142.430 9 0 10 -5 268.970 139.005 10 0 10 -5 169.965 133.749 15 0 10 -4-198.275 162.582 9 0 10 -4 100.099 121.989 11 0 10 -4 195.498 135.773 10 0 10 -3 1570.05 217.620 10 0 10 -3 1721.74 366.555 6 0 10 -3 1640.93 226.415 11 0 10 -3 1753.37 222.043 9 0 10 -2-118.437 221.479 6 0 10 -2-3.76361 126.700 9 0 10 -2 81.8659 128.829 11 0 10 -1 2140.23 246.920 9 0 10 -1 2142.78 244.199 11 0 10 -1 2071.12 376.863 6 0 10 0 35252.8 1519.81 6 0 10 0 33708.5 1024.52 11 0 10 0 32192.0 1011.49 9 0 10 0 31696.7 1013.63 17 0 10 1 186.891 146.072 16 0 10 1 14.1574 113.558 17 0 10 1 117.758 193.563 6 0 10 1 107.396 124.126 9 0 10 1 41.6034 122.314 21 0 10 1 61.1409 117.566 11 0 10 2 1425.45 196.564 16 0 10 2 1949.87 224.413 11 0 10 2 1321.17 192.596 21 0 10 2 1754.86 206.063 9 0 10 2 1550.62 307.296 6 0 10 3 1729.96 212.773 16 0 10 3 1786.19 339.399 6 0 10 3 1756.21 209.736 21 0 10 4 882.112 173.860 16 0 10 4 527.636 213.017 6 0 10 4 814.113 176.303 21 0 10 5 222.834 144.180 16 0 10 5 6.91391 137.841 21 0 10 5 440.368 218.654 6 0 10 6 19.7056 106.904 16 0 10 6 64.5504 145.575 6 0 10 6-143.139 144.672 21 0 10 7-18.6208 144.827 21 0 10 7-21.2925 129.844 18 0 10 7 199.813 168.118 6 0 10 7-49.7895 118.400 17 0 10 7 76.0938 115.449 16 0 10 8 8063.17 633.794 2 0 10 8 8068.65 442.986 16 0 10 8 8353.39 460.635 18 0 10 9 15289.5 655.846 18 0 10 9 14602.2 614.808 16 0 10 9 15183.2 929.386 2 0 10 10 3252.53 461.865 2 0 10 10 3784.83 322.490 18 0 10 10 3333.86 287.572 16 0 10 11 13250.3 623.998 18 0 10 11 11747.9 532.694 16 0 10 11 10953.9 862.727 2 0 10 12 2237.87 277.835 18 0 10 13 340.902 175.996 18 0 10 14 4300.28 369.956 18 0 10 15 502.092 182.887 18 0 10 16 276.411 171.664 18 0 10 17 373.836 147.511 18 0 10 18 8012.46 396.878 18 0 10 19 3756.78 234.146 18 0 11 -9 541.708 123.763 12 0 11 -9 508.643 111.434 15 0 11 -8 12186.8 487.726 15 0 11 -8 13985.9 539.896 9 0 11 -7 281.050 143.335 9 0 11 -7 263.439 120.903 15 0 11 -6 17065.4 647.330 10 0 11 -6 17356.1 655.767 15 0 11 -5 773.066 164.187 10 0 11 -5 836.950 189.957 9 0 11 -4 2835.71 285.445 9 0 11 -4 3072.28 266.043 10 0 11 -3 2207.53 227.862 10 0 11 -3 2219.24 262.288 9 0 11 -3 2656.69 267.585 11 0 11 -2 7629.81 453.012 9 0 11 -2 7757.14 447.562 11 0 11 -1 319.674 139.017 9 0 11 -1 221.395 139.100 11 0 11 0 98.4274 218.526 6 0 11 0-33.6985 132.599 9 0 11 0 5.33257 148.086 11 0 11 1 23239.3 838.257 17 0 11 1 24499.1 1290.43 6 0 11 1 23586.2 845.445 11 0 11 1 23850.6 840.247 9 0 11 2 6341.83 629.664 6 0 11 2 6438.66 389.558 9 0 11 2 7106.65 414.500 11 0 11 2 5716.97 383.059 17 0 11 3 6797.58 413.875 17 0 11 3 6377.37 630.344 6 0 11 3 7129.57 410.133 9 0 11 3 7588.97 430.901 11 0 11 3 7077.44 431.826 16 0 11 4 25527.7 1272.24 6 0 11 4 23154.1 870.420 16 0 11 4 25852.6 883.456 21 0 11 4 23064.4 828.720 17 0 11 5 16902.7 706.849 16 0 11 5 16232.8 662.777 17 0 11 5 16499.4 976.539 6 0 11 5 18021.9 710.956 21 0 11 6 4264.30 321.568 17 0 11 6 4186.28 476.283 6 0 11 6 4394.15 334.633 16 0 11 7 5203.38 356.444 17 0 11 7 5632.34 378.314 16 0 11 7 5356.90 374.076 18 0 11 7 4870.94 506.275 6 0 11 8 37453.0 1158.20 16 0 11 8 37795.9 1176.04 18 0 11 8 38180.2 1144.81 17 0 11 9 7565.20 441.642 16 0 11 9 7836.52 441.826 17 0 11 9 8305.02 476.838 18 0 11 10 38259.6 1176.34 16 0 11 10 41358.2 1255.12 18 0 11 11 434.986 129.125 16 0 11 11 262.857 155.292 18 0 11 12 4584.38 368.767 18 0 11 12 3702.19 295.009 16 0 11 13 27295.4 973.591 18 0 11 14 9542.41 522.986 18 0 11 15 30038.3 1009.28 18 0 11 16 2160.36 243.639 18 0 11 17 10014.6 469.858 18 0 11 18 2219.40 204.136 18 0 11 19 6579.46 267.206 17 0 11 19 6564.79 294.788 18 0 12 -7 698.143 143.927 9 0 12 -7 554.393 97.0214 12 0 12 -6 2893.70 248.890 9 0 12 -5 1011.88 185.859 9 0 12 -5 980.942 154.075 19 0 12 -4 3520.23 311.214 9 0 12 -3 5238.72 369.555 9 0 12 -3 4717.77 342.277 11 0 12 -2-9.74628 167.256 9 0 12 -2 57.7180 143.975 11 0 12 -1 2301.66 257.445 11 0 12 -1 2996.23 293.591 9 0 12 0 221.283 152.902 9 0 12 0 33.3604 132.751 11 0 12 1 2496.59 271.578 11 0 12 1 2925.59 280.389 9 0 12 2 54.6909 130.764 9 0 12 2 163.818 133.928 17 0 12 2 69.7276 131.340 11 0 12 3 36.2895 120.445 17 0 12 3-14.6209 132.121 11 0 12 3 183.996 122.289 9 0 12 4 17862.2 721.925 17 0 12 4 19676.1 777.350 16 0 12 4 18343.5 711.848 9 0 12 4 19989.4 770.065 11 0 12 5 39762.9 1213.56 16 0 12 5 37043.5 1159.59 17 0 12 5 38629.4 1134.14 9 0 12 6 562.208 178.271 16 0 12 6 239.824 132.760 17 0 12 7 106509. 2538.30 16 0 12 7 101208. 2490.10 18 0 12 7 105654. 2490.01 17 0 12 8 23648.4 846.752 17 0 12 8 24312.0 875.981 16 0 12 8 24690.5 886.068 18 0 12 9 24443.5 865.677 17 0 12 9 25032.9 883.108 16 0 12 9 25358.1 909.588 18 0 12 10 5488.42 378.417 16 0 12 10 6338.46 425.317 18 0 12 10 6218.25 399.068 17 0 12 11 4927.65 352.856 17 0 12 11 4613.42 332.092 16 0 12 11 5248.47 384.891 18 0 12 12 843.234 169.502 17 0 12 12 821.580 170.126 16 0 12 12 547.322 184.512 18 0 12 13 159.127 153.563 18 0 12 13 136.550 103.285 16 0 12 14 356.533 155.302 18 0 12 15-44.3143 128.650 18 0 12 16 3838.94 294.849 18 0 12 17 4411.08 254.218 17 0 12 17 4422.25 290.267 18 0 12 18 212.812 70.1195 17 0 12 18 54.9137 86.5463 18 0 13 -6 314.681 105.054 9 0 13 -5 4838.69 303.880 9 0 13 -4 1782.77 207.397 9 0 13 -4 1759.11 181.725 19 0 13 -3 249.515 127.375 9 0 13 -2 956.279 173.991 11 0 13 -2 1147.32 206.846 9 0 13 -1 181.953 128.213 11 0 13 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237.116 169.538 2 2 3 8 286.505 171.362 4 2 3 9 8924.58 584.836 4 2 3 9 8780.12 577.421 2 2 3 9 9210.47 613.173 1 2 3 10 11861.4 727.816 1 -2 -3 -10 10825.5 659.359 3 2 3 10 11468.0 704.848 4 2 3 10 11554.5 706.975 2 2 3 11 2230.91 355.296 4 -2 -3 -11 2073.97 328.310 3 2 3 11 2451.34 364.185 2 2 3 11 1962.15 345.880 1 2 3 12 2484.48 386.290 4 2 3 12 2321.36 373.156 2 2 3 12 2751.99 424.853 1 -2 -3 -12 2912.04 396.435 3 2 3 13 1570.35 343.263 4 -2 -3 -13 1500.33 204.911 8 2 3 13 1671.15 332.883 1 -2 -3 -13 1887.40 240.166 15 -2 -3 -13 1621.68 347.898 3 2 3 13 1346.59 289.680 2 -2 -3 -14 867.657 195.644 15 2 3 14 620.327 283.824 1 -2 -3 -14 765.645 192.373 8 2 3 14 632.505 261.142 4 2 3 14 625.582 268.680 2 -2 -3 -14 710.292 246.491 3 -2 -3 -15 90689.3 2297.66 15 -2 -3 -15 97654.4 2354.51 8 -2 -3 -16 10938.7 560.680 8 -2 -3 -16 9690.08 517.020 15 -2 -3 -17 28777.7 962.024 15 -2 -3 -17 33206.6 1054.81 8 -2 -3 -18 1920.68 246.786 8 -2 -3 -19 12690.0 527.604 8 -2 -3 -20 520.820 120.285 8 2 4 -15 4217.42 269.111 15 2 4 -14 3738.66 292.188 15 2 4 -13 6478.80 416.506 15 2 4 -12 2737.91 262.959 8 2 4 -12 3392.84 322.872 15 2 4 -11 3752.85 340.067 15 2 4 -11 3409.48 303.786 8 2 4 -10 61810.2 1664.02 8 2 4 -10 67852.8 1735.06 10 2 4 -9 26599.6 1443.39 3 2 4 -9 28195.2 937.307 10 2 4 -8 13516.8 582.814 10 2 4 -8 13199.5 948.876 3 2 4 -7 15113.4 958.829 3 2 4 -6 4655.81 503.656 3 2 4 -5 1251.46 270.370 3 -2 -4 4 1855.12 225.666 1 2 4 -4 2202.90 327.446 3 2 4 -3 11249.6 648.079 3 2 4 -3 12186.3 631.941 4 2 4 -2 13232.7 624.486 4 2 4 -2 12390.4 660.724 3 2 4 -1 1571.55 220.914 4 2 4 -1 1602.89 249.090 3 2 4 0 33719.1 1029.44 4 2 4 1 3453.67 282.270 4 2 4 2 21151.1 731.071 4 2 4 3 17646.1 666.152 4 2 4 4 913.362 185.633 4 2 4 5 103278. 2486.38 4 2 4 5 105316. 2506.06 2 2 4 6 1551.30 244.887 2 2 4 6 1514.75 233.543 4 2 4 7 1896.18 265.309 4 2 4 7 1517.33 256.728 2 2 4 7 1323.61 126.191 6 2 4 8 1596.05 275.458 2 2 4 8 1625.53 275.213 4 2 4 9 3966.24 409.171 2 2 4 9 4367.29 426.607 1 2 4 9 4390.01 415.375 4 2 4 10 2511.80 353.800 2 2 4 10 2428.08 324.161 4 2 4 10 2818.15 366.664 1 2 4 11 6575.24 567.705 4 2 4 11 6544.90 579.250 1 2 4 11 6848.58 589.902 2 -2 -4 -11 6385.50 527.831 3 2 4 12-47.0649 180.400 1 -2 -4 -12 301.915 197.004 3 2 4 12 407.920 200.156 4 2 4 12 353.236 218.353 2 2 4 13 9238.41 752.868 4 2 4 13 8494.48 452.059 18 2 4 13 9404.00 766.305 1 2 4 13 8852.63 740.159 2 -2 -4 -13 9218.17 703.442 3 -2 -4 -13 9664.12 493.091 8 2 4 14 274.867 213.265 1 -2 -4 -14 192.811 140.427 8 2 4 14 246.787 221.589 4 -2 -4 -14 224.815 188.302 3 2 4 14 113.660 207.496 2 2 4 14 415.723 148.723 18 -2 -4 -15 46088.8 1369.17 8 -2 -4 -16 11126.9 566.719 8 -2 -4 -17 9775.60 523.347 8 -2 -4 -18 466.294 153.587 8 -2 -4 -19 437.644 138.917 8 -2 -4 -20-81.1616 102.306 8 -2 -4 -21 3447.31 189.391 8 2 5 -15 73.5157 87.5678 15 2 5 -14 7766.71 391.008 15 2 5 -13 18955.0 722.632 15 2 5 -12 11.4288 165.326 15 2 5 -11 215.682 157.057 15 2 5 -10 1518.61 240.646 10 2 5 -9 15945.9 1145.29 3 2 5 -9 17872.6 669.630 9 2 5 -9 19138.0 753.534 10 2 5 -9 17208.0 1098.42 4 2 5 -8-70.5657 208.476 4 2 5 -8-91.7138 220.638 3 2 5 -8 140.645 129.169 10 2 5 -8 131.172 116.608 9 2 5 -7 21965.8 1236.84 3 2 5 -7 23121.6 797.687 10 2 5 -7 21123.5 726.501 9 2 5 -7 22066.3 1152.41 4 2 5 -6 8268.03 706.842 3 2 5 -6 7325.57 571.646 6 2 5 -6 8001.54 642.345 4 2 5 -5 96411.6 2829.80 3 2 5 -5 96263.3 2680.06 4 2 5 -4 1318.89 293.543 3 2 5 -4 1606.20 269.712 4 2 5 -3 2966.18 378.268 3 2 5 -3 2482.97 306.327 4 2 5 -2 4033.11 407.685 3 2 5 -2 3277.75 339.338 4 2 5 -1 21156.9 892.063 3 2 5 -1 18625.7 779.511 4 2 5 0 2984.04 288.141 4 2 5 1 944.373 174.376 4 2 5 2 131.745 127.152 4 2 5 3 2967.48 285.364 4 2 5 4 101249. 2435.18 4 2 5 5 138430. 3208.21 2 2 5 5 136552. 3173.30 4 2 5 6 95963.5 2409.41 4 2 5 6 96295.9 2440.38 2 2 5 7 104533. 2561.73 4 2 5 7 104333. 2606.60 2 2 5 7 97234.2 2244.68 6 2 5 8 19629.3 903.567 2 2 5 8 19059.4 860.773 4 2 5 9 164757. 3972.99 4 2 5 9 162568. 4013.49 2 2 5 9 170594. 4031.49 1 2 5 10 24557.9 1118.89 1 2 5 10 23458.8 1105.92 2 2 5 10 25430.4 1102.21 4 2 5 11 1847.65 331.396 2 2 5 11 1717.96 325.360 1 2 5 11 2062.33 332.314 4 2 5 12 2412.74 414.392 1 2 5 12 2629.64 395.719 4 2 5 12 2264.86 387.092 2 -2 -5 -12 2431.38 348.528 3 -2 -5 -13 38044.3 1148.21 8 2 5 13 38571.5 1669.61 2 2 5 13 38932.2 1667.67 1 -2 -5 -13 37634.5 1530.66 3 2 5 13 36737.8 1134.49 18 2 5 13 37722.7 1601.22 4 -2 -5 -14 9360.53 742.745 3 2 5 14 9241.55 775.489 4 2 5 14 9737.14 826.822 1 2 5 14 9676.93 811.962 2 2 5 14 8837.53 483.378 18 -2 -5 -14 9828.53 510.764 8 -2 -5 -15 388.349 172.978 8 2 5 15 353.479 130.958 18 2 5 16 9309.84 484.929 18 -2 -5 -16 9657.35 520.541 8 -2 -5 -17 14708.1 644.887 8 -2 -5 -18 16615.9 663.014 8 -2 -5 -19 12803.8 529.719 8 -2 -5 -20 15916.8 549.303 8 -2 -5 -21 1077.10 113.294 8 2 6 -14 2660.11 214.358 15 2 6 -13 507.586 143.875 15 2 6 -12 2822.24 276.938 15 2 6 -11 1574.77 246.847 15 2 6 -10 8870.08 446.933 9 2 6 -10 9219.39 512.879 10 2 6 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135649. 3348.79 4 2 6 9 40838.6 1504.09 2 2 6 9 40640.5 1468.31 1 2 6 9 40866.8 1443.52 4 2 6 10 66721.6 2147.84 2 2 6 10 69138.2 2140.40 1 2 6 10 65298.8 2053.56 4 2 6 11 56249.0 1954.27 1 2 6 11 56649.4 1993.70 2 2 6 11 55018.8 1886.81 4 2 6 12 30215.1 1361.55 4 -2 -6 -12 31082.3 1312.80 3 2 6 12 30260.2 1429.89 2 2 6 12 32024.4 1432.75 1 2 6 12 30515.6 993.337 18 2 6 13 8980.55 487.023 18 2 6 13 9656.63 765.455 4 2 6 13 9108.95 785.771 2 -2 -6 -13 9767.17 729.742 3 -2 -6 -13 9504.21 481.908 8 2 6 13 9318.59 773.755 1 2 6 14 356.448 151.557 18 2 6 14 195.027 220.768 2 2 6 14 870.046 301.024 4 -2 -6 -14 291.802 148.709 8 -2 -6 -14 405.201 234.421 3 2 6 14 164.439 220.568 1 2 6 15 1692.05 238.983 18 -2 -6 -15 1700.52 241.392 8 -2 -6 -16 9695.78 503.960 8 2 6 16 9688.48 510.341 18 -2 -6 -17 2748.48 270.447 8 2 6 17 2691.83 261.081 18 -2 -6 -18 1991.44 227.806 8 2 6 18 2104.89 219.850 18 -2 -6 -19 159.085 117.544 8 -2 -6 -20 6002.92 304.941 8 -2 -6 -21 180.782 67.1132 8 2 7 -13 263.952 126.053 15 2 7 -12 394.221 154.175 15 2 7 -11 148.643 164.211 15 2 7 -10-72.3520 155.846 15 2 7 -10-68.5218 111.754 9 2 7 -10-149.857 167.723 10 2 7 -9 4833.95 332.845 9 2 7 -9 5325.85 384.430 10 2 7 -8 131.923 127.091 9 2 7 -8 660.637 191.266 10 2 7 -7 11327.9 525.405 9 2 7 -7 10846.7 556.994 10 2 7 -6 31924.6 1576.88 3 2 7 -6 29386.7 940.855 9 2 7 -6 29861.2 995.732 10 2 7 -5 18375.3 686.283 9 2 7 -5 18899.1 1150.45 3 2 7 -5 18222.4 712.555 10 2 7 -5 17987.7 1011.18 6 2 7 -5 17321.8 983.207 4 2 7 -4 26676.9 1196.41 4 2 7 -4 26761.3 1242.56 6 2 7 -4 26770.6 886.904 10 2 7 -3 84.2015 138.172 4 2 7 -3 111.998 200.493 6 2 7 -2 6512.91 507.004 4 2 7 -1 44954.9 1472.10 4 2 7 0 8362.88 536.411 4 2 7 1 8830.01 532.256 4 2 7 2 4605.19 374.282 4 2 7 3 4724.13 386.851 4 2 7 4 27779.5 1044.42 2 2 7 4 28379.0 1027.22 4 2 7 5 732.743 189.079 4 2 7 5 613.318 192.304 6 2 7 5 459.006 174.193 2 2 7 6 92062.3 2343.99 6 2 7 6 91718.3 2469.66 2 2 7 6 92554.1 2407.78 4 2 7 7 1270.62 226.919 4 2 7 7 902.133 240.600 2 2 7 7 1218.62 204.978 6 2 7 8 75315.5 2154.12 1 2 7 8 74461.5 2223.31 2 2 7 8 74198.2 2128.46 4 2 7 9 18887.0 938.191 1 2 7 9 18660.1 976.448 2 2 7 9 18819.7 913.221 4 2 7 10 133007. 3482.48 4 2 7 10 138281. 3576.36 1 2 7 10 137437. 3649.29 2 2 7 11 6066.34 593.162 2 2 7 11 5629.57 527.937 4 2 7 11 5841.69 575.008 1 2 7 12 402.551 196.595 1 2 7 12-37.8922 199.984 2 2 7 12 135.678 123.970 18 2 7 12 139.510 172.280 4 -2 -7 -13 852.868 226.028 3 -2 -7 -13 964.090 176.482 8 2 7 13 1146.32 211.208 18 2 7 13 1076.60 335.376 2 2 7 13 445.401 218.610 1 2 7 13 1159.70 280.519 4 2 7 14 1323.54 363.705 1 2 7 14 1246.58 330.236 4 2 7 14 1968.33 244.757 18 2 7 14 2344.94 454.183 2 -2 -7 -14 1942.08 224.525 8 -2 -7 -15 6819.83 421.347 8 2 7 15 7793.48 469.753 18 -2 -7 -16 387.325 163.653 8 2 7 16 402.035 150.924 18 2 7 17 2314.34 255.323 18 -2 -7 -17 2184.59 248.741 8 -2 -7 -18 9661.30 465.135 8 2 7 18 8780.59 441.686 18 -2 -7 -19 2133.28 207.752 8 2 7 19 2052.20 191.678 18 -2 -7 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5 1529.18 261.399 6 2 8 6-91.6324 132.663 2 2 8 6 37.1655 136.461 6 2 8 6 40.7358 102.030 1 2 8 6 149.059 145.470 4 2 8 7 3032.85 374.621 2 2 8 7 2581.20 321.986 4 2 8 7 2731.98 314.663 1 2 8 7 2658.63 311.655 6 2 8 8 4576.45 432.808 1 2 8 8 4588.62 462.355 2 2 8 8 4010.09 413.861 4 2 8 9 8736.94 608.827 4 2 8 9 8877.30 678.258 2 2 8 9 9175.87 641.257 1 2 8 10 24713.6 1213.95 2 2 8 10 24223.7 1151.89 1 2 8 10 24109.7 1099.55 4 2 8 11 18715.3 1044.02 1 2 8 11 20047.7 767.432 18 2 8 11 19887.7 1120.79 2 2 8 11 18116.1 975.418 4 2 8 12 187161. 4817.74 4 2 8 12 199415. 5105.18 2 2 8 12 194969. 4984.86 1 2 8 12 201342. 4334.38 18 2 8 13 937.751 205.318 18 2 8 13 482.843 202.730 1 2 8 13 1030.85 348.374 2 2 8 13 382.317 223.984 4 2 8 14 26081.9 947.346 18 -2 -8 -15 1916.32 235.435 8 2 8 15 2389.85 274.163 18 2 8 16 1886.73 256.182 18 -2 -8 -16 1376.86 197.929 8 2 8 17 18.5818 151.463 18 -2 -8 -17-253.735 131.360 8 2 8 18 4499.34 313.846 18 -2 -8 -18 4540.15 294.068 8 -2 -8 -19 333.758 111.363 8 2 8 19 213.847 96.4969 18 -2 -8 -20 9282.02 342.984 8 2 9 -11 4260.09 258.640 15 2 9 -10 364.251 140.934 15 2 9 -9 1999.30 238.904 15 2 9 -9 2248.58 212.818 9 2 9 -8 6775.05 384.844 9 2 9 -8 6386.64 421.616 10 2 9 -8 6246.14 415.837 15 2 9 -7 35.2885 142.637 10 2 9 -7 37.9209 123.166 9 2 9 -6 8274.57 476.910 10 2 9 -6 8254.14 460.486 9 2 9 -5 12077.9 581.836 10 2 9 -5 11773.3 565.994 9 2 9 -4 19285.6 759.770 10 2 9 -4 18835.3 1122.68 6 2 9 -4 20484.5 764.551 9 2 9 -3 15741.5 1008.38 6 2 9 -3 14967.8 641.944 10 2 9 -3 15480.0 650.721 9 2 9 -2 71388.6 1841.66 9 2 9 -2 75124.5 2491.47 6 2 9 -1 6309.05 386.836 9 2 9 -1 6690.36 633.543 6 2 9 0 1293.37 203.938 17 2 9 0 1000.45 283.879 6 2 9 0 1294.05 193.604 9 2 9 1 7167.67 633.389 6 2 9 2 8655.42 675.566 6 2 9 3 3984.44 442.505 6 2 9 4 10953.5 736.741 6 2 9 5 16194.7 879.814 6 2 9 5 15746.3 816.891 2 2 9 6 10112.8 668.182 2 2 9 6 10163.0 664.767 6 2 9 7 17195.9 910.778 2 2 9 7 17368.5 863.370 6 2 9 8 3161.75 403.382 2 2 9 9 213.235 143.757 1 2 9 9 335.076 140.798 18 2 9 9 275.940 165.409 2 2 9 10 3445.33 310.976 18 2 9 10 3243.96 446.701 2 2 9 10 3389.31 414.189 1 2 9 11 2102.74 253.988 18 2 9 11 2316.66 414.189 2 2 9 11 1906.24 339.719 1 2 9 12-139.716 200.761 1 2 9 12 123.732 151.340 18 2 9 12 456.973 254.363 2 2 9 13 132383. 3114.45 18 2 9 14 13989.4 667.845 18 2 9 15 656.830 175.420 18 2 9 16 8452.39 485.922 18 2 9 17 2392.98 258.821 18 2 9 18 4312.72 310.501 18 2 9 19 297.181 115.726 18 2 9 20 62.5416 69.6817 18 2 10 -10 3611.53 230.711 15 2 10 -9 653.708 151.862 15 2 10 -8 9590.29 464.655 15 2 10 -8 10048.6 441.308 9 2 10 -8 9733.90 461.034 10 2 10 -7 3641.37 306.167 15 2 10 -7 3926.77 293.078 9 2 10 -7 3500.22 307.044 10 2 10 -6 8.64667 129.551 9 2 10 -6 58.5355 131.513 10 2 10 -5 5164.74 363.628 9 2 10 -5 5062.58 374.559 10 2 10 -4 1044.64 210.060 10 2 10 -4 1179.99 202.888 9 2 10 -3 63.8396 143.028 10 2 10 -3 112.935 143.646 9 2 10 -2 1758.60 226.005 10 2 10 -2 2089.08 259.090 9 2 10 -1 1383.29 223.804 9 2 10 -1 1403.56 340.518 6 2 10 0 5794.12 360.440 11 2 10 0 5802.78 381.069 9 2 10 0 6224.14 645.172 6 2 10 0 5826.32 403.153 17 2 10 1 14843.9 639.760 17 2 10 1 15224.6 973.580 6 2 10 1 13895.2 577.126 11 2 10 1 13743.4 603.952 9 2 10 2 64103.2 1669.22 17 2 10 2 64895.6 2211.96 6 2 10 2 59855.5 1581.04 11 2 10 3 6407.82 399.677 17 2 10 3 6127.61 589.640 6 2 10 4 15896.9 937.606 6 2 10 4 16266.6 664.184 17 2 10 5 1179.82 195.382 16 2 10 5 1307.26 194.765 17 2 10 5 1507.01 302.047 6 2 10 5 1062.33 194.723 18 2 10 6 5000.83 359.471 16 2 10 6 6324.74 389.007 17 2 10 6 5810.40 390.070 18 2 10 6 6302.05 564.416 6 2 10 7 218.072 117.687 16 2 10 7 262.746 156.414 18 2 10 7 329.230 145.875 17 2 10 7 393.380 210.767 2 2 10 7 487.532 206.477 6 2 10 8 4138.82 323.263 17 2 10 8 3920.80 340.148 18 2 10 8 3893.85 296.581 16 2 10 8 3303.51 422.712 2 2 10 9 3927.67 339.243 18 2 10 9 3185.98 280.020 16 2 10 9 3506.49 459.658 2 2 10 10 195.652 127.836 18 2 10 10 627.035 264.186 2 2 10 11 4531.69 547.166 2 2 10 11 5897.05 419.979 18 2 10 12 4435.95 379.174 18 2 10 13 60841.3 1708.70 18 2 10 14 4683.29 382.873 18 2 10 15-36.1403 160.324 18 2 10 16 6691.94 430.889 18 2 10 17 360.010 142.440 18 2 10 18 6117.12 351.814 18 2 10 19 1728.34 172.276 18 2 10 20 629.819 94.0844 18 2 11 -9 1198.89 128.681 15 2 11 -8 4574.25 263.895 15 2 11 -7 321.145 119.249 9 2 11 -7 285.165 133.657 15 2 11 -7 211.567 117.057 10 2 11 -6 1.42363 112.746 9 2 11 -6 77.3083 122.228 15 2 11 -6 197.197 141.927 10 2 11 -5 1216.19 200.867 9 2 11 -5 1477.20 210.820 10 2 11 -4 877.695 171.037 10 2 11 -4 841.706 190.643 9 2 11 -3 16633.6 684.989 9 2 11 -3 15841.9 668.074 10 2 11 -2 165.894 141.996 10 2 11 -2 462.400 185.459 9 2 11 -1 23493.7 795.586 11 2 11 -1 23331.6 832.071 10 2 11 -1 23994.5 866.925 9 2 11 0 1672.00 204.927 11 2 11 0 1706.72 231.527 9 2 11 1 148.254 125.822 11 2 11 1-107.128 148.149 9 2 11 1 48.5777 132.134 17 2 11 1-95.8168 218.030 6 2 11 2 662.300 190.079 17 2 11 2 587.081 244.185 6 2 11 2 560.803 155.861 11 2 11 2 513.258 155.623 9 2 11 3 5710.26 609.878 6 2 11 3 6247.55 391.046 11 2 11 3 6392.91 419.905 17 2 11 4 746.925 162.221 17 2 11 4 753.527 268.935 6 2 11 5 37696.7 1598.80 6 2 11 5 38802.6 1191.10 17 2 11 6 14412.1 909.493 6 2 11 6 15130.2 648.390 17 2 11 6 14004.6 641.018 18 2 11 7 8638.94 502.557 18 2 11 7 9550.29 503.628 17 2 11 7 8271.45 669.959 6 2 11 7 8460.40 479.362 16 2 11 8 166.547 126.335 17 2 11 8 89.0288 117.901 16 2 11 8 286.336 142.170 18 2 11 9 1322.02 208.302 17 2 11 9 1056.91 197.105 18 2 11 9 836.107 188.299 16 2 11 10 734.580 187.798 18 2 11 10 838.595 182.343 17 2 11 10 488.948 148.150 16 2 11 11 74.1457 147.307 18 2 11 12 2246.09 287.123 18 2 11 13 4877.95 396.812 18 2 11 14 4114.76 358.659 18 2 11 15 3082.76 303.409 18 2 11 16 551.896 160.737 18 2 11 17 50703.3 1373.61 18 2 11 18 207.037 122.995 18 2 11 19 18846.4 592.508 18 2 11 20 202.145 64.1956 17 2 12 -7 3057.84 189.922 15 2 12 -7 3483.23 215.123 9 2 12 -6 361.030 111.974 15 2 12 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9295.51 509.119 17 2 12 12 9187.19 527.482 18 2 12 13 3780.15 316.497 17 2 12 13 3292.54 320.133 18 2 12 14 907.197 189.431 17 2 12 14 843.102 190.858 18 2 12 15 595.904 171.754 17 2 12 15 202.843 141.656 18 2 12 16 3881.11 285.005 17 2 12 16 3909.30 302.845 18 2 12 17 2241.14 207.106 17 2 12 17 2377.15 228.466 18 2 12 18 427.367 114.098 17 2 12 18 395.037 116.196 18 2 12 19 8103.37 307.760 17 2 12 19 7653.74 317.825 18 2 13 -6 314.756 85.7260 9 2 13 -5 8336.11 355.920 9 2 13 -4 3651.74 256.825 9 2 13 -4 3029.66 214.694 10 2 13 -3 107.359 90.3214 10 2 13 -3 27.9622 114.892 9 2 13 -2-7.77586 102.772 10 2 13 -2-137.993 139.003 9 2 13 -1-76.1476 133.888 9 2 13 -1 342.593 112.199 10 2 13 0-93.2052 108.462 10 2 13 0 82.9282 103.930 11 2 13 0 119.241 144.294 9 2 13 1 59.2390 144.731 9 2 13 1-100.562 120.119 11 2 13 2 2665.29 250.976 11 2 13 2 2972.18 297.109 9 2 13 3 9134.25 472.526 11 2 13 3 8873.71 496.715 9 2 13 3 8469.45 488.406 17 2 13 4 10627.9 523.349 9 2 13 4 9437.42 518.302 17 2 13 4 9800.76 510.060 11 2 13 5 4495.83 326.988 11 2 13 5 3874.94 334.539 17 2 13 5 4132.08 329.106 9 2 13 6 26696.7 941.507 17 2 13 6 25483.0 889.027 11 2 13 7 36457.0 1162.02 17 2 13 8 2943.85 297.300 17 2 13 9 2821.23 291.332 17 2 13 10 1137.44 204.144 17 2 13 10 878.439 192.988 18 2 13 11 10.5058 140.972 18 2 13 11-33.4459 148.896 17 2 13 12 335.965 157.236 17 2 13 12 224.129 137.502 18 2 13 13 2699.80 282.408 18 2 13 13 2284.19 247.001 17 2 13 14 2039.20 223.734 17 2 13 14 1836.78 233.948 18 2 13 15 10230.2 463.383 17 2 13 15 10313.0 496.268 18 2 13 16 1098.44 159.359 17 2 13 16 1094.63 181.592 18 2 13 17 6277.98 305.513 17 2 13 17 6667.19 337.680 18 2 13 18 479.240 92.9477 17 2 14 -4 476.886 99.7755 9 2 14 -3 456.057 120.826 9 2 14 -2 447.526 125.886 9 2 14 -1 3963.39 274.274 9 2 14 0 10501.6 477.974 9 2 14 1 414.937 145.020 9 2 14 1 437.302 126.124 11 2 14 2 10933.9 475.522 11 2 14 2 11284.7 518.272 9 2 14 3 21.8917 117.286 11 2 14 3-61.8903 134.824 9 2 14 4 22291.8 792.575 9 2 14 4 22411.9 774.994 11 2 14 5 70.5913 133.003 17 2 14 5-25.6595 132.546 9 2 14 5-82.6023 119.181 11 2 14 6 7059.49 403.363 9 2 14 6 6875.75 421.864 17 2 14 6 6867.44 401.494 11 2 14 7 1783.84 228.236 17 2 14 7 1957.41 229.293 11 2 14 7 1869.04 216.757 9 2 14 8 9278.71 468.552 11 2 14 8 8405.07 439.288 9 2 14 8 9171.57 483.349 17 2 14 9 17377.3 693.383 17 2 14 10 3053.57 275.878 17 2 14 11 34659.8 1050.67 17 2 14 12 959.890 172.302 17 2 14 13 9328.96 445.019 17 2 14 14 876.965 156.490 17 2 14 15 249.303 107.389 17 2 14 16-28.2482 82.2396 17 2 14 17 320.409 76.6518 17 2 15 -2 15722.5 480.929 9 2 15 -1 205.277 77.5932 19 2 15 -1-123.412 88.5542 9 2 15 0 245.032 106.895 9 2 15 1 1233.29 163.758 9 2 15 2 303.307 122.143 9 2 15 2 391.686 99.1406 11 2 15 3 104.742 105.993 9 2 15 3 170.405 107.419 11 2 15 4 867.803 151.241 9 2 15 4 864.448 138.813 11 2 15 5 2201.97 211.195 11 2 15 5 2494.17 234.054 9 2 15 6 10366.1 457.838 11 2 15 6 10656.0 467.948 9 2 15 7 11480.6 480.967 9 2 15 7 11303.4 503.722 17 2 15 7 11790.5 503.773 11 2 15 8 11364.3 504.479 17 2 15 8 11774.0 500.379 11 2 15 8 11416.2 469.142 9 2 15 9 1520.50 189.371 17 2 15 9 1667.58 179.640 9 2 15 9 1658.60 205.023 11 2 15 10 703.490 126.979 9 2 15 10 487.926 124.952 17 2 15 11 106.277 87.9430 9 2 15 11 62.8640 112.921 11 2 15 11 108.625 101.215 17 2 15 12 700.171 131.267 17 2 15 13 66.5070 86.1607 17 2 15 14 2506.42 191.482 17 2 15 15 1452.95 133.889 17 2 15 16 128.897 64.6230 11 2 16 1 240.296 75.4206 9 2 16 2 111.428 85.8752 9 2 16 3 738.402 98.1616 11 2 16 3 887.092 127.074 9 2 16 4 2428.24 187.866 9 2 16 4 2616.44 181.158 11 2 16 5 1708.86 158.058 11 2 16 5 1543.46 159.413 9 2 16 6 3044.07 214.017 11 2 16 6 2984.12 207.068 9 2 16 7 206.113 92.3985 9 2 16 7 209.215 116.537 11 2 16 8 5569.91 271.893 9 2 16 8 6024.01 305.467 11 2 16 9 435.334 105.636 17 2 16 9 267.589 81.2743 9 2 16 9 455.955 114.730 11 2 16 10 2804.24 194.586 17 2 16 10 2998.48 210.699 11 2 16 11 240.392 88.9154 17 2 16 11 439.841 114.241 11 2 16 12 8834.81 345.851 11 2 16 12 8035.12 326.805 17 2 16 13 1683.01 136.325 17 2 16 13 1755.05 143.491 11 2 16 14 1654.33 124.617 11 2 17 8 48.4302 60.7382 11 2 17 9 1674.75 126.806 11 2 17 10 2699.52 156.808 11 -3 16 9 138.571 74.5780 11 -3 16 8 5250.29 252.604 11 -3 16 7 6541.49 296.746 11 -3 16 6 944.208 130.960 11 -3 16 6 1080.70 112.310 19 -3 16 5 1237.65 127.305 19 -3 16 5 1059.47 133.811 11 -3 16 4 3052.78 211.302 11 -3 16 4 3114.69 194.327 19 -3 16 3 100.611 86.4299 11 -3 16 3 57.2005 79.7547 19 -3 16 2 4536.64 235.228 19 -3 16 1 1820.99 153.515 19 -3 16 0 3864.51 197.865 19 -3 15 12 2791.24 187.490 16 -3 15 11-70.2292 91.6085 16 -3 15 11 18.1597 63.2877 11 -3 15 10 1376.55 167.161 16 -3 15 10 1031.99 126.221 11 -3 15 9 373.625 126.391 16 -3 15 9 225.988 97.5477 11 -3 15 8 100.237 97.6193 11 -3 15 8-44.3111 104.967 16 -3 15 7 8899.03 426.731 16 -3 15 7 8563.44 395.701 11 -3 15 6 3497.48 256.211 11 -3 15 5 1944.04 200.681 11 -3 15 4 2065.50 215.325 11 -3 15 3 1820.83 204.035 11 -3 15 2 1042.90 167.034 11 -3 15 1 31.3467 102.618 11 -3 15 1-93.6828 108.650 19 -3 15 0 2689.28 215.895 19 -3 15 -1 79.6807 92.3592 19 -3 15 -2 1336.98 146.753 19 -3 15 -3 91.6460 69.5956 19 -3 14 14 535.308 87.9694 16 -3 14 13 2126.67 174.729 16 -3 14 12 7172.97 348.682 16 -3 14 11 3670.97 263.948 16 -3 14 11 3277.81 217.542 11 -3 14 10 1709.06 173.067 11 -3 14 10 1789.49 202.367 16 -3 14 9 3036.61 263.407 16 -3 14 9 2794.00 232.746 11 -3 14 8-21.7090 119.819 11 -3 14 8 68.7677 126.709 16 -3 14 7 4008.55 323.838 16 -3 14 7 4305.14 298.901 11 -3 14 6 419.192 142.364 11 -3 14 6 417.629 153.107 16 -3 14 5-111.647 143.410 11 -3 14 5-88.7959 132.161 16 -3 14 4 402.995 157.707 11 -3 14 4 292.238 143.268 16 -3 14 3 18401.2 696.381 11 -3 14 2 3865.71 310.298 11 -3 14 1 5506.19 352.157 11 -3 14 0 8208.02 428.978 11 -3 14 -1 1141.36 151.877 9 -3 14 -1 1128.32 183.361 11 -3 14 -1 1245.12 188.981 19 -3 14 -2 6414.30 346.998 19 -3 14 -2 5311.92 290.742 9 -3 14 -3 1094.10 153.241 19 -3 14 -3 978.316 141.231 9 -3 14 -4 1376.54 152.243 19 -3 14 -5 872.654 110.332 19 -3 13 15 3540.34 210.072 18 -3 13 14-29.8860 74.6104 16 -3 13 14 10.5935 87.9291 18 -3 13 13 711.181 128.082 16 -3 13 13 565.814 117.770 18 -3 13 12 674.851 159.206 16 -3 13 12 704.770 140.005 18 -3 13 11 236.319 110.670 11 -3 13 11 167.959 131.457 16 -3 13 10 11739.6 538.036 16 -3 13 10 11160.4 476.795 11 -3 13 9 6561.95 410.077 16 -3 13 9 6405.43 366.805 11 -3 13 8 229.086 131.070 11 -3 13 8 275.209 141.430 21 -3 13 8 350.005 155.773 16 -3 13 7 3402.74 317.732 16 -3 13 7 3377.72 301.804 21 -3 13 7 3390.13 289.251 11 -3 13 6-85.3522 173.606 21 -3 13 6-202.415 142.906 11 -3 13 6 235.377 172.463 16 -3 13 5 17940.1 735.708 16 -3 13 5 17640.0 729.422 21 -3 13 5 17151.9 689.302 11 -3 13 4 702.611 168.933 21 -3 13 4 591.199 171.900 11 -3 13 4 1079.05 198.323 16 -3 13 3 26530.4 932.583 16 -3 13 3 28050.8 961.996 21 -3 13 3 28300.1 952.294 11 -3 13 2-6.79206 133.868 16 -3 13 2 262.503 157.959 11 -3 13 2 108.973 147.685 21 -3 13 1 70.2228 139.140 11 -3 13 1-219.708 172.988 21 -3 13 0 7259.53 383.033 9 -3 13 0 8251.18 458.015 11 -3 13 -1 4069.86 283.076 9 -3 13 -1 4165.14 327.156 11 -3 13 -2 6648.98 372.367 9 -3 13 -2 7187.47 411.550 19 -3 13 -2 7297.91 427.464 11 -3 13 -3 6128.04 362.983 19 -3 13 -3 5332.82 328.477 9 -3 13 -4 7132.32 344.686 12 -3 13 -4 7752.64 394.289 19 -3 13 -5 1218.70 159.752 9 -3 13 -5 1464.82 172.162 19 -3 13 -5 1522.87 159.336 12 -3 13 -6 4658.40 240.578 12 -3 13 -6 4753.82 252.440 19 -3 12 17 87.6534 61.4503 18 -3 12 16 19.7522 78.9707 18 -3 12 15 302.927 114.785 18 -3 12 14 2355.45 199.174 16 -3 12 14 1976.97 204.582 18 -3 12 13 33459.7 969.590 16 -3 12 13 33672.8 1003.29 18 -3 12 12 7748.07 421.567 16 -3 12 12 8564.99 441.726 18 -3 12 11 19479.0 724.304 16 -3 12 11 18580.2 706.484 18 -3 12 10 256.248 145.342 16 -3 12 10 193.289 116.074 18 -3 12 9 15591.6 618.173 11 -3 12 9 15282.6 629.444 21 -3 12 9 16076.4 673.678 16 -3 12 8 2902.29 301.072 16 -3 12 8 3065.12 271.551 11 -3 12 8 2843.78 284.663 21 -3 12 7 9046.88 502.932 16 -3 12 7 9581.29 483.195 11 -3 12 7 9536.26 502.928 21 -3 12 6 8051.27 475.422 16 -3 12 6 8262.38 451.685 11 -3 12 6 7870.66 460.160 21 -3 12 5 401.975 165.398 16 -3 12 5 235.570 152.697 21 -3 12 5 10.0859 136.731 11 -3 12 4 150.316 143.502 16 -3 12 4 275.482 137.424 11 -3 12 4 90.6349 160.635 21 -3 12 3 9557.43 509.591 16 -3 12 3 10171.0 534.982 21 -3 12 3 9242.47 499.603 11 -3 12 2 109.078 136.104 16 -3 12 2 157.826 161.216 21 -3 12 2-48.8621 146.155 11 -3 12 1-78.9011 126.148 16 -3 12 1 131.256 156.423 11 -3 12 1 74.3706 151.410 21 -3 12 0 666.936 180.297 11 -3 12 0 558.504 145.029 9 -3 12 0 366.319 177.253 21 -3 12 -1 20484.6 741.888 9 -3 12 -1 22263.3 824.890 11 -3 12 -1 20230.2 767.682 21 -3 12 -2-40.5678 116.369 12 -3 12 -2 73.6933 143.088 11 -3 12 -2 1.17596 127.910 9 -3 12 -3 7972.95 433.917 9 -3 12 -3 8218.56 434.099 12 -3 12 -3 8097.05 468.345 11 -3 12 -4 1336.69 206.052 9 -3 12 -4 1539.58 218.710 19 -3 12 -4 1509.45 204.343 12 -3 12 -5 857.721 156.584 12 -3 12 -5 1165.15 182.454 19 -3 12 -5 1124.10 186.282 9 -3 12 -6 2593.56 230.364 19 -3 12 -6 3043.79 250.291 12 -3 12 -6 2933.94 251.142 9 -3 12 -7 459.696 120.072 19 -3 12 -7 475.398 128.949 12 -3 12 -8 1721.85 167.163 12 -3 12 -9 29.0100 65.2282 12 -3 11 17 6104.76 292.957 18 -3 11 16 696.283 136.448 18 -3 11 15 20441.5 704.599 18 -3 11 14 2820.68 227.523 16 -3 11 14 3346.77 287.497 18 -3 11 13 223.946 135.574 18 -3 11 13-23.7031 126.478 16 -3 11 12 479.857 149.479 16 -3 11 12 698.326 175.678 18 -3 11 11 22.0038 127.151 18 -3 11 11 64.7722 139.600 16 -3 11 10 169.375 136.731 16 -3 11 10 257.507 146.337 18 -3 11 9 3094.01 280.097 21 -3 11 9 3398.73 313.836 16 -3 11 9 3635.15 302.803 18 -3 11 8 2846.80 266.594 21 -3 11 8 2803.61 276.567 16 -3 11 7 21464.5 804.672 21 -3 11 7 22136.1 823.292 16 -3 11 6 3809.60 326.448 16 -3 11 6 3372.28 295.469 11 -3 11 6 3529.67 319.928 21 -3 11 5 22431.8 1213.84 6 -3 11 5 24482.1 846.369 11 -3 11 5 24532.0 876.867 21 -3 11 5 25123.7 889.835 16 -3 11 4 7377.93 679.716 6 -3 11 4 7240.97 423.952 11 -3 11 4 7105.92 444.490 21 -3 11 4 8111.90 461.066 16 -3 11 3 7800.19 464.254 16 -3 11 3 8666.53 750.183 6 -3 11 3 8063.39 453.823 11 -3 11 3 8237.62 476.849 21 -3 11 2 1391.83 216.279 16 -3 11 2 1285.41 204.061 11 -3 11 2 1197.52 304.826 6 -3 11 2 1827.55 241.863 21 -3 11 1 994.677 195.381 16 -3 11 1 1034.99 192.145 21 -3 11 1 941.567 191.583 11 -3 11 0 312.621 155.344 21 -3 11 0 412.090 138.566 16 -3 11 0 432.098 152.054 11 -3 11 0 534.665 159.588 9 -3 11 -1-70.5868 120.085 12 -3 11 -1 241.537 146.491 11 -3 11 -1-150.005 138.172 21 -3 11 -1-189.445 140.785 9 -3 11 -2 858.513 180.365 12 -3 11 -2 1267.85 219.004 11 -3 11 -2 1138.36 179.938 21 -3 11 -2 983.894 180.861 9 -3 11 -3 2871.38 283.476 9 -3 11 -3 2839.91 275.858 12 -3 11 -3 3097.98 305.300 11 -3 11 -3 2453.95 248.706 21 -3 11 -4 820.781 176.515 19 -3 11 -4 1352.21 222.500 12 -3 11 -4 1342.22 215.849 11 -3 11 -4 973.325 192.952 9 -3 11 -5 29068.1 955.893 9 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3 8 6 30733.8 1249.47 2 3 8 6 29994.2 1209.89 4 3 8 6 30219.8 1182.37 6 3 8 7 4203.84 423.005 4 3 8 7 3916.59 424.677 2 3 8 7 3949.10 387.956 6 3 8 8 34830.7 1366.85 4 3 8 8 34787.3 1419.88 2 3 8 9 75171.5 2379.74 2 3 8 9 74324.5 2269.64 1 3 8 9 71099.0 2243.31 4 3 8 10 124.299 148.329 1 3 8 10-3.40612 146.509 4 3 8 10 71.5162 126.006 18 3 8 10 57.4145 209.888 2 3 8 11 51160.4 1850.22 4 3 8 11 50384.6 1876.82 1 3 8 11 52479.2 1975.86 2 3 8 11 49482.7 1437.07 18 3 8 12-74.4422 194.009 2 3 8 12 128.402 176.001 4 3 8 12 507.820 286.713 1 3 8 12 40.8721 135.677 18 3 8 13 5170.11 582.038 1 3 8 13 5649.44 645.299 2 3 8 13 5481.44 573.140 4 3 8 13 5537.14 404.383 18 -3 -8 -14 23001.7 803.576 8 3 8 14 22518.9 868.944 18 -3 -8 -15 61.8490 123.025 8 3 8 15 111.681 144.486 18 -3 -8 -16-71.7612 119.910 8 3 8 16-11.1175 134.212 18 -3 -8 -17 236.803 135.011 8 3 8 17 370.426 141.638 18 -3 -8 -18 252.948 123.279 8 3 8 18 29.9289 108.296 18 -3 -8 -19 5740.76 307.731 8 3 8 19 5986.23 314.947 18 -3 -8 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3543.00 303.012 10 3 10 -5 4858.24 332.121 9 3 10 -5 4412.32 345.853 10 3 10 -4 65339.7 1703.12 9 3 10 -4 65157.9 1730.95 10 3 10 -3 10429.1 542.211 10 3 10 -3 10579.8 532.337 9 3 10 -2 88332.2 2139.22 9 3 10 -2 83213.2 2126.74 10 3 10 -1 1369.08 223.885 9 3 10 0 52255.9 1456.77 9 3 10 0 52666.0 2052.73 6 3 10 1 170.000 144.240 17 3 10 1 296.409 181.825 6 3 10 1 228.879 137.943 9 3 10 2 1840.74 242.449 17 3 10 2 1508.39 347.394 6 3 10 3 856.055 187.082 17 3 10 3 1011.77 314.827 6 3 10 4 12475.2 851.320 6 3 10 4 12098.6 577.502 17 3 10 5 49.1109 125.596 17 3 10 5 158.070 171.087 6 3 10 6 10498.7 739.487 2 3 10 6 11291.3 768.310 6 3 10 6 10490.4 549.396 18 3 10 6 11188.7 537.245 17 3 10 7 3170.69 278.450 17 3 10 7 3529.28 320.720 18 3 10 7 3354.10 410.112 6 3 10 7 3263.41 429.167 2 3 10 8 15878.2 663.614 17 3 10 8 15083.9 929.071 2 3 10 8 15255.5 683.863 18 3 10 9 3143.78 294.529 17 3 10 9 2971.67 435.174 2 3 10 9 3256.14 317.179 18 3 10 10 26484.3 968.416 18 3 10 10 25438.4 1305.05 2 3 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50.4261 172.725 4 4 5 0 142358. 3494.80 4 4 5 1 155.087 168.326 4 4 5 2 91420.1 2419.36 4 4 5 3 53782.2 1652.10 4 4 5 4 1443.98 263.317 4 4 5 5 14389.2 766.788 4 4 5 6 81360.2 2284.90 4 4 5 7 11142.4 691.996 2 4 5 7 12097.6 721.142 4 4 5 8 54412.7 1802.40 4 4 5 8 55366.6 1815.09 2 4 5 9 1375.16 309.876 4 4 5 9 1090.36 253.529 2 4 5 10 51723.2 1831.68 2 4 5 10 50676.6 1819.13 4 4 5 11 5713.52 571.535 4 4 5 11 5589.98 569.426 2 4 5 12 24055.1 1243.14 4 4 5 12 24805.6 1255.15 2 4 5 12 25063.6 1273.38 1 -4 -5 -12 23449.8 832.813 8 4 5 13 14211.1 974.350 1 4 5 13 14747.8 990.110 2 4 5 13 13843.1 948.129 4 -4 -5 -13 15099.2 968.245 3 -4 -5 -13 14830.7 644.993 8 4 5 14 8234.21 761.552 4 4 5 14 7744.38 742.751 1 4 5 14 7976.00 762.879 2 -4 -5 -14 7677.57 706.269 3 -4 -5 -14 7394.74 458.554 8 -4 -5 -15 5286.03 390.156 8 -4 -5 -16 2078.15 255.573 8 -4 -5 -17 284.713 159.748 8 -4 -5 -18 40688.6 1199.84 8 -4 -5 -19 977.541 173.861 8 -4 -5 -20 18477.0 579.477 7 -4 -5 -20 19758.4 633.259 8 -4 -5 -21 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55633.3 1573.68 18 4 9 10 12385.1 853.538 4 4 9 10 10867.8 792.127 1 4 9 10 12774.0 901.513 2 4 9 10 13069.8 625.830 18 4 9 11 28079.0 1375.21 4 4 9 11 27806.3 1362.34 1 4 9 11 30463.5 1495.03 2 4 9 11 32081.0 1076.20 18 4 9 12 7127.04 662.410 4 4 9 12 6532.86 654.979 1 4 9 12 7160.75 708.092 2 4 9 12 8034.31 497.358 18 4 9 13 207.645 160.826 18 4 9 14 12739.1 631.966 18 4 9 15 952.753 193.575 18 4 9 16 70.4017 129.632 18 4 9 17 4461.66 324.482 18 -4 -9 -18-61.9312 89.8627 8 4 9 18 499.424 139.497 18 4 9 19 6133.76 309.360 18 -4 -9 -20 134.303 100.122 7 4 10 -9 5583.17 272.534 15 4 10 -8 2486.60 209.074 15 4 10 -7 5186.87 329.642 15 4 10 -7 5645.59 340.461 10 4 10 -6 379.304 145.183 10 4 10 -6 486.999 127.765 9 4 10 -5 12963.5 537.189 9 4 10 -5 13540.4 597.500 10 4 10 -4 2417.21 250.381 9 4 10 -4 2552.44 285.797 10 4 10 -3 10773.8 521.156 9 4 10 -3 9733.66 536.286 10 4 10 -2 48.8485 129.985 9 4 10 -1 20501.9 781.860 9 4 10 0-70.3358 153.183 9 4 10 1 1438.24 222.354 9 4 10 1 1571.48 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347.345 17 4 13 11-108.175 147.302 17 4 13 12 2384.71 259.500 17 4 13 13-141.017 140.302 17 4 13 14 692.898 169.149 17 4 13 15 1570.98 184.184 17 4 13 16 744.008 135.384 17 4 13 17 13690.2 481.909 17 4 13 18 13398.0 431.646 17 4 14 -2 788.444 109.249 9 4 14 -2 536.520 86.4085 10 4 14 -1 176.650 84.9353 10 4 14 -1 83.5859 89.8861 9 4 14 0 15274.5 509.157 10 4 14 0 16084.4 557.328 9 4 14 1 866.485 154.079 9 4 14 1 728.637 131.888 10 4 14 2 4962.47 284.511 10 4 14 2 4702.07 312.379 9 4 14 3 5814.10 314.204 10 4 14 3 6476.90 369.535 9 4 14 4 14847.0 544.722 10 4 14 4 16116.1 616.786 9 4 14 5 73.8141 145.869 9 4 14 6 1727.11 235.453 17 4 14 6 2192.60 204.965 11 4 14 6 2031.84 219.278 9 4 14 7 208.037 136.566 17 4 14 7 38.8758 106.915 11 4 14 7 439.744 154.048 9 4 14 8 9102.27 486.022 17 4 14 8 8617.95 419.801 11 4 14 9 503.908 155.684 17 4 14 10 304.620 156.458 17 4 14 11 3054.63 270.414 17 4 14 12 17783.4 666.235 17 4 14 13 63.5838 112.749 17 4 14 14 9271.42 420.484 17 4 14 15 520.847 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1502.25 283.516 4 5 2 8 1680.16 311.504 4 5 2 8 2014.95 317.348 2 5 2 9 5539.36 532.075 4 5 2 9 5628.32 497.987 2 5 2 10 44660.3 1682.93 4 5 2 10 44897.0 1616.41 2 5 2 11 44065.0 1715.31 4 5 2 11 43387.3 1616.92 2 -5 -2 -11 43850.4 1692.98 3 5 2 12 69164.6 2331.57 1 5 2 12 65331.3 2284.66 4 -5 -2 -12 64994.8 1794.12 15 5 2 12 65953.9 2178.54 2 -5 -2 -12 67798.4 2302.46 3 -5 -2 -12 67287.1 1760.59 8 -5 -2 -13 164.628 143.889 8 -5 -2 -13 101.002 156.043 15 5 2 13 487.015 271.391 4 5 2 13 225.167 206.540 1 -5 -2 -13 436.713 252.088 3 -5 -2 -14 3739.65 352.056 15 -5 -2 -14 3694.01 341.466 8 -5 -2 -15 1016.84 207.142 15 -5 -2 -15 1472.35 239.893 8 -5 -2 -16 8981.81 478.313 14 -5 -2 -16 9183.95 518.983 8 -5 -2 -17 7099.79 400.834 14 -5 -2 -17 7065.52 375.261 7 -5 -2 -17 7842.21 459.957 8 -5 -2 -18 544.753 162.267 8 -5 -2 -18 645.765 141.490 14 -5 -2 -19 1722.02 190.709 8 -5 -2 -20 2364.08 182.134 8 5 3 -14 3084.53 189.231 8 5 3 -13 3109.47 232.415 8 5 3 -13 3431.10 225.558 15 5 3 -12 6295.42 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2598.71 256.836 18 -6 9 9 50636.2 1405.98 16 -6 9 9 46679.3 1333.04 18 -6 9 8 329.654 180.927 16 -6 9 7 51106.2 1429.63 16 -6 9 7 46814.0 1346.23 21 -6 9 6 1165.44 203.647 16 -6 9 6 1021.04 201.069 21 -6 9 5 11821.2 564.215 16 -6 9 5 10880.7 544.232 21 -6 9 4 1947.06 239.933 16 -6 9 4 1910.11 240.452 12 -6 9 4 1745.24 242.433 21 -6 9 3 3340.03 296.636 16 -6 9 3 3104.94 309.349 12 -6 9 3 3185.06 480.360 5 -6 9 3 3343.38 305.946 21 -6 9 2 656.744 166.647 16 -6 9 2 876.877 325.748 5 -6 9 2 779.888 196.550 12 -6 9 2 969.438 202.403 21 -6 9 1 6841.20 400.283 16 -6 9 1 6987.11 438.216 12 -6 9 1 6663.54 670.415 5 -6 9 1 6666.30 439.558 21 -6 9 1 6191.65 371.897 19 -6 9 0 13246.8 623.718 21 -6 9 0 13346.2 620.057 12 -6 9 0 12863.8 555.285 11 -6 9 0 13194.6 967.837 5 -6 9 0 12657.2 554.793 19 -6 9 -1 31417.7 1040.05 12 -6 9 -1 29420.5 952.214 11 -6 9 -1 32052.6 1036.47 21 -6 9 -1 28821.5 954.933 19 -6 9 -2 50767.6 1440.84 21 -6 9 -2 50784.0 1466.02 12 -6 9 -2 51084.4 1393.82 11 -6 9 -2 49449.6 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266.923 16 -6 7 6 2018.57 364.619 5 -6 7 6 2173.29 242.477 21 -6 7 5 15629.1 651.566 16 -6 7 5 14381.7 912.095 5 -6 7 5 14663.1 617.741 21 -6 7 4 6749.30 407.956 16 -6 7 4 7036.69 426.008 12 -6 7 4 6919.96 642.698 5 -6 7 4 6334.50 394.853 21 -6 7 3-73.9651 121.647 16 -6 7 3 60.0585 126.699 21 -6 7 3-49.3630 135.575 12 -6 7 3 127.021 173.971 5 -6 7 2 307.089 110.858 16 -6 7 2 221.852 144.904 12 -6 7 2 274.150 221.034 5 -6 7 2 369.084 140.359 21 -6 7 1 536.688 147.589 12 -6 7 1 677.836 161.288 21 -6 7 1 978.193 309.515 5 -6 7 0 729.415 173.590 12 -6 7 0 606.712 257.364 5 -6 7 0 805.558 174.073 21 -6 7 -1 34.8991 150.257 12 -6 7 -1 188.288 204.698 5 -6 7 -1 88.4898 129.779 21 -6 7 -1-28.3335 107.497 19 -6 7 -2 3156.13 453.093 5 -6 7 -2 3248.88 295.088 12 -6 7 -2 2847.47 251.133 11 -6 7 -2 3051.55 270.068 21 -6 7 -2 3058.54 258.754 19 -6 7 -3 14218.4 632.928 12 -6 7 -3 13807.0 564.091 11 -6 7 -3 13430.2 892.683 5 -6 7 -3 13471.3 603.022 21 -6 7 -3 13439.2 572.214 19 -6 7 -4 6678.45 438.448 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9003.58 349.142 17 7 13 16 6860.10 270.851 17 7 14 2 306.836 75.2668 10 7 14 3 368.321 92.0663 10 7 14 3 221.528 76.9726 9 7 14 4 1655.33 151.325 10 7 14 4 1921.18 152.508 9 7 14 5 6210.24 289.446 9 7 14 6 323.637 95.6683 9 -7 -14 -7 88.1071 86.3751 13 7 14 7-72.7922 90.1560 9 -7 -14 -8 1625.63 157.916 13 7 14 8 1573.79 155.022 9 -7 -14 -9 286.638 106.104 13 7 14 9 227.456 98.7877 9 -7 -14 -10 2662.92 191.223 13 7 14 10 2176.99 193.398 17 7 14 11 1999.00 179.862 17 -7 -14 -11 2003.88 178.219 13 -7 -14 -12 14172.3 472.388 13 7 14 12 13992.0 484.489 17 -7 -14 -13 2555.28 179.937 13 7 14 13 2683.10 187.664 17 -7 -14 -14 3766.81 202.349 13 7 14 14 3493.35 193.289 17 7 15 7 415.472 82.2023 9 7 15 8 5503.55 238.175 9 7 15 9 793.648 101.211 9 7 15 10 2347.73 157.033 9 7 15 11 2373.07 151.312 9 7 15 12 44.5897 53.0912 9 -8 14 3 1131.56 121.177 21 -8 13 8 862.543 104.096 16 -8 13 7 2337.84 162.808 16 -8 13 7 1858.13 141.560 21 -8 13 6-13.2402 73.4240 16 -8 13 6-38.9893 87.8476 21 -8 13 5 5557.90 258.534 16 -8 13 5 5591.68 278.839 21 -8 13 4 3662.42 203.412 16 -8 13 4 3756.33 237.465 21 -8 13 3 989.878 140.238 21 -8 13 2 587.733 125.164 21 -8 13 1 650.423 132.651 21 -8 13 0 58.1614 89.8971 21 -8 13 -1 182.934 89.7564 21 -8 13 -2 243.370 79.2236 21 -8 12 10 157.873 71.0158 16 -8 12 9 5657.94 273.039 16 -8 12 8 59.1822 88.1047 16 -8 12 7 5959.17 307.129 16 -8 12 7 5131.38 265.132 21 -8 12 6 1121.42 143.677 16 -8 12 6 968.193 146.821 21 -8 12 5 1945.09 187.985 16 -8 12 5 1934.29 200.225 21 -8 12 4-39.0917 93.1063 16 -8 12 4 202.837 125.774 21 -8 12 3 6846.38 329.260 16 -8 12 3 7664.34 394.928 21 -8 12 2 683.452 157.842 21 -8 12 1 7035.23 374.470 21 -8 12 0 3747.39 275.584 21 -8 12 -1 3426.44 249.966 12 -8 12 -1 3523.34 257.697 21 -8 12 -2 4008.54 268.085 12 -8 12 -2 3589.66 243.599 21 -8 12 -3 2036.18 193.271 12 -8 12 -3 1698.92 156.386 21 -8 12 -4 415.862 113.126 12 -8 12 -5 1245.49 140.744 12 -8 12 -6 91.5654 78.1463 12 -8 11 11 916.369 111.855 16 -8 11 10-80.5647 95.8613 16 -8 11 9 268.466 109.857 16 -8 11 8 135.836 110.998 16 -8 11 7 8756.44 406.592 16 -8 11 7 7620.39 367.197 21 -8 11 6 9899.40 450.997 16 -8 11 6 9134.48 424.518 21 -8 11 5 6337.09 356.245 16 -8 11 5 5537.86 355.243 21 -8 11 4 1125.16 173.251 16 -8 11 4 1120.17 194.278 21 -8 11 3 10849.1 472.922 16 -8 11 3 10994.3 524.503 21 -8 11 2 2970.05 232.549 16 -8 11 2 2997.05 283.577 21 -8 11 1 240.690 167.963 12 -8 11 1 75.6939 156.625 21 -8 11 0 255.933 145.060 12 -8 11 0 168.455 148.714 21 -8 11 -1 4169.54 317.441 12 -8 11 -1 4011.38 316.139 21 -8 11 -2 129.486 143.630 12 -8 11 -2 91.2221 129.566 21 -8 11 -3 43.1687 129.395 12 -8 11 -3 252.707 121.998 21 -8 11 -4 131.655 127.202 12 -8 11 -4 66.7280 95.3822 21 -8 11 -5 223.005 127.897 12 -8 11 -6-0.99702 105.489 12 -8 11 -7 782.345 130.217 12 -8 11 -8 1108.69 127.053 12 -8 10 12 2073.98 152.437 16 -8 10 11 11676.5 431.053 16 -8 10 10 1201.95 158.756 16 -8 10 9 4189.04 285.846 16 -8 10 8 6180.24 360.868 16 -8 10 7 1801.56 213.776 16 -8 10 7 1288.97 175.544 21 -8 10 6 3017.93 277.450 16 -8 10 6 2587.26 250.219 21 -8 10 5 3380.05 279.705 16 -8 10 5 2996.81 276.713 21 -8 10 4-7.16504 126.218 16 -8 10 4-118.018 148.326 21 -8 10 3 1407.73 193.718 16 -8 10 3 1507.53 217.000 21 -8 10 2 424.506 137.551 16 -8 10 2 210.135 175.429 21 -8 10 1 23779.0 847.375 12 -8 10 1 22872.4 850.188 21 -8 10 0 897.698 207.208 12 -8 10 0 590.777 171.784 21 -8 10 -1 23197.3 842.137 12 -8 10 -1 22679.9 828.855 21 -8 10 -2 53.1363 151.225 12 -8 10 -2-111.013 153.747 21 -8 10 -3 10912.6 536.605 12 -8 10 -3 9946.04 491.125 21 -8 10 -4 147.507 147.420 12 -8 10 -4 335.769 137.549 21 -8 10 -5-291.451 166.637 12 -8 10 -5-89.1970 96.8158 21 -8 10 -6 696.380 165.639 12 -8 10 -7-113.292 134.471 12 -8 10 -8-0.14517 105.648 12 -8 10 -9 1297.80 152.859 12 -8 10 -10-54.4910 68.9738 12 -8 9 13 243.159 66.5187 16 -8 9 12 9945.27 379.374 16 -8 9 11 8247.04 372.669 16 -8 9 10 164.096 106.189 16 -8 9 9 529.814 152.544 16 -8 9 8-25.8850 126.340 16 -8 9 7 12001.0 547.537 16 -8 9 7 11156.5 484.650 21 -8 9 6 871.628 177.357 16 -8 9 6 749.544 164.058 21 -8 9 5 320.722 140.018 16 -8 9 5 199.086 140.488 21 -8 9 4 38874.7 1173.04 16 -8 9 4 40214.3 1201.23 21 -8 9 3 2854.45 274.791 16 -8 9 3 3340.06 328.108 21 -8 9 2 146.341 136.399 16 -8 9 2 95.7254 177.911 12 -8 9 2 336.779 200.652 21 -8 9 1 135.189 124.804 16 -8 9 1 32.9062 185.133 12 -8 9 1 275.546 169.181 21 -8 9 0 4824.18 396.062 12 -8 9 0 5100.65 404.262 21 -8 9 -1 2555.71 297.496 12 -8 9 -1 2087.75 271.344 21 -8 9 -1 2331.77 241.241 19 -8 9 -2 696.554 200.521 12 -8 9 -2 754.123 189.812 21 -8 9 -2 454.097 158.416 19 -8 9 -3 2985.22 308.166 12 -8 9 -3 3705.79 318.127 21 -8 9 -3 3616.84 292.765 19 -8 9 -4 3090.10 305.956 12 -8 9 -4 2917.42 273.439 21 -8 9 -5 12989.8 596.093 12 -8 9 -5 10368.9 492.842 21 -8 9 -6 109.059 160.265 12 -8 9 -7 1126.05 196.043 12 -8 9 -8 387.866 150.672 12 -8 9 -9 150.299 114.819 12 -8 9 -10 52.5919 100.556 12 -8 9 -11 259.101 82.1735 12 -8 8 13 368.515 81.8853 16 -8 8 12 17433.7 545.991 16 -8 8 12 14876.3 504.089 18 -8 8 11 905.386 158.579 16 -8 8 11 483.273 113.983 18 -8 8 10 10747.1 477.372 16 -8 8 10 9638.25 423.387 18 -8 8 9-45.3269 129.720 16 -8 8 8 360.924 162.703 16 -8 8 7 186.147 145.535 16 -8 8 6 245.788 148.750 16 -8 8 6 10.5743 118.699 21 -8 8 5 1883.88 237.030 16 -8 8 5 2204.39 255.900 21 -8 8 4 26.4308 133.691 16 -8 8 4 32.6728 142.036 21 -8 8 3 8190.31 463.635 16 -8 8 3 8966.14 512.326 21 -8 8 2 4051.75 315.423 16 -8 8 2 4760.15 381.701 12 -8 8 2 3586.06 335.947 21 -8 8 1 236.514 140.251 16 -8 8 1 33.0938 157.914 12 -8 8 1 136.677 164.390 21 -8 8 0 17219.3 757.335 12 -8 8 0 18598.4 755.930 21 -8 8 -1-74.9494 173.089 12 -8 8 -1 349.077 192.965 21 -8 8 -1-62.1521 111.117 19 -8 8 -2 3614.89 333.913 12 -8 8 -2 3943.25 349.110 21 -8 8 -2 3265.37 288.867 19 -8 8 -3 1363.36 235.859 12 -8 8 -3 1677.26 246.758 21 -8 8 -3 1447.12 210.606 19 -8 8 -4 4433.46 378.186 12 -8 8 -4 4327.35 342.110 21 -8 8 -5 56.8147 176.031 12 -8 8 -5-181.971 148.897 21 -8 8 -6 5956.76 429.580 12 -8 8 -6 5182.06 343.620 21 -8 8 -7 1904.70 262.657 12 -8 8 -8 124.492 144.355 12 -8 8 -9 583.537 163.961 12 -8 8 -10-1.36110 127.045 12 -8 8 -11 111.612 107.361 12 -8 8 -12 1057.20 127.460 12 -8 7 13 227.305 87.9378 16 -8 7 13 130.991 79.2961 18 -8 7 12 11517.0 442.253 16 -8 7 12 10552.5 435.897 18 -8 7 11 610.631 140.883 16 -8 7 11 986.113 161.549 18 -8 7 10 18339.7 673.068 16 -8 7 10 16207.4 625.970 18 -8 7 9 3550.06 307.658 16 -8 7 8 7149.97 440.152 16 -8 7 7 32898.7 1066.41 16 -8 7 6 8505.60 479.557 16 -8 7 6 7567.69 424.847 21 -8 7 5 377.989 158.655 16 -8 7 5-47.9674 122.173 21 -8 7 4 5690.41 399.106 16 -8 7 4 5586.74 385.026 21 -8 7 3 133.349 138.996 16 -8 7 3 266.657 152.666 21 -8 7 2 2162.78 245.185 16 -8 7 2 2855.16 314.835 12 -8 7 2 2259.68 281.104 21 -8 7 1-13.5263 107.809 16 -8 7 1 48.2681 175.499 12 -8 7 1 24.6394 144.225 21 -8 7 0-27.7108 164.768 12 -8 7 0 249.898 171.302 21 -8 7 -1 447.642 187.139 12 -8 7 -1 306.088 183.447 21 -8 7 -2 1544.04 249.240 12 -8 7 -2 1875.04 238.051 21 -8 7 -3 21507.6 847.536 12 -8 7 -3 21310.1 824.702 21 -8 7 -4 66316.4 1789.07 12 -8 7 -4 63646.9 1727.99 21 -8 7 -5 3271.11 314.019 21 -8 7 -5 2784.20 331.373 12 -8 7 -6 29790.4 1017.45 12 -8 7 -6 27203.7 920.306 21 -8 7 -7 2331.96 243.484 14 -8 7 -7 2783.63 314.190 12 -8 7 -8 9933.12 495.588 14 -8 7 -8 11266.7 558.053 12 -8 7 -9-79.1658 107.264 14 -8 7 -9-9.31000 142.280 12 -8 7 -10-213.407 110.378 14 -8 7 -10 142.812 140.125 12 -8 7 -11 350.653 120.667 14 -8 7 -11 392.511 135.696 12 -8 7 -12 3367.65 226.261 14 -8 7 -12 3066.16 230.736 12 -8 7 -13 54.3339 69.8903 14 -8 7 -13-44.1151 83.4176 12 -8 6 13 21.9755 75.9522 16 -8 6 13-71.8751 89.5370 18 -8 6 12 1763.51 183.069 16 -8 6 12 1137.59 162.327 18 -8 6 11 251.319 128.117 16 -8 6 10 1898.11 225.377 16 -8 6 9 1034.40 208.522 16 -8 6 8 5308.00 392.393 16 -8 6 8 4335.20 326.659 20 -8 6 7 8396.80 481.785 16 -8 6 7 7244.69 417.411 20 -8 6 6 23511.2 879.383 16 -8 6 5 4121.34 342.283 16 -8 6 5 3252.23 284.483 21 -8 6 4 9232.52 505.144 16 -8 6 4 8418.16 472.549 21 -8 6 3 3616.70 320.799 16 -8 6 3 2650.07 437.473 5 -8 6 3 3053.23 293.018 21 -8 6 2 2873.92 279.104 16 -8 6 2 2401.27 415.010 5 -8 6 2 2833.90 285.641 21 -8 6 1 2776.96 260.177 16 -8 6 1 2927.98 323.291 12 -8 6 1 2621.07 282.843 21 -8 6 1 3388.30 504.198 5 -8 6 0 1238.74 239.927 12 -8 6 0 1219.97 351.669 5 -8 6 0 1366.46 230.110 21 -8 6 -1 10665.0 571.852 12 -8 6 -1 10225.7 834.408 5 -8 6 -1 10710.7 549.489 21 -8 6 -2 4176.67 363.172 12 -8 6 -2 4481.17 358.146 21 -8 6 -2 3789.34 531.217 5 -8 6 -3 4318.29 358.435 12 -8 6 -3 4915.36 590.569 5 -8 6 -3 4682.92 358.737 21 -8 6 -4 1267.96 228.373 12 -8 6 -4 1017.76 205.903 21 -8 6 -5 221.205 133.361 14 -8 6 -5 45.3423 150.573 12 -8 6 -5 37.6867 131.190 21 -8 6 -6 27134.2 940.380 14 -8 6 -6 29340.6 1008.13 12 -8 6 -6 27023.6 925.510 21 -8 6 -7 3152.80 296.813 14 -8 6 -7 3608.82 347.144 12 -8 6 -8 41178.7 1235.41 14 -8 6 -8 40619.5 1261.11 12 -8 6 -9 2395.06 279.423 14 -8 6 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143.833 21 -8 5 2 52.7514 145.843 16 -8 5 2-112.371 233.339 5 -8 5 2-14.6022 131.978 21 -8 5 1 373.426 137.223 16 -8 5 1 430.502 220.445 5 -8 5 1 294.414 173.694 12 -8 5 1 266.960 124.704 21 -8 5 0 350.758 180.422 12 -8 5 0 267.709 211.127 5 -8 5 0 286.117 139.841 21 -8 5 -1 230.735 213.108 5 -8 5 -1 434.496 160.659 12 -8 5 -1 617.049 184.022 21 -8 5 -2 6726.27 408.562 14 -8 5 -2 7028.01 445.775 12 -8 5 -2 7713.96 713.193 5 -8 5 -2 7132.89 433.399 21 -8 5 -3 2357.92 260.375 14 -8 5 -3 1871.47 247.127 12 -8 5 -3 2184.23 409.656 5 -8 5 -3 2262.16 266.857 21 -8 5 -4 8010.16 458.072 14 -8 5 -4 7389.95 460.810 12 -8 5 -4 8075.25 708.380 5 -8 5 -4 8061.93 460.362 21 -8 5 -5 22665.7 830.898 14 -8 5 -5 21923.3 839.402 12 -8 5 -5 21845.1 1208.49 5 -8 5 -5 21854.9 810.602 21 -8 5 -6 19335.5 758.764 14 -8 5 -6 19072.0 770.844 12 -8 5 -6 18129.3 1093.74 5 -8 5 -6 18073.4 724.208 21 -8 5 -7 34665.4 1103.14 14 -8 5 -7 34037.4 1106.38 12 -8 5 -7 31611.3 1020.59 21 -8 5 -8 635.705 185.260 14 -8 5 -8 945.025 213.968 12 -8 5 -9 1800.95 249.272 14 -8 5 -9 1740.60 245.290 12 -8 5 -10 3868.39 333.659 14 -8 5 -10 3410.16 307.658 12 -8 5 -11 2477.46 268.605 14 -8 5 -11 2310.24 259.940 12 -8 5 -12 14953.5 617.657 14 -8 5 -12 13495.6 566.662 12 -8 5 -13 1843.35 215.137 14 -8 5 -13 1476.09 177.555 12 -8 5 -14 1378.20 169.339 14 -8 5 -14 1335.76 147.384 12 -8 5 -15 922.392 119.470 14 -8 4 14 280.880 84.4259 18 -8 4 13 152.595 77.5318 16 8 -4 -13 198.875 89.4328 8 8 -4 -12 4877.58 293.668 8 -8 4 12 4488.23 282.786 16 8 -4 -11 17836.3 651.424 8 -8 4 11 18344.7 669.990 16 -8 4 10 822.563 173.233 16 8 -4 -10 737.738 169.646 8 -8 4 10 774.863 192.794 20 -8 4 9 8818.86 497.157 16 -8 4 9 9543.42 516.039 20 -8 4 8 14020.5 664.734 16 -8 4 8 17503.2 711.953 20 -8 4 7 2743.87 271.072 13 -8 4 7 3211.56 309.088 20 -8 4 6 18437.5 743.943 20 -8 4 5 12443.3 581.817 20 -8 4 4 29296.2 1355.56 5 -8 4 4 29034.4 945.896 21 -8 4 4 29073.5 959.745 20 -8 4 3 25209.5 868.211 21 -8 4 3 26348.8 1288.89 5 -8 4 2 47373.2 1816.94 5 -8 4 2 46154.3 1309.54 21 -8 4 1 6973.33 417.402 16 -8 4 1 8342.37 477.884 12 -8 4 1 7879.51 698.592 5 -8 4 1 7874.35 448.291 21 -8 4 0 41558.9 1257.26 14 -8 4 0 45491.0 1317.17 12 -8 4 0 45293.9 1774.19 5 -8 4 0 45454.9 1290.16 21 -8 4 -1 18763.4 729.058 14 -8 4 -1 19089.4 758.229 12 -8 4 -1 19993.5 1111.02 5 -8 4 -1 19539.8 745.445 21 -8 4 -2 7303.93 426.880 14 -8 4 -2 6963.77 432.891 12 -8 4 -2 6947.75 646.729 5 -8 4 -2 7026.00 429.476 21 -8 4 -3 1422.29 225.111 14 -8 4 -3 1269.68 206.155 12 -8 4 -3 1680.09 369.338 5 -8 4 -3 1291.57 214.006 21 -8 4 -4 2082.74 244.705 14 -8 4 -4 2066.09 249.740 12 -8 4 -4 2183.86 381.344 5 -8 4 -4 1975.45 243.286 21 -8 4 -5 10765.0 543.011 14 -8 4 -5 10669.6 537.271 12 -8 4 -5 12047.8 861.795 5 -8 4 -5 10796.1 537.636 21 -8 4 -6 561.093 144.452 14 -8 4 -6 713.735 182.248 12 -8 4 -6 913.111 262.771 5 -8 4 -6 1128.99 198.696 21 -8 4 -7 4663.45 363.005 14 -8 4 -7 4458.54 367.384 12 -8 4 -7 4419.29 324.879 21 -8 4 -8 472.388 155.578 14 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21816.3 787.110 21 -8 3 1 1063.51 316.774 5 -8 3 1 753.989 162.034 21 -8 3 0 149.587 128.509 14 -8 3 0 289.253 159.691 12 -8 3 0 368.785 236.653 5 -8 3 0 254.942 128.423 21 -8 3 -1 20071.4 739.296 7 -8 3 -1 20662.2 772.249 14 -8 3 -1 21210.5 783.103 12 -8 3 -1 20891.7 1110.99 5 -8 3 -1 20818.2 762.078 21 -8 3 -2 18570.2 727.658 14 -8 3 -2 19175.1 722.745 21 -8 3 -2 18133.6 716.131 12 -8 3 -2 19597.0 1078.37 5 -8 3 -3 7234.57 429.892 14 -8 3 -3 6703.93 406.374 12 -8 3 -3 8167.04 690.251 5 -8 3 -3 7188.52 412.798 21 -8 3 -4 6243.69 400.320 14 -8 3 -4 5571.98 375.972 12 -8 3 -4 6641.16 624.870 5 -8 3 -4 6021.52 387.831 21 -8 3 -5 15134.2 652.028 14 -8 3 -5 14380.5 620.146 12 -8 3 -5 15397.5 955.422 5 -8 3 -5 15260.7 631.619 21 -8 3 -6 10643.9 552.368 14 -8 3 -6 10447.3 520.426 12 -8 3 -6 11198.1 811.140 5 -8 3 -6 11047.3 526.646 21 -8 3 -7 63.4446 134.448 14 -8 3 -7 207.737 153.789 12 -8 3 -7-1.65134 190.573 5 -8 3 -7 89.5249 128.399 21 -8 3 -8 856.481 200.491 14 -8 3 -8 708.133 176.157 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3658.99 452.674 5 -8 2 -1 108871. 3080.87 5 -8 2 -1 105497. 2484.54 21 -8 2 -2 10164.5 746.598 5 -8 2 -2 10314.0 497.773 21 -8 2 -3 601.514 233.315 5 -8 2 -3 366.726 135.278 21 -8 2 -4 621.274 179.243 14 -8 2 -4 559.218 226.546 5 -8 2 -4 630.636 147.359 21 -8 2 -5 130.704 136.460 14 -8 2 -5 78.4859 128.801 12 -8 2 -5-33.0264 175.981 5 -8 2 -5 133.612 114.929 21 -8 2 -6 113.217 129.128 14 -8 2 -6 141.491 127.747 12 -8 2 -6 578.428 240.572 5 -8 2 -6 269.727 129.634 21 -8 2 -7 411.184 163.395 8 -8 2 -7 623.967 192.393 14 -8 2 -7 438.446 149.608 12 -8 2 -7 618.787 228.385 5 -8 2 -7 434.615 146.528 21 -8 2 -8 2897.17 302.567 14 -8 2 -8 2223.03 381.637 5 -8 2 -8 2863.21 287.899 8 -8 2 -9 697.846 180.745 8 -8 2 -9 1150.67 239.873 14 -8 2 -10 8027.14 497.967 14 -8 2 -10 7405.29 448.673 8 -8 2 -11 15000.9 693.485 14 -8 2 -11 14035.8 631.557 8 -8 2 -12 107.605 137.585 8 -8 2 -12 340.347 223.520 14 -8 2 -13 2461.34 260.701 8 -8 2 -13 2887.31 302.756 14 -8 2 -14 1449.77 188.173 8 -8 2 -14 1584.07 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481.059 21 -9 5 0 916.876 227.432 12 -9 5 0 415.973 160.544 21 -9 5 -1 1477.46 264.673 12 -9 5 -1 1245.39 233.204 21 -9 5 -2 57093.4 1595.18 14 -9 5 -2 58405.2 1648.09 12 -9 5 -2 62599.0 1656.95 21 -9 5 -3 3855.74 320.271 14 -9 5 -3 4024.12 358.657 12 -9 5 -3 3885.28 339.401 21 -9 5 -4 5953.28 401.980 14 -9 5 -4 5984.42 423.992 12 -9 5 -4 5862.60 400.896 21 -9 5 -5 224.246 134.717 14 -9 5 -5 242.655 153.531 12 -9 5 -5 159.268 141.186 21 -9 5 -6 889.248 193.513 14 -9 5 -6 499.622 174.398 12 -9 5 -6 809.332 180.545 21 -9 5 -7 1620.04 245.487 14 -9 5 -7 1095.41 208.071 12 -9 5 -7 1563.53 219.491 21 -9 5 -8 7265.66 452.919 14 -9 5 -8 6075.69 415.227 12 -9 5 -9 7718.60 452.783 14 -9 5 -9 7300.33 435.507 12 -9 5 -10 683.983 172.519 14 -9 5 -10 652.921 162.420 12 -9 5 -11 5862.44 369.502 14 -9 5 -11 5257.72 342.868 12 -9 5 -12 5393.57 334.152 14 -9 5 -12 5424.43 312.413 12 -9 5 -13 287.483 122.226 14 -9 5 -14 1292.14 149.427 14 -9 4 12 644.852 102.675 16 9 -4 -12 521.703 95.7581 8 -9 4 11 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3 -7 171.062 139.349 12 -9 3 -7 151.774 157.455 21 -9 3 -8 18598.6 769.261 14 -9 3 -8 17506.9 702.245 12 -9 3 -8 17454.9 689.743 21 -9 3 -9 1112.47 212.605 14 -9 3 -9 939.202 173.727 12 -9 3 -10 27379.4 966.951 14 -9 3 -10 24749.3 857.898 12 -9 3 -11 1141.80 214.131 14 -9 3 -12 17202.3 712.508 14 -9 3 -13 40.0652 143.600 14 -9 3 -14 3094.94 260.700 14 -9 3 -15 2178.43 201.396 14 -9 3 -16 66.7817 87.1896 14 -9 2 12 860.179 98.3539 16 9 -2 -12 1396.05 135.104 8 -9 2 11 792.707 137.895 16 9 -2 -11 1075.12 153.713 8 -9 2 10-89.7826 107.325 16 9 -2 -10 78.4662 120.478 8 -9 2 9 3167.87 291.084 20 -9 2 8 349.768 144.566 13 -9 2 8 674.232 194.028 20 -9 2 7 13624.1 591.771 13 -9 2 7 14833.4 658.172 20 -9 2 6 24473.2 860.365 13 -9 2 6 26939.4 949.569 20 -9 2 5 22452.8 804.374 13 -9 2 5 24180.7 885.133 20 -9 2 4 35153.2 1062.25 13 -9 2 3 54148.0 1470.70 21 -9 2 2 22622.4 1207.48 5 -9 2 2 22698.1 817.361 21 -9 2 1 8596.73 731.917 5 -9 2 1 8796.97 470.318 21 -9 2 0 936.913 294.049 5 -9 2 0 1031.84 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1620.85 189.008 13 -9 -11 -4 1069.33 168.047 13 -9 -11 -5 52.4898 128.639 13 -9 -11 -6 2824.92 257.262 13 9 11 6 2716.56 207.845 9 -9 -11 -7 14683.3 592.503 13 -9 -11 -8 242.497 139.541 13 -9 -11 -9 11525.8 513.338 13 -9 -11 -10 979.186 170.345 13 -9 -11 -11 7892.85 405.262 13 -9 -11 -12 83.2103 126.207 13 -9 -11 -13 367.100 109.603 7 -9 -11 -13 438.749 128.708 13 -9 -11 -14 809.838 120.924 7 -9 -11 -14 900.678 142.861 13 -9 -11 -15-39.2407 82.6598 7 -9 -11 -15 131.682 97.6086 13 -9 -11 -16 252.249 79.2248 13 9 12 1 2509.25 158.131 10 9 12 2 2574.08 173.974 10 -9 -12 -3 2448.48 175.043 13 9 12 3 2887.82 199.183 10 -9 -12 -4 8532.64 356.250 13 -9 -12 -5 570.256 128.492 13 -9 -12 -6 3315.52 232.627 13 9 12 6 3121.31 193.718 9 -9 -12 -7 39.9130 102.321 13 9 12 7 90.7530 78.4251 9 -9 -12 -8 1055.69 163.678 13 9 12 8 1220.74 145.194 9 -9 -12 -9-79.1520 115.371 13 -9 -12 -10 2870.63 227.005 13 -9 -12 -11 5344.02 298.174 13 -9 -12 -12 578.959 116.883 13 -9 -12 -13 3614.39 224.179 13 -9 -12 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336.040 135.876 21 -12 2 -8 5845.64 374.168 14 -12 2 -8 5618.26 333.884 21 -12 2 -9 310.552 133.372 14 -12 2 -9 66.3748 97.9066 21 -12 2 -10 12348.3 527.487 14 -12 2 -11 6755.19 358.450 14 -12 2 -12 91.5007 103.036 14 -12 2 -13 1792.85 161.653 14 -12 1 6 292.595 81.3748 16 -12 1 6 366.878 96.3528 20 -12 1 5 158.133 83.3740 16 -12 1 5 98.1464 85.9291 20 -12 1 4 15952.9 543.926 16 -12 1 4 16902.7 576.601 20 -12 1 3 728.519 133.482 16 -12 1 3 509.343 138.156 20 -12 1 2 16584.4 603.578 16 -12 1 2 18143.7 593.894 21 -12 1 2 18314.0 646.056 20 -12 1 1 3836.68 260.811 16 -12 1 1 4503.33 286.927 21 -12 1 1 3977.61 291.911 20 -12 1 0 8051.63 413.993 21 -12 1 -1 171.924 141.336 21 -12 1 -2 210.967 134.477 21 -12 1 -3 5173.75 363.345 21 -12 1 -4 1647.77 235.471 21 -12 1 -5 4183.99 328.656 21 -12 1 -6 3749.53 308.003 21 -12 1 -7 1617.66 211.424 21 -12 1 -8 40682.1 1219.07 14 -12 1 -8 41972.8 1157.28 21 -12 1 -9 2267.96 254.571 14 -12 1 -9 2017.63 203.773 21 -12 1 -10 5104.29 338.576 14 -12 1 -10 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21 -13 -1 0 1737.84 170.677 20 -13 -1 -1 650.648 119.621 21 -13 -1 -2 2560.60 209.177 21 -13 -1 -3 834.791 147.824 21 -13 -1 -4 4034.16 281.465 21 -13 -1 -5 40.1101 111.516 21 -13 -1 -6 516.494 145.122 21 -13 -1 -7 1358.15 174.664 21 -13 -1 -8 684.066 131.799 21 -13 -1 -9 136.448 95.2038 21 -13 -1 -10 3810.86 219.090 21 -13 -2 2 9003.34 339.710 20 -13 -2 1 108.447 85.6794 20 -13 -2 0 7973.73 311.127 21 -13 -2 0 10644.2 403.796 20 -13 -2 -1 2130.17 169.980 21 -13 -2 -2 7016.78 336.196 21 -13 -2 -3 516.111 122.068 21 -13 -2 -4 247.129 132.060 21 -13 -2 -5 223.879 123.170 21 -13 -2 -6 50.4704 115.360 21 -13 -2 -7 129.189 108.322 21 -13 -2 -8 9910.63 424.235 21 -13 -2 -9 743.424 139.593 21 -13 -2 -10 13478.6 457.673 21 -13 -3 1-4.98887 75.6993 20 -13 -3 0 3847.07 232.172 20 -13 -3 -1 826.180 113.285 21 -13 -3 -2 14141.2 485.266 21 -13 -3 -3 1143.26 149.437 21 -13 -3 -4 19458.0 640.831 21 -13 -3 -5 47.9949 114.612 21 -13 -3 -6 4653.87 288.405 21 -13 -3 -7 2079.40 201.760 21 -13 -3 -8 269.015 111.815 21 -13 -3 -9-54.0678 95.8304 21 -13 -3 -10-147.505 112.025 7 -13 -3 -10-112.255 85.3049 21 -13 -3 -11 1654.56 170.137 7 -13 -3 -11 1202.40 116.644 21 -13 -3 -12 3235.04 200.130 7 -13 -4 0 6017.93 273.681 20 -13 -4 -1 12698.8 452.905 20 -13 -4 -2 685.953 111.961 21 -13 -4 -3 2121.30 176.408 21 -13 -4 -4 134.219 86.7349 21 -13 -4 -5 958.991 148.915 21 -13 -4 -6 3143.96 230.148 21 -13 -4 -7 1424.96 170.998 21 -13 -4 -8 1156.56 150.337 21 -13 -4 -9 361.237 110.056 21 -13 -4 -10 338.414 121.487 7 -13 -4 -10 253.522 99.8657 21 -13 -4 -11 1227.52 154.025 7 -13 -4 -11 1218.93 119.074 21 -13 -4 -12 307.920 94.8190 7 -13 -5 -1 3954.45 209.722 20 -13 -5 -3 589.686 83.9861 13 -13 -5 -3 922.960 121.429 21 -13 -5 -4 16.6975 54.8980 13 -13 -5 -4 4490.98 233.818 21 -13 -5 -5 16603.8 549.676 21 -13 -5 -6 11035.1 426.218 21 -13 -5 -7 2963.27 219.894 21 -13 -5 -8 3464.69 229.726 21 -13 -5 -9 942.639 132.650 21 -13 -5 -10 261.062 104.662 7 -13 -5 -10 226.466 85.6167 21 -13 -5 -11 305.439 102.883 7 -13 -5 -11 161.928 66.1067 21 -13 -5 -12 737.594 120.632 7 -13 -6 -4 243.123 78.8478 21 -13 -6 -5 876.813 114.268 21 -13 -6 -6 78.0336 84.7706 21 -13 -6 -7 6841.31 304.173 21 -13 -6 -8 3383.27 212.697 21 -13 -6 -9 5854.61 270.583 21 -13 -6 -10 2207.53 151.300 21 -13 -7 -6 2278.01 153.191 21 -13 -7 -7 4453.95 219.282 21 -13 -7 -8 1670.86 138.676 21 -13 -7 -9 56.3842 61.9063 21 -14 3 -3 3370.12 184.092 21 -14 3 -4 7537.96 289.188 21 -14 2 -2 3598.26 187.049 21 -14 2 -3 5748.36 255.470 21 -14 2 -4 7778.01 307.526 21 -14 2 -5 1603.04 140.229 21 -14 2 -6 17140.4 496.730 21 -14 1 -2 5101.85 229.202 21 -14 1 -3 8696.34 329.796 21 -14 1 -4 1586.86 141.531 21 -14 1 -5 1847.62 151.991 21 -14 1 -6-59.6788 81.6198 21 -14 1 -7 237.565 73.4096 21 -14 0 -3 952.415 113.506 21 -14 0 -4 496.010 95.2507 21 -14 0 -5 6011.80 275.087 21 -14 0 -6 5551.47 259.314 21 -14 0 -7 12046.9 399.478 21 -14 -1 -3 795.531 97.5267 21 -14 -1 -4 2860.57 178.314 21 -14 -1 -5-226.896 95.0716 21 -14 -1 -6-27.8035 78.0541 21 -14 -1 -7 497.963 98.9285 21 -14 -1 -8-57.7952 65.7261 21 -14 -2 -4 1094.59 114.582 21 -14 -2 -5 86.5878 74.5477 21 -14 -2 -6 8837.46 333.725 21 -14 -2 -7 4158.86 215.940 21 -14 -2 -8 2720.13 164.935 21 -14 -3 -5 192.783 68.0654 21 -14 -3 -6 110.521 73.8444 21 -14 -3 -7 279.527 80.6997 21 -14 -3 -8 4713.67 215.154 21 0 0 0 0.00 0.00 0 TITL exp_52 in P-1 REM P-1 (#2 in standard setting) CELL 1.54184 11.453855 13.941578 17.084729 70.2054 75.9055 88.9214 ZERR 3.00 0.000381 0.000421 0.000552 0.0029 0.0029 0.0026 LATT 1 SFAC C H N Cl Zn UNIT 120.00 90.00 6.00 6.00 3.00 TREF HKLF 4 END ; _shelx_hkl_checksum 54803 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp C1 C 0.01403(16) 0.17866(13) 0.03728(11) 0.0204(3) Uani 1 1 d . . C2 C 0.02124(17) 0.17368(14) -0.04858(12) 0.0226(4) Uani 1 1 d . . C3 C 0.10368(19) 0.21034(15) -0.12784(12) 0.0277(4) Uani 1 1 d . . H3 H 0.1767 0.2473 -0.1351 0.033 Uiso 1 1 calc R U C4 C 0.0761(2) 0.19115(15) -0.19807(13) 0.0315(4) Uani 1 1 d . . H4 H 0.1314 0.2171 -0.2530 0.038 Uiso 1 1 calc R U C5 C -0.0273(2) 0.13658(15) -0.18967(13) 0.0303(4) Uani 1 1 d . . H5 H -0.0423 0.1260 -0.2385 0.036 Uiso 1 1 calc R U C6 C -0.11234(18) 0.09563(14) -0.10840(12) 0.0252(4) Uani 1 1 d . . C7 C -0.08509(17) 0.11680(13) -0.03973(12) 0.0220(4) Uani 1 1 d . . C8 C -0.22175(19) 0.03650(16) -0.08943(13) 0.0300(4) Uani 1 1 d . . H8 H -0.2452 0.0218 -0.1340 0.036 Uiso 1 1 calc R U C9 C -0.29399(19) 0.00036(16) -0.00709(14) 0.0308(4) Uani 1 1 d . . H9 H -0.3658 -0.0404 0.0040 0.037 Uiso 1 1 calc R U C10 C -0.26566(17) 0.02142(15) 0.06171(13) 0.0254(4) Uani 1 1 d . . H10 H -0.3168 -0.0050 0.1182 0.030 Uiso 1 1 calc R U C11 C -0.16175(16) 0.08137(14) 0.04456(11) 0.0210(3) Uani 1 1 d . . C12 C -0.10364(16) 0.12140(13) 0.09603(11) 0.0197(3) Uani 1 1 d . . C13 C 0.19619(16) 0.26951(14) 0.02005(11) 0.0215(3) Uani 1 1 d . . C14 C 0.29935(17) 0.22805(14) 0.04309(11) 0.0225(4) Uani 1 1 d . . H14 H 0.2927 0.1685 0.0924 0.027 Uiso 1 1 calc R U C15 C 0.41232(18) 0.27403(15) -0.00637(12) 0.0266(4) Uani 1 1 d . . C16 C 0.41872(18) 0.36450(16) -0.07561(13) 0.0300(4) Uani 1 1 d . . H16 H 0.4957 0.3966 -0.1093 0.036 Uiso 1 1 calc R U C17 C 0.31616(19) 0.40904(15) -0.09686(12) 0.0283(4) Uani 1 1 d . . C18 C 0.20323(18) 0.36033(15) -0.04843(12) 0.0257(4) Uani 1 1 d . . H18 H 0.1318 0.3890 -0.0622 0.031 Uiso 1 1 calc R U C19 C 0.52539(19) 0.22604(19) 0.01324(15) 0.0373(5) Uani 1 1 d . . H19A H 0.5040 0.1661 0.0660 0.056 Uiso 1 1 calc R U H19B H 0.5768 0.2757 0.0211 0.056 Uiso 1 1 calc R U H19C H 0.5691 0.2050 -0.0346 0.056 Uiso 1 1 calc R U C20 C 0.3260(2) 0.50721(17) -0.17231(14) 0.0405(5) Uani 1 1 d . . H20A H 0.3760 0.5592 -0.1663 0.061 Uiso 1 1 calc R U H20B H 0.2453 0.5312 -0.1737 0.061 Uiso 1 1 calc R U H20C H 0.3630 0.4948 -0.2258 0.061 Uiso 1 1 calc R U C21 C -0.23860(16) 0.06131(13) 0.23303(11) 0.0194(3) Uani 1 1 d . . C22 C -0.22781(16) -0.02974(14) 0.29650(11) 0.0210(3) Uani 1 1 d . . H22 H -0.1503 -0.0514 0.3023 0.025 Uiso 1 1 calc R U C23 C -0.33116(17) -0.08920(14) 0.35158(12) 0.0230(4) Uani 1 1 d . . C24 C -0.44340(17) -0.05329(14) 0.34395(12) 0.0233(4) Uani 1 1 d . . H24 H -0.5142 -0.0931 0.3819 0.028 Uiso 1 1 calc R U C25 C -0.45484(16) 0.03964(14) 0.28212(12) 0.0219(4) Uani 1 1 d . . C26 C -0.35054(17) 0.09731(14) 0.22624(11) 0.0216(3) Uani 1 1 d . . H26 H -0.3563 0.1609 0.1838 0.026 Uiso 1 1 calc R U C27 C -0.3214(2) -0.19184(16) 0.41645(14) 0.0348(5) Uani 1 1 d . . H27A H -0.3514 -0.2459 0.4003 0.052 Uiso 1 1 calc R U H27B H -0.3695 -0.1955 0.4734 0.052 Uiso 1 1 calc R U H27C H -0.2367 -0.2008 0.4178 0.052 Uiso 1 1 calc R U C28 C -0.57789(18) 0.07355(16) 0.27428(14) 0.0330(4) Uani 1 1 d . . H28A H -0.5699 0.1367 0.2247 0.050 Uiso 1 1 calc R U H28B H -0.6208 0.0860 0.3267 0.050 Uiso 1 1 calc R U H28C H -0.6233 0.0202 0.2664 0.050 Uiso 1 1 calc R U C29 C 0.14912(16) 0.63393(13) 0.33287(11) 0.0202(3) Uani 1 1 d . . C30 C 0.02497(16) 0.59145(13) 0.35317(11) 0.0207(3) Uani 1 1 d . . C31 C -0.03440(17) 0.53464(14) 0.32078(12) 0.0245(4) Uani 1 1 d . . H31 H 0.0066 0.5162 0.2730 0.029 Uiso 1 1 calc R U C32 C -0.15810(18) 0.50437(15) 0.36047(13) 0.0282(4) Uani 1 1 d . . H32 H -0.2000 0.4660 0.3380 0.034 Uiso 1 1 calc R U C33 C -0.21987(17) 0.52849(14) 0.43040(13) 0.0265(4) Uani 1 1 d . . H33 H -0.3032 0.5077 0.4546 0.032 Uiso 1 1 calc R U C34 C -0.16003(16) 0.58423(13) 0.46665(11) 0.0216(4) Uani 1 1 d . . C35 C -0.03841(16) 0.61583(13) 0.42576(11) 0.0197(3) Uani 1 1 d . . C36 C -0.21004(17) 0.61066(14) 0.54049(12) 0.0253(4) Uani 1 1 d . . H36 H -0.2923 0.5913 0.5703 0.030 Uiso 1 1 calc R U C37 C -0.14048(18) 0.66413(15) 0.56931(12) 0.0268(4) Uani 1 1 d . . H37 H -0.1761 0.6802 0.6193 0.032 Uiso 1 1 calc R U C38 C -0.01814(17) 0.69604(14) 0.52734(12) 0.0249(4) Uani 1 1 d . . H38 H 0.0279 0.7329 0.5485 0.030 Uiso 1 1 calc R U C39 C 0.03279(16) 0.67225(13) 0.45477(11) 0.0205(3) Uani 1 1 d . . C40 C 0.15423(16) 0.68613(13) 0.39742(11) 0.0197(3) Uani 1 1 d . . C41 C 0.25319(16) 0.58023(14) 0.21890(11) 0.0213(4) Uani 1 1 d . . C42 C 0.20404(18) 0.61968(15) 0.14880(13) 0.0264(4) Uani 1 1 d . . H42 H 0.1639 0.6813 0.1406 0.032 Uiso 1 1 calc R U C43 C 0.21394(18) 0.56830(15) 0.09049(12) 0.0265(4) Uani 1 1 d . . C44 C 0.27129(18) 0.47772(15) 0.10488(12) 0.0258(4) Uani 1 1 d . . H44 H 0.2773 0.4420 0.0657 0.031 Uiso 1 1 calc R U C45 C 0.32030(18) 0.43801(14) 0.17535(12) 0.0257(4) Uani 1 1 d . . C46 C 0.31352(17) 0.49170(14) 0.23136(11) 0.0230(4) Uani 1 1 d . . H46 H 0.3502 0.4676 0.2781 0.028 Uiso 1 1 calc R U C47 C 0.1632(3) 0.6097(2) 0.01281(16) 0.0442(6) Uani 1 1 d . . H47A H 0.1364 0.5528 -0.0015 0.066 Uiso 1 1 d R U H47B H 0.2258 0.6534 -0.0360 0.066 Uiso 1 1 d R U H47C H 0.0946 0.6498 0.0255 0.066 Uiso 1 1 d R U C48 C 0.3764(3) 0.33676(18) 0.19254(17) 0.0452(6) Uani 1 1 d . . H48A H 0.3139 0.2821 0.2069 0.068 Uiso 1 1 calc R U H48B H 0.4136 0.3245 0.2407 0.068 Uiso 1 1 calc R U H48C H 0.4381 0.3378 0.1412 0.068 Uiso 1 1 calc R U C49 C 0.26908(16) 0.77474(14) 0.45259(11) 0.0215(4) Uani 1 1 d . . C50 C 0.21450(17) 0.86555(14) 0.44855(11) 0.0228(4) Uani 1 1 d . . H50 H 0.1668 0.8929 0.4088 0.027 Uiso 1 1 calc R U C51 C 0.23040(18) 0.91620(15) 0.50328(12) 0.0254(4) Uani 1 1 d . . C52 C 0.29987(19) 0.87312(15) 0.56142(12) 0.0264(4) Uani 1 1 d . . H52 H 0.3103 0.9070 0.5992 0.032 Uiso 1 1 calc R U C53 C 0.35440(18) 0.78209(15) 0.56583(12) 0.0258(4) Uani 1 1 d . . C54 C 0.34072(17) 0.73387(14) 0.50890(11) 0.0226(4) Uani 1 1 d . . H54 H 0.3803 0.6734 0.5087 0.027 Uiso 1 1 calc R U C55 C 0.1728(2) 1.01517(17) 0.49969(14) 0.0349(5) Uani 1 1 d . . H55A H 0.1377 1.0386 0.4501 0.052 Uiso 1 1 calc R U H55B H 0.2341 1.0669 0.4941 0.052 Uiso 1 1 calc R U H55C H 0.1093 1.0045 0.5526 0.052 Uiso 1 1 calc R U C56 C 0.4267(2) 0.73674(17) 0.63090(14) 0.0373(5) Uani 1 1 d . . H56A H 0.4894 0.7876 0.6246 0.056 Uiso 1 1 calc R U H56B H 0.4645 0.6766 0.6214 0.056 Uiso 1 1 calc R U H56C H 0.3732 0.7165 0.6890 0.056 Uiso 1 1 calc R U Cl1 Cl 0.10356(5) 0.06860(5) 0.27780(3) 0.03873(12) Uani 1 1 d . . Cl2 Cl -0.04443(7) 0.32839(5) 0.22842(5) 0.05887(19) Uani 1 1 d . . Cl3 Cl 0.50168(5) 0.57662(5) 0.36219(4) 0.04072(13) Uani 1 1 d . . Cl4 Cl 0.47086(6) 0.83993(5) 0.19085(3) 0.04537(14) Uani 1 1 d . . N1 N 0.08264(13) 0.21619(11) 0.07033(9) 0.0210(3) Uani 1 1 d . . N2 N -0.12968(13) 0.11676(11) 0.17457(9) 0.0203(3) Uani 1 1 d . . N3 N 0.24792(14) 0.63188(12) 0.27910(10) 0.0219(3) Uani 1 1 d . . N4 N 0.25676(14) 0.72395(12) 0.39440(9) 0.0216(3) Uani 1 1 d . . Zn1 Zn 0.00614(2) 0.18854(2) 0.20254(2) 0.02380(7) Uani 1 1 d . . Zn2 Zn 0.39648(2) 0.69967(2) 0.29850(2) 0.02518(7) Uani 1 1 d . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.0195(8) 0.0204(8) 0.0205(8) -0.0068(7) -0.0041(7) 0.0018(7) C2 0.0250(9) 0.0219(8) 0.0223(9) -0.0100(7) -0.0051(7) 0.0028(7) C3 0.0297(10) 0.0280(9) 0.0241(9) -0.0125(8) 0.0008(8) -0.0023(8) C4 0.0424(12) 0.0287(10) 0.0215(9) -0.0121(8) 0.0003(8) 0.0007(9) C5 0.0418(12) 0.0306(10) 0.0238(9) -0.0161(8) -0.0083(8) 0.0046(9) C6 0.0312(10) 0.0241(9) 0.0240(9) -0.0128(7) -0.0077(8) 0.0049(8) C7 0.0236(9) 0.0207(8) 0.0236(9) -0.0099(7) -0.0064(7) 0.0043(7) C8 0.0339(11) 0.0336(10) 0.0321(10) -0.0205(9) -0.0128(8) 0.0034(8) C9 0.0271(10) 0.0343(10) 0.0384(11) -0.0215(9) -0.0084(8) -0.0013(8) C10 0.0228(9) 0.0279(9) 0.0281(10) -0.0144(8) -0.0043(7) 0.0011(7) C11 0.0212(8) 0.0225(8) 0.0222(9) -0.0109(7) -0.0063(7) 0.0033(7) C12 0.0171(8) 0.0199(8) 0.0219(8) -0.0072(7) -0.0045(7) 0.0016(6) C13 0.0215(9) 0.0253(8) 0.0192(8) -0.0119(7) -0.0013(7) -0.0039(7) C14 0.0224(9) 0.0268(9) 0.0198(8) -0.0113(7) -0.0031(7) -0.0016(7) C15 0.0233(9) 0.0351(10) 0.0254(9) -0.0178(8) -0.0024(7) -0.0020(8) C16 0.0265(10) 0.0352(10) 0.0258(10) -0.0145(8) 0.0048(8) -0.0080(8) C17 0.0352(11) 0.0288(9) 0.0187(9) -0.0110(8) 0.0016(8) -0.0054(8) C18 0.0289(10) 0.0280(9) 0.0219(9) -0.0116(8) -0.0051(7) -0.0002(8) C19 0.0235(10) 0.0519(13) 0.0363(11) -0.0181(10) -0.0028(8) 0.0007(9) C20 0.0479(14) 0.0352(11) 0.0278(11) -0.0053(9) 0.0022(9) -0.0034(10) C21 0.0201(8) 0.0229(8) 0.0165(8) -0.0099(7) -0.0025(6) -0.0017(7) C22 0.0213(9) 0.0245(8) 0.0201(8) -0.0110(7) -0.0058(7) 0.0034(7) C23 0.0272(9) 0.0211(8) 0.0225(9) -0.0095(7) -0.0067(7) 0.0006(7) C24 0.0219(9) 0.0244(9) 0.0210(8) -0.0072(7) -0.0015(7) -0.0033(7) C25 0.0210(9) 0.0223(8) 0.0233(9) -0.0097(7) -0.0042(7) 0.0004(7) C26 0.0224(9) 0.0217(8) 0.0196(8) -0.0056(7) -0.0055(7) 0.0005(7) C27 0.0337(11) 0.0274(10) 0.0363(11) -0.0012(9) -0.0099(9) 0.0009(8) C28 0.0212(9) 0.0322(10) 0.0386(11) -0.0048(9) -0.0053(8) 0.0021(8) C29 0.0216(9) 0.0213(8) 0.0207(8) -0.0101(7) -0.0069(7) 0.0019(7) C30 0.0226(9) 0.0203(8) 0.0193(8) -0.0062(7) -0.0063(7) 0.0016(7) C31 0.0243(9) 0.0262(9) 0.0251(9) -0.0105(7) -0.0073(7) -0.0014(7) C32 0.0265(10) 0.0297(9) 0.0302(10) -0.0088(8) -0.0122(8) -0.0038(8) C33 0.0199(9) 0.0262(9) 0.0302(10) -0.0040(8) -0.0086(7) -0.0014(7) C34 0.0196(8) 0.0207(8) 0.0215(8) -0.0023(7) -0.0067(7) 0.0021(7) C35 0.0207(8) 0.0190(8) 0.0188(8) -0.0050(7) -0.0062(7) 0.0023(7) C36 0.0204(9) 0.0258(9) 0.0233(9) -0.0025(7) -0.0023(7) 0.0020(7) C37 0.0284(10) 0.0282(9) 0.0195(9) -0.0070(7) -0.0002(7) 0.0019(8) C38 0.0253(9) 0.0276(9) 0.0214(9) -0.0102(7) -0.0027(7) -0.0007(7) C39 0.0208(9) 0.0213(8) 0.0193(8) -0.0072(7) -0.0045(7) 0.0007(7) C40 0.0217(9) 0.0210(8) 0.0174(8) -0.0079(7) -0.0047(7) 0.0006(7) C41 0.0185(8) 0.0267(9) 0.0201(8) -0.0127(7) -0.0003(7) -0.0044(7) C42 0.0264(9) 0.0281(9) 0.0300(10) -0.0150(8) -0.0101(8) 0.0066(8) C43 0.0277(10) 0.0319(10) 0.0256(9) -0.0147(8) -0.0102(8) 0.0038(8) C44 0.0296(10) 0.0298(9) 0.0247(9) -0.0171(8) -0.0079(8) 0.0021(8) C45 0.0304(10) 0.0234(9) 0.0260(9) -0.0114(8) -0.0079(8) 0.0022(7) C46 0.0250(9) 0.0258(9) 0.0187(8) -0.0078(7) -0.0062(7) -0.0019(7) C47 0.0601(16) 0.0516(14) 0.0412(13) -0.0294(11) -0.0317(12) 0.0262(12) C48 0.0685(17) 0.0361(12) 0.0494(14) -0.0243(11) -0.0359(13) 0.0221(12) C49 0.0211(8) 0.0272(9) 0.0165(8) -0.0111(7) 0.0009(6) -0.0070(7) C50 0.0220(9) 0.0289(9) 0.0185(8) -0.0100(7) -0.0040(7) -0.0017(7) C51 0.0293(10) 0.0276(9) 0.0195(8) -0.0110(7) -0.0019(7) -0.0030(8) C52 0.0348(10) 0.0295(9) 0.0181(8) -0.0121(7) -0.0067(7) -0.0028(8) C53 0.0317(10) 0.0273(9) 0.0179(8) -0.0066(7) -0.0065(7) -0.0034(8) C54 0.0265(9) 0.0211(8) 0.0185(8) -0.0060(7) -0.0036(7) -0.0031(7) C55 0.0445(12) 0.0373(11) 0.0326(11) -0.0215(9) -0.0140(9) 0.0095(9) C56 0.0544(14) 0.0359(11) 0.0286(10) -0.0119(9) -0.0220(10) 0.0053(10) Cl1 0.0316(3) 0.0556(3) 0.0281(2) -0.0089(2) -0.0138(2) 0.0062(2) Cl2 0.0568(4) 0.0498(3) 0.0782(5) -0.0449(4) 0.0013(3) -0.0022(3) Cl3 0.0307(3) 0.0569(3) 0.0435(3) -0.0250(3) -0.0153(2) 0.0123(2) Cl4 0.0509(3) 0.0485(3) 0.0314(3) -0.0144(2) 0.0019(2) -0.0212(3) N1 0.0184(7) 0.0237(7) 0.0197(7) -0.0070(6) -0.0033(6) -0.0014(6) N2 0.0182(7) 0.0238(7) 0.0193(7) -0.0076(6) -0.0047(6) -0.0003(6) N3 0.0209(7) 0.0267(8) 0.0220(7) -0.0137(6) -0.0049(6) -0.0003(6) N4 0.0216(7) 0.0268(7) 0.0194(7) -0.0128(6) -0.0033(6) -0.0013(6) Zn1 0.02025(13) 0.03241(14) 0.02051(13) -0.01181(10) -0.00412(9) -0.00265(10) Zn2 0.01901(13) 0.03640(15) 0.02439(13) -0.01770(11) -0.00243(10) -0.00295(10) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Zn Zn -1.5491 0.6778 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle N1 C1 C2 135.30(17) N1 C1 C12 117.69(15) C2 C1 C12 106.98(15) C3 C2 C7 119.38(17) C3 C2 C1 135.00(18) C7 C2 C1 105.62(15) C2 C3 C4 118.09(19) C2 C3 H3 121.0 C4 C3 H3 121.0 C5 C4 C3 122.55(19) C5 C4 H4 118.7 C3 C4 H4 118.7 C4 C5 C6 120.62(18) C4 C5 H5 119.7 C6 C5 H5 119.7 C7 C6 C8 116.62(18) C7 C6 C5 116.29(18) C8 C6 C5 127.09(18) C6 C7 C2 123.04(17) C6 C7 C11 122.42(17) C2 C7 C11 114.53(16) C9 C8 C6 120.53(18) C9 C8 H8 119.7 C6 C8 H8 119.7 C8 C9 C10 122.52(19) C8 C9 H9 118.7 C10 C9 H9 118.7 C11 C10 C9 118.17(18) C11 C10 H10 120.9 C9 C10 H10 120.9 C10 C11 C7 119.70(17) C10 C11 C12 134.66(17) C7 C11 C12 105.64(16) N2 C12 C11 134.93(17) N2 C12 C1 117.88(15) C11 C12 C1 107.18(15) C14 C13 C18 121.20(17) C14 C13 N1 117.47(16) C18 C13 N1 121.32(17) C15 C14 C13 119.72(18) C15 C14 H14 120.1 C13 C14 H14 120.1 C14 C15 C16 118.64(18) C14 C15 C19 120.66(19) C16 C15 C19 120.69(18) C17 C16 C15 122.06(18) C17 C16 H16 119.0 C15 C16 H16 119.0 C16 C17 C18 118.77(18) C16 C17 C20 120.85(19) C18 C17 C20 120.4(2) C13 C18 C17 119.47(18) C13 C18 H18 120.3 C17 C18 H18 120.3 C15 C19 H19A 109.5 C15 C19 H19B 109.5 H19A C19 H19B 109.5 C15 C19 H19C 109.5 H19A C19 H19C 109.5 H19B C19 H19C 109.5 C17 C20 H20A 109.5 C17 C20 H20B 109.5 H20A C20 H20B 109.5 C17 C20 H20C 109.5 H20A C20 H20C 109.5 H20B C20 H20C 109.5 C26 C21 C22 121.22(16) C26 C21 N2 121.10(16) C22 C21 N2 117.68(16) C21 C22 C23 119.73(17) C21 C22 H22 120.1 C23 C22 H22 120.1 C24 C23 C22 118.78(17) C24 C23 C27 120.69(18) C22 C23 C27 120.51(18) C23 C24 C25 121.75(17) C23 C24 H24 119.1 C25 C24 H24 119.1 C24 C25 C26 118.80(17) C24 C25 C28 119.86(17) C26 C25 C28 121.29(17) C21 C26 C25 119.63(17) C21 C26 H26 120.2 C25 C26 H26 120.2 C23 C27 H27A 109.5 C23 C27 H27B 109.5 H27A C27 H27B 109.5 C23 C27 H27C 109.5 H27A C27 H27C 109.5 H27B C27 H27C 109.5 C25 C28 H28A 109.5 C25 C28 H28B 109.5 H28A C28 H28B 109.5 C25 C28 H28C 109.5 H28A C28 H28C 109.5 H28B C28 H28C 109.5 N3 C29 C30 135.15(16) N3 C29 C40 117.43(16) C30 C29 C40 107.31(14) C31 C30 C35 119.36(17) C31 C30 C29 134.96(17) C35 C30 C29 105.62(15) C30 C31 C32 118.31(17) C30 C31 H31 120.8 C32 C31 H31 120.8 C33 C32 C31 122.42(18) C33 C32 H32 118.8 C31 C32 H32 118.8 C32 C33 C34 120.43(18) C32 C33 H33 119.8 C34 C33 H33 119.8 C35 C34 C33 116.70(17) C35 C34 C36 116.47(17) C33 C34 C36 126.82(18) C34 C35 C39 122.93(16) C34 C35 C30 122.73(16) C39 C35 C30 114.32(16) C37 C36 C34 120.58(17) C37 C36 H36 119.7 C34 C36 H36 119.7 C36 C37 C38 122.47(17) C36 C37 H37 118.8 C38 C37 H37 118.8 C39 C38 C37 118.28(18) C39 C38 H38 120.9 C37 C38 H38 120.9 C38 C39 C35 119.26(17) C38 C39 C40 134.73(17) C35 C39 C40 105.88(15) N4 C40 C39 135.10(16) N4 C40 C29 117.85(15) C39 C40 C29 106.86(15) C46 C41 C42 121.22(16) C46 C41 N3 117.35(16) C42 C41 N3 121.37(17) C41 C42 C43 119.50(18) C41 C42 H42 120.2 C43 C42 H42 120.2 C44 C43 C42 118.97(18) C44 C43 C47 120.03(17) C42 C43 C47 121.00(18) C43 C44 C45 121.50(17) C43 C44 H44 119.2 C45 C44 H44 119.2 C46 C45 C44 118.99(17) C46 C45 C48 120.23(18) C44 C45 C48 120.75(17) C41 C46 C45 119.72(17) C41 C46 H46 120.1 C45 C46 H46 120.1 C43 C47 H47A 109.5 C43 C47 H47B 109.5 H47A C47 H47B 109.5 C43 C47 H47C 109.5 H47A C47 H47C 109.5 H47B C47 H47C 109.5 C45 C48 H48A 109.5 C45 C48 H48B 109.5 H48A C48 H48B 109.5 C45 C48 H48C 109.5 H48A C48 H48C 109.5 H48B C48 H48C 109.5 C54 C49 C50 121.61(16) C54 C49 N4 118.51(16) C50 C49 N4 119.81(16) C49 C50 C51 119.41(17) C49 C50 H50 120.3 C51 C50 H50 120.3 C50 C51 C52 118.63(18) C50 C51 C55 120.40(18) C52 C51 C55 120.97(17) C53 C52 C51 122.14(17) C53 C52 H52 118.9 C51 C52 H52 118.9 C52 C53 C54 118.59(18) C52 C53 C56 120.57(18) C54 C53 C56 120.85(18) C49 C54 C53 119.54(17) C49 C54 H54 120.2 C53 C54 H54 120.2 C51 C55 H55A 109.5 C51 C55 H55B 109.5 H55A C55 H55B 109.5 C51 C55 H55C 109.5 H55A C55 H55C 109.5 H55B C55 H55C 109.5 C53 C56 H56A 109.5 C53 C56 H56B 109.5 H56A C56 H56B 109.5 C53 C56 H56C 109.5 H56A C56 H56C 109.5 H56B C56 H56C 109.5 C1 N1 C13 121.40(15) C1 N1 Zn1 111.85(12) C13 N1 Zn1 126.75(11) C12 N2 C21 119.86(15) C12 N2 Zn1 112.39(12) C21 N2 Zn1 127.64(11) C29 N3 C41 121.45(15) C29 N3 Zn2 112.38(12) C41 N3 Zn2 125.95(12) C40 N4 C49 121.28(15) C40 N4 Zn2 112.22(12) C49 N4 Zn2 126.50(12) N2 Zn1 N1 80.14(6) N2 Zn1 Cl2 114.20(5) N1 Zn1 Cl2 112.27(5) N2 Zn1 Cl1 108.03(4) N1 Zn1 Cl1 108.52(4) Cl2 Zn1 Cl1 124.77(3) N4 Zn2 N3 80.07(6) N4 Zn2 Cl4 113.47(5) N3 Zn2 Cl4 111.65(5) N4 Zn2 Cl3 108.00(5) N3 Zn2 Cl3 108.27(5) Cl4 Zn2 Cl3 125.93(3) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance C1 N1 1.281(2) C1 C2 1.474(2) C1 C12 1.517(2) C2 C3 1.383(3) C2 C7 1.414(3) C3 C4 1.420(3) C3 H3 0.9500 C4 C5 1.370(3) C4 H4 0.9500 C5 C6 1.424(3) C5 H5 0.9500 C6 C7 1.406(3) C6 C8 1.420(3) C7 C11 1.417(3) C8 C9 1.373(3) C8 H8 0.9500 C9 C10 1.413(3) C9 H9 0.9500 C10 C11 1.379(3) C10 H10 0.9500 C11 C12 1.469(2) C12 N2 1.281(2) C13 C14 1.390(3) C13 C18 1.390(3) C13 N1 1.429(2) C14 C15 1.390(3) C14 H14 0.9500 C15 C16 1.395(3) C15 C19 1.505(3) C16 C17 1.387(3) C16 H16 0.9500 C17 C18 1.396(3) C17 C20 1.512(3) C18 H18 0.9500 C19 H19A 0.9800 C19 H19B 0.9800 C19 H19C 0.9800 C20 H20A 0.9800 C20 H20B 0.9800 C20 H20C 0.9800 C21 C26 1.385(3) C21 C22 1.389(3) C21 N2 1.435(2) C22 C23 1.393(3) C22 H22 0.9500 C23 C24 1.390(3) C23 C27 1.506(3) C24 C25 1.395(3) C24 H24 0.9500 C25 C26 1.395(3) C25 C28 1.501(3) C26 H26 0.9500 C27 H27A 0.9800 C27 H27B 0.9800 C27 H27C 0.9800 C28 H28A 0.9800 C28 H28B 0.9800 C28 H28C 0.9800 C29 N3 1.279(2) C29 C30 1.465(2) C29 C40 1.525(2) C30 C31 1.377(3) C30 C35 1.421(2) C31 C32 1.416(3) C31 H31 0.9500 C32 C33 1.376(3) C32 H32 0.9500 C33 C34 1.418(3) C33 H33 0.9500 C34 C35 1.401(2) C34 C36 1.418(3) C35 C39 1.419(2) C36 C37 1.377(3) C36 H36 0.9500 C37 C38 1.412(3) C37 H37 0.9500 C38 C39 1.381(2) C38 H38 0.9500 C39 C40 1.466(2) C40 N4 1.279(2) C41 C46 1.381(3) C41 C42 1.387(3) C41 N3 1.432(2) C42 C43 1.394(3) C42 H42 0.9500 C43 C44 1.387(3) C43 C47 1.508(3) C44 C45 1.392(3) C44 H44 0.9500 C45 C46 1.389(3) C45 C48 1.506(3) C46 H46 0.9500 C47 H47A 0.9800 C47 H47B 0.9800 C47 H47C 0.9800 C48 H48A 0.9800 C48 H48B 0.9800 C48 H48C 0.9800 C49 C54 1.385(3) C49 C50 1.389(3) C49 N4 1.435(2) C50 C51 1.393(3) C50 H50 0.9500 C51 C52 1.394(3) C51 C55 1.507(3) C52 C53 1.391(3) C52 H52 0.9500 C53 C54 1.394(3) C53 C56 1.508(3) C54 H54 0.9500 C55 H55A 0.9800 C55 H55B 0.9800 C55 H55C 0.9800 C56 H56A 0.9800 C56 H56B 0.9800 C56 H56C 0.9800 Cl1 Zn1 2.2061(6) Cl2 Zn1 2.1792(6) Cl3 Zn2 2.2081(6) Cl4 Zn2 2.1899(6) N1 Zn1 2.1160(15) N2 Zn1 2.0964(15) N3 Zn2 2.1086(15) N4 Zn2 2.1067(15) loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion N1 C1 C2 C3 -2.3(4) C12 C1 C2 C3 179.7(2) N1 C1 C2 C7 177.7(2) C12 C1 C2 C7 -0.27(19) C7 C2 C3 C4 1.5(3) C1 C2 C3 C4 -178.40(19) C2 C3 C4 C5 -1.2(3) C3 C4 C5 C6 -0.4(3) C4 C5 C6 C7 1.6(3) C4 C5 C6 C8 -178.9(2) C8 C6 C7 C2 179.23(17) C5 C6 C7 C2 -1.2(3) C8 C6 C7 C11 0.1(3) C5 C6 C7 C11 179.71(17) C3 C2 C7 C6 -0.4(3) C1 C2 C7 C6 179.59(16) C3 C2 C7 C11 178.79(17) C1 C2 C7 C11 -1.3(2) C7 C6 C8 C9 -1.8(3) C5 C6 C8 C9 178.7(2) C6 C8 C9 C10 1.5(3) C8 C9 C10 C11 0.6(3) C9 C10 C11 C7 -2.2(3) C9 C10 C11 C12 178.43(19) C6 C7 C11 C10 1.9(3) C2 C7 C11 C10 -177.31(17) C6 C7 C11 C12 -178.58(16) C2 C7 C11 C12 2.3(2) C10 C11 C12 N2 -1.7(4) C7 C11 C12 N2 178.8(2) C10 C11 C12 C1 177.2(2) C7 C11 C12 C1 -2.25(19) N1 C1 C12 N2 2.3(2) C2 C1 C12 N2 -179.28(15) N1 C1 C12 C11 -176.83(16) C2 C1 C12 C11 1.58(19) C18 C13 C14 C15 -4.4(3) N1 C13 C14 C15 176.70(16) C13 C14 C15 C16 3.5(3) C13 C14 C15 C19 -175.22(17) C14 C15 C16 C17 -0.6(3) C19 C15 C16 C17 178.09(18) C15 C16 C17 C18 -1.5(3) C15 C16 C17 C20 179.97(18) C14 C13 C18 C17 2.2(3) N1 C13 C18 C17 -178.87(16) C16 C17 C18 C13 0.7(3) C20 C17 C18 C13 179.24(17) C26 C21 C22 C23 3.6(3) N2 C21 C22 C23 -176.28(15) C21 C22 C23 C24 -2.8(3) C21 C22 C23 C27 175.42(17) C22 C23 C24 C25 0.8(3) C27 C23 C24 C25 -177.44(17) C23 C24 C25 C26 0.5(3) C23 C24 C25 C28 177.87(17) C22 C21 C26 C25 -2.3(3) N2 C21 C26 C25 177.63(16) C24 C25 C26 C21 0.2(3) C28 C25 C26 C21 -177.13(17) N3 C29 C30 C31 -1.9(4) C40 C29 C30 C31 -177.8(2) N3 C29 C30 C35 175.1(2) C40 C29 C30 C35 -0.77(19) C35 C30 C31 C32 1.3(3) C29 C30 C31 C32 177.99(19) C30 C31 C32 C33 -0.9(3) C31 C32 C33 C34 -1.0(3) C32 C33 C34 C35 2.4(3) C32 C33 C34 C36 -177.03(18) C33 C34 C35 C39 179.92(16) C36 C34 C35 C39 -0.6(3) C33 C34 C35 C30 -2.0(3) C36 C34 C35 C30 177.50(16) C31 C30 C35 C34 0.1(3) C29 C30 C35 C34 -177.42(16) C31 C30 C35 C39 178.39(16) C29 C30 C35 C39 0.8(2) C35 C34 C36 C37 -0.3(3) C33 C34 C36 C37 179.08(18) C34 C36 C37 C38 0.7(3) C36 C37 C38 C39 -0.1(3) C37 C38 C39 C35 -0.9(3) C37 C38 C39 C40 -176.11(19) C34 C35 C39 C38 1.2(3) C30 C35 C39 C38 -177.02(17) C34 C35 C39 C40 177.72(16) C30 C35 C39 C40 -0.5(2) C38 C39 C40 N4 1.0(4) C35 C39 C40 N4 -174.7(2) C38 C39 C40 C29 175.7(2) C35 C39 C40 C29 0.00(19) N3 C29 C40 N4 -0.5(3) C30 C29 C40 N4 176.23(16) N3 C29 C40 C39 -176.25(16) C30 C29 C40 C39 0.48(19) C46 C41 C42 C43 1.0(3) N3 C41 C42 C43 178.33(17) C41 C42 C43 C44 1.0(3) C41 C42 C43 C47 -179.1(2) C42 C43 C44 C45 -0.9(3) C47 C43 C44 C45 179.3(2) C43 C44 C45 C46 -1.3(3) C43 C44 C45 C48 176.7(2) C42 C41 C46 C45 -3.2(3) N3 C41 C46 C45 179.35(16) C44 C45 C46 C41 3.4(3) C48 C45 C46 C41 -174.7(2) C54 C49 C50 C51 -1.0(3) N4 C49 C50 C51 -177.79(16) C49 C50 C51 C52 -0.8(3) C49 C50 C51 C55 179.57(18) C50 C51 C52 C53 0.6(3) C55 C51 C52 C53 -179.73(19) C51 C52 C53 C54 1.3(3) C51 C52 C53 C56 -178.69(19) C50 C49 C54 C53 3.0(3) N4 C49 C54 C53 179.78(16) C52 C53 C54 C49 -3.0(3) C56 C53 C54 C49 176.95(19) C2 C1 N1 C13 0.9(3) C12 C1 N1 C13 178.75(15) C2 C1 N1 Zn1 -179.10(17) C12 C1 N1 Zn1 -1.26(19) C14 C13 N1 C1 -117.39(19) C18 C13 N1 C1 63.7(2) C14 C13 N1 Zn1 62.6(2) C18 C13 N1 Zn1 -116.31(17) C11 C12 N2 C21 0.4(3) C1 C12 N2 C21 -178.48(15) C11 C12 N2 Zn1 176.84(17) C1 C12 N2 Zn1 -1.99(19) C26 C21 N2 C12 -70.4(2) C22 C21 N2 C12 109.54(19) C26 C21 N2 Zn1 113.74(17) C22 C21 N2 Zn1 -66.4(2) C30 C29 N3 C41 1.3(3) C40 C29 N3 C41 176.87(16) C30 C29 N3 Zn2 -173.62(18) C40 C29 N3 Zn2 2.0(2) C46 C41 N3 C29 -110.0(2) C42 C41 N3 C29 72.6(2) C46 C41 N3 Zn2 64.2(2) C42 C41 N3 Zn2 -113.21(18) C39 C40 N4 C49 -6.1(3) C29 C40 N4 C49 179.68(15) C39 C40 N4 Zn2 172.98(17) C29 C40 N4 Zn2 -1.2(2) C54 C49 N4 C40 117.6(2) C50 C49 N4 C40 -65.5(2) C54 C49 N4 Zn2 -61.3(2) C50 C49 N4 Zn2 115.55(17)