Crystallography Open Database

Information card for entry 4103684

Preview

Coordinates	4103684.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C140 H116 N20 O8 U4
Calculated formula	C140 H116 N20 O8 U4
Title of publication	Multielectron Redox Reactions Involving C-C Coupling and Cleavage in Uranium Schiff Base Complexes
Authors of publication	Clément Camp; Victor Mougel; Pawel Horeglad; Jacques Pécaut; Marinella Mazzanti
Journal of publication	Journal of the American Chemical Society
Year of publication	2010
Journal volume	132
Pages of publication	17374 - 17377
a	11.6556 ± 0.0002 Å
b	12.0214 ± 0.0002 Å
c	22.0847 ± 0.0004 Å
α	103.13 ± 0.0014°
β	99.9454 ± 0.0015°
γ	91.5909 ± 0.0014°
Cell volume	2961.01 ± 0.09 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0721
Residual factor for significantly intense reflections	0.0459
Weighted residual factors for significantly intense reflections	0.1039
Weighted residual factors for all reflections included in the refinement	0.1083
Goodness-of-fit parameter for all reflections included in the refinement	0.853
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178782 (current)	2016-03-21	cif/4/10/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/10/36.	4103684.cif
120076	2014-07-11	Adding DOIs to range 4/10 structures.	4103684.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4103684.cif
26717	2011-09-24	../uploads/cif-deposit/cod/cif Adding structures of 4103684 via cif-deposit CGI script.	4103684.cif