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Information card for entry 4103699
Preview
| Coordinates | 4103699.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C118 H56 La2 Si |
|---|---|
| Calculated formula | C118 H56 La2.002 Si |
| Title of publication | Thermal Carbosilylation of Endohedral Dimetallofullerene La2@Ih-C80 with Silirane |
| Authors of publication | Michio Yamada; Mari Minowa; Satoru Sato; Masahiro Kako; Zdenek Slanina; Naomi Mizorogi; Takahiro Tsuchiya; Yutaka Maeda; Shigeru Nagase; Takeshi Akasaka |
| Journal of publication | Journal of the American Chemical Society |
| Year of publication | 2010 |
| Journal volume | 132 |
| Pages of publication | 17953 - 17960 |
| a | 14.097 ± 0.006 Å |
| b | 14.762 ± 0.007 Å |
| c | 34.122 ± 0.014 Å |
| α | 90° |
| β | 90.415 ± 0.007° |
| γ | 90° |
| Cell volume | 7101 ± 5 Å3 |
| Cell temperature | 90 ± 2 K |
| Ambient diffraction temperature | 90 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.2287 |
| Residual factor for significantly intense reflections | 0.1214 |
| Weighted residual factors for significantly intense reflections | 0.3428 |
| Weighted residual factors for all reflections included in the refinement | 0.368 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.978 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.6889 Å |
| Diffraction radiation type | synchrotron |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 295947 (current) | 2024-11-16 | Replaced the '\/Y' character sequence with the backslash character ('\') in multiple data values. |
4103699.cif |
| 178782 | 2016-03-21 | cif/4/10/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/10/36. |
4103699.cif |
| 120076 | 2014-07-11 | Adding DOIs to range 4/10 structures. | 4103699.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4103699.cif |
| 26732 | 2011-09-24 | ../uploads/cif-deposit/cod/cif Adding structures of 4103699 via cif-deposit CGI script. |
4103699.cif |
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Users of the data should acknowledge the original authors of the
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