Crystallography Open Database

Information card for entry 4103826

Preview

Coordinates	4103826.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	Br4 Tc
Calculated formula	Br4 Tc
SMILES	[Tc+4].[Br-].[Br-].[Br-].[Br-]
Title of publication	Preparation of the Binary Technetium Bromides: TcBr3 and TcBr4
Authors of publication	Frederic Poineau; Efrain E. Rodriguez; Paul M. Forster; Alfred P. Sattelberger; Anthony K. Cheetham; Kenneth R. Czerwinski
Journal of publication	Journal of the American Chemical Society
Year of publication	2009
Journal volume	131
Pages of publication	910 - 911
a	6.3237 ± 0.0005 Å
b	12.1777 ± 0.0009 Å
c	14.7397 ± 0.0011 Å
α	90°
β	90°
γ	90°
Cell volume	1135.08 ± 0.15 Å³
Cell temperature	157 ± 2 K
Ambient diffraction temperature	157 ± 2 K
Number of distinct elements	2
Space group number	61
Hermann-Mauguin space group symbol	P b c a
Hall space group symbol	-P 2ac 2ab
Residual factor for all reflections	0.0306
Residual factor for significantly intense reflections	0.0216
Weighted residual factors for significantly intense reflections	0.0441
Weighted residual factors for all reflections included in the refinement	0.0466
Goodness-of-fit parameter for all reflections included in the refinement	1.071
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178784 (current)	2016-03-21	cif/4/10/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/10/38.	4103826.cif
120076	2014-07-11	Adding DOIs to range 4/10 structures.	4103826.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4103826.cif
28301	2011-10-24	../uploads/cif-deposit/cod/cif Adding structures of 4103826 via cif-deposit CGI script.	4103826.cif