Crystallography Open Database

Information card for entry 4105343

Preview

Coordinates	4105343.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C16 H16 O6
Calculated formula	C16 H15.94 O6
Title of publication	Concise Syntheses of (-)-Galanthamine and (\±)-Codeine via Intramolecular Alkylation of a Phenol Derivative
Authors of publication	Philip Magnus; Neeraj Sane; Benjamin P. Fauber; Vince Lynch
Journal of publication	Journal of the American Chemical Society
Year of publication	2009
Journal volume	131
Pages of publication	16045 - 16047
a	9.6329 ± 0.0002 Å
b	20.8917 ± 0.0006 Å
c	7.191 ± 0.0003 Å
α	90°
β	109.168 ± 0.0013°
γ	90°
Cell volume	1366.94 ± 0.08 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	3
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.064
Residual factor for significantly intense reflections	0.042
Weighted residual factors for significantly intense reflections	0.0927
Weighted residual factors for all reflections included in the refinement	0.1028
Goodness-of-fit parameter for all reflections included in the refinement	1.032
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178799 (current)	2016-03-21	cif/4/10/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/10/53.	4105343.cif
120076	2014-07-11	Adding DOIs to range 4/10 structures.	4105343.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4105343.cif
30538	2011-11-13	../uploads/cif-deposit/cod/cif Adding structures of 4105343 via cif-deposit CGI script.	4105343.cif