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Information card for entry 4114565
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Coordinates | 4114565.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C36 H57.33 K2 O10 Si |
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Calculated formula | C32 H48 K2 O10 Si |
Title of publication | Structure and Chemistry of 1-Silafluorenyl Dianion, Its Derivatives, and an Organosilicon Diradical Dianion |
Authors of publication | Yuxia Liu; Thomas C. Stringfellow; David Ballweg; Ilia A. Guzei; Robert West |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2002 |
Journal volume | 124 |
Pages of publication | 49 - 57 |
a | 10.5459 ± 0.0009 Å |
b | 15.9281 ± 0.0012 Å |
c | 17.8197 ± 0.0015 Å |
α | 95.02 ± 0.002° |
β | 98.726 ± 0.002° |
γ | 96.053 ± 0.002° |
Cell volume | 2925.8 ± 0.4 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1203 |
Residual factor for significantly intense reflections | 0.063 |
Weighted residual factors for significantly intense reflections | 0.169 |
Weighted residual factors for all reflections included in the refinement | 0.1963 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.026 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
178916 (current) | 2016-03-22 | cif/4/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/11/45. |
4114565.cif |
120077 | 2014-07-12 | Adding DOIs to range 4/11 structures. | 4114565.cif |
67895 | 2012-10-08 | cif/ Adding structures of 4114565 via cif-deposit CGI script. |
4114565.cif |
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Users of the data should acknowledge the original authors of the
structural data.