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Information card for entry 4116444
Preview
Coordinates | 4116444.cif |
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Original paper (by DOI) | HTML |
Formula | C44 H93 O2.5 P2 Ru Si3 |
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Calculated formula | C44 H93 O2.5 P2 Ru Si3 |
Title of publication | Ruthenium Complexes Containing Two Ru-(η2-Si-H) Bonds: Synthesis, Spectroscopic Properties, Structural Data, Theoretical Calculations, and Reactivity Studies |
Authors of publication | Fabien Delpech; Sylviane Sabo-Etienne; Jean-Claude Daran; Bruno Chaudret; Khansaa Hussein; Colin J. Marsden; Jean-Claude Barthelat |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 1999 |
Journal volume | 121 |
Journal issue | 28 |
Pages of publication | 6668 - 6682 |
a | 20.272 ± 0.002 Å |
b | 19.862 ± 0.003 Å |
c | 24.91 ± 0.003 Å |
α | 90° |
β | 93.943 ± 0.014° |
γ | 90° |
Cell volume | 10006 ± 2 Å3 |
Cell temperature | 180 ± 2 K |
Ambient diffraction temperature | 180 ± 2 K |
Number of distinct elements | 6 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for significantly intense reflections | 0.0326 |
Weighted residual factors for significantly intense reflections | 0.04 |
Goodness-of-fit parameter for significantly intense reflections | 1.0951 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
176467 (current) | 2016-02-16 | cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4. |
4116444.cif |
78899 | 2013-04-03 | cif/4/ (antanas@lokys) Added closing parentheses to _atom_site_aniso_U_12 values as well as _atom_site_type_symbol label and values to CIFs 4116442, 4116443, 4116444. |
4116444.cif |
71763 | 2013-01-21 | cif/ Adding structures of 4116444 via cif-deposit CGI script. |
4116444.cif |
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Users of the data should acknowledge the original authors of the
structural data.