Crystallography Open Database

Information card for entry 4124278

Preview

Coordinates	4124278.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C44 H86 K2 N4 O2 Si4 Th
Calculated formula	C44 H86 K2 N4 O2 Si4 Th
Title of publication	Thorium Mono- and Bis(imido) Complexes Made by Reprotonation of cyclo-Metalated Amides.
Authors of publication	Bell, Nicola L.; Maron, Laurent; Arnold, Polly L.
Journal of publication	Journal of the American Chemical Society
Year of publication	2015
Pages of publication	150814165612001
a	13.1981 ± 0.0003 Å
b	13.8897 ± 0.0003 Å
c	18.8942 ± 0.0004 Å
α	94.64 ± 0.002°
β	94.357 ± 0.002°
γ	116.604 ± 0.002°
Cell volume	3062.21 ± 0.13 Å³
Cell temperature	170 ± 2 K
Ambient diffraction temperature	170 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.047
Residual factor for significantly intense reflections	0.0367
Weighted residual factors for significantly intense reflections	0.089
Weighted residual factors for all reflections included in the refinement	0.0927
Goodness-of-fit parameter for all reflections included in the refinement	1.028
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
154654 (current)	2015-09-06	cif/ Updating files of 4124276, 4124277, 4124278 Original log message: Adding full bibliography for 4124276--4124278.cif.	4124278.cif
153452	2015-08-16	cif/ Adding structures of 4124276, 4124277, 4124278 via cif-deposit CGI script.	4124278.cif