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Information card for entry 4124294
Preview
| Coordinates | 4124294.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C28.25 H39 Cl N O3.25 |
|---|---|
| Calculated formula | C28.25 H39 Cl N O3.25 |
| Title of publication | Total Synthesis of the Galbulimima Alkaloids Himandravine and GB17 Using Biomimetic Diels-Alder Reactions of Double Diene Precursors. |
| Authors of publication | Larson, Reed T.; Pemberton, Ryan P.; Franke, Jenna M.; Tantillo, Dean J.; Thomson, Regan J. |
| Journal of publication | Journal of the American Chemical Society |
| Year of publication | 2015 |
| Journal volume | 137 |
| Journal issue | 34 |
| Pages of publication | 11197 - 11204 |
| a | 19.3133 ± 0.001 Å |
| b | 8.6913 ± 0.0004 Å |
| c | 18.1902 ± 0.0013 Å |
| α | 90° |
| β | 99.683 ± 0.005° |
| γ | 90° |
| Cell volume | 3009.9 ± 0.3 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 K |
| Number of distinct elements | 5 |
| Space group number | 5 |
| Hermann-Mauguin space group symbol | C 1 2 1 |
| Hall space group symbol | C 2y |
| Residual factor for all reflections | 0.1655 |
| Residual factor for significantly intense reflections | 0.0996 |
| Weighted residual factors for significantly intense reflections | 0.2531 |
| Weighted residual factors for all reflections included in the refinement | 0.3085 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.006 |
| Diffraction radiation wavelength | 1.54178 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 154649 (current) | 2015-09-06 | cif/ Updating files of 4124293, 4124294, 4124295 Original log message: Adding full bibliography for 4124293--4124295.cif. |
4124294.cif |
| 153649 | 2015-08-26 | cif/ Adding structures of 4124294 via cif-deposit CGI script. |
4124294.cif |
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Users of the data should acknowledge the original authors of the
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