#------------------------------------------------------------------------------ #$Date: 2016-06-17 01:46:50 +0300 (Fri, 17 Jun 2016) $ #$Revision: 183572 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/12/50/4125092.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4125092 loop_ _publ_author_name 'Transue, Wesley J.' 'Velian, Alexandra' 'Nava, Matthew' 'Martin-Drumel, Marie-Aline' 'Womack, Caroline C.' 'Jiang, Jun' 'Hou, Gao-Lei' 'Wang, Xue-Bin' 'McCarthy, Michael C.' 'Field, Robert W.' 'Cummins, Christopher C.' _publ_section_title ; A Molecular Precursor to Phosphaethyne and Its Application in Synthesis of the Aromatic 1,2,3,4-Phosphatriazolate Anion. ; _journal_issue 21 _journal_name_full 'Journal of the American Chemical Society' _journal_page_first 6731 _journal_page_last 6734 _journal_paper_doi 10.1021/jacs.6b03910 _journal_volume 138 _journal_year 2016 _chemical_formula_sum 'C33 H59 K N5 O7 P' _chemical_formula_weight 707.92 _chemical_name_systematic ; ? ; _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2014 _cell_angle_alpha 83.904(3) _cell_angle_beta 82.249(3) _cell_angle_gamma 85.085(3) _cell_formula_units_Z 2 _cell_length_a 11.0044(17) _cell_length_b 12.0737(19) _cell_length_c 13.946(2) _cell_measurement_reflns_used 9966 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 26.38 _cell_measurement_theta_min 2.23 _cell_volume 1820.8(5) _computing_cell_refinement 'SAINT 7.46A (Bruker-AXS, 2011)' _computing_data_collection 'APEX2 v2011.4.0 (Bruker-AXS, 2011)' _computing_data_reduction 'SAINT 7.46A (Bruker-AXS, 2011)' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _computing_structure_refinement 'SHELXL-2014 (Sheldrick, 2014)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 2008)' _diffrn_ambient_temperature 100(2) _diffrn_detector_area_resol_mean 8.3 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measurement_device_type 'Bruker Smart APEX2 CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0309 _diffrn_reflns_av_unetI/netI 0.0129 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 17 _diffrn_reflns_limit_l_min -17 _diffrn_reflns_number 103411 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.998 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 26.410 _diffrn_reflns_theta_min 1.480 _diffrn_source 'I\mS micro-focus sealed tube, multilayer optics' _exptl_absorpt_coefficient_mu 0.242 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS (Sheldrick, 2009)' _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.291 _exptl_crystal_density_method 'not measured' _exptl_crystal_description needle _exptl_crystal_F_000 764 _exptl_crystal_size_max 0.200 _exptl_crystal_size_mid 0.150 _exptl_crystal_size_min 0.020 _exptl_transmission_factor_max 0.7454 _exptl_transmission_factor_min 0.7175 _refine_diff_density_max 0.299 _refine_diff_density_min -0.228 _refine_diff_density_rms 0.037 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.037 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 424 _refine_ls_number_reflns 7470 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.037 _refine_ls_R_factor_all 0.0300 _refine_ls_R_factor_gt 0.0271 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0307P)^2^+0.7815P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0684 _refine_ls_wR_factor_ref 0.0704 _reflns_Friedel_coverage 0.000 _reflns_number_gt 6849 _reflns_number_total 7470 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ja6b03910_si_003.cif _cod_data_source_block main _cod_depositor_comments 'Adding full bibliography for 4125091--4125093.cif.' _cod_original_cell_volume 1820.9(5) _cod_database_code 4125092 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.953 _shelx_estimated_absorpt_t_max 0.995 _shelxl_version_number 2014-3 _shelx_res_file ; TITL mo_X8_15016_0m_a.res in P-1 REM Old TITL mo_X8_15016_0m in P-1 REM SHELXT solution in P-1 REM R1 0.103, Rweak 0.004, Alpha 0.051, Orientation as input REM Formula found by SHELXT: C33 K N5 O7 P CELL 0.71073 11.0044 12.0737 13.9465 83.904 82.249 85.085 ZERR 2.000 0.0017 0.0019 0.0022 0.003 0.003 0.003 LATT 1 SFAC C H K N O P UNIT 66 118 2 10 14 2 TEMP -173.160 SIZE 0.020 0.150 0.200 ACTA OMIT 3 3 9 OMIT 0 9 3 L.S. 10 BOND $H FMAP 2 PLAN 20 REM AdCPN3 anion WGHT 0.030700 0.781500 FVAR 0.60742 N1 4 0.612545 0.703486 0.204929 11.00000 0.02026 0.01935 = 0.02205 -0.00258 -0.00846 0.00015 N2 4 0.664470 0.731781 0.280281 11.00000 0.02146 0.02370 = 0.02160 -0.00203 -0.00795 -0.00301 N3 4 0.619632 0.827690 0.313091 11.00000 0.01961 0.02380 = 0.01951 -0.00228 -0.00214 -0.00674 P4 6 0.507908 0.890863 0.250557 11.00000 0.01970 0.01813 = 0.01980 -0.00576 -0.00252 -0.00119 C5 1 0.524199 0.780194 0.178498 11.00000 0.01516 0.01538 = 0.01663 -0.00092 -0.00095 -0.00210 C10 1 0.458410 0.762936 0.093605 11.00000 0.01552 0.01385 = 0.01524 -0.00130 -0.00236 -0.00019 C11 1 0.435918 0.638553 0.092818 11.00000 0.01883 0.01471 = 0.01456 -0.00143 -0.00289 -0.00041 AFIX 23 H11A 2 0.515577 0.593402 0.088741 11.00000 -1.20000 H11B 2 0.385511 0.612685 0.154066 11.00000 -1.20000 AFIX 0 C12 1 0.369602 0.621789 0.006087 11.00000 0.02335 0.01602 = 0.01738 -0.00370 -0.00461 -0.00202 AFIX 13 H12 2 0.355281 0.540993 0.006924 11.00000 -1.20000 AFIX 0 C13 1 0.245953 0.691060 0.013054 11.00000 0.01957 0.02373 = 0.01908 -0.00200 -0.00584 -0.00375 AFIX 23 H13A 2 0.194312 0.666634 0.074122 11.00000 -1.20000 H13B 2 0.202088 0.679474 -0.042154 11.00000 -1.20000 AFIX 0 C14 1 0.267397 0.815141 0.011117 11.00000 0.01678 0.02076 = 0.02043 -0.00085 -0.00511 0.00251 AFIX 13 H14 2 0.186589 0.860204 0.015426 11.00000 -1.20000 AFIX 0 C15 1 0.347081 0.852779 -0.083647 11.00000 0.02540 0.02296 = 0.01841 0.00324 -0.00645 0.00094 AFIX 23 H15A 2 0.304462 0.842719 -0.139927 11.00000 -1.20000 H15B 2 0.360802 0.932959 -0.085220 11.00000 -1.20000 AFIX 0 C16 1 0.470781 0.783516 -0.090188 11.00000 0.02255 0.02523 = 0.01385 0.00193 0.00001 -0.00084 AFIX 13 H16 2 0.522770 0.808125 -0.151980 11.00000 -1.20000 AFIX 0 C17 1 0.448765 0.659753 -0.088878 11.00000 0.02553 0.02572 = 0.01482 -0.00443 -0.00358 0.00168 AFIX 23 H17A 2 0.528482 0.614705 -0.094136 11.00000 -1.20000 H17B 2 0.406514 0.648456 -0.145041 11.00000 -1.20000 AFIX 0 C18 1 0.333656 0.832019 0.097994 11.00000 0.01656 0.01618 = 0.01874 -0.00192 -0.00222 0.00120 AFIX 23 H18A 2 0.281630 0.809011 0.159269 11.00000 -1.20000 H18B 2 0.347026 0.912133 0.097530 11.00000 -1.20000 AFIX 0 C19 1 0.536696 0.800528 -0.003251 11.00000 0.01603 0.01905 = 0.01911 0.00032 -0.00086 -0.00126 AFIX 23 H19A 2 0.551754 0.880384 -0.004597 11.00000 -1.20000 H19B 2 0.617259 0.756835 -0.007949 11.00000 -1.20000 AFIX 0 REM K(Kryptofix-2.2.2) cation K1 3 0.922984 0.269003 0.397616 11.00000 0.01532 0.01470 = 0.01592 -0.00172 -0.00365 -0.00192 N01 4 0.651081 0.294749 0.459453 11.00000 0.01812 0.01929 = 0.01614 -0.00249 -0.00197 -0.00008 C21 1 0.609402 0.181703 0.488954 11.00000 0.01451 0.02505 = 0.02337 0.00183 -0.00073 -0.00312 AFIX 23 H21A 2 0.518384 0.186421 0.497531 11.00000 -1.20000 H21B 2 0.636581 0.154831 0.552746 11.00000 -1.20000 AFIX 0 C22 1 0.655998 0.097365 0.418035 11.00000 0.01655 0.02047 = 0.02929 -0.00043 -0.00589 -0.00567 AFIX 23 H22A 2 0.616189 0.026644 0.438241 11.00000 -1.20000 H22B 2 0.635232 0.125639 0.352529 11.00000 -1.20000 AFIX 0 O23 5 0.786059 0.077638 0.415073 11.00000 0.01651 0.01941 = 0.02274 -0.00633 -0.00320 -0.00313 C24 1 0.833214 0.004096 0.342809 11.00000 0.02677 0.01908 = 0.02851 -0.01005 -0.00256 -0.00564 AFIX 23 H24A 2 0.822980 0.041320 0.277346 11.00000 -1.20000 H24B 2 0.787276 -0.064066 0.352986 11.00000 -1.20000 AFIX 0 C25 1 0.966376 -0.026567 0.349837 11.00000 0.02597 0.01383 = 0.03543 -0.00552 0.00095 -0.00256 AFIX 23 H25A 2 0.977233 -0.058334 0.416815 11.00000 -1.20000 H25B 2 0.997863 -0.083655 0.304903 11.00000 -1.20000 AFIX 0 O26 5 1.033000 0.070565 0.325188 11.00000 0.01813 0.01427 = 0.03293 -0.00255 0.00078 -0.00024 C27 1 1.161911 0.044701 0.323307 11.00000 0.01978 0.01920 = 0.03872 -0.00197 0.00199 0.00291 AFIX 23 H27A 2 1.188860 -0.017290 0.282431 11.00000 -1.20000 H27B 2 1.181780 0.021055 0.389918 11.00000 -1.20000 AFIX 0 C28 1 1.227530 0.147595 0.282133 11.00000 0.01828 0.02193 = 0.03406 -0.00222 0.00535 0.00079 AFIX 23 H28A 2 1.317335 0.129229 0.278733 11.00000 -1.20000 H28B 2 1.208364 0.168805 0.214987 11.00000 -1.20000 AFIX 0 C31 1 0.622929 0.363286 0.541992 11.00000 0.02192 0.02973 = 0.02255 -0.00903 0.00192 0.00163 AFIX 23 H31A 2 0.538039 0.351734 0.573053 11.00000 -1.20000 H31B 2 0.625779 0.443004 0.516961 11.00000 -1.20000 AFIX 0 C32 1 0.709184 0.337839 0.618043 11.00000 0.03102 0.03428 = 0.01611 -0.00675 0.00161 -0.00533 AFIX 23 H32A 2 0.679451 0.380470 0.674520 11.00000 -1.20000 H32B 2 0.711454 0.257263 0.640786 11.00000 -1.20000 AFIX 0 O33 5 0.829786 0.367443 0.577963 11.00000 0.02686 0.02332 = 0.01537 -0.00202 -0.00587 -0.00295 C34 1 0.911927 0.347305 0.649785 11.00000 0.03773 0.01914 = 0.01495 -0.00404 -0.00958 0.00112 AFIX 23 H34A 2 0.912721 0.268012 0.676630 11.00000 -1.20000 H34B 2 0.883776 0.394216 0.703718 11.00000 -1.20000 AFIX 0 C35 1 1.038504 0.374195 0.605316 11.00000 0.03820 0.02082 = 0.02132 -0.00404 -0.01545 -0.00499 AFIX 23 H35A 2 1.037301 0.452654 0.576193 11.00000 -1.20000 H35B 2 1.094523 0.365169 0.655949 11.00000 -1.20000 AFIX 0 O36 5 1.081178 0.301009 0.532300 11.00000 0.02271 0.02670 = 0.02183 -0.00452 -0.00798 -0.00673 C37 1 1.210007 0.308688 0.501716 11.00000 0.02365 0.04054 = 0.02419 0.00377 -0.01257 -0.01327 AFIX 23 H37A 2 1.256078 0.292534 0.558471 11.00000 -1.20000 H37B 2 1.225481 0.385198 0.472072 11.00000 -1.20000 AFIX 0 C38 1 1.252591 0.225877 0.428792 11.00000 0.01531 0.03502 = 0.02941 0.00716 -0.00751 -0.00176 AFIX 23 H38A 2 1.342583 0.228377 0.411112 11.00000 -1.20000 H38B 2 1.236896 0.150057 0.460071 11.00000 -1.20000 AFIX 0 C41 1 0.589548 0.349259 0.377695 11.00000 0.01610 0.02192 = 0.02388 -0.00234 -0.00508 0.00137 AFIX 23 H41A 2 0.506465 0.379734 0.403182 11.00000 -1.20000 H41B 2 0.579470 0.292512 0.333637 11.00000 -1.20000 AFIX 0 C42 1 0.658502 0.442315 0.320261 11.00000 0.01921 0.01885 = 0.02274 -0.00282 -0.00443 0.00304 AFIX 23 H42A 2 0.609495 0.480715 0.270355 11.00000 -1.20000 H42B 2 0.673980 0.497665 0.363913 11.00000 -1.20000 AFIX 0 O43 5 0.772839 0.394642 0.274697 11.00000 0.01907 0.01628 = 0.02055 0.00154 -0.00201 0.00118 C44 1 0.829436 0.472243 0.201459 11.00000 0.02307 0.01633 = 0.01639 0.00004 -0.00609 -0.00063 AFIX 23 H44A 2 0.837205 0.543192 0.229013 11.00000 -1.20000 H44B 2 0.778381 0.488283 0.147670 11.00000 -1.20000 AFIX 0 C45 1 0.954434 0.422570 0.163954 11.00000 0.02269 0.02039 = 0.01480 -0.00114 -0.00576 -0.00117 AFIX 23 H45A 2 0.947050 0.347957 0.142848 11.00000 -1.20000 H45B 2 0.990261 0.470704 0.107039 11.00000 -1.20000 AFIX 0 O46 5 1.033263 0.412683 0.238458 11.00000 0.01698 0.02198 = 0.01562 -0.00204 -0.00419 -0.00118 C47 1 1.157685 0.384733 0.199476 11.00000 0.01851 0.02197 = 0.01952 0.00036 0.00028 -0.00315 AFIX 23 H47A 2 1.192523 0.450616 0.160438 11.00000 -1.20000 H47B 2 1.160522 0.324140 0.156473 11.00000 -1.20000 AFIX 0 C48 1 1.232518 0.347186 0.281942 11.00000 0.01549 0.02218 = 0.02474 0.00096 -0.00223 -0.00474 AFIX 23 H48A 2 1.320034 0.335598 0.254812 11.00000 -1.20000 H48B 2 1.225872 0.407407 0.325730 11.00000 -1.20000 AFIX 0 N02 4 1.194078 0.243781 0.339240 11.00000 0.01605 0.01919 = 0.02077 0.00124 -0.00280 -0.00192 REM THF solvent O50 5 1.098341 0.210932 0.035933 11.00000 0.05747 0.02171 = 0.02214 -0.00348 -0.00233 0.00741 C51 1 1.134190 0.098675 0.015124 11.00000 0.02839 0.01815 = 0.02536 -0.00169 -0.00360 -0.00141 AFIX 23 H51A 2 1.069860 0.048608 0.044952 11.00000 -1.20000 H51B 2 1.211875 0.072608 0.041561 11.00000 -1.20000 AFIX 0 C52 1 1.151578 0.097899 -0.095114 11.00000 0.02483 0.02343 = 0.02474 -0.00384 0.00202 0.00037 AFIX 23 H52A 2 1.119033 0.030892 -0.114677 11.00000 -1.20000 H52B 2 1.239427 0.100215 -0.121931 11.00000 -1.20000 AFIX 0 C53 1 1.077413 0.204241 -0.128692 11.00000 0.02177 0.03149 = 0.02295 0.00027 -0.00048 0.00138 AFIX 23 H53A 2 1.109718 0.234082 -0.195266 11.00000 -1.20000 H53B 2 0.989253 0.191784 -0.126289 11.00000 -1.20000 AFIX 0 C54 1 1.098040 0.280429 -0.053773 11.00000 0.02920 0.02131 = 0.02867 0.00172 -0.00141 0.00377 AFIX 23 H54A 2 1.177559 0.314609 -0.071934 11.00000 -1.20000 H54B 2 1.031334 0.340742 -0.048253 11.00000 -1.20000 AFIX 0 HKLF 4 REM mo_X8_15016_0m_a.res in P-1 REM R1 = 0.0271 for 6849 Fo > 4sig(Fo) and 0.0300 for all 7470 data REM 424 parameters refined using 0 restraints END WGHT 0.0307 0.7815 REM Highest difference peak 0.299, deepest hole -0.228, 1-sigma level 0.037 Q1 1 0.5278 0.8343 0.2009 11.00000 0.05 0.30 Q2 1 0.2994 0.8185 0.0558 11.00000 0.05 0.29 Q3 1 0.5055 0.8204 0.2181 11.00000 0.05 0.29 Q4 1 0.4072 0.6413 -0.0400 11.00000 0.05 0.29 Q5 1 0.3952 0.7935 0.0975 11.00000 0.05 0.29 Q6 1 0.4527 0.7042 0.0900 11.00000 0.05 0.28 Q7 1 0.8927 0.4489 0.1852 11.00000 0.05 0.27 Q8 1 0.4092 0.8161 -0.0845 11.00000 0.05 0.26 Q9 1 0.4939 0.7721 0.1350 11.00000 0.05 0.26 Q10 1 0.2577 0.7539 0.0115 11.00000 0.05 0.26 Q11 1 0.5000 0.7902 -0.0459 11.00000 0.05 0.26 Q12 1 0.3112 0.6563 0.0124 11.00000 0.05 0.26 Q13 1 1.1911 0.0992 0.3073 11.00000 0.05 0.25 Q14 1 0.3986 0.6256 0.0529 11.00000 0.05 0.25 Q15 1 1.1925 0.3639 0.2429 11.00000 0.05 0.24 Q16 1 0.4569 0.7230 -0.0845 11.00000 0.05 0.24 Q17 1 0.4957 0.7813 0.0449 11.00000 0.05 0.24 Q18 1 0.3063 0.8329 -0.0373 11.00000 0.05 0.24 Q19 1 1.2236 0.2663 0.4645 11.00000 0.05 0.24 Q20 1 0.6379 0.1490 0.4475 11.00000 0.05 0.23 ; _shelx_res_checksum 97493 _shelx_hkl_file ; -1 0 0 96.39 2.70 -1 0 0 78.39 2.40 -1 0 0 95.49 3.00 -1 0 0 87.69 2.60 -1 0 0 92.79 2.90 -1 0 0 99.59 2.60 -1 0 0 87.09 2.20 -1 0 0 97.29 2.80 -1 0 0 96.59 2.60 -1 0 0 92.99 2.90 1 0 0 92.99 2.90 1 0 0 91.99 2.80 1 0 0 96.09 2.80 1 0 0 97.09 2.90 1 0 0 101.09 3.00 1 0 0 95.99 2.90 1 0 0 101.49 2.50 -2 0 0 69.99 3.30 -2 0 0 74.69 2.90 -2 0 0 70.09 3.20 -2 0 0 85.39 2.90 -2 0 0 75.39 3.30 -2 0 0 76.59 2.80 -2 0 0 77.69 3.30 -2 0 0 76.99 3.40 -2 0 0 79.09 2.60 -2 0 0 75.59 3.40 -2 0 0 77.39 2.30 -2 0 0 75.69 3.20 -2 0 0 77.29 3.30 -2 0 0 78.39 3.10 -2 0 0 77.99 2.60 2 0 0 81.49 3.60 2 0 0 87.89 3.50 2 0 0 73.59 3.00 2 0 0 74.19 2.60 2 0 0 76.69 3.30 2 0 0 75.09 3.10 2 0 0 69.89 3.30 2 0 0 84.49 3.10 2 0 0 83.19 3.40 2 0 0 80.79 3.40 -3 0 0 217.58 7.40 -3 0 0 234.08 7.40 -3 0 0 220.18 7.50 -3 0 0 208.58 6.50 -3 0 0 219.38 7.30 -3 0 0 213.48 6.50 -3 0 0 216.68 7.50 -3 0 0 212.38 5.90 -3 0 0 222.98 7.30 -3 0 0 224.58 7.10 -3 0 0 231.18 7.40 -3 0 0 215.38 6.80 -3 0 0 211.58 6.30 -3 0 0 213.68 5.50 -3 0 0 221.08 6.00 3 0 0 202.68 7.40 3 0 0 214.88 6.10 3 0 0 223.28 7.40 3 0 0 220.38 7.50 3 0 0 207.28 7.40 3 0 0 231.18 7.40 3 0 0 213.48 6.70 3 0 0 213.78 7.20 3 0 0 217.08 6.70 3 0 0 229.78 7.10 3 0 0 195.28 7.10 3 0 0 221.18 7.40 -4 0 0 69.39 2.70 -4 0 0 61.79 4.20 -4 0 0 71.49 4.40 -4 0 0 72.19 3.60 -4 0 0 67.09 3.60 -4 0 0 72.99 4.20 -4 0 0 70.69 3.10 -4 0 0 67.29 4.40 -4 0 0 64.69 3.60 -4 0 0 69.49 4.00 -4 0 0 71.09 4.20 -4 0 0 72.39 3.90 -4 0 0 68.19 3.40 -4 0 0 66.59 4.20 -4 0 0 68.99 4.40 -4 0 0 66.29 3.00 4 0 0 75.59 4.60 4 0 0 69.99 4.30 4 0 0 61.69 3.60 4 0 0 74.39 4.40 4 0 0 71.29 4.40 4 0 0 60.79 4.10 4 0 0 71.59 3.80 4 0 0 61.89 4.20 4 0 0 70.49 4.30 4 0 0 61.59 4.20 4 0 0 64.69 3.90 4 0 0 65.99 3.20 -5 0 0 58.59 4.00 -5 0 0 59.09 3.50 -5 0 0 62.39 4.60 -5 0 0 60.49 4.50 -5 0 0 63.29 3.20 -5 0 0 63.09 3.20 -5 0 0 61.99 3.90 -5 0 0 56.99 4.20 -5 0 0 62.09 4.70 -5 0 0 52.79 4.20 -5 0 0 54.69 3.70 -5 0 0 52.29 4.90 -5 0 0 52.59 3.50 -5 0 0 54.89 4.40 -5 0 0 62.69 2.80 5 0 0 64.89 4.80 5 0 0 58.19 3.90 5 0 0 60.69 3.90 5 0 0 56.79 4.30 5 0 0 61.29 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30.20 0 3 0 1401.66 30.20 0 3 0 1470.55 30.60 0 3 0 1478.25 30.20 0 3 0 1415.26 30.90 -1 -3 0 4903.21 99.89 -1 -3 0 4974.70 99.89 -1 -3 0 4869.51 102.59 -1 -3 0 4986.60 101.79 -1 -3 0 5211.08 101.59 -1 -3 0 4930.61 103.59 -1 -3 0 5167.68 100.29 1 3 0 5233.68 101.79 1 3 0 4845.02 101.59 1 3 0 4957.00 101.99 1 3 0 4905.91 103.59 1 3 0 5010.00 101.59 1 3 0 5025.90 102.79 1 3 0 5023.50 101.49 1 3 0 4869.01 100.39 1 3 0 5206.58 101.99 1 3 0 4945.01 99.99 1 3 0 4767.82 102.29 1 3 0 4855.21 100.09 1 3 0 5055.49 102.19 1 3 0 4984.80 102.09 1 3 0 4940.51 100.19 1 3 0 5235.38 104.99 -2 -3 0 1336.97 30.10 -2 -3 0 1351.36 28.10 -2 -3 0 1348.17 29.90 -2 -3 0 1342.57 29.80 -2 -3 0 1382.66 29.90 -2 -3 0 1394.86 28.40 -2 -3 0 1370.26 29.60 -2 -3 0 1392.46 29.30 -2 -3 0 1356.66 28.90 2 3 0 1341.57 28.70 2 3 0 1351.36 29.90 2 3 0 1369.76 29.90 2 3 0 1339.47 29.10 2 3 0 1355.96 30.90 2 3 0 1355.56 29.80 2 3 0 1366.46 30.00 2 3 0 1368.06 27.80 2 3 0 1373.86 29.60 2 3 0 1348.97 28.00 2 3 0 1328.67 30.50 2 3 0 1373.76 29.80 2 3 0 1338.07 28.80 2 3 0 1387.86 30.10 2 3 0 1351.66 29.80 2 3 0 1353.56 30.00 2 3 0 1373.06 29.70 2 3 0 1344.17 29.50 2 3 0 1375.06 29.40 -3 -3 0 312.37 8.70 -3 -3 0 316.77 8.40 -3 -3 0 320.37 9.20 -3 -3 0 318.57 9.70 -3 -3 0 337.67 10.20 -3 -3 0 311.97 8.80 -3 -3 0 305.97 9.50 -3 -3 0 318.07 8.00 -3 -3 0 320.77 10.20 -3 -3 0 310.57 9.80 3 3 0 321.07 10.00 3 3 0 307.77 9.40 3 3 0 313.07 9.50 3 3 0 303.97 9.80 3 3 0 318.07 9.00 3 3 0 306.87 10.00 3 3 0 311.17 9.80 3 3 0 316.77 8.90 3 3 0 327.07 9.90 3 3 0 317.67 9.60 3 3 0 305.47 10.20 3 3 0 313.67 9.80 3 3 0 318.57 9.60 3 3 0 317.37 9.50 3 3 0 320.97 10.10 3 3 0 319.77 8.60 -4 -3 0 587.84 15.60 -4 -3 0 570.14 13.20 -4 -3 0 560.64 16.20 -4 -3 0 536.85 14.70 -4 -3 0 551.34 16.30 -4 -3 0 543.65 15.00 -4 -3 0 603.44 16.30 -4 -3 0 582.04 14.00 -4 -3 0 586.84 14.60 -4 -3 0 574.94 15.90 4 3 0 562.84 16.00 4 3 0 567.74 15.70 4 3 0 564.34 16.20 4 3 0 572.44 15.50 4 3 0 568.94 15.50 4 3 0 562.14 15.70 4 3 0 560.64 15.90 4 3 0 549.85 16.20 4 3 0 568.24 14.80 4 3 0 564.04 16.20 4 3 0 561.24 14.50 4 3 0 546.25 14.40 4 3 0 551.04 16.20 -5 -3 0 26.40 3.90 -5 -3 0 20.00 2.70 -5 -3 0 26.10 3.40 -5 -3 0 24.60 2.90 -5 -3 0 26.90 3.40 -5 -3 0 17.30 2.30 -5 -3 0 22.80 2.80 -5 -3 0 28.60 3.70 -5 -3 0 19.30 3.10 -5 -3 0 24.00 1.90 -5 -3 0 27.60 3.50 -5 -3 0 29.30 3.90 -5 -3 0 21.50 2.50 5 3 0 22.20 3.20 5 3 0 21.40 2.40 5 3 0 24.80 3.50 5 3 0 29.40 3.60 5 3 0 28.10 3.80 5 3 0 23.70 3.30 5 3 0 23.70 3.70 5 3 0 22.50 3.00 5 3 0 27.40 3.10 5 3 0 27.10 3.80 5 3 0 23.90 3.50 5 3 0 35.80 4.40 5 3 0 17.90 3.20 -6 -3 0 25.10 4.00 -6 -3 0 27.30 3.20 -6 -3 0 20.20 2.90 -6 -3 0 21.80 2.20 -6 -3 0 29.60 3.90 -6 -3 0 28.00 4.00 -6 -3 0 26.90 3.80 -6 -3 0 28.50 3.90 6 3 0 19.80 2.60 6 3 0 26.60 4.10 6 3 0 17.90 3.00 6 3 0 23.80 3.30 6 3 0 33.20 4.50 6 3 0 19.30 3.40 6 3 0 27.10 3.90 6 3 0 33.20 4.30 -7 -3 0 84.29 6.00 -7 -3 0 80.99 5.90 -7 -3 0 78.39 4.90 -7 -3 0 79.89 3.90 -7 -3 0 80.09 6.50 -7 -3 0 79.39 5.10 -7 -3 0 88.89 6.30 -7 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18.00 -11 4 0 357.16 18.30 -11 4 0 374.96 17.70 -11 4 0 377.36 17.50 -11 4 0 370.46 12.00 -11 4 0 344.27 16.50 -11 4 0 359.56 13.60 -11 4 0 369.96 15.80 -11 4 0 351.16 18.10 -11 4 0 351.96 17.00 -11 4 0 351.86 9.50 10 -4 0 39.70 6.90 10 -4 0 40.90 6.00 10 -4 0 31.30 6.10 10 -4 0 34.40 6.20 -10 4 0 29.30 5.40 -10 4 0 34.40 5.10 -10 4 0 29.30 2.20 -10 4 0 37.00 6.10 -10 4 0 34.70 4.50 -10 4 0 35.10 6.40 -10 4 0 31.30 3.50 -10 4 0 49.30 7.30 -10 4 0 18.40 4.40 -10 4 0 41.90 6.60 9 -4 0 84.39 7.90 9 -4 0 86.99 9.00 9 -4 0 82.49 8.10 9 -4 0 85.29 8.80 9 -4 0 73.79 8.60 -9 4 0 81.09 8.40 -9 4 0 73.39 8.00 -9 4 0 73.79 8.50 -9 4 0 85.09 8.80 -9 4 0 89.99 5.70 -9 4 0 80.39 4.60 -9 4 0 90.89 6.80 -9 4 0 84.99 8.90 -9 4 0 87.09 3.60 -9 4 0 74.59 7.70 8 -4 0 35.20 5.70 8 -4 0 39.00 5.00 8 -4 0 45.00 5.50 8 -4 0 46.20 6.30 8 -4 0 34.50 5.30 8 -4 0 41.50 5.40 -8 4 0 37.90 5.50 -8 4 0 34.80 4.10 -8 4 0 41.00 4.30 -8 4 0 33.40 5.10 -8 4 0 33.40 4.50 -8 4 0 38.00 4.20 -8 4 0 42.40 5.70 -8 4 0 33.30 2.80 -8 4 0 34.40 2.10 -8 4 0 37.30 5.50 -8 4 0 40.00 5.40 -8 4 0 29.20 5.20 7 -4 0 21.90 4.30 7 -4 0 21.00 3.60 7 -4 0 17.30 3.00 7 -4 0 14.90 3.50 7 -4 0 24.30 4.20 7 -4 0 13.00 3.10 7 -4 0 18.90 3.40 -7 4 0 17.10 3.60 -7 4 0 17.30 2.60 -7 4 0 15.80 3.30 -7 4 0 17.90 3.10 -7 4 0 18.80 3.90 -7 4 0 15.90 2.10 -7 4 0 19.10 1.60 -7 4 0 14.30 2.60 -7 4 0 15.40 2.50 -7 4 0 18.00 3.90 -7 4 0 23.50 3.80 -7 4 0 12.20 2.90 6 -4 0 112.49 6.90 6 -4 0 118.09 6.90 6 -4 0 116.09 6.50 6 -4 0 117.49 6.90 6 -4 0 106.29 6.10 6 -4 0 121.29 6.90 6 -4 0 101.59 5.80 -6 4 0 113.49 3.30 -6 4 0 110.49 4.40 -6 4 0 119.79 6.90 -6 4 0 120.49 7.00 -6 4 0 106.39 5.90 -6 4 0 117.29 5.20 -6 4 0 117.09 5.60 -6 4 0 120.59 7.30 -6 4 0 113.79 5.20 -6 4 0 109.39 3.20 -6 4 0 116.39 6.70 -6 4 0 102.39 6.70 -6 4 0 125.69 7.00 -6 4 0 115.09 6.80 5 -4 0 917.91 23.60 5 -4 0 840.72 23.20 5 -4 0 866.41 22.30 5 -4 0 839.12 21.50 5 -4 0 873.81 22.60 5 -4 0 865.91 22.90 5 -4 0 891.31 23.20 5 -4 0 901.11 22.50 5 -4 0 895.61 23.10 -5 4 0 890.11 20.30 -5 4 0 854.51 23.00 -5 4 0 836.32 22.90 -5 4 0 870.81 22.80 -5 4 0 841.42 22.90 -5 4 0 879.21 23.30 -5 4 0 840.62 23.50 -5 4 0 872.91 20.40 -5 4 0 861.31 22.00 -5 4 0 881.41 23.80 -5 4 0 871.31 21.10 -5 4 0 879.91 19.40 -5 4 0 859.91 23.00 4 -4 0 31.80 3.50 4 -4 0 29.80 3.20 4 -4 0 29.10 3.30 4 -4 0 34.30 2.70 4 -4 0 37.30 3.50 4 -4 0 32.40 3.50 4 -4 0 33.30 3.50 4 -4 0 34.40 3.70 4 -4 0 35.10 3.80 -4 4 0 28.50 3.80 -4 4 0 33.80 3.60 -4 4 0 31.70 3.70 -4 4 0 34.10 3.70 -4 4 0 33.70 2.20 -4 4 0 32.70 2.70 -4 4 0 32.70 3.50 -4 4 0 30.60 1.60 -4 4 0 32.20 3.80 -4 4 0 32.90 3.40 -4 4 0 34.70 1.90 -4 4 0 37.40 4.10 -4 4 0 34.90 3.70 3 -4 0 8.90 1.80 3 -4 0 14.10 2.10 3 -4 0 18.00 2.30 3 -4 0 12.30 2.00 3 -4 0 14.40 2.10 3 -4 0 14.30 2.10 3 -4 0 13.10 1.70 3 -4 0 10.40 1.70 3 -4 0 13.80 2.20 -3 4 0 12.00 2.30 -3 4 0 15.00 2.30 -3 4 0 11.50 1.90 -3 4 0 11.50 1.30 -3 4 0 15.20 2.20 -3 4 0 12.50 1.80 -3 4 0 9.90 2.10 -3 4 0 11.80 2.00 -3 4 0 15.40 2.30 -3 4 0 8.90 1.60 -3 4 0 12.90 1.60 -3 4 0 13.50 2.10 -3 4 0 18.50 2.80 2 -4 0 77.59 3.50 2 -4 0 71.59 3.40 2 -4 0 80.79 3.20 2 -4 0 81.29 3.70 2 -4 0 76.29 3.70 2 -4 0 79.69 3.80 2 -4 0 84.99 3.80 -2 4 0 80.19 3.10 -2 4 0 86.09 4.40 -2 4 0 67.09 4.10 -2 4 0 79.09 3.90 -2 4 0 77.59 3.70 -2 4 0 76.69 3.80 -2 4 0 74.19 4.60 -2 4 0 73.79 3.80 -2 4 0 76.69 3.30 -2 4 0 86.09 3.50 -2 4 0 74.09 3.70 -2 4 0 80.49 3.70 -2 4 0 70.69 4.00 1 -4 0 976.20 21.40 1 -4 0 969.60 21.40 1 -4 0 995.00 21.90 1 -4 0 959.20 21.30 1 -4 0 1011.60 22.00 1 -4 0 1005.30 21.90 1 -4 0 1011.70 21.90 -1 4 0 1012.20 23.80 -1 4 0 1019.20 22.90 -1 4 0 1003.70 20.00 -1 4 0 990.50 22.00 -1 4 0 1006.40 21.20 -1 4 0 982.70 22.20 -1 4 0 975.40 21.90 -1 4 0 1004.90 21.80 -1 4 0 998.30 23.30 -1 4 0 952.60 22.00 -1 4 0 989.00 22.00 -1 4 0 989.00 24.70 -1 4 0 999.20 23.00 -1 4 0 997.50 21.40 -1 4 0 968.90 20.80 0 -4 0 910.81 19.90 0 -4 0 887.61 19.70 0 -4 0 901.71 19.50 0 -4 0 880.11 19.90 0 -4 0 887.41 19.90 0 -4 0 895.41 19.20 0 4 0 884.41 20.10 0 4 0 911.21 19.50 0 4 0 873.01 20.70 0 4 0 872.41 19.00 0 4 0 910.71 19.70 0 4 0 909.41 19.90 0 4 0 905.41 19.30 0 4 0 888.51 21.90 0 4 0 928.21 20.00 0 4 0 915.91 21.60 0 4 0 881.41 20.70 0 4 0 874.11 19.80 0 4 0 859.41 22.60 0 4 0 914.11 20.10 -1 -4 0 594.14 14.00 -1 -4 0 606.84 12.60 -1 -4 0 587.34 14.10 -1 -4 0 579.74 14.40 -1 -4 0 618.94 13.70 -1 -4 0 602.54 14.40 -1 -4 0 576.84 14.20 1 4 0 572.24 16.00 1 4 0 573.14 16.20 1 4 0 596.44 14.50 1 4 0 584.94 14.60 1 4 0 595.54 14.20 1 4 0 595.64 14.40 1 4 0 597.04 12.70 1 4 0 607.14 14.60 1 4 0 608.84 14.20 1 4 0 599.84 14.10 1 4 0 600.34 13.90 1 4 0 602.84 13.50 1 4 0 606.74 16.90 1 4 0 590.04 14.20 1 4 0 581.14 14.30 -2 -4 0 23.00 1.80 -2 -4 0 22.80 2.50 -2 -4 0 20.70 1.40 -2 -4 0 22.80 2.50 -2 -4 0 23.40 2.50 -2 -4 0 26.40 1.60 -2 -4 0 26.40 2.80 -2 -4 0 24.00 2.30 -2 -4 0 22.90 2.30 2 4 0 20.70 2.30 2 4 0 28.70 2.90 2 4 0 23.90 2.50 2 4 0 25.70 2.70 2 4 0 22.60 2.40 2 4 0 23.50 2.50 2 4 0 22.40 1.60 2 4 0 20.40 2.40 2 4 0 25.00 3.10 2 4 0 22.30 3.10 2 4 0 21.70 1.60 2 4 0 22.40 2.30 2 4 0 21.50 1.80 2 4 0 18.20 2.30 2 4 0 21.60 2.40 -3 -4 0 8.50 1.30 -3 -4 0 7.80 1.90 -3 -4 0 9.90 1.40 -3 -4 0 7.90 1.40 -3 -4 0 6.10 1.60 -3 -4 0 9.00 1.80 -3 -4 0 8.10 1.80 -3 -4 0 10.70 2.00 -3 -4 0 8.10 1.80 -3 -4 0 8.40 1.50 3 4 0 9.50 1.70 3 4 0 5.40 1.60 3 4 0 10.90 1.60 3 4 0 7.70 1.80 3 4 0 7.70 1.60 3 4 0 11.60 2.10 3 4 0 5.20 1.50 3 4 0 10.90 1.20 3 4 0 9.70 1.80 3 4 0 8.60 1.90 3 4 0 9.80 1.80 3 4 0 10.30 1.30 3 4 0 7.30 1.80 3 4 0 6.40 1.80 3 4 0 4.60 1.50 3 4 0 8.90 1.90 3 4 0 8.90 2.10 3 4 0 9.00 1.90 3 4 0 9.50 1.50 -4 -4 0 252.37 7.70 -4 -4 0 248.28 8.10 -4 -4 0 250.37 8.20 -4 -4 0 246.28 9.00 -4 -4 0 251.47 9.30 -4 -4 0 252.77 9.50 -4 -4 0 259.07 9.80 -4 -4 0 248.18 9.10 -4 -4 0 252.37 8.60 -4 -4 0 242.18 7.00 4 4 0 243.28 9.00 4 4 0 252.57 8.90 4 4 0 249.58 8.90 4 4 0 247.08 8.90 4 4 0 245.18 9.20 4 4 0 234.08 9.20 4 4 0 256.17 8.20 4 4 0 231.38 9.40 4 4 0 258.67 9.00 4 4 0 237.78 9.40 4 4 0 234.88 9.30 4 4 0 257.97 8.40 4 4 0 249.58 7.70 4 4 0 256.57 9.60 -5 -4 0 39.70 4.20 -5 -4 0 35.20 4.20 -5 -4 0 37.50 2.40 -5 -4 0 36.40 4.10 -5 -4 0 31.70 3.60 -5 -4 0 36.30 3.10 -5 -4 0 39.00 2.80 -5 -4 0 35.20 4.10 -5 -4 0 42.00 4.10 -5 -4 0 34.00 4.30 5 4 0 34.30 3.80 5 4 0 42.00 5.00 5 4 0 33.80 4.30 5 4 0 36.60 4.10 5 4 0 40.60 3.30 5 4 0 37.60 3.00 5 4 0 37.30 3.70 5 4 0 34.20 4.20 5 4 0 37.30 4.40 5 4 0 38.00 4.80 5 4 0 42.40 4.40 5 4 0 31.70 4.20 5 4 0 37.40 3.90 -6 -4 0 367.26 12.40 -6 -4 0 360.46 11.10 -6 -4 0 357.46 11.00 -6 -4 0 339.07 11.50 -6 -4 0 355.06 13.10 -6 -4 0 366.16 13.70 -6 -4 0 352.96 13.30 -6 -4 0 356.96 12.90 -6 -4 0 337.67 12.00 -6 -4 0 349.96 9.80 -6 -4 0 342.47 11.30 -6 -4 0 360.66 12.60 -6 -4 0 366.56 14.00 6 4 0 354.26 11.50 6 4 0 357.96 11.80 6 4 0 361.96 12.80 6 4 0 351.86 13.20 6 4 0 357.66 13.40 6 4 0 361.46 13.70 6 4 0 341.37 11.40 6 4 0 354.36 12.90 6 4 0 351.16 13.80 6 4 0 363.06 13.10 6 4 0 347.77 12.70 6 4 0 344.37 13.60 6 4 0 338.47 13.50 -7 -4 0 103.69 7.40 -7 -4 0 94.39 5.60 -7 -4 0 91.99 6.50 -7 -4 0 94.19 7.10 -7 -4 0 107.59 4.70 -7 -4 0 86.69 6.70 -7 -4 0 100.69 5.50 -7 -4 0 97.59 5.80 -7 -4 0 102.29 6.40 -7 -4 0 93.89 6.80 7 4 0 88.19 6.30 7 4 0 86.69 6.80 7 4 0 100.49 5.80 7 4 0 94.99 6.60 7 4 0 88.49 6.70 7 4 0 90.19 6.70 7 4 0 98.69 6.00 7 4 0 112.59 7.70 7 4 0 92.99 7.10 7 4 0 102.89 7.50 7 4 0 112.29 7.10 7 4 0 92.89 5.60 7 4 0 94.29 6.80 -8 -4 0 732.13 22.40 -8 -4 0 737.13 21.10 -8 -4 0 750.42 24.20 -8 -4 0 744.13 20.60 -8 -4 0 712.23 18.20 -8 -4 0 740.03 21.00 -8 -4 0 767.82 23.20 -8 -4 0 713.83 23.10 8 4 0 700.43 23.40 8 4 0 706.53 23.00 8 4 0 721.23 23.90 8 4 0 721.13 21.00 8 4 0 762.02 23.20 8 4 0 740.73 23.40 8 4 0 737.83 22.80 8 4 0 730.93 21.50 8 4 0 716.23 24.30 8 4 0 719.83 24.20 -9 -4 0 25.20 3.90 -9 -4 0 27.30 5.30 -9 -4 0 12.70 3.20 -9 -4 0 33.10 4.60 -9 -4 0 24.60 5.20 -9 -4 0 31.30 3.40 -9 -4 0 35.60 5.50 9 4 0 34.50 5.30 9 4 0 24.60 5.10 9 4 0 34.50 6.10 9 4 0 26.10 5.20 9 4 0 26.00 4.90 9 4 0 41.50 5.60 9 4 0 32.50 5.90 9 4 0 36.20 5.10 9 4 0 30.10 5.30 -10 -4 0 10.10 3.80 -10 -4 0 13.20 3.30 -10 -4 0 8.20 2.60 -10 -4 0 9.90 3.40 -10 -4 0 12.60 2.30 -10 -4 0 16.70 3.50 10 4 0 9.30 3.60 10 4 0 5.20 2.60 10 4 0 -0.30 2.80 10 4 0 7.20 3.80 10 4 0 7.50 3.30 10 4 0 10.40 4.20 10 4 0 4.90 3.00 -11 -4 0 212.98 11.00 -11 -4 0 216.58 11.20 -11 -4 0 213.48 8.70 -11 -4 0 200.78 13.60 -11 -4 0 229.78 11.60 11 4 0 210.08 11.20 11 4 0 221.08 13.10 11 4 0 218.48 13.60 11 4 0 215.28 12.90 11 4 0 211.58 14.10 -12 -4 0 28.00 5.20 -12 -4 0 31.30 5.50 -12 -4 0 39.00 4.50 -12 -4 0 46.90 8.60 -12 -4 0 30.60 5.40 12 4 0 34.40 5.70 12 4 0 33.00 6.80 12 4 0 41.90 8.10 12 4 0 47.40 8.00 12 4 0 41.20 7.30 -13 -4 0 9.60 4.80 -13 -4 0 6.60 2.40 -13 -4 0 14.60 4.40 -13 -4 0 14.60 4.00 -13 -4 0 5.10 3.20 13 4 0 10.70 3.80 13 4 0 12.60 5.30 13 4 0 6.30 3.90 13 4 0 12.80 4.90 12 -5 0 -2.60 2.50 12 -5 0 2.00 3.30 12 -5 0 -1.90 2.60 -12 5 0 -0.30 3.00 -12 5 0 0.00 1.40 -12 5 0 1.30 2.40 -12 5 0 -2.10 1.90 -12 5 0 0.20 2.50 -12 5 0 0.30 2.80 -12 5 0 -1.00 1.00 -12 5 0 0.10 2.90 11 -5 0 48.90 7.40 11 -5 0 42.50 7.40 11 -5 0 32.20 6.50 -11 5 0 42.50 4.40 -11 5 0 50.39 7.30 -11 5 0 43.10 7.40 -11 5 0 48.30 6.60 -11 5 0 51.19 7.50 -11 5 0 45.60 3.40 -11 5 0 34.60 6.50 -11 5 0 55.09 8.60 -11 5 0 36.80 6.80 10 -5 0 14.90 4.50 10 -5 0 17.40 4.50 10 -5 0 8.90 3.80 -10 5 0 8.20 2.10 -10 5 0 14.70 2.20 -10 5 0 7.10 2.90 -10 5 0 10.60 3.80 -10 5 0 11.80 3.80 -10 5 0 10.40 4.00 -10 5 0 13.20 4.10 -10 5 0 12.90 3.50 -10 5 0 10.50 3.90 9 -5 0 5.70 2.90 9 -5 0 1.90 2.40 9 -5 0 -2.70 1.50 -9 5 0 -0.10 1.70 -9 5 0 -0.50 1.80 -9 5 0 -1.50 1.40 -9 5 0 -0.70 0.70 -9 5 0 3.30 2.60 -9 5 0 1.10 2.20 -9 5 0 -1.60 1.60 -9 5 0 -1.40 1.70 -9 5 0 2.50 1.70 -9 5 0 0.30 1.10 8 -5 0 116.89 8.40 8 -5 0 124.69 8.40 8 -5 0 131.69 7.90 8 -5 0 116.19 8.40 -8 5 0 122.99 4.90 -8 5 0 122.29 8.60 -8 5 0 126.39 5.60 -8 5 0 122.29 8.20 -8 5 0 117.29 8.20 -8 5 0 119.59 6.60 -8 5 0 112.79 8.40 -8 5 0 138.49 8.80 -8 5 0 138.19 7.80 -8 5 0 124.89 8.10 7 -5 0 307.37 13.10 7 -5 0 321.57 13.00 7 -5 0 323.47 11.90 7 -5 0 305.97 13.10 7 -5 0 312.17 12.00 7 -5 0 304.47 13.00 7 -5 0 304.97 12.00 7 -5 0 305.17 13.00 -7 5 0 281.77 12.40 -7 5 0 316.47 8.50 -7 5 0 309.47 9.10 -7 5 0 310.87 13.40 -7 5 0 278.77 11.90 -7 5 0 322.17 13.00 -7 5 0 315.67 11.70 -7 5 0 299.17 12.70 -7 5 0 303.37 13.30 -7 5 0 298.07 10.70 6 -5 0 26.20 3.50 6 -5 0 21.80 3.40 6 -5 0 14.00 3.10 6 -5 0 21.00 3.60 6 -5 0 19.40 3.40 6 -5 0 15.70 3.10 6 -5 0 26.60 3.60 6 -5 0 20.60 3.60 -6 5 0 25.60 4.10 -6 5 0 24.00 3.60 -6 5 0 17.50 3.40 -6 5 0 20.80 3.90 -6 5 0 17.60 3.20 -6 5 0 22.00 1.70 -6 5 0 21.70 3.20 -6 5 0 24.30 3.90 -6 5 0 24.80 2.70 -6 5 0 19.50 1.50 -6 5 0 24.60 3.70 5 -5 0 9.00 2.10 5 -5 0 16.40 2.90 5 -5 0 15.20 2.60 5 -5 0 15.80 2.80 5 -5 0 12.80 2.70 5 -5 0 18.30 3.20 5 -5 0 12.10 2.60 5 -5 0 11.90 2.40 5 -5 0 12.30 2.30 -5 5 0 15.40 2.80 -5 5 0 10.30 2.50 -5 5 0 18.20 2.60 -5 5 0 13.40 2.50 -5 5 0 12.90 2.80 -5 5 0 7.50 2.10 -5 5 0 11.40 2.80 -5 5 0 13.30 2.60 -5 5 0 12.50 2.60 -5 5 0 17.40 3.30 -5 5 0 14.30 1.80 4 -5 0 13.30 2.10 4 -5 0 15.40 2.60 4 -5 0 19.90 2.90 4 -5 0 22.60 3.00 4 -5 0 25.20 3.10 4 -5 0 15.40 2.70 4 -5 0 18.40 2.60 4 -5 0 19.40 2.90 4 -5 0 21.60 2.60 -4 5 0 20.00 3.00 -4 5 0 18.80 2.70 -4 5 0 17.60 2.90 -4 5 0 19.90 3.10 -4 5 0 20.70 2.90 -4 5 0 16.10 2.20 -4 5 0 19.80 3.10 -4 5 0 19.80 2.80 -4 5 0 17.80 2.20 -4 5 0 22.90 3.60 -4 5 0 18.40 3.10 -4 5 0 21.30 1.60 -4 5 0 18.10 2.50 3 -5 0 67.19 3.90 3 -5 0 56.29 3.80 3 -5 0 63.59 3.90 3 -5 0 61.59 3.80 3 -5 0 69.69 3.50 3 -5 0 65.19 3.80 3 -5 0 67.69 3.70 -3 5 0 59.09 4.10 -3 5 0 56.89 4.10 -3 5 0 59.69 4.00 -3 5 0 66.39 3.60 -3 5 0 63.69 4.10 -3 5 0 66.59 3.10 -3 5 0 67.29 4.00 -3 5 0 67.59 4.10 -3 5 0 65.19 3.50 -3 5 0 54.89 3.70 -3 5 0 64.79 3.90 -3 5 0 62.89 4.70 -3 5 0 62.49 4.50 2 -5 0 48.50 3.10 2 -5 0 48.90 2.80 2 -5 0 46.40 2.80 2 -5 0 44.00 2.90 2 -5 0 44.20 2.90 2 -5 0 48.20 3.00 -2 5 0 46.20 2.30 -2 5 0 46.20 2.60 -2 5 0 44.10 3.00 -2 5 0 46.00 2.90 -2 5 0 45.80 2.50 -2 5 0 42.60 3.00 -2 5 0 42.40 3.10 -2 5 0 45.10 3.60 -2 5 0 42.00 2.50 -2 5 0 49.50 3.50 -2 5 0 50.99 3.10 -2 5 0 47.80 3.20 -2 5 0 47.90 3.70 -2 5 0 55.29 5.30 -2 5 0 45.20 3.00 1 -5 0 295.27 8.30 1 -5 0 290.17 8.40 1 -5 0 277.57 8.20 1 -5 0 287.27 7.80 1 -5 0 282.37 7.80 1 -5 0 288.07 8.30 -1 5 0 263.87 9.20 -1 5 0 277.77 9.10 -1 5 0 288.67 10.00 -1 5 0 281.07 8.30 -1 5 0 278.07 8.40 -1 5 0 281.87 8.40 -1 5 0 287.07 7.90 -1 5 0 280.37 10.80 -1 5 0 267.77 9.10 -1 5 0 284.17 7.20 -1 5 0 266.97 8.20 -1 5 0 273.07 6.90 -1 5 0 277.87 7.70 -1 5 0 304.57 8.40 0 5 0 11.90 2.00 -1 -5 0 441.86 11.00 -1 -5 0 428.36 11.60 -1 -5 0 439.26 11.30 -1 -5 0 439.56 9.70 -1 -5 0 425.66 11.80 -1 -5 0 433.26 11.70 -1 -5 0 445.46 11.30 1 5 0 440.26 10.40 1 5 0 437.16 14.40 1 5 0 445.66 11.40 1 5 0 420.76 11.60 1 5 0 433.06 11.80 1 5 0 444.86 11.80 1 5 0 425.16 11.60 1 5 0 433.36 11.40 1 5 0 438.96 13.70 1 5 0 451.65 11.40 1 5 0 420.46 13.50 1 5 0 435.16 10.90 1 5 0 429.86 11.10 1 5 0 437.96 12.10 -2 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-4 -5 0 110.49 6.00 -4 -5 0 108.09 5.80 -4 -5 0 109.49 4.70 4 5 0 103.69 5.70 4 5 0 112.59 5.00 4 5 0 111.19 5.70 4 5 0 111.79 5.30 4 5 0 98.99 6.40 4 5 0 105.49 5.90 4 5 0 104.39 4.60 4 5 0 99.79 5.50 4 5 0 102.19 3.90 4 5 0 104.19 5.70 4 5 0 104.69 5.80 4 5 0 112.89 6.10 4 5 0 102.49 6.20 4 5 0 105.59 5.40 4 5 0 102.29 5.50 4 5 0 97.49 5.90 4 5 0 103.99 3.70 4 5 0 101.29 5.90 -5 -5 0 521.75 15.60 -5 -5 0 535.05 17.30 -5 -5 0 557.64 15.10 -5 -5 0 560.34 15.30 -5 -5 0 542.35 17.00 -5 -5 0 520.55 16.60 -5 -5 0 538.15 16.50 -5 -5 0 527.85 16.30 -5 -5 0 529.85 14.20 -5 -5 0 543.65 13.60 5 5 0 550.34 17.30 5 5 0 543.85 15.10 5 5 0 512.35 16.80 5 5 0 488.35 15.80 5 5 0 553.74 15.20 5 5 0 545.45 16.10 5 5 0 545.95 17.20 5 5 0 558.04 16.90 5 5 0 553.94 16.40 5 5 0 525.65 16.80 5 5 0 552.94 14.10 5 5 0 550.34 17.10 5 5 0 573.24 16.70 5 5 0 543.75 17.30 5 5 0 501.45 15.60 -6 -5 0 0.60 1.70 -6 -5 0 1.20 1.40 -6 -5 0 3.10 1.90 -6 -5 0 4.10 1.60 -6 -5 0 6.40 2.50 -6 -5 0 2.90 1.30 -6 -5 0 2.90 2.00 -6 -5 0 2.00 1.30 -6 -5 0 2.70 1.60 -6 -5 0 1.30 0.90 6 5 0 2.70 1.80 6 5 0 3.60 2.10 6 5 0 2.60 1.60 6 5 0 0.40 1.50 6 5 0 4.10 2.20 6 5 0 3.40 2.10 6 5 0 3.00 1.70 6 5 0 4.50 2.00 6 5 0 2.50 1.30 6 5 0 4.20 1.90 6 5 0 6.10 2.20 6 5 0 2.90 1.50 6 5 0 3.50 1.40 -7 -5 0 89.29 6.60 -7 -5 0 111.19 6.60 -7 -5 0 105.39 7.70 -7 -5 0 95.69 5.70 -7 -5 0 106.79 5.70 -7 -5 0 106.89 7.60 -7 -5 0 100.49 4.70 -7 -5 0 101.79 6.10 -7 -5 0 91.19 6.80 7 5 0 105.09 6.10 7 5 0 87.89 5.40 7 5 0 106.89 7.60 7 5 0 106.99 7.10 7 5 0 104.39 7.50 7 5 0 111.59 7.70 7 5 0 100.69 7.20 7 5 0 114.79 7.20 7 5 0 111.39 7.20 7 5 0 102.69 6.10 7 5 0 110.19 7.90 7 5 0 98.49 6.80 -8 -5 0 216.58 9.50 -8 -5 0 204.78 10.10 -8 -5 0 201.48 9.40 -8 -5 0 205.68 7.60 -8 -5 0 225.48 11.10 -8 -5 0 220.98 9.10 -8 -5 0 231.08 11.90 8 5 0 208.98 10.80 8 5 0 214.18 10.80 8 5 0 187.08 11.00 8 5 0 206.98 11.70 8 5 0 216.88 11.00 8 5 0 198.68 10.60 8 5 0 227.18 12.00 8 5 0 181.68 10.90 8 5 0 213.18 9.70 8 5 0 215.18 9.30 -9 -5 0 47.70 5.20 -9 -5 0 38.80 5.10 -9 -5 0 40.60 3.90 -9 -5 0 41.90 6.90 -9 -5 0 48.20 6.70 -9 -5 0 49.20 5.70 9 5 0 43.10 6.60 9 5 0 39.40 5.90 9 5 0 44.80 6.80 9 5 0 41.10 6.10 9 5 0 50.79 5.60 9 5 0 51.09 6.90 9 5 0 33.10 6.10 9 5 0 45.50 5.90 9 5 0 42.70 6.50 -10 -5 0 202.88 10.20 -10 -5 0 185.28 9.80 -10 -5 0 192.48 9.80 -10 -5 0 195.58 11.80 -10 -5 0 203.08 8.10 -10 -5 0 192.28 12.40 10 5 0 175.78 12.30 10 5 0 206.68 12.60 10 5 0 191.48 12.60 10 5 0 192.38 11.50 10 5 0 199.98 11.70 10 5 0 199.48 11.80 10 5 0 210.58 12.90 10 5 0 170.38 9.40 10 5 0 164.88 9.50 -11 -5 0 -0.60 1.90 -11 -5 0 5.70 2.70 -11 -5 0 5.80 3.90 -11 -5 0 1.30 1.30 -11 -5 0 3.30 2.50 11 5 0 1.10 2.70 11 5 0 1.10 3.40 11 5 0 1.60 3.00 11 5 0 3.60 3.80 11 5 0 4.30 2.60 11 5 0 -1.20 2.50 -12 -5 0 496.85 22.70 -12 -5 0 458.15 18.20 -12 -5 0 456.05 18.40 -12 -5 0 480.15 18.40 -12 -5 0 459.85 14.90 12 5 0 430.06 21.10 12 5 0 459.35 17.70 12 5 0 421.26 20.00 12 5 0 478.15 22.60 12 5 0 455.25 20.50 -13 -5 0 -0.10 2.30 -13 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463.85 15.20 1 6 0 477.15 11.10 1 6 0 454.95 15.10 1 6 0 483.15 12.50 1 6 0 473.45 13.00 1 6 0 449.56 11.70 1 6 0 475.15 12.70 1 6 0 462.95 12.80 1 6 0 457.95 13.00 1 6 0 466.45 12.90 -2 -6 0 1353.06 30.50 -2 -6 0 1386.96 31.30 -2 -6 0 1385.16 31.00 -2 -6 0 1345.97 31.50 -2 -6 0 1422.46 28.30 -2 -6 0 1362.36 31.70 -2 -6 0 1386.66 32.10 -2 -6 0 1372.36 29.30 2 6 0 1388.16 31.70 2 6 0 1383.96 30.90 2 6 0 1391.56 28.30 2 6 0 1338.07 31.10 2 6 0 1371.86 31.30 2 6 0 1376.66 35.20 2 6 0 1407.76 31.10 2 6 0 1344.77 31.50 2 6 0 1384.56 35.00 2 6 0 1364.26 31.80 2 6 0 1419.56 31.50 2 6 0 1406.26 34.50 2 6 0 1419.06 32.00 2 6 0 1371.86 30.40 -3 -6 0 1.10 1.20 -3 -6 0 -0.20 1.10 -3 -6 0 0.40 0.60 -3 -6 0 2.00 1.20 -3 -6 0 0.10 0.60 -3 -6 0 0.30 0.80 -3 -6 0 0.20 1.00 -3 -6 0 0.60 0.90 3 6 0 -0.60 0.70 3 6 0 -0.10 1.50 3 6 0 -1.90 1.20 3 6 0 1.10 1.20 3 6 0 1.00 1.10 3 6 0 2.00 1.20 3 6 0 0.50 1.00 3 6 0 2.70 1.30 3 6 0 0.60 1.10 3 6 0 -1.40 1.10 3 6 0 -0.10 1.00 3 6 0 0.40 1.10 3 6 0 -0.10 1.00 3 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171.68 7.50 -6 -6 0 162.68 9.20 -6 -6 0 180.68 8.40 -6 -6 0 170.48 6.90 -6 -6 0 167.18 6.30 -6 -6 0 170.98 9.10 -6 -6 0 168.88 7.70 6 6 0 175.98 8.30 6 6 0 165.38 9.10 6 6 0 180.68 9.30 6 6 0 183.18 8.90 6 6 0 167.08 6.40 6 6 0 170.58 9.40 6 6 0 163.58 9.10 6 6 0 172.78 9.20 6 6 0 168.68 9.40 6 6 0 182.08 8.30 6 6 0 151.58 8.30 6 6 0 174.28 9.20 6 6 0 163.38 7.40 6 6 0 163.18 7.20 -7 -6 0 24.10 4.10 -7 -6 0 32.30 4.30 -7 -6 0 34.40 3.90 -7 -6 0 27.00 3.90 -7 -6 0 27.40 3.00 -7 -6 0 31.60 5.10 -7 -6 0 30.90 5.10 7 6 0 23.60 4.40 7 6 0 19.90 4.10 7 6 0 21.10 4.20 7 6 0 24.60 3.60 7 6 0 25.10 4.30 7 6 0 24.30 3.90 7 6 0 27.50 4.60 7 6 0 24.80 4.40 7 6 0 20.70 3.90 7 6 0 33.00 3.70 7 6 0 32.60 4.60 7 6 0 30.90 4.20 7 6 0 29.40 5.00 -8 -6 0 2.80 1.90 -8 -6 0 9.50 3.30 -8 -6 0 9.10 2.50 -8 -6 0 7.90 3.20 -8 -6 0 8.20 1.80 -8 -6 0 6.90 2.30 -8 -6 0 8.30 2.80 8 6 0 6.60 2.60 8 6 0 11.70 3.70 8 6 0 6.60 2.10 8 6 0 5.40 3.10 8 6 0 6.60 2.10 8 6 0 7.80 2.80 8 6 0 5.00 2.70 8 6 0 10.80 3.60 8 6 0 9.40 3.40 8 6 0 4.90 2.00 8 6 0 8.90 3.10 8 6 0 6.20 2.70 -9 -6 0 14.90 3.10 -9 -6 0 23.60 4.00 -9 -6 0 18.60 2.60 -9 -6 0 17.90 3.50 -9 -6 0 17.70 4.30 -9 -6 0 13.40 4.20 9 6 0 13.00 3.20 9 6 0 21.90 5.10 9 6 0 18.00 4.80 9 6 0 23.70 4.70 9 6 0 17.50 4.10 9 6 0 21.10 5.10 9 6 0 19.50 3.40 9 6 0 20.80 4.80 9 6 0 11.00 3.70 9 6 0 20.10 4.70 -10 -6 0 3.50 1.70 -10 -6 0 3.90 2.40 -10 -6 0 3.20 2.60 -10 -6 0 2.30 2.80 -10 -6 0 6.60 2.80 -10 -6 0 6.40 2.50 10 6 0 2.00 2.10 10 6 0 4.90 3.00 10 6 0 1.40 2.90 10 6 0 3.20 2.10 10 6 0 4.60 3.00 10 6 0 4.70 3.00 10 6 0 2.50 3.20 10 6 0 5.70 3.40 10 6 0 4.20 3.00 10 6 0 6.00 3.50 -11 -6 0 262.27 12.20 -11 -6 0 249.68 12.30 -11 -6 0 239.38 15.00 -11 -6 0 235.68 12.00 -11 -6 0 247.68 14.30 -11 -6 0 258.87 9.90 11 6 0 257.07 15.70 11 6 0 263.27 15.70 11 6 0 231.58 13.50 11 6 0 253.47 12.50 11 6 0 265.27 11.80 11 6 0 225.58 14.60 11 6 0 243.88 13.70 11 6 0 248.28 15.10 11 6 0 256.37 14.30 -12 -6 0 19.90 4.40 -12 -6 0 31.80 5.70 -12 -6 0 24.30 4.80 -12 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17.80 -7 7 0 458.35 16.30 -7 7 0 421.66 14.40 -7 7 0 410.16 16.50 -7 7 0 430.26 14.30 -7 7 0 436.96 16.20 -7 7 0 412.26 13.00 -7 7 0 413.06 16.50 6 -7 0 127.99 7.70 6 -7 0 113.59 6.60 6 -7 0 119.99 7.50 6 -7 0 108.29 7.30 6 -7 0 126.69 7.10 -6 7 0 117.89 8.30 -6 7 0 122.19 7.90 -6 7 0 124.19 6.40 -6 7 0 120.49 7.90 -6 7 0 107.69 6.90 -6 7 0 111.79 6.80 -6 7 0 114.09 5.50 -6 7 0 110.69 6.10 -6 7 0 116.79 7.30 5 -7 0 6.30 2.30 5 -7 0 6.30 1.90 5 -7 0 9.60 2.50 5 -7 0 6.80 2.30 5 -7 0 6.70 2.00 -5 7 0 5.80 2.10 -5 7 0 5.80 2.00 -5 7 0 6.00 2.10 -5 7 0 5.80 2.40 -5 7 0 7.20 1.80 -5 7 0 3.90 1.30 -5 7 0 4.80 2.50 -5 7 0 9.40 2.50 -5 7 0 2.30 1.90 -5 7 0 3.80 1.50 4 -7 0 40.00 4.50 4 -7 0 45.20 4.50 4 -7 0 42.90 4.50 4 -7 0 44.80 4.50 4 -7 0 33.60 3.80 -4 7 0 44.00 3.20 -4 7 0 36.00 4.20 -4 7 0 32.30 4.00 -4 7 0 44.30 3.50 -4 7 0 39.40 4.30 -4 7 0 41.00 2.90 -4 7 0 38.10 4.20 -4 7 0 37.40 2.50 -4 7 0 42.00 5.20 -4 7 0 36.50 5.00 -4 7 0 55.69 5.90 3 -7 0 994.20 24.30 3 -7 0 920.31 23.60 3 -7 0 963.90 23.80 3 -7 0 982.50 24.00 3 -7 0 947.31 24.10 3 -7 0 948.01 22.50 3 -7 0 980.20 24.20 -3 7 0 969.50 23.00 -3 7 0 979.40 24.50 -3 7 0 939.71 20.80 -3 7 0 972.80 26.40 -3 7 0 1007.40 24.50 -3 7 0 952.10 22.40 -3 7 0 963.00 24.10 -3 7 0 953.20 25.60 -3 7 0 925.21 21.10 -3 7 0 934.51 24.00 -3 7 0 974.10 23.90 -3 7 0 958.10 25.70 -3 7 0 968.10 27.40 2 -7 0 9.50 2.00 2 -7 0 14.60 2.00 2 -7 0 12.60 2.20 2 -7 0 11.50 2.20 2 -7 0 8.70 1.80 2 -7 0 11.00 2.10 -2 7 0 9.90 1.60 -2 7 0 16.70 3.70 -2 7 0 9.80 2.10 -2 7 0 9.10 1.90 -2 7 0 9.30 2.20 -2 7 0 7.50 2.50 -2 7 0 10.70 2.00 -2 7 0 8.30 2.30 -2 7 0 8.40 2.40 -2 7 0 10.70 1.70 -2 7 0 14.40 2.50 -2 7 0 11.50 2.20 1 -7 0 31.80 2.30 1 -7 0 28.30 3.00 1 -7 0 35.40 2.70 1 -7 0 32.90 2.70 1 -7 0 35.90 3.40 1 -7 0 29.70 3.10 -1 7 0 39.40 3.00 -1 7 0 28.20 3.80 -1 7 0 32.30 3.30 -1 7 0 29.80 3.60 -1 7 0 36.40 5.10 -1 7 0 30.40 2.20 -1 7 0 37.30 3.60 -1 7 0 41.90 4.40 -1 7 0 34.00 3.50 -1 7 0 35.70 2.50 -1 7 0 41.50 5.00 -1 7 0 35.70 3.50 0 -7 0 218.18 8.00 0 -7 0 202.38 7.40 0 -7 0 215.68 6.80 0 -7 0 208.48 6.30 0 -7 0 210.18 7.60 0 -7 0 214.68 7.10 0 -7 0 203.98 7.60 0 7 0 226.48 9.40 0 7 0 221.38 7.80 0 7 0 223.08 8.70 0 7 0 229.48 10.20 0 7 0 228.68 8.00 0 7 0 216.08 7.70 0 7 0 217.18 6.80 0 7 0 228.68 7.10 0 7 0 226.18 8.80 0 7 0 220.48 7.70 0 7 0 213.78 7.60 0 7 0 214.58 7.60 0 7 0 235.88 11.10 -1 -7 0 231.18 7.60 -1 -7 0 237.08 8.40 -1 -7 0 225.48 5.90 -1 -7 0 238.68 8.30 -1 -7 0 243.08 8.10 -1 -7 0 231.98 8.60 -1 -7 0 242.08 7.70 1 7 0 237.58 6.30 1 7 0 229.48 8.20 1 7 0 246.78 9.00 1 7 0 223.88 10.30 1 7 0 217.38 8.30 1 7 0 226.08 8.30 1 7 0 233.18 8.10 1 7 0 241.98 7.70 1 7 0 230.18 6.80 1 7 0 239.08 6.70 1 7 0 247.18 8.60 1 7 0 257.17 11.80 1 7 0 232.08 7.70 1 7 0 224.48 10.20 -2 -7 0 182.38 5.80 -2 -7 0 176.98 7.70 -2 -7 0 194.98 7.60 -2 -7 0 196.28 7.20 -2 -7 0 183.38 4.60 -2 -7 0 170.28 7.30 -2 -7 0 183.28 6.70 -2 -7 0 183.28 7.00 2 7 0 187.08 7.70 2 7 0 197.78 10.20 2 7 0 181.68 6.40 2 7 0 187.98 6.80 2 7 0 184.18 9.60 2 7 0 181.98 7.60 2 7 0 168.68 6.90 2 7 0 180.78 7.00 2 7 0 182.88 7.40 2 7 0 176.18 9.20 2 7 0 186.68 6.60 2 7 0 166.38 7.20 2 7 0 176.58 7.20 -3 -7 0 139.19 7.10 -3 -7 0 126.59 6.30 -3 -7 0 136.49 5.10 -3 -7 0 132.99 4.20 -3 -7 0 138.59 6.80 -3 -7 0 127.09 6.30 -3 -7 0 139.09 6.00 -3 -7 0 125.19 6.00 3 7 0 138.89 6.20 3 7 0 135.59 6.40 3 7 0 131.69 6.70 3 7 0 151.18 8.90 3 7 0 132.79 6.10 3 7 0 138.79 6.70 3 7 0 137.69 6.40 3 7 0 138.19 4.60 3 7 0 135.09 8.80 3 7 0 151.08 7.10 3 7 0 135.89 6.70 3 7 0 132.69 6.50 3 7 0 137.79 6.30 3 7 0 133.09 8.00 -4 -7 0 267.67 10.40 -4 -7 0 294.57 11.70 -4 -7 0 290.47 8.60 -4 -7 0 289.77 8.20 -4 -7 0 281.67 9.70 -4 -7 0 285.17 10.20 -4 -7 0 292.37 10.90 4 7 0 280.17 13.70 4 7 0 288.87 10.70 4 7 0 297.57 11.30 4 7 0 268.47 8.90 4 7 0 286.57 6.90 4 7 0 275.67 10.80 4 7 0 273.47 10.30 4 7 0 282.87 10.50 4 7 0 290.37 7.00 4 7 0 289.17 11.20 4 7 0 265.97 10.30 4 7 0 272.77 12.40 4 7 0 295.67 10.70 4 7 0 286.47 12.90 4 7 0 285.07 11.00 -5 -7 0 281.57 8.90 -5 -7 0 293.77 9.70 -5 -7 0 289.27 11.40 -5 -7 0 286.67 9.20 -5 -7 0 289.27 11.60 -5 -7 0 285.97 10.30 -5 -7 0 299.47 11.00 -5 -7 0 293.37 12.40 5 7 0 285.97 11.30 5 7 0 284.37 12.00 5 7 0 287.87 9.00 5 7 0 301.27 11.70 5 7 0 284.17 9.20 5 7 0 310.97 11.90 5 7 0 296.07 10.20 5 7 0 302.87 11.50 5 7 0 285.17 13.20 5 7 0 284.57 11.70 5 7 0 258.47 10.80 5 7 0 289.07 11.80 5 7 0 305.87 11.50 5 7 0 310.67 13.40 -6 -7 0 208.08 8.20 -6 -7 0 192.78 9.90 -6 -7 0 213.28 7.40 -6 -7 0 208.58 9.90 -6 -7 0 202.08 10.60 -6 -7 0 188.48 7.70 -6 -7 0 206.48 8.80 6 7 0 213.78 7.30 6 7 0 198.48 8.00 6 7 0 183.58 8.10 6 7 0 204.78 9.80 6 7 0 185.98 9.40 6 7 0 210.28 11.30 6 7 0 219.48 9.20 6 7 0 192.68 10.30 6 7 0 206.08 10.30 6 7 0 196.68 10.80 6 7 0 197.18 9.90 6 7 0 194.68 10.00 6 7 0 200.38 10.40 6 7 0 197.88 5.70 -7 -7 0 53.69 5.20 -7 -7 0 50.99 4.00 -7 -7 0 47.00 5.10 -7 -7 0 61.29 6.80 -7 -7 0 49.99 3.50 -7 -7 0 39.90 5.60 -7 -7 0 56.29 7.00 7 7 0 49.60 4.00 7 7 0 40.90 5.70 7 7 0 48.20 6.60 7 7 0 53.19 3.40 7 7 0 53.19 5.70 7 7 0 42.50 5.30 7 7 0 52.39 6.30 7 7 0 56.59 4.50 7 7 0 55.19 6.70 7 7 0 50.39 6.80 7 7 0 61.29 5.00 7 7 0 40.30 5.90 7 7 0 59.89 6.90 7 7 0 64.29 7.50 -8 -7 0 54.69 6.50 -8 -7 0 63.99 4.30 -8 -7 0 70.39 6.50 -8 -7 0 66.99 5.00 -8 -7 0 69.49 5.60 -8 -7 0 70.79 7.80 8 7 0 62.79 7.50 8 7 0 75.49 8.20 8 7 0 63.59 6.50 8 7 0 67.59 7.60 8 7 0 79.29 8.60 8 7 0 73.29 7.20 8 7 0 65.79 7.90 8 7 0 59.59 4.20 8 7 0 64.59 7.80 8 7 0 63.49 5.20 8 7 0 66.09 5.10 8 7 0 67.29 7.90 8 7 0 74.79 8.20 -9 -7 0 51.69 7.10 -9 -7 0 65.19 4.40 -9 -7 0 60.19 7.90 -9 -7 0 65.39 6.70 -9 -7 0 61.19 6.40 -9 -7 0 60.49 5.90 9 7 0 66.59 7.10 9 7 0 61.89 8.20 9 7 0 56.49 7.70 9 7 0 64.79 8.10 9 7 0 68.89 8.10 9 7 0 62.79 7.70 9 7 0 55.69 7.20 9 7 0 45.00 6.70 9 7 0 55.69 4.40 9 7 0 51.79 7.50 9 7 0 61.09 5.30 -10 -7 0 15.50 4.30 -10 -7 0 15.60 3.70 -10 -7 0 20.30 3.30 -10 -7 0 25.60 4.40 -10 -7 0 13.70 4.60 -10 -7 0 17.20 3.90 10 7 0 22.20 4.10 10 7 0 20.40 5.20 10 7 0 23.90 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0 167.98 7.70 4 -8 0 152.18 7.50 4 -8 0 155.68 7.70 4 -8 0 158.48 7.80 -4 8 0 157.08 9.40 -4 8 0 165.78 7.70 -4 8 0 153.78 6.30 -4 8 0 166.98 8.60 -4 8 0 160.58 9.20 -4 8 0 150.28 5.00 -4 8 0 163.78 8.10 -4 8 0 159.08 4.80 -4 8 0 149.49 8.50 -4 8 0 162.98 7.80 -4 8 0 165.98 6.80 3 -8 0 261.37 9.60 3 -8 0 271.97 10.00 3 -8 0 264.87 9.80 3 -8 0 270.67 9.90 -3 8 0 255.57 11.40 -3 8 0 259.17 11.10 -3 8 0 265.47 9.80 -3 8 0 264.37 9.70 -3 8 0 267.37 8.30 -3 8 0 264.17 10.10 -3 8 0 263.17 12.50 -3 8 0 263.57 11.30 -3 8 0 258.47 9.90 -3 8 0 259.67 8.50 2 -8 0 67.49 4.30 2 -8 0 71.49 4.50 2 -8 0 66.09 4.40 2 -8 0 67.89 4.20 2 -8 0 64.99 4.40 -2 8 0 68.99 5.30 -2 8 0 64.09 4.40 -2 8 0 69.89 4.50 -2 8 0 63.29 4.20 -2 8 0 63.99 7.10 -2 8 0 58.49 4.50 -2 8 0 66.09 6.40 -2 8 0 71.89 3.40 -2 8 0 66.29 3.40 -2 8 0 61.29 4.10 -2 8 0 69.99 5.50 -2 8 0 59.29 4.30 1 -8 0 10.80 2.00 1 -8 0 10.40 2.20 1 -8 0 10.90 2.10 1 -8 0 10.50 2.00 1 -8 0 8.40 1.90 -1 8 0 11.60 2.30 -1 8 0 10.20 2.70 -1 8 0 11.10 2.10 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8 0 244.48 8.90 2 8 0 273.37 9.90 2 8 0 268.87 9.90 2 8 0 281.07 12.60 2 8 0 262.27 9.50 2 8 0 268.07 10.00 2 8 0 261.37 9.00 2 8 0 266.67 8.20 2 8 0 251.07 9.50 2 8 0 262.37 12.10 -3 -8 0 415.76 12.70 -3 -8 0 398.96 13.10 -3 -8 0 402.16 12.20 -3 -8 0 384.66 13.70 -3 -8 0 396.86 12.60 3 8 0 394.66 16.50 3 8 0 405.06 15.90 3 8 0 398.26 13.30 3 8 0 410.96 12.20 3 8 0 389.86 16.30 3 8 0 374.26 12.60 3 8 0 384.76 12.00 3 8 0 367.46 13.10 3 8 0 416.36 12.70 3 8 0 388.56 12.10 3 8 0 405.26 13.50 3 8 0 390.76 12.80 -4 -8 0 78.89 6.00 -4 -8 0 100.09 5.40 -4 -8 0 91.69 5.90 -4 -8 0 85.69 5.60 -4 -8 0 98.99 5.70 4 8 0 86.49 6.00 4 8 0 94.59 5.70 4 8 0 92.29 5.70 4 8 0 93.79 7.30 4 8 0 86.69 6.10 4 8 0 90.59 9.00 4 8 0 90.29 5.50 4 8 0 82.89 5.70 4 8 0 98.19 5.80 4 8 0 78.79 8.70 4 8 0 89.29 5.70 -5 -8 0 0.70 1.30 -5 -8 0 3.30 1.70 -5 -8 0 0.30 1.40 -5 -8 0 0.50 1.40 -5 -8 0 2.10 1.80 -5 -8 0 -0.80 1.20 5 8 0 1.00 1.70 5 8 0 1.30 2.10 5 8 0 -1.00 1.10 5 8 0 0.50 1.40 5 8 0 1.30 1.50 5 8 0 1.60 1.70 5 8 0 0.20 2.20 5 8 0 3.40 2.20 5 8 0 -0.30 1.40 5 8 0 3.50 2.00 5 8 0 -0.30 2.20 -6 -8 0 35.00 5.50 -6 -8 0 27.10 4.40 -6 -8 0 38.00 4.60 -6 -8 0 32.50 3.80 -6 -8 0 31.80 5.00 6 8 0 27.60 3.00 6 8 0 26.30 4.30 6 8 0 22.10 4.90 6 8 0 31.10 4.50 6 8 0 27.30 4.50 6 8 0 31.90 4.90 6 8 0 26.40 4.80 6 8 0 25.80 4.50 6 8 0 27.50 4.30 6 8 0 38.30 6.50 6 8 0 35.00 3.30 -7 -8 0 52.99 4.20 -7 -8 0 38.20 5.50 -7 -8 0 65.19 6.30 -7 -8 0 47.10 3.70 -7 -8 0 58.49 7.50 7 8 0 59.69 6.70 7 8 0 41.80 6.50 7 8 0 50.49 7.50 7 8 0 50.69 6.50 7 8 0 53.39 6.70 7 8 0 50.29 6.50 7 8 0 49.60 4.20 7 8 0 48.60 4.00 7 8 0 49.99 6.40 7 8 0 39.80 5.90 7 8 0 68.89 7.00 -8 -8 0 168.58 8.90 -8 -8 0 160.18 10.00 -8 -8 0 164.98 7.00 -8 -8 0 170.58 8.10 8 8 0 148.29 9.50 8 8 0 160.58 11.00 8 8 0 194.38 11.80 8 8 0 143.79 9.90 8 8 0 145.19 10.20 8 8 0 164.28 10.70 8 8 0 157.78 6.90 8 8 0 165.38 8.00 8 8 0 157.18 5.30 8 8 0 156.38 10.50 8 8 0 149.69 8.20 8 8 0 163.08 10.00 -9 -8 0 7.30 2.20 -9 -8 0 6.30 2.60 -9 -8 0 10.00 3.30 -9 -8 0 9.20 2.70 -9 -8 0 8.30 2.90 9 8 0 5.30 3.20 9 8 0 10.40 4.00 9 8 0 3.60 3.20 9 8 0 8.00 1.90 9 8 0 8.30 3.60 9 8 0 8.90 3.70 9 8 0 8.10 3.60 9 8 0 10.60 2.70 9 8 0 6.20 2.60 9 8 0 5.20 3.20 9 8 0 8.20 2.70 9 8 0 7.60 3.40 -10 -8 0 23.90 3.70 -10 -8 0 25.50 4.70 -10 -8 0 21.80 4.20 -10 -8 0 23.90 5.20 -10 -8 0 24.70 4.20 10 8 0 24.60 5.50 10 8 0 30.70 6.50 10 8 0 25.70 5.90 10 8 0 15.60 4.80 10 8 0 22.60 5.30 10 8 0 20.90 4.30 10 8 0 18.40 2.90 10 8 0 22.30 5.50 10 8 0 16.80 3.50 10 8 0 27.40 6.10 -11 -8 0 21.90 4.80 -11 -8 0 22.50 5.70 -11 -8 0 18.90 3.20 -11 -8 0 17.20 4.20 11 8 0 26.40 3.80 11 8 0 17.70 5.50 11 8 0 22.80 6.20 11 8 0 14.00 3.90 11 8 0 23.90 6.10 11 8 0 29.60 4.90 11 8 0 22.20 5.80 11 8 0 15.70 5.20 11 8 0 20.40 5.70 -12 -8 0 0.30 1.70 -12 -8 0 -2.00 2.10 -12 -8 0 2.90 2.50 12 8 0 2.00 3.80 12 8 0 1.80 3.40 12 8 0 -2.60 2.20 12 8 0 -0.80 2.20 12 8 0 1.90 2.10 12 8 0 1.30 3.70 12 8 0 2.30 3.80 12 8 0 1.10 3.10 12 8 0 -0.20 1.80 10 -9 0 132.49 10.80 10 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235.08 12.10 -6 9 0 259.87 9.40 -6 9 0 236.78 10.90 -6 9 0 222.98 12.50 -6 9 0 241.98 9.70 -6 9 0 232.98 10.90 -6 9 0 236.78 11.50 5 -9 0 114.99 7.00 5 -9 0 121.19 7.40 5 -9 0 114.79 7.20 5 -9 0 106.89 7.10 -5 9 0 122.49 7.70 -5 9 0 131.89 8.90 -5 9 0 117.49 8.60 -5 9 0 120.59 8.30 -5 9 0 120.39 5.80 -5 9 0 116.99 7.00 -5 9 0 123.19 6.10 -5 9 0 127.59 7.40 4 -9 0 182.78 8.80 4 -9 0 188.88 8.90 4 -9 0 183.78 8.70 4 -9 0 195.28 9.00 -4 9 0 199.58 7.30 -4 9 0 179.98 10.30 -4 9 0 199.98 10.10 -4 9 0 192.58 8.70 -4 9 0 199.18 7.00 -4 9 0 192.78 8.80 -4 9 0 184.58 9.90 -4 9 0 184.48 10.90 -4 9 0 194.98 9.10 3 -9 0 2149.88 50.29 3 -9 0 2243.28 51.09 3 -9 0 2325.97 51.29 3 -9 0 2346.17 51.39 -3 9 0 2259.07 53.99 -3 9 0 2224.18 47.40 -3 9 0 2284.07 54.29 -3 9 0 2256.47 47.70 -3 9 0 2309.57 50.79 -3 9 0 2265.97 51.09 -3 9 0 2230.48 50.69 -3 9 0 2233.38 53.49 -3 9 0 2274.97 56.49 2 -9 0 4.60 1.70 2 -9 0 6.80 1.90 2 -9 0 5.20 1.80 2 -9 0 11.00 2.40 -2 9 0 9.00 3.70 -2 9 0 10.20 2.30 -2 9 0 10.80 2.90 -2 9 0 8.80 2.80 -2 9 0 6.00 1.30 -2 9 0 9.00 2.40 -2 9 0 8.40 2.90 -2 9 0 9.40 2.40 -2 9 0 8.10 2.20 -2 9 0 11.90 2.80 -2 9 0 9.30 1.50 1 -9 0 496.15 13.90 1 -9 0 468.55 14.00 1 -9 0 453.95 14.10 1 -9 0 492.15 14.70 1 -9 0 452.65 12.80 -1 9 0 457.75 11.30 -1 9 0 448.76 13.70 -1 9 0 490.15 11.60 -1 9 0 443.46 17.00 -1 9 0 480.15 16.00 -1 9 0 457.35 18.60 -1 9 0 460.95 14.10 -1 9 0 468.25 14.00 -1 9 0 475.15 15.70 -1 9 0 461.35 14.00 -1 9 0 452.35 14.00 -1 9 0 467.45 16.00 0 -9 0 18.50 2.90 0 -9 0 20.70 2.80 0 -9 0 16.70 2.90 0 -9 0 19.60 2.90 0 9 0 20.50 2.10 0 9 0 20.80 2.10 0 9 0 19.50 2.90 0 9 0 19.00 3.40 0 9 0 21.20 3.00 0 9 0 19.10 3.00 0 9 0 22.30 4.70 0 9 0 18.40 2.80 0 9 0 22.40 4.20 0 9 0 20.00 3.80 -1 -9 0 214.68 9.10 -1 -9 0 202.48 8.50 -1 -9 0 228.38 8.60 -1 -9 0 227.68 8.20 1 9 0 227.38 9.00 1 9 0 207.28 8.40 1 9 0 200.78 10.60 1 9 0 216.88 7.30 1 9 0 218.68 9.50 1 9 0 206.58 8.50 1 9 0 209.78 7.40 1 9 0 211.58 11.20 1 9 0 219.78 12.20 1 9 0 223.88 8.80 -2 -9 0 233.48 9.90 -2 -9 0 240.08 9.00 -2 -9 0 233.08 8.60 -2 -9 0 225.08 9.20 2 9 0 223.18 12.60 2 9 0 227.08 6.90 2 9 0 229.18 9.20 2 9 0 231.98 10.40 2 9 0 224.48 6.80 2 9 0 221.28 8.30 2 9 0 215.48 8.90 2 9 0 266.97 12.80 2 9 0 222.58 8.30 2 9 0 221.98 11.70 2 9 0 232.18 9.50 -3 -9 0 76.59 5.90 -3 -9 0 70.79 4.90 -3 -9 0 72.29 5.20 -3 -9 0 82.39 5.00 3 9 0 74.39 7.90 3 9 0 75.19 8.00 3 9 0 82.89 4.50 3 9 0 80.49 5.70 3 9 0 80.49 5.30 3 9 0 64.79 7.90 3 9 0 77.69 5.00 3 9 0 80.89 4.50 3 9 0 73.89 4.50 3 9 0 90.39 5.80 3 9 0 91.49 5.40 -4 -9 0 245.08 10.60 -4 -9 0 261.97 10.30 -4 -9 0 271.37 10.00 -4 -9 0 256.87 11.60 4 9 0 272.97 10.80 4 9 0 250.87 10.50 4 9 0 253.47 13.70 4 9 0 260.47 11.20 4 9 0 260.67 10.30 4 9 0 254.97 14.10 4 9 0 273.27 13.60 4 9 0 262.27 10.00 4 9 0 274.67 10.30 4 9 0 264.17 9.90 4 9 0 253.07 10.90 -5 -9 0 118.19 7.00 -5 -9 0 111.59 7.20 -5 -9 0 112.09 7.80 -5 -9 0 118.39 6.60 5 9 0 124.49 7.60 5 9 0 123.99 7.90 5 9 0 111.39 11.80 5 9 0 98.19 9.60 5 9 0 114.29 7.50 5 9 0 113.19 9.10 5 9 0 117.49 7.20 5 9 0 112.69 7.00 5 9 0 113.69 6.80 5 9 0 129.09 7.30 -6 -9 0 34.00 4.40 -6 -9 0 39.10 4.20 -6 -9 0 44.60 6.40 -6 -9 0 47.10 5.90 6 9 0 32.10 5.30 6 9 0 47.00 5.90 6 9 0 41.30 7.90 6 9 0 38.60 6.40 6 9 0 42.70 5.40 6 9 0 49.00 6.00 6 9 0 37.90 5.40 6 9 0 36.90 5.00 6 9 0 43.00 5.60 6 9 0 40.40 6.60 6 9 0 49.80 6.00 -7 -9 0 62.49 6.90 -7 -9 0 75.59 5.00 -7 -9 0 72.59 5.70 -7 -9 0 69.79 8.40 7 9 0 81.59 8.50 7 9 0 63.29 6.70 7 9 0 63.89 3.60 7 9 0 66.99 7.60 7 9 0 70.29 8.80 7 9 0 69.99 7.40 7 9 0 74.29 3.70 7 9 0 69.69 8.50 7 9 0 61.29 7.40 7 9 0 61.99 7.20 7 9 0 80.09 8.40 -8 -9 0 44.90 6.30 -8 -9 0 49.10 5.20 -8 -9 0 39.50 5.20 8 9 0 41.50 4.30 8 9 0 37.90 6.50 8 9 0 49.80 6.80 8 9 0 41.20 6.90 8 9 0 41.00 6.60 8 9 0 48.10 3.90 8 9 0 50.09 8.10 8 9 0 55.69 7.20 8 9 0 49.50 7.40 8 9 0 44.70 6.40 -9 -9 0 41.50 6.90 -9 -9 0 38.90 5.60 -9 -9 0 44.00 5.60 -9 -9 0 36.10 4.70 9 9 0 40.20 6.90 9 9 0 35.70 6.00 9 9 0 38.30 7.10 9 9 0 38.50 6.70 9 9 0 35.80 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52.79 7.70 -7 10 0 60.99 7.80 -7 10 0 60.59 4.50 -7 10 0 68.59 7.90 -7 10 0 62.49 7.10 -7 10 0 62.69 7.10 6 -10 0 102.39 7.10 6 -10 0 114.99 7.90 6 -10 0 91.49 7.10 -6 10 0 108.29 7.40 -6 10 0 111.29 8.70 -6 10 0 103.79 7.10 -6 10 0 97.89 10.10 -6 10 0 100.49 9.80 -6 10 0 87.99 5.10 -6 10 0 88.49 7.20 -6 10 0 96.79 5.60 5 -10 0 20.60 4.00 5 -10 0 15.20 3.30 5 -10 0 18.90 3.80 5 -10 0 13.60 3.10 -5 10 0 19.60 4.60 -5 10 0 17.10 3.50 -5 10 0 22.10 5.10 -5 10 0 18.10 3.90 -5 10 0 23.10 5.10 -5 10 0 20.30 2.70 -5 10 0 16.90 3.50 -5 10 0 15.50 2.30 4 -10 0 27.40 4.10 4 -10 0 23.10 3.80 4 -10 0 32.50 4.30 4 -10 0 26.70 4.20 -4 10 0 27.20 2.50 -4 10 0 25.30 5.20 -4 10 0 28.80 5.10 -4 10 0 28.00 4.10 -4 10 0 33.50 4.70 -4 10 0 28.60 2.40 -4 10 0 32.20 4.30 -4 10 0 35.20 5.80 -4 10 0 22.10 4.20 3 -10 0 36.10 4.40 3 -10 0 36.80 4.50 3 -10 0 36.60 4.50 3 -10 0 45.90 5.10 -3 10 0 37.10 2.10 -3 10 0 44.20 4.80 -3 10 0 34.00 5.30 -3 10 0 42.20 5.80 -3 10 0 40.80 4.60 -3 10 0 43.50 5.70 -3 10 0 36.50 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7.80 -2 -10 0 1.20 1.20 -2 -10 0 1.10 1.60 -2 -10 0 3.80 1.60 -2 -10 0 2.60 1.60 2 10 0 2.70 2.70 2 10 0 2.90 1.40 2 10 0 0.20 2.30 2 10 0 0.80 2.30 2 10 0 4.80 2.00 2 10 0 3.70 1.90 2 10 0 3.00 1.70 2 10 0 1.30 1.30 -3 -10 0 132.89 7.20 -3 -10 0 168.58 9.00 -3 -10 0 143.19 7.80 -3 -10 0 147.19 7.20 3 10 0 163.68 10.80 3 10 0 154.48 8.00 3 10 0 153.48 7.20 3 10 0 168.48 8.00 3 10 0 144.69 7.00 3 10 0 147.39 10.50 3 10 0 156.98 8.20 3 10 0 144.69 5.60 3 10 0 153.38 5.90 3 10 0 155.38 11.10 -4 -10 0 30.40 4.90 -4 -10 0 35.60 4.50 -4 -10 0 32.60 4.20 -4 -10 0 30.10 4.50 4 10 0 32.00 6.30 4 10 0 25.30 4.20 4 10 0 40.90 4.70 4 10 0 34.10 4.80 4 10 0 32.60 4.60 4 10 0 34.40 4.40 4 10 0 28.40 3.50 4 10 0 29.40 5.70 4 10 0 22.20 5.50 -5 -10 0 129.19 7.20 -5 -10 0 131.99 8.10 -5 -10 0 136.09 8.90 5 10 0 134.59 8.00 5 10 0 144.29 8.70 5 10 0 137.09 8.50 5 10 0 110.89 10.90 5 10 0 138.99 7.40 5 10 0 130.39 7.30 5 10 0 131.69 7.90 5 10 0 141.59 10.90 5 10 0 136.19 11.10 -6 -10 0 -0.30 1.20 -6 -10 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86.69 9.90 10 10 0 71.69 10.30 10 10 0 80.09 9.90 10 10 0 77.79 8.90 10 10 0 75.49 5.10 10 10 0 88.29 10.60 10 10 0 75.19 10.90 10 10 0 81.29 10.20 10 10 0 76.29 9.90 10 10 0 85.49 5.40 8 -11 0 49.00 6.20 8 -11 0 40.50 6.30 8 -11 0 47.30 7.10 -8 11 0 58.59 7.80 -8 11 0 53.19 8.60 -8 11 0 45.10 7.20 -8 11 0 51.49 6.90 -8 11 0 46.20 4.60 -8 11 0 50.09 7.10 7 -11 0 6.20 2.90 7 -11 0 2.90 2.20 7 -11 0 4.70 2.80 -7 11 0 4.80 2.60 -7 11 0 5.10 3.60 -7 11 0 5.10 3.00 -7 11 0 2.60 3.10 -7 11 0 3.70 1.60 -7 11 0 3.80 2.40 -7 11 0 5.00 1.70 6 -11 0 124.79 8.00 6 -11 0 120.79 8.40 6 -11 0 130.49 8.50 -6 11 0 120.19 9.60 -6 11 0 124.79 9.50 -6 11 0 122.19 11.70 -6 11 0 114.69 8.30 -6 11 0 108.09 7.60 -6 11 0 124.49 5.20 -6 11 0 111.79 7.70 -6 11 0 118.99 5.00 5 -11 0 5.40 2.20 5 -11 0 3.30 2.20 5 -11 0 4.20 2.20 -5 11 0 2.30 2.30 -5 11 0 4.20 2.00 -5 11 0 10.40 4.00 -5 11 0 2.90 2.10 -5 11 0 2.30 0.80 -5 11 0 6.00 3.00 -5 11 0 2.30 2.70 4 -11 0 94.59 6.70 4 -11 0 96.39 6.70 4 -11 0 101.29 6.80 4 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0 95.49 6.30 -2 12 0 94.89 10.90 -2 12 0 84.59 5.80 -2 12 0 89.79 6.00 -2 12 0 86.49 5.90 -2 12 0 95.39 7.60 -2 12 0 101.79 9.70 -2 12 0 98.99 10.00 -2 12 0 84.99 6.20 1 -12 0 0.90 1.70 1 -12 0 0.10 1.40 1 -12 0 1.60 1.60 1 -12 0 1.70 1.50 -1 12 0 0.00 2.40 -1 12 0 3.30 1.80 -1 12 0 4.20 1.90 -1 12 0 0.30 2.70 -1 12 0 2.00 2.30 -1 12 0 0.60 1.30 0 -12 0 18.70 3.20 0 -12 0 19.60 3.40 0 -12 0 23.90 3.90 0 -12 0 17.90 3.60 0 12 0 21.20 3.50 0 12 0 21.50 5.20 0 12 0 21.00 4.30 0 12 0 19.00 3.40 0 12 0 24.80 6.10 0 12 0 24.20 3.90 -1 -12 0 94.89 6.90 -1 -12 0 88.39 6.00 -1 -12 0 86.29 6.10 -1 -12 0 94.79 6.00 1 12 0 92.09 6.10 1 12 0 90.49 6.10 1 12 0 97.39 6.40 1 12 0 88.59 10.90 1 12 0 83.09 10.10 1 12 0 95.79 10.30 1 12 0 102.79 7.30 -2 -12 0 8.60 2.50 -2 -12 0 3.20 2.10 -2 -12 0 6.00 2.20 -2 -12 0 9.00 2.60 2 12 0 6.50 2.40 2 12 0 6.50 1.30 2 12 0 9.60 4.30 2 12 0 6.40 2.40 2 12 0 3.50 3.40 2 12 0 8.10 1.50 2 12 0 12.90 4.10 2 12 0 9.70 2.90 -3 -12 0 297.27 12.30 -3 -12 0 300.37 13.50 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11.00 -7 -4 9 128.19 8.50 -7 -4 9 146.59 10.80 6 4 -9 29.80 5.30 6 4 -9 49.40 6.40 6 4 -9 46.90 7.40 6 4 -9 45.20 7.50 6 4 -9 32.20 5.90 -6 -4 9 38.60 6.80 -6 -4 9 36.70 5.20 -6 -4 9 37.20 6.00 -6 -4 9 30.30 6.10 -6 -4 9 36.70 6.60 -6 -4 9 46.90 5.80 -6 -4 9 39.00 4.00 5 4 -9 368.46 16.00 5 4 -9 368.26 16.50 5 4 -9 389.46 17.30 5 4 -9 385.36 16.90 5 4 -9 374.06 14.70 5 4 -9 376.06 16.90 -5 -4 9 371.26 17.40 -5 -4 9 382.86 14.40 -5 -4 9 338.57 16.70 -5 -4 9 401.16 16.50 -5 -4 9 389.06 17.40 -5 -4 9 387.16 14.40 -5 -4 9 363.16 11.70 4 4 -9 15.60 4.20 4 4 -9 16.20 4.20 4 4 -9 18.30 4.50 4 4 -9 12.30 3.50 4 4 -9 17.30 4.50 4 4 -9 15.20 3.40 -4 -4 9 18.30 2.80 -4 -4 9 17.00 4.50 -4 -4 9 18.30 4.90 -4 -4 9 17.70 4.30 -4 -4 9 14.00 3.10 -4 -4 9 13.70 3.70 -4 -4 9 22.90 4.00 -4 -4 9 17.10 4.50 3 4 -9 32.00 5.30 3 4 -9 28.00 4.90 3 4 -9 34.40 5.50 3 4 -9 31.70 4.70 3 4 -9 32.40 5.70 3 4 -9 35.30 5.80 3 4 -9 30.60 5.10 -3 -4 9 28.40 4.20 -3 -4 9 30.90 5.40 -3 -4 9 32.00 5.30 -3 -4 9 40.30 6.10 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44.40 7.50 -11 4 -9 41.00 8.50 11 -4 9 33.70 7.20 11 -4 9 43.30 6.70 11 -4 9 37.40 7.40 10 3 -9 165.48 13.30 10 3 -9 184.68 14.20 10 3 -9 183.58 12.70 10 3 -9 183.18 12.10 -10 -3 9 155.08 10.80 -10 -3 9 159.58 12.80 -10 -3 9 189.18 7.70 -10 -3 9 177.28 13.30 -10 -3 9 193.78 11.40 -10 -3 9 172.78 13.90 9 3 -9 226.08 14.60 9 3 -9 212.08 14.70 9 3 -9 214.78 13.30 9 3 -9 235.28 13.10 -9 -3 9 226.08 11.50 -9 -3 9 232.18 12.10 -9 -3 9 219.18 12.20 -9 -3 9 266.47 15.30 -9 -3 9 219.28 15.10 -9 -3 9 235.78 8.70 -9 -3 9 244.28 15.00 8 3 -9 129.89 9.90 8 3 -9 93.19 10.90 8 3 -9 105.79 8.50 8 3 -9 96.59 11.30 -8 -3 9 102.49 7.60 -8 -3 9 128.99 12.50 -8 -3 9 139.29 9.00 -8 -3 9 101.99 7.40 -8 -3 9 98.19 11.10 -8 -3 9 109.49 5.50 -8 -3 9 106.79 10.90 -8 -3 9 105.99 11.30 7 3 -9 2.40 2.90 7 3 -9 6.30 3.60 7 3 -9 -0.20 2.20 7 3 -9 5.80 3.00 7 3 -9 9.00 3.50 7 3 -9 7.80 3.80 -7 -3 9 5.50 2.90 -7 -3 9 0.80 2.60 -7 -3 9 7.00 3.40 -7 -3 9 5.20 1.60 -7 -3 9 2.80 3.20 -7 -3 9 4.90 2.50 -7 -3 9 2.70 2.10 -7 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11.70 0 -3 9 243.58 11.80 0 -3 9 229.68 10.80 0 -3 9 242.48 11.90 0 -3 9 253.67 11.70 0 -3 9 218.58 10.00 0 -3 9 257.17 11.40 0 -3 9 219.88 8.40 -1 3 -9 608.54 19.00 -1 3 -9 624.04 20.90 -1 3 -9 609.54 20.70 -1 3 -9 610.54 17.60 -1 3 -9 629.04 19.80 -1 3 -9 650.33 20.90 -1 3 -9 638.74 20.60 -1 3 -9 651.23 20.90 -1 3 -9 646.14 16.10 -1 3 -9 634.14 19.00 -1 3 -9 638.04 21.40 1 -3 9 631.84 21.20 1 -3 9 674.43 21.80 1 -3 9 628.94 17.30 1 -3 9 626.24 20.20 1 -3 9 626.14 19.80 1 -3 9 642.74 21.20 1 -3 9 642.24 19.30 1 -3 9 595.94 20.20 1 -3 9 640.94 19.30 1 -3 9 582.14 20.70 -2 3 -9 132.79 8.50 -2 3 -9 136.99 8.30 -2 3 -9 142.59 9.00 -2 3 -9 136.89 8.70 -2 3 -9 140.69 8.80 -2 3 -9 126.19 8.20 -2 3 -9 138.19 7.90 -2 3 -9 142.39 7.80 -2 3 -9 139.49 6.70 -2 3 -9 144.29 8.50 -2 3 -9 138.19 7.40 2 -3 9 150.18 8.00 2 -3 9 140.49 8.90 2 -3 9 143.89 9.00 2 -3 9 131.59 8.00 2 -3 9 131.69 8.40 2 -3 9 134.59 8.90 2 -3 9 145.59 6.80 2 -3 9 128.39 8.60 2 -3 9 145.69 8.50 -3 3 -9 4.70 1.70 -3 3 -9 7.40 2.80 -3 3 -9 12.10 3.30 -3 3 -9 7.80 3.00 -3 3 -9 8.40 2.90 -3 3 -9 9.70 3.00 -3 3 -9 5.50 2.30 -3 3 -9 12.70 3.00 -3 3 -9 7.70 2.70 -3 3 -9 7.80 2.60 3 -3 9 9.90 3.20 3 -3 9 7.20 2.50 3 -3 9 6.90 2.80 3 -3 9 4.90 2.30 3 -3 9 6.00 2.90 3 -3 9 12.50 2.70 3 -3 9 6.40 2.80 3 -3 9 5.80 2.40 3 -3 9 5.00 2.30 -4 3 -9 232.38 10.80 -4 3 -9 237.48 12.00 -4 3 -9 225.18 11.90 -4 3 -9 248.08 12.40 -4 3 -9 230.38 10.70 -4 3 -9 246.38 12.20 -4 3 -9 239.88 9.30 -4 3 -9 230.88 11.30 -4 3 -9 244.88 9.70 4 -3 9 237.18 11.90 4 -3 9 256.67 12.60 4 -3 9 236.08 12.30 4 -3 9 242.08 11.20 4 -3 9 248.88 9.90 4 -3 9 238.48 12.10 4 -3 9 247.38 11.90 4 -3 9 243.88 12.60 4 -3 9 234.68 11.60 -5 3 -9 21.30 4.40 -5 3 -9 15.20 3.60 -5 3 -9 13.50 3.90 -5 3 -9 19.60 4.30 -5 3 -9 16.20 2.90 -5 3 -9 13.90 3.30 -5 3 -9 21.50 4.70 -5 3 -9 17.40 4.20 -5 3 -9 18.90 3.70 5 -3 9 15.80 3.20 5 -3 9 24.80 4.80 5 -3 9 19.70 4.10 5 -3 9 22.50 5.10 5 -3 9 17.80 4.00 5 -3 9 17.40 4.30 5 -3 9 22.60 4.40 5 -3 9 19.50 4.80 -6 3 -9 252.67 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8.70 6 4 -10 41.40 5.80 6 4 -10 55.99 7.60 6 4 -10 58.49 8.50 -6 -4 10 64.29 6.80 -6 -4 10 57.19 4.10 -6 -4 10 50.19 7.90 -6 -4 10 75.29 7.70 -6 -4 10 54.89 8.10 -6 -4 10 65.29 8.20 5 4 -10 5.40 2.90 5 4 -10 0.20 2.00 5 4 -10 -0.40 1.70 5 4 -10 0.30 2.40 5 4 -10 4.10 3.00 -5 -4 10 1.10 2.00 -5 -4 10 -0.90 1.50 -5 -4 10 -1.90 2.10 -5 -4 10 3.00 2.80 -5 -4 10 3.30 3.10 -5 -4 10 1.10 1.20 -5 -4 10 1.00 2.40 4 4 -10 97.79 8.30 4 4 -10 108.19 7.50 4 4 -10 101.09 8.00 4 4 -10 85.29 9.50 4 4 -10 123.39 9.40 -4 -4 10 101.49 5.50 -4 -4 10 125.69 10.30 -4 -4 10 129.59 9.10 -4 -4 10 96.09 6.80 -4 -4 10 119.99 9.50 -4 -4 10 106.29 10.80 -4 -4 10 94.89 10.30 -4 -4 10 103.09 7.10 3 4 -10 4.80 2.70 3 4 -10 4.70 2.70 3 4 -10 7.70 3.20 3 4 -10 2.30 2.00 3 4 -10 8.20 3.30 3 4 -10 5.60 2.90 -3 -4 10 1.80 2.40 -3 -4 10 -1.40 2.10 -3 -4 10 4.60 3.10 -3 -4 10 2.40 2.80 -3 -4 10 4.40 1.70 -3 -4 10 3.00 2.00 -3 -4 10 4.50 2.50 2 4 -10 252.97 10.80 2 4 -10 210.48 12.00 2 4 -10 220.18 12.20 2 4 -10 231.38 11.90 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-1.30 2.50 3 0 17 5.40 3.80 3 0 17 0.10 1.10 3 0 17 -0.10 2.60 3 0 17 0.50 1.40 3 0 17 1.80 3.10 3 0 17 -0.70 2.90 -4 0 -17 35.00 6.60 -4 0 -17 45.90 8.90 -4 0 -17 44.50 8.40 -4 0 -17 32.80 5.60 4 0 17 36.50 7.70 4 0 17 41.60 4.60 4 0 17 35.50 7.40 4 0 17 53.39 9.00 4 0 17 44.60 8.30 4 0 17 46.00 8.00 1 -1 -17 0.10 3.70 1 -1 -17 1.80 3.00 1 -1 -17 0.70 3.00 -1 1 17 -0.60 2.60 -1 1 17 6.00 3.70 -1 1 17 4.30 3.50 -1 1 17 4.10 2.80 -1 1 17 5.00 3.80 -1 1 17 2.40 2.10 0 -1 -17 120.19 10.10 0 -1 -17 104.79 12.80 0 -1 -17 112.99 12.00 0 1 17 113.49 7.80 0 1 17 124.49 13.10 0 1 17 93.89 11.20 0 1 17 111.69 12.00 0 1 17 87.49 10.90 0 1 17 109.19 9.20 -1 -1 -17 10.30 4.10 -1 -1 -17 6.70 3.90 -1 -1 -17 6.30 4.30 1 1 17 19.60 5.40 1 1 17 20.00 5.90 1 1 17 16.10 3.70 1 1 17 27.00 6.60 1 1 17 18.60 5.60 1 1 17 16.40 4.30 -2 -1 -17 1.00 3.10 -2 -1 -17 11.30 5.10 -2 -1 -17 1.60 2.90 2 1 17 2.80 3.20 2 1 17 5.10 3.40 2 1 17 5.90 3.40 2 1 17 5.60 1.10 2 1 17 4.10 3.70 2 1 17 10.60 4.40 2 1 17 5.20 2.50 -3 -1 -17 80.79 9.80 -3 -1 -17 86.39 10.50 -3 -1 -17 76.19 11.50 3 1 17 89.39 11.10 3 1 17 92.89 11.10 3 1 17 87.39 9.90 3 1 17 87.79 10.70 3 1 17 89.69 11.30 3 1 17 89.09 4.10 3 1 17 99.29 7.50 -4 -1 -17 118.29 10.00 -4 -1 -17 124.79 13.40 -4 -1 -17 125.69 14.50 4 1 17 127.89 13.40 4 1 17 120.69 5.40 4 1 17 126.79 10.30 4 1 17 127.09 13.30 4 1 17 92.19 11.50 4 1 17 102.49 11.50 1 -2 -17 145.29 11.20 1 -2 -17 120.09 12.50 1 -2 -17 119.79 13.60 -1 2 17 137.29 13.50 -1 2 17 118.49 9.00 -1 2 17 152.48 12.00 -1 2 17 136.29 11.20 -1 2 17 124.89 7.60 -1 2 17 113.49 11.80 0 -2 -17 0.10 2.90 0 -2 -17 4.20 4.10 0 -2 -17 2.90 2.90 0 2 17 1.80 3.10 0 2 17 4.20 3.40 0 2 17 -0.50 2.50 0 2 17 0.80 1.60 0 2 17 2.80 3.30 0 2 17 3.50 2.60 -1 -2 -17 11.10 4.40 -1 -2 -17 11.80 4.10 -1 -2 -17 14.90 5.40 1 2 17 12.40 4.60 1 2 17 13.30 4.00 1 2 17 16.00 5.20 1 2 17 17.10 3.50 1 2 17 9.50 4.20 1 2 17 17.90 5.20 -2 -2 -17 110.29 13.20 -2 -2 -17 123.69 9.90 -2 -2 -17 112.19 11.70 2 2 17 148.59 11.60 2 2 17 119.09 12.30 2 2 17 108.79 9.00 2 2 17 123.59 7.80 2 2 17 104.29 11.40 2 2 17 125.69 12.70 -3 -2 -17 -1.40 2.20 -3 -2 -17 1.50 2.90 -3 -2 -17 -1.40 3.20 3 2 17 0.10 2.70 3 2 17 1.30 1.70 3 2 17 -0.30 2.30 3 2 17 3.40 3.50 3 2 17 -1.10 2.30 3 2 17 -3.80 2.30 -4 -2 -17 180.38 14.80 -4 -2 -17 176.88 13.00 -4 -2 -17 167.48 11.60 4 2 17 170.58 13.10 4 2 17 159.98 12.40 4 2 17 175.98 12.60 4 2 17 185.18 13.20 4 2 17 182.58 9.80 4 2 17 195.18 12.20 0 -3 -17 9.60 4.70 0 -3 -17 8.40 4.20 0 -3 -17 8.20 3.80 0 3 17 5.90 2.10 0 3 17 4.80 3.40 0 3 17 1.60 2.80 0 3 17 3.60 2.50 0 3 17 12.40 4.70 0 3 17 8.50 4.00 0 3 17 7.20 2.50 -1 -3 -17 89.19 9.70 -1 -3 -17 78.99 11.40 -1 -3 -17 106.69 11.70 1 3 17 110.69 6.50 1 3 17 110.29 12.00 1 3 17 111.29 8.30 1 3 17 99.19 11.10 1 3 17 88.29 10.50 1 3 17 98.89 11.10 1 3 17 101.39 6.90 -2 -3 -17 -1.60 2.10 -2 -3 -17 1.80 3.70 -2 -3 -17 0.30 2.50 2 3 17 2.80 3.10 2 3 17 -0.90 1.30 2 3 17 4.30 3.30 2 3 17 -0.10 2.40 2 3 17 -0.60 1.70 2 3 17 1.80 2.80 2 3 17 0.60 2.20 -3 -3 -17 3.30 4.20 -3 -3 -17 10.40 4.50 -3 -3 -17 7.50 3.80 3 3 17 17.70 4.40 3 3 17 8.20 4.20 3 3 17 16.50 5.00 3 3 17 19.90 5.60 3 3 17 13.20 4.60 3 3 17 9.20 3.10 3 3 17 11.50 2.90 -4 -3 -17 6.70 3.50 -4 -3 -17 13.10 5.70 -4 -3 -17 11.20 4.00 4 3 17 18.30 5.40 4 3 17 11.10 4.20 4 3 17 1.40 3.20 4 3 17 8.40 2.70 4 3 17 17.80 5.40 4 3 17 5.50 2.90 0 -4 -17 12.40 4.30 0 -4 -17 28.80 7.20 0 -4 -17 9.00 4.00 0 4 17 9.30 4.10 0 4 17 9.30 4.10 0 4 17 12.60 4.60 0 4 17 7.60 2.00 0 4 17 14.10 4.90 0 4 17 9.30 2.90 0 4 17 14.80 2.40 -1 -4 -17 6.20 4.30 -1 -4 -17 9.10 4.00 -1 -4 -17 10.30 4.00 1 4 17 11.50 4.30 1 4 17 6.10 1.80 1 4 17 11.60 4.20 1 4 17 13.70 4.70 1 4 17 6.00 2.00 1 4 17 10.70 4.40 1 4 17 11.90 3.20 -2 -4 -17 19.30 5.20 -2 -4 -17 27.90 5.50 -2 -4 -17 21.90 7.10 2 4 17 29.10 4.90 2 4 17 25.90 3.60 2 4 17 31.60 6.30 2 4 17 21.90 5.70 2 4 17 14.60 4.60 2 4 17 17.20 5.10 2 4 17 23.90 3.30 -3 -4 -17 21.10 5.30 -3 -4 -17 20.70 5.00 -3 -4 -17 31.80 7.50 3 4 17 24.40 5.90 3 4 17 21.10 5.60 3 4 17 30.30 3.90 3 4 17 27.50 4.20 3 4 17 26.10 4.70 3 4 17 24.00 5.80 3 4 17 23.20 5.50 -4 -4 -17 43.50 7.20 -4 -4 -17 43.00 9.20 -4 -4 -17 46.70 7.30 4 4 17 42.80 5.40 4 4 17 47.70 5.00 4 4 17 47.10 8.10 4 4 17 33.90 6.90 4 4 17 40.30 7.10 4 4 17 43.00 6.30 4 4 17 49.40 7.80 _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 65674 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp N1 N 0.61255(9) 0.70349(8) 0.20493(7) 0.0201(2) Uani 1 1 d . . N2 N 0.66447(9) 0.73178(9) 0.28028(7) 0.0217(2) Uani 1 1 d . . N3 N 0.61963(9) 0.82769(8) 0.31309(7) 0.0207(2) Uani 1 1 d . . P4 P 0.50791(3) 0.89086(2) 0.25056(2) 0.01893(7) Uani 1 1 d . . C5 C 0.52420(10) 0.78019(9) 0.17850(8) 0.0158(2) Uani 1 1 d . . C10 C 0.45841(10) 0.76294(9) 0.09360(8) 0.0149(2) Uani 1 1 d . . C11 C 0.43592(10) 0.63855(9) 0.09282(8) 0.0160(2) Uani 1 1 d . . H11A H 0.5156 0.5934 0.0887 0.019 Uiso 1 1 calc R U H11B H 0.3855 0.6127 0.1541 0.019 Uiso 1 1 calc R U C12 C 0.36960(11) 0.62179(9) 0.00609(8) 0.0185(2) Uani 1 1 d . . H12 H 0.3553 0.5410 0.0069 0.022 Uiso 1 1 calc R U C13 C 0.24595(11) 0.69106(10) 0.01305(9) 0.0204(2) Uani 1 1 d . . H13A H 0.1943 0.6666 0.0741 0.024 Uiso 1 1 calc R U H13B H 0.2021 0.6795 -0.0422 0.024 Uiso 1 1 calc R U C14 C 0.26740(10) 0.81514(10) 0.01112(8) 0.0194(2) Uani 1 1 d . . H14 H 0.1866 0.8602 0.0154 0.023 Uiso 1 1 calc R U C15 C 0.34708(11) 0.85278(10) -0.08365(9) 0.0225(2) Uani 1 1 d . . H15A H 0.3045 0.8427 -0.1399 0.027 Uiso 1 1 calc R U H15B H 0.3608 0.9330 -0.0852 0.027 Uiso 1 1 calc R U C16 C 0.47078(11) 0.78352(10) -0.09019(8) 0.0211(2) Uani 1 1 d . . H16 H 0.5228 0.8081 -0.1520 0.025 Uiso 1 1 calc R U C17 C 0.44877(11) 0.65975(10) -0.08888(8) 0.0220(2) Uani 1 1 d . . H17A H 0.5285 0.6147 -0.0941 0.026 Uiso 1 1 calc R U H17B H 0.4065 0.6485 -0.1450 0.026 Uiso 1 1 calc R U C18 C 0.33366(10) 0.83202(9) 0.09799(8) 0.0173(2) Uani 1 1 d . . H18A H 0.2816 0.8090 0.1593 0.021 Uiso 1 1 calc R U H18B H 0.3470 0.9121 0.0975 0.021 Uiso 1 1 calc R U C19 C 0.53670(10) 0.80053(10) -0.00325(8) 0.0183(2) Uani 1 1 d . . H19A H 0.5518 0.8804 -0.0046 0.022 Uiso 1 1 calc R U H19B H 0.6173 0.7568 -0.0079 0.022 Uiso 1 1 calc R U K1 K 0.92298(2) 0.26900(2) 0.39762(2) 0.01510(6) Uani 1 1 d . . N01 N 0.65108(9) 0.29475(8) 0.45945(7) 0.0179(2) Uani 1 1 d . . C21 C 0.60940(10) 0.18170(10) 0.48895(9) 0.0213(2) Uani 1 1 d . . H21A H 0.5184 0.1864 0.4975 0.026 Uiso 1 1 calc R U H21B H 0.6366 0.1548 0.5527 0.026 Uiso 1 1 calc R U C22 C 0.65600(10) 0.09736(10) 0.41804(9) 0.0217(2) Uani 1 1 d . . H22A H 0.6162 0.0266 0.4382 0.026 Uiso 1 1 calc R U H22B H 0.6352 0.1256 0.3525 0.026 Uiso 1 1 calc R U O23 O 0.78606(7) 0.07764(7) 0.41507(6) 0.01907(17) Uani 1 1 d . . C24 C 0.83321(11) 0.00410(10) 0.34281(9) 0.0241(3) Uani 1 1 d . . H24A H 0.8230 0.0413 0.2773 0.029 Uiso 1 1 calc R U H24B H 0.7873 -0.0641 0.3530 0.029 Uiso 1 1 calc R U C25 C 0.96638(11) -0.02657(10) 0.34984(10) 0.0252(3) Uani 1 1 d . . H25A H 0.9772 -0.0583 0.4168 0.030 Uiso 1 1 calc R U H25B H 0.9979 -0.0837 0.3049 0.030 Uiso 1 1 calc R U O26 O 1.03300(7) 0.07057(7) 0.32519(6) 0.02218(18) Uani 1 1 d . . C27 C 1.16191(11) 0.04470(10) 0.32331(10) 0.0267(3) Uani 1 1 d . . H27A H 1.1889 -0.0173 0.2824 0.032 Uiso 1 1 calc R U H27B H 1.1818 0.0211 0.3899 0.032 Uiso 1 1 calc R U C28 C 1.22753(11) 0.14760(10) 0.28213(10) 0.0257(3) Uani 1 1 d . . H28A H 1.3173 0.1292 0.2787 0.031 Uiso 1 1 calc R U H28B H 1.2084 0.1688 0.2150 0.031 Uiso 1 1 calc R U C31 C 0.62293(11) 0.36329(11) 0.54199(9) 0.0249(3) Uani 1 1 d . . H31A H 0.5380 0.3517 0.5731 0.030 Uiso 1 1 calc R U H31B H 0.6258 0.4430 0.5170 0.030 Uiso 1 1 calc R U C32 C 0.70918(12) 0.33784(12) 0.61804(9) 0.0271(3) Uani 1 1 d . . H32A H 0.6795 0.3805 0.6745 0.032 Uiso 1 1 calc R U H32B H 0.7115 0.2573 0.6408 0.032 Uiso 1 1 calc R U O33 O 0.82979(8) 0.36744(7) 0.57796(6) 0.02148(18) Uani 1 1 d . . C34 C 0.91193(12) 0.34730(10) 0.64978(8) 0.0234(3) Uani 1 1 d . . H34A H 0.9127 0.2680 0.6766 0.028 Uiso 1 1 calc R U H34B H 0.8838 0.3942 0.7037 0.028 Uiso 1 1 calc R U C35 C 1.03850(12) 0.37419(10) 0.60532(9) 0.0254(3) Uani 1 1 d . . H35A H 1.0373 0.4527 0.5762 0.030 Uiso 1 1 calc R U H35B H 1.0945 0.3652 0.6559 0.030 Uiso 1 1 calc R U O36 O 1.08118(8) 0.30101(7) 0.53230(6) 0.02283(18) Uani 1 1 d . . C37 C 1.21001(12) 0.30869(12) 0.50172(9) 0.0284(3) Uani 1 1 d . . H37A H 1.2561 0.2925 0.5585 0.034 Uiso 1 1 calc R U H37B H 1.2255 0.3852 0.4721 0.034 Uiso 1 1 calc R U C38 C 1.25259(11) 0.22588(11) 0.42879(9) 0.0269(3) Uani 1 1 d . . H38A H 1.3426 0.2284 0.4111 0.032 Uiso 1 1 calc R U H38B H 1.2369 0.1501 0.4601 0.032 Uiso 1 1 calc R U C41 C 0.58955(10) 0.34926(10) 0.37769(9) 0.0205(2) Uani 1 1 d . . H41A H 0.5065 0.3797 0.4032 0.025 Uiso 1 1 calc R U H41B H 0.5795 0.2925 0.3336 0.025 Uiso 1 1 calc R U C42 C 0.65850(11) 0.44231(10) 0.32026(9) 0.0203(2) Uani 1 1 d . . H42A H 0.6095 0.4807 0.2704 0.024 Uiso 1 1 calc R U H42B H 0.6740 0.4977 0.3639 0.024 Uiso 1 1 calc R U O43 O 0.77284(7) 0.39464(7) 0.27470(6) 0.01906(17) Uani 1 1 d . . C44 C 0.82944(11) 0.47224(9) 0.20146(8) 0.0184(2) Uani 1 1 d . . H44A H 0.8372 0.5432 0.2290 0.022 Uiso 1 1 calc R U H44B H 0.7784 0.4883 0.1477 0.022 Uiso 1 1 calc R U C45 C 0.95443(11) 0.42257(10) 0.16395(8) 0.0190(2) Uani 1 1 d . . H45A H 0.9471 0.3480 0.1428 0.023 Uiso 1 1 calc R U H45B H 0.9903 0.4707 0.1070 0.023 Uiso 1 1 calc R U O46 O 1.03326(7) 0.41268(7) 0.23846(6) 0.01799(17) Uani 1 1 d . . C47 C 1.15769(10) 0.38473(10) 0.19948(8) 0.0203(2) Uani 1 1 d . . H47A H 1.1925 0.4506 0.1604 0.024 Uiso 1 1 calc R U H47B H 1.1605 0.3241 0.1565 0.024 Uiso 1 1 calc R U C48 C 1.23252(10) 0.34719(10) 0.28194(9) 0.0209(2) Uani 1 1 d . . H48A H 1.3200 0.3356 0.2548 0.025 Uiso 1 1 calc R U H48B H 1.2259 0.4074 0.3257 0.025 Uiso 1 1 calc R U N02 N 1.19408(9) 0.24378(8) 0.33924(7) 0.0188(2) Uani 1 1 d . . O50 O 1.09834(10) 0.21093(8) 0.03593(7) 0.0345(2) Uani 1 1 d . . C51 C 1.13419(12) 0.09868(10) 0.01512(9) 0.0240(3) Uani 1 1 d . . H51A H 1.0699 0.0486 0.0450 0.029 Uiso 1 1 calc R U H51B H 1.2119 0.0726 0.0416 0.029 Uiso 1 1 calc R U C52 C 1.15158(12) 0.09790(11) -0.09511(9) 0.0248(3) Uani 1 1 d . . H52A H 1.1190 0.0309 -0.1147 0.030 Uiso 1 1 calc R U H52B H 1.2394 0.1002 -0.1219 0.030 Uiso 1 1 calc R U C53 C 1.07741(12) 0.20424(11) -0.12869(9) 0.0260(3) Uani 1 1 d . . H53A H 1.1097 0.2341 -0.1953 0.031 Uiso 1 1 calc R U H53B H 0.9893 0.1918 -0.1263 0.031 Uiso 1 1 calc R U C54 C 1.09804(12) 0.28043(10) -0.05377(9) 0.0272(3) Uani 1 1 d . . H54A H 1.1776 0.3146 -0.0719 0.033 Uiso 1 1 calc R U H54B H 1.0313 0.3407 -0.0483 0.033 Uiso 1 1 calc R U loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 N1 0.0203(5) 0.0193(5) 0.0220(5) -0.0026(4) -0.0085(4) 0.0002(4) N2 0.0215(5) 0.0237(5) 0.0216(5) -0.0020(4) -0.0080(4) -0.0030(4) N3 0.0196(5) 0.0238(5) 0.0195(5) -0.0023(4) -0.0021(4) -0.0067(4) P4 0.01970(15) 0.01813(15) 0.01980(15) -0.00576(11) -0.00252(11) -0.00119(11) C5 0.0152(5) 0.0154(5) 0.0166(5) -0.0009(4) -0.0010(4) -0.0021(4) C10 0.0155(5) 0.0139(5) 0.0152(5) -0.0013(4) -0.0024(4) -0.0002(4) C11 0.0188(5) 0.0147(5) 0.0146(5) -0.0014(4) -0.0029(4) -0.0004(4) C12 0.0233(6) 0.0160(5) 0.0174(5) -0.0037(4) -0.0046(4) -0.0020(4) C13 0.0196(6) 0.0237(6) 0.0191(6) -0.0020(5) -0.0058(4) -0.0037(5) C14 0.0168(5) 0.0208(6) 0.0204(6) -0.0009(4) -0.0051(4) 0.0025(4) C15 0.0254(6) 0.0230(6) 0.0184(6) 0.0032(5) -0.0065(5) 0.0009(5) C16 0.0226(6) 0.0252(6) 0.0138(5) 0.0019(4) 0.0000(4) -0.0008(5) C17 0.0255(6) 0.0257(6) 0.0148(5) -0.0044(5) -0.0036(5) 0.0017(5) C18 0.0166(5) 0.0162(5) 0.0187(5) -0.0019(4) -0.0022(4) 0.0012(4) C19 0.0160(5) 0.0190(6) 0.0191(6) 0.0003(4) -0.0009(4) -0.0013(4) K1 0.01532(11) 0.01470(12) 0.01592(12) -0.00172(9) -0.00365(8) -0.00192(8) N01 0.0181(5) 0.0193(5) 0.0161(5) -0.0025(4) -0.0020(4) -0.0001(4) C21 0.0145(5) 0.0250(6) 0.0234(6) 0.0018(5) -0.0007(4) -0.0031(4) C22 0.0165(5) 0.0205(6) 0.0293(6) -0.0004(5) -0.0059(5) -0.0057(4) O23 0.0165(4) 0.0194(4) 0.0227(4) -0.0063(3) -0.0032(3) -0.0031(3) C24 0.0268(6) 0.0191(6) 0.0285(6) -0.0101(5) -0.0026(5) -0.0056(5) C25 0.0260(6) 0.0138(5) 0.0354(7) -0.0055(5) 0.0010(5) -0.0026(5) O26 0.0181(4) 0.0143(4) 0.0329(5) -0.0025(3) 0.0008(3) -0.0002(3) C27 0.0198(6) 0.0192(6) 0.0387(7) -0.0020(5) 0.0020(5) 0.0029(5) C28 0.0183(6) 0.0219(6) 0.0341(7) -0.0022(5) 0.0053(5) 0.0008(5) C31 0.0219(6) 0.0297(7) 0.0225(6) -0.0090(5) 0.0019(5) 0.0016(5) C32 0.0310(7) 0.0343(7) 0.0161(6) -0.0068(5) 0.0016(5) -0.0053(5) O33 0.0269(4) 0.0233(4) 0.0154(4) -0.0020(3) -0.0059(3) -0.0029(3) C34 0.0377(7) 0.0191(6) 0.0149(5) -0.0040(4) -0.0096(5) 0.0011(5) C35 0.0382(7) 0.0208(6) 0.0213(6) -0.0040(5) -0.0154(5) -0.0050(5) O36 0.0227(4) 0.0267(4) 0.0218(4) -0.0045(3) -0.0080(3) -0.0067(3) C37 0.0236(6) 0.0405(8) 0.0242(6) 0.0038(5) -0.0126(5) -0.0133(5) C38 0.0153(6) 0.0350(7) 0.0294(7) 0.0072(5) -0.0075(5) -0.0018(5) C41 0.0161(5) 0.0219(6) 0.0239(6) -0.0023(5) -0.0051(4) 0.0014(4) C42 0.0192(6) 0.0189(6) 0.0227(6) -0.0028(5) -0.0044(5) 0.0030(4) O43 0.0191(4) 0.0163(4) 0.0205(4) 0.0015(3) -0.0020(3) 0.0012(3) C44 0.0231(6) 0.0163(5) 0.0164(5) 0.0000(4) -0.0061(4) -0.0006(4) C45 0.0227(6) 0.0204(6) 0.0148(5) -0.0011(4) -0.0058(4) -0.0012(4) O46 0.0170(4) 0.0220(4) 0.0156(4) -0.0020(3) -0.0042(3) -0.0012(3) C47 0.0185(6) 0.0220(6) 0.0195(6) 0.0004(5) 0.0003(4) -0.0032(4) C48 0.0155(5) 0.0222(6) 0.0247(6) 0.0010(5) -0.0022(4) -0.0047(4) N02 0.0160(5) 0.0192(5) 0.0208(5) 0.0012(4) -0.0028(4) -0.0019(4) O50 0.0575(7) 0.0217(5) 0.0221(5) -0.0035(4) -0.0023(4) 0.0074(4) C51 0.0284(6) 0.0181(6) 0.0254(6) -0.0017(5) -0.0036(5) -0.0014(5) C52 0.0248(6) 0.0234(6) 0.0247(6) -0.0038(5) 0.0020(5) 0.0004(5) C53 0.0218(6) 0.0315(7) 0.0229(6) 0.0003(5) -0.0005(5) 0.0014(5) C54 0.0292(7) 0.0213(6) 0.0287(7) 0.0017(5) -0.0014(5) 0.0038(5) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_publ_flag C5 N1 N2 112.22(10) y N3 N2 N1 114.80(9) y N2 N3 P4 112.38(8) y N3 P4 C5 89.56(5) y N1 C5 C10 119.19(10) y N1 C5 P4 111.04(8) y C10 C5 P4 129.74(8) y C5 C10 C18 110.83(9) ? C5 C10 C11 110.92(9) ? C18 C10 C11 108.75(9) ? C5 C10 C19 110.14(9) ? C18 C10 C19 108.02(9) ? C11 C10 C19 108.08(9) ? C12 C11 C10 110.53(9) ? C12 C11 H11A 109.5 ? C10 C11 H11A 109.5 ? C12 C11 H11B 109.5 ? C10 C11 H11B 109.5 ? H11A C11 H11B 108.1 ? C13 C12 C17 109.40(9) ? C13 C12 C11 109.40(9) ? C17 C12 C11 109.57(9) ? C13 C12 H12 109.5 ? C17 C12 H12 109.5 ? C11 C12 H12 109.5 ? C12 C13 C14 109.72(9) ? C12 C13 H13A 109.7 ? C14 C13 H13A 109.7 ? C12 C13 H13B 109.7 ? C14 C13 H13B 109.7 ? H13A C13 H13B 108.2 ? C15 C14 C13 109.59(10) ? C15 C14 C18 109.42(9) ? C13 C14 C18 109.10(9) ? C15 C14 H14 109.6 ? C13 C14 H14 109.6 ? C18 C14 H14 109.6 ? C16 C15 C14 109.49(9) ? C16 C15 H15A 109.8 ? C14 C15 H15A 109.8 ? C16 C15 H15B 109.8 ? C14 C15 H15B 109.8 ? H15A C15 H15B 108.2 ? C17 C16 C15 109.42(10) ? C17 C16 C19 109.57(9) ? C15 C16 C19 109.40(10) ? C17 C16 H16 109.5 ? C15 C16 H16 109.5 ? C19 C16 H16 109.5 ? C16 C17 C12 109.52(9) ? C16 C17 H17A 109.8 ? C12 C17 H17A 109.8 ? C16 C17 H17B 109.8 ? C12 C17 H17B 109.8 ? H17A C17 H17B 108.2 ? C14 C18 C10 110.75(9) ? C14 C18 H18A 109.5 ? C10 C18 H18A 109.5 ? C14 C18 H18B 109.5 ? C10 C18 H18B 109.5 ? H18A C18 H18B 108.1 ? C16 C19 C10 110.68(9) ? C16 C19 H19A 109.5 ? C10 C19 H19A 109.5 ? C16 C19 H19B 109.5 ? C10 C19 H19B 109.5 ? H19A C19 H19B 108.1 ? O43 K1 O36 139.41(3) ? O43 K1 O26 114.02(3) ? O36 K1 O26 100.84(3) ? O43 K1 O23 93.97(3) ? O36 K1 O23 122.12(3) ? O26 K1 O23 60.20(3) ? O43 K1 O46 60.89(2) ? O36 K1 O46 97.48(3) ? O26 K1 O46 94.71(3) ? O23 K1 O46 135.08(2) ? O43 K1 O33 98.85(3) ? O36 K1 O33 59.02(3) ? O26 K1 O33 142.48(3) ? O23 K1 O33 101.64(3) ? O46 K1 O33 117.71(3) ? O43 K1 N02 119.97(3) ? O36 K1 N02 60.87(3) ? O26 K1 N02 59.80(3) ? O23 K1 N02 118.87(3) ? O46 K1 N02 60.55(2) ? O33 K1 N02 118.83(3) ? O43 K1 N01 60.70(3) ? O36 K1 N01 118.25(3) ? O26 K1 N01 120.61(3) ? O23 K1 N01 61.38(3) ? O46 K1 N01 119.96(3) ? O33 K1 N01 60.34(2) ? N02 K1 N01 179.12(3) ? C41 N01 C31 108.88(9) ? C41 N01 C21 110.95(9) ? C31 N01 C21 109.60(9) ? C41 N01 K1 109.39(7) ? C31 N01 K1 110.82(7) ? C21 N01 K1 107.21(6) ? N01 C21 C22 114.35(10) ? N01 C21 H21A 108.7 ? C22 C21 H21A 108.7 ? N01 C21 H21B 108.7 ? C22 C21 H21B 108.7 ? H21A C21 H21B 107.6 ? O23 C22 C21 109.53(9) ? O23 C22 H22A 109.8 ? C21 C22 H22A 109.8 ? O23 C22 H22B 109.8 ? C21 C22 H22B 109.8 ? H22A C22 H22B 108.2 ? C22 O23 C24 110.33(9) ? C22 O23 K1 116.57(6) ? C24 O23 K1 111.44(6) ? O23 C24 C25 109.15(10) ? O23 C24 H24A 109.9 ? C25 C24 H24A 109.9 ? O23 C24 H24B 109.9 ? C25 C24 H24B 109.9 ? H24A C24 H24B 108.3 ? O26 C25 C24 109.17(10) ? O26 C25 H25A 109.8 ? C24 C25 H25A 109.8 ? O26 C25 H25B 109.8 ? C24 C25 H25B 109.8 ? H25A C25 H25B 108.3 ? C25 O26 C27 111.60(9) ? C25 O26 K1 116.69(7) ? C27 O26 K1 120.15(7) ? O26 C27 C28 108.60(10) ? O26 C27 H27A 110.0 ? C28 C27 H27A 110.0 ? O26 C27 H27B 110.0 ? C28 C27 H27B 110.0 ? H27A C27 H27B 108.4 ? N02 C28 C27 113.67(10) ? N02 C28 H28A 108.8 ? C27 C28 H28A 108.8 ? N02 C28 H28B 108.8 ? C27 C28 H28B 108.8 ? H28A C28 H28B 107.7 ? N01 C31 C32 114.11(10) ? N01 C31 H31A 108.7 ? C32 C31 H31A 108.7 ? N01 C31 H31B 108.7 ? C32 C31 H31B 108.7 ? H31A C31 H31B 107.6 ? O33 C32 C31 109.76(10) ? O33 C32 H32A 109.7 ? C31 C32 H32A 109.7 ? O33 C32 H32B 109.7 ? C31 C32 H32B 109.7 ? H32A C32 H32B 108.2 ? C34 O33 C32 110.59(9) ? C34 O33 K1 113.29(7) ? C32 O33 K1 113.85(6) ? O33 C34 C35 109.70(10) ? O33 C34 H34A 109.7 ? C35 C34 H34A 109.7 ? O33 C34 H34B 109.7 ? C35 C34 H34B 109.7 ? H34A C34 H34B 108.2 ? O36 C35 C34 109.17(9) ? O36 C35 H35A 109.8 ? C34 C35 H35A 109.8 ? O36 C35 H35B 109.8 ? C34 C35 H35B 109.8 ? H35A C35 H35B 108.3 ? C35 O36 C37 110.75(9) ? C35 O36 K1 118.26(7) ? C37 O36 K1 120.26(7) ? O36 C37 C38 109.01(10) ? O36 C37 H37A 109.9 ? C38 C37 H37A 109.9 ? O36 C37 H37B 109.9 ? C38 C37 H37B 109.9 ? H37A C37 H37B 108.3 ? N02 C38 C37 115.05(10) ? N02 C38 H38A 108.5 ? C37 C38 H38A 108.5 ? N02 C38 H38B 108.5 ? C37 C38 H38B 108.5 ? H38A C38 H38B 107.5 ? N01 C41 C42 113.42(9) ? N01 C41 H41A 108.9 ? C42 C41 H41A 108.9 ? N01 C41 H41B 108.9 ? C42 C41 H41B 108.9 ? H41A C41 H41B 107.7 ? O43 C42 C41 108.15(9) ? O43 C42 H42A 110.1 ? C41 C42 H42A 110.1 ? O43 C42 H42B 110.1 ? C41 C42 H42B 110.1 ? H42A C42 H42B 108.4 ? C44 O43 C42 111.10(8) ? C44 O43 K1 117.60(6) ? C42 O43 K1 116.23(6) ? O43 C44 C45 108.70(9) ? O43 C44 H44A 109.9 ? C45 C44 H44A 109.9 ? O43 C44 H44B 109.9 ? C45 C44 H44B 109.9 ? H44A C44 H44B 108.3 ? O46 C45 C44 110.00(9) ? O46 C45 H45A 109.7 ? C44 C45 H45A 109.7 ? O46 C45 H45B 109.7 ? C44 C45 H45B 109.7 ? H45A C45 H45B 108.2 ? C47 O46 C45 110.68(8) ? C47 O46 K1 118.12(6) ? C45 O46 K1 107.22(6) ? O46 C47 C48 109.32(9) ? O46 C47 H47A 109.8 ? C48 C47 H47A 109.8 ? O46 C47 H47B 109.8 ? C48 C47 H47B 109.8 ? H47A C47 H47B 108.3 ? N02 C48 C47 113.79(9) ? N02 C48 H48A 108.8 ? C47 C48 H48A 108.8 ? N02 C48 H48B 108.8 ? C47 C48 H48B 108.8 ? H48A C48 H48B 107.7 ? C38 N02 C28 109.49(10) ? C38 N02 C48 110.28(9) ? C28 N02 C48 110.36(9) ? C38 N02 K1 107.37(7) ? C28 N02 K1 110.82(7) ? C48 N02 K1 108.47(7) ? C51 O50 C54 108.82(9) ? O50 C51 C52 107.22(10) ? O50 C51 H51A 110.3 ? C52 C51 H51A 110.3 ? O50 C51 H51B 110.3 ? C52 C51 H51B 110.3 ? H51A C51 H51B 108.5 ? C51 C52 C53 102.95(10) ? C51 C52 H52A 111.2 ? C53 C52 H52A 111.2 ? C51 C52 H52B 111.2 ? C53 C52 H52B 111.2 ? H52A C52 H52B 109.1 ? C54 C53 C52 100.84(10) ? C54 C53 H53A 111.6 ? C52 C53 H53A 111.6 ? C54 C53 H53B 111.6 ? C52 C53 H53B 111.6 ? H53A C53 H53B 109.4 ? O50 C54 C53 105.74(10) ? O50 C54 H54A 110.6 ? C53 C54 H54A 110.6 ? O50 C54 H54B 110.6 ? C53 C54 H54B 110.6 ? H54A C54 H54B 108.7 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_publ_flag N1 C5 1.3449(15) y N1 N2 1.3488(14) y N2 N3 1.3219(15) y N3 P4 1.6856(11) y P4 C5 1.7387(11) y C5 C10 1.5096(15) y C10 C18 1.5415(15) ? C10 C11 1.5442(15) ? C10 C19 1.5478(15) ? C11 C12 1.5336(15) ? C11 H11A 0.9900 ? C11 H11B 0.9900 ? C12 C13 1.5320(16) ? C12 C17 1.5334(16) ? C12 H12 1.0000 ? C13 C14 1.5333(16) ? C13 H13A 0.9900 ? C13 H13B 0.9900 ? C14 C15 1.5330(16) ? C14 C18 1.5354(16) ? C14 H14 1.0000 ? C15 C16 1.5324(17) ? C15 H15A 0.9900 ? C15 H15B 0.9900 ? C16 C17 1.5320(17) ? C16 C19 1.5343(16) ? C16 H16 1.0000 ? C17 H17A 0.9900 ? C17 H17B 0.9900 ? C18 H18A 0.9900 ? C18 H18B 0.9900 ? C19 H19A 0.9900 ? C19 H19B 0.9900 ? K1 O43 2.7842(9) ? K1 O36 2.8035(9) ? K1 O26 2.8131(9) ? K1 O23 2.8366(9) ? K1 O46 2.8680(9) ? K1 O33 2.9191(9) ? K1 N02 2.9828(11) ? K1 N01 2.9991(11) ? N01 C41 1.4712(15) ? N01 C31 1.4724(15) ? N01 C21 1.4764(15) ? C21 C22 1.5052(17) ? C21 H21A 0.9900 ? C21 H21B 0.9900 ? C22 O23 1.4264(14) ? C22 H22A 0.9900 ? C22 H22B 0.9900 ? O23 C24 1.4295(14) ? C24 C25 1.4940(18) ? C24 H24A 0.9900 ? C24 H24B 0.9900 ? C25 O26 1.4229(14) ? C25 H25A 0.9900 ? C25 H25B 0.9900 ? O26 C27 1.4235(14) ? C27 C28 1.5116(17) ? C27 H27A 0.9900 ? C27 H27B 0.9900 ? C28 N02 1.4706(16) ? C28 H28A 0.9900 ? C28 H28B 0.9900 ? C31 C32 1.5075(18) ? C31 H31A 0.9900 ? C31 H31B 0.9900 ? C32 O33 1.4284(15) ? C32 H32A 0.9900 ? C32 H32B 0.9900 ? O33 C34 1.4263(14) ? C34 C35 1.4940(19) ? C34 H34A 0.9900 ? C34 H34B 0.9900 ? C35 O36 1.4245(15) ? C35 H35A 0.9900 ? C35 H35B 0.9900 ? O36 C37 1.4323(15) ? C37 C38 1.504(2) ? C37 H37A 0.9900 ? C37 H37B 0.9900 ? C38 N02 1.4686(15) ? C38 H38A 0.9900 ? C38 H38B 0.9900 ? C41 C42 1.5069(17) ? C41 H41A 0.9900 ? C41 H41B 0.9900 ? C42 O43 1.4339(14) ? C42 H42A 0.9900 ? C42 H42B 0.9900 ? O43 C44 1.4262(14) ? C44 C45 1.5022(16) ? C44 H44A 0.9900 ? C44 H44B 0.9900 ? C45 O46 1.4302(13) ? C45 H45A 0.9900 ? C45 H45B 0.9900 ? O46 C47 1.4294(14) ? C47 C48 1.5123(16) ? C47 H47A 0.9900 ? C47 H47B 0.9900 ? C48 N02 1.4709(15) ? C48 H48A 0.9900 ? C48 H48B 0.9900 ? O50 C51 1.4275(15) ? O50 C54 1.4307(16) ? C51 C52 1.5244(17) ? C51 H51A 0.9900 ? C51 H51B 0.9900 ? C52 C53 1.5264(17) ? C52 H52A 0.9900 ? C52 H52B 0.9900 ? C53 C54 1.5144(19) ? C53 H53A 0.9900 ? C53 H53B 0.9900 ? C54 H54A 0.9900 ? C54 H54B 0.9900 ?