Crystallography Open Database

Information card for entry 4302820

Preview

Coordinates	4302820.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H28 N16 Ni2 O4
Calculated formula	C28 H28 N16 Ni2 O4
Title of publication	Two EE-Azido-Bridged Nickel(II) Layered Compounds: Vigorous Twisted Torsion Angle Ni-N3-Ni Results in Ferromagnetic Behavior
Authors of publication	Ru-Yin Li; Bing-Wu Wang; Xin-Yi Wang; Xiu-Teng Wang; Zhe-Ming Wang; Song Gao
Journal of publication	Inorganic Chemistry
Year of publication	2009
Journal volume	48
Pages of publication	7174 - 7180
a	11.8326 ± 0.0004 Å
b	8.2663 ± 0.0003 Å
c	8.0851 ± 0.0007 Å
α	90°
β	91.93 ± 0.002°
γ	90°
Cell volume	790.37 ± 0.08 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1044
Residual factor for significantly intense reflections	0.0355
Weighted residual factors for significantly intense reflections	0.0622
Weighted residual factors for all reflections included in the refinement	0.0729
Goodness-of-fit parameter for all reflections included in the refinement	0.917
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179066 (current)	2016-03-22	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/28.	4302820.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4302820.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4302820.cif
1125	2010-04-25	cif/4/ Adding CIFs for the Inorg-Chem-2009_11-24 deposition.	4302820.cif