Crystallography Open Database

Information card for entry 4302977

Preview

Coordinates	4302977.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C65 H89 N4 Ni P4 Si
Calculated formula	C65 H89 N4 Ni P4 Si
Title of publication	Side-on Coordination of a P-P Bond in Heterobinuclear Tetraphosphorus Complexes with a [Si(μ,η2:2-P4)Ni] Core and Nickel(I) Centers
Authors of publication	Yun Xiong; Shenglai Yao; Eckhard Bill; Matthias Driess
Journal of publication	Inorganic Chemistry
Year of publication	2009
Journal volume	48
Pages of publication	7522 - 7524
a	21.8775 ± 0.0014 Å
b	12.1597 ± 0.0006 Å
c	24.278 ± 0.0014 Å
α	90°
β	106.187 ± 0.006°
γ	90°
Cell volume	6202.5 ± 0.6 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1308
Residual factor for significantly intense reflections	0.0565
Weighted residual factors for significantly intense reflections	0.1239
Weighted residual factors for all reflections included in the refinement	0.1397
Goodness-of-fit parameter for all reflections included in the refinement	0.919
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179067 (current)	2016-03-22	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/29.	4302977.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4302977.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4302977.cif
1125	2010-04-25	cif/4/ Adding CIFs for the Inorg-Chem-2009_11-24 deposition.	4302977.cif