Crystallography Open Database

Information card for entry 4310004

Preview

Coordinates	4310004.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C159.25 H162 Cl6.5 N3 O25.25 P6 Rh6
Calculated formula	C159.25 H126.5 Cl6.5 N3 O25.25 P6 Rh6
Title of publication	Chiral Organometallic Triangles with Rh-Rh Bonds. 2. Compounds Prepared from Enantiopure cis-Rh2(C6H4PPh2)2(OAc)2(HOAc)2 and Their Catalytic Potentials
Authors of publication	F. Albert Cotton; Carlos A. Murillo; Salah E. Stiriba; Xiaoping Wang; Rongmin Yu
Journal of publication	Inorganic Chemistry
Year of publication	2005
Journal volume	44
Pages of publication	8223 - 8233
a	21.651 ± 0.004 Å
b	21.922 ± 0.004 Å
c	22.055 ± 0.004 Å
α	82.113 ± 0.003°
β	61.153 ± 0.003°
γ	64.889 ± 0.003°
Cell volume	8272 ± 3 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	7
Space group number	1
Hermann-Mauguin space group symbol	P 1
Hall space group symbol	P 1
Residual factor for all reflections	0.1633
Residual factor for significantly intense reflections	0.0873
Weighted residual factors for significantly intense reflections	0.2195
Weighted residual factors for all reflections included in the refinement	0.2786
Goodness-of-fit parameter for all reflections included in the refinement	1.013
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4310004.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4310004.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4310004.cif
1526	2010-09-26	cif/4/ Adding new CIFs from Inorg. Chem. 2005 deposited via Web deposition site to the COD test database (and transferede to the main COD database after renaming).	4310004.cif