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Information card for entry 4311645
Preview
| Coordinates | 4311645.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | B4 Ge H4 K2 O11 |
|---|---|
| Calculated formula | B4 Ge K2 O11 |
| Title of publication | K2[Ge(B4O9)].2H2O: A Unique 3D Alternating Linkage Mode of a B4O9 Cluster and GeO4 Unit in Borogermanate with Two Pairs of Interweaving Double Helical Channels |
| Authors of publication | Hong-Xia Zhang; Jie Zhang; Shou-Tian Zheng; Guo-Ming Wang; Guo-Yu Yang |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 2004 |
| Journal volume | 43 |
| Pages of publication | 6148 - 6150 |
| a | 6.7934 ± 0.0015 Å |
| b | 12.069 ± 0.003 Å |
| c | 11.895 ± 0.003 Å |
| α | 90° |
| β | 91.156 ± 0.004° |
| γ | 90° |
| Cell volume | 975.1 ± 0.4 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 9 |
| Hermann-Mauguin space group symbol | C 1 c 1 |
| Hall space group symbol | C -2yc |
| Residual factor for all reflections | 0.0527 |
| Residual factor for significantly intense reflections | 0.0448 |
| Weighted residual factors for significantly intense reflections | 0.1023 |
| Weighted residual factors for all reflections included in the refinement | 0.1093 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.064 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 176467 (current) | 2016-02-16 | cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4. |
4311645.cif |
| 120093 | 2014-07-12 | Adding DOIs to range 4/31 structures. | 4311645.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4311645.cif |
| 31986 | 2012-01-04 | cif/ Changing more tags to match the dictionary specifications: -_diffrn_standards_interval_count none -_diffrn_standards_interval_time none -_diffrn_standards_number none +_diffrn_standards_interval_count 0 +_diffrn_standards_interval_time . +_diffrn_standards_number 0 |
4311645.cif |
| 31985 | 2012-01-04 | cif/ Canging data item '_diffrn_standards_decay_% none' to '_diffrn_standards_decay_% 0'. |
4311645.cif |
| 3144 | 2010-11-13 | ../uploads/cif-deposit/cod/cif Adding structures of 4311645 via cif-deposit CGI script. |
4311645.cif |
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