#------------------------------------------------------------------------------ #$Date: 2012-02-04 18:30:22 +0200 (Sat, 04 Feb 2012) $ #$Revision: 32116 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/4/4311660.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4311660 loop_ _publ_author_name 'Boris M. Bulychev' 'Roman V. Shpanchenko' 'Evgeny V. Antipov' 'Denis V. Sheptyakov' 'Svetlana N. Bushmeleva' 'Anatoly M. Balagurov' _publ_contact_author_address 'Department of Chemistry, Moscow State University, 119992 Moscow, Russia' _publ_contact_author_email shpanchenko@icr.chem.msu.ru _publ_contact_author_fax 7-(095)-9394788 _publ_contact_author_name 'Roman V. Shpanchenko' _publ_contact_author_phone 7-(095)-9393490 _publ_section_title ; Synthesis and Crystal Structure of Lithium Beryllium Deuteride Li2BeD4 ; _journal_name_full 'Inorganic Chemistry' _journal_page_first 6371 _journal_page_last 6376 _journal_volume 43 _journal_year 2004 _chemical_formula_moiety 'D4 Be 2(Li)' _chemical_formula_structural 'Li2 [Be D4]' _chemical_formula_sum 'Be D4 Li2' _chemical_formula_weight 30.95 _chemical_name_systematic 'Lithium Beryllium Deuteride' _space_group_IT_number 14 _symmetry_cell_setting monoclinic _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _audit_author_name Li2BeH4 _audit_creation_date 2004-05-29T17:52 _audit_creation_method 'from EXP file using GSAS2CIF' _audit_update_record ' 2004-05-29T17:52 Initial CIF as created by GSAS2CIF' _cell_angle_alpha 90.0 _cell_angle_beta 93.5772(13) _cell_angle_gamma 90.0 _cell_formula_units_Z 8 _cell_length_a 7.06228(9) _cell_length_b 8.33780(10) _cell_length_c 8.34652(10) _cell_measurement_temperature 293 _cell_volume 490.518(10) _computing_structure_refinement GSAS _pd_block_id 2004-05-29T19:48|FINAL_phase1|Li2BeH4|| _pd_char_colour White _pd_phase_name Li2BeD4 _pd_proc_ls_prof_R_factor 0.0624 _pd_proc_ls_prof_wR_factor 0.0514 _[local]_cod_data_source_file ic049267fsi20040605_090318.hkl loop_ _[local]_cod_data_source_block FINAL_p_01 FINAL_p_03 _[local]_cod_cif_authors_sg_Hall -P2ybc _cod_original_cell_volume 490.52(1) _cod_database_code 4311660 loop_ _symmetry_equiv_pos_site_id _symmetry_equiv_pos_as_xyz 1 +x,+y,+z 2 -x,+y+1/2,-z+1/2 -1 -x,-y,-z -2 +x,-y+1/2,+z+1/2 data_FINAL_p_01 _pd_block_id 2004-05-29T19:48|FINAL_H_01|Li2BeH4|HRFD #============================================================================== # 9. INSTRUMENT CHARACTERIZATION _exptl_special_details ; ? ; # if regions of the data are excluded, the reason(s) are supplied here: _pd_proc_info_excluded_regions ; ? ; # The following item is used to identify the equipment used to record # the powder pattern when the diffractogram was measured at a laboratory # other than the authors' home institution, e.g. when neutron or synchrotron # radiation is used. _pd_instr_location "High Resolution Fourier Diffractometer, JINR, 141980 Dubna, Russia" _pd_calibration_special_details # description of the method used # to calibrate the instrument ; Vanadium incoherent scattering pattern has been used for the incident TOF spectrum calibration; Al2O3 standard sample was used for the calibration of the instrumental parameters like: flight path, scattering angle, pulse delay time, etc. ; _diffrn_ambient_temperature 293 _diffrn_source neutron _diffrn_source_target ? _diffrn_source_type 'pulsed nuclear reactor' _diffrn_measurement_device_type 'HRFD' _diffrn_detector 'multy-detector in a time-focusing geometry' _diffrn_detector_type ? # make or model of detector _pd_meas_scan_method TOF # options are 'step', 'cont', # 'tof', 'fixed' or # 'disp' (= dispersive) _pd_spec_mounting 'Vanadium container' # This field should be # used to give details of the # container. _pd_spec_mount_mode transmission # options are 'reflection' # or 'transmission' _pd_spec_shape cylinder # options are 'cylinder' # 'flat_sheet' or 'irregular' # phase table loop_ _pd_phase_id _pd_phase_block_id _pd_phase_mass_% _pd_proc_ls_profile_function _pd_proc_ls_peak_cutoff 1 2004-05-29T19:48|FINAL_phase1|Li2BeH4|| ? ; TOF Profile function number 1 with 12 terms Profile coefficients for Von Dreele, Jorgensen & Windsor convolution function J. Appl. Cryst., 15,581-589(1982) Modified by Von Dreele - unpublished (1983). #1(alp-0) = 0.1013 #3(bet-0) = 3.0867E-01 #5(sig-0) = 41.789 #2(alp-1) = 0.0030 #4(bet-1) = 2.8312E+00 #6(sig-1) = 10.000 #8(rstr ) = 0.000 #9(rsta ) = 0.000 #7(sig-2) = 4.847 #10(rsca) = 0.000 #11(s1ec) = 0.00 #12(s2ec) = 0.00 Peak tails are ignored where the intensity is below 0.0002 times the peak Aniso. broadening axis 0.0 0.0 1.0 ; 0.00020 loop_ _atom_type_symbol _atom_type_scat_length_neutron _atom_type_scat_source LI -0.1900 International_Tables_Vol_C BE 0.7790 International_Tables_Vol_C D 0.6671 International_Tables_Vol_C _diffrn_radiation_probe neutron _pd_proc_ls_prof_R_factor 0.0629 _pd_proc_ls_prof_wR_factor 0.0471 _pd_proc_ls_prof_wR_expected 0.0280 _refine_ls_R_Fsqd_factor 0.72689 _pd_proc_ls_background_function ; GSAS Background function number 1 with 10 terms. Shifted Chebyshev function of 1st kind 1: 1256.21 2: -273.832 3: -9.19689 4: 16.5265 5: -12.7139 6: 27.6245 7: 4.48164 8: -4.63152 9: 3.28928 10: -3.35016 ; _exptl_absorpt_process_details ; GSAS Absorption/surface roughness correction: function number 0 Debye-Scherrer absorption correction Term (= MU.r/wave) = 0.50000 Correction is not refined. ; _exptl_absorpt_correction_T_min 0.08961 _exptl_absorpt_correction_T_max 0.39557 # Extinction correction _gsas_exptl_extinct_corr_T_min 1.00000 _gsas_exptl_extinct_corr_T_max 1.00000 _pd_proc_info_datetime 2004-05-29T19:48:32 _pd_calc_method "Rietveld Refinement" _pd_meas_2theta_fixed 152.00 #---- raw/calc data loop ----- loop_ _pd_meas_time_of_flight _pd_proc_d_spacing _pd_meas_intensity_total _pd_proc_ls_weight _pd_proc_intensity_bkg_calc _pd_calc_intensity_total # ; ? ? ? ? ? ? _pd_meas_number_of_points 8189 _pd_proc_number_of_points 8189 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_observed_status _refln_F_squared_meas _refln_F_squared_calc _refln_phase_calc _refln_d_spacing _gsas_i100_meas 1 1 -2 o 16.332 13.205 180.00 3.37282 48.30 1 2 -1 o 27.321 35.502 180.00 3.33421 78.07 1 2 1 o 15.281 22.275 0.00 3.25812 40.77 2 1 0 o 3.773 7.529 0.00 3.24618 9.96 1 1 2 o 2.496 1.813 0.00 3.22068 6.43 2 1 -1 o 8.593 6.057 0.00 3.08522 19.75 2 0 -2 o 0.000 1.157 180.00 2.77720 0.00 1 2 -2 o 11.921 7.756 180.00 2.76227 19.63 2 2 0 o 12.011 10.467 180.00 2.69141 18.29 1 2 2 o 11.635 7.141 0.00 2.67682 17.43 0 3 1 o 45.811 40.777 180.00 2.63639 65.55 2 1 -2 o 41.186 38.544 0.00 2.63488 58.83 0 1 3 o 70.033 62.417 0.00 2.63450 100.00 2 0 2 o 31.150 10.202 180.00 2.61126 21.65 2 2 -1 o 11.643 13.426 180.00 2.59752 15.93 1 3 0 o 3.796 6.135 180.00 2.58552 5.12 2 2 1 o 1.214 0.441 180.00 2.52608 1.53 1 1 -3 o 16.964 12.395 0.00 2.51711 21.12 2 1 2 o 26.140 30.923 180.00 2.49191 31.58 1 3 -1 o 25.307 22.064 0.00 2.48547 30.33 1 3 1 o 0.000 0.049 0.00 2.45347 0.00 1 1 3 o 0.000 0.700 0.00 2.42120 0.00 3 0 0 o 16.218 16.837 0.00 2.34951 8.21 0 3 2 o 20.938 15.720 0.00 2.31184 20.19 2 2 -2 o 0.622 0.501 180.00 2.31129 0.60 0 2 3 o 57.481 47.173 0.00 2.31104 55.37 3 1 0 o 0.000 5.589 0.00 2.26143 0.00 1 2 -3 o 13.210 5.057 0.00 2.23057 11.44 1 3 -2 o 116.592 104.137 180.00 2.21958 99.47 3 1 -1 o 0.400 0.413 0.00 2.21636 0.34 2 2 2 o 16.341 12.536 180.00 2.21298 13.82 2 3 0 o 35.046 43.227 0.00 2.18231 28.42 1 3 2 o 1.826 1.637 0.00 2.17451 1.46 2 1 -3 o 3.285 2.319 180.00 2.17267 2.63 1 2 3 o 5.407 8.201 180.00 2.16301 4.27 3 1 1 o 55.400 53.763 0.00 2.15004 42.95 2 3 -1 o 0.000 0.760 0.00 2.13135 0.00 3 0 -2 o 97.698 71.061 0.00 2.10331 35.46 2 3 1 o 7.051 4.730 0.00 2.09135 5.03 0 4 0 o 4.606 6.268 180.00 2.08444 1.63 0 0 4 o 6.149 8.099 180.00 2.08257 2.17 2 1 3 o 0.000 4.109 180.00 2.05263 0.00 3 2 0 o 0.000 1.429 180.00 2.04682 0.00 3 1 -2 o 10.624 17.318 180.00 2.03942 7.03 1 0 -4 o 2.347 7.232 180.00 2.03196 0.77 0 4 1 o 0.000 1.056 0.00 2.02210 0.00 0 1 4 o 1.066 0.577 180.00 2.02049 0.69 3 2 -1 o 41.809 21.365 180.00 2.01322 26.60 1 4 0 o 8.833 9.800 0.00 1.99887 5.50 3 0 2 o 10.497 17.498 180.00 1.99384 3.24 2 2 -3 o 0.840 2.077 0.00 1.98031 0.51 1 1 -4 o 3.192 0.359 180.00 1.97418 1.91 2 3 -2 o 4.410 3.991 180.00 1.96450 2.61 0 3 3 o 0.460 0.422 0.00 1.96434 0.27 1 0 4 o 77.484 71.705 180.00 1.96419 22.89 3 2 1 o 55.622 52.442 0.00 1.96313 32.81 1 4 -1 o 12.597 3.968 180.00 1.95154 7.30 3 1 2 o 1.954 0.169 0.00 1.93916 1.11 1 4 1 o 3.518 1.692 180.00 1.93594 1.99 1 3 -3 o 16.126 12.619 0.00 1.91421 8.82 1 1 4 o 0.392 0.731 0.00 1.91185 0.21 2 3 2 o 6.011 10.082 0.00 1.90306 3.23 2 2 3 o 16.385 19.729 0.00 1.88814 8.60 3 2 -2 o 1.718 0.270 0.00 1.87784 0.89 1 3 3 o 6.797 4.081 0.00 1.87100 3.47 0 4 2 o 0.117 0.062 0.00 1.86404 0.06 0 2 4 o 4.851 4.759 180.00 1.86304 2.44 2 0 -4 o 31.289 40.123 180.00 1.84403 7.64 1 2 -4 o 0.802 0.572 0.00 1.82655 0.38 1 4 -2 o 5.175 7.116 180.00 1.81466 2.41 3 1 -3 o 0.000 0.100 0.00 1.80744 0.00 2 1 -4 o 0.125 0.580 0.00 1.80052 0.06 3 2 2 o 4.227 5.770 180.00 1.79870 1.92 3 3 0 o 16.551 12.434 0.00 1.79427 7.45 2 4 0 o 16.636 12.493 180.00 1.79412 7.49 1 4 2 o 0.000 0.277 0.00 1.78978 0.00 1 2 4 o 0.000 6.329 0.00 1.77685 0.00 3 3 -1 o 0.000 0.027 0.00 1.77150 0.00 2 4 -1 o 2.616 4.605 180.00 1.76548 1.12 4 0 0 o 33.263 54.661 0.00 1.76213 7.09 2 3 -3 o 0.461 0.335 0.00 1.74896 0.19 2 0 4 o 0.208 0.914 180.00 1.74585 0.04 2 4 1 o 8.035 9.428 0.00 1.74255 3.31 3 3 1 o 5.359 0.182 0.00 1.73709 2.19 4 1 0 o 18.349 8.923 0.00 1.72405 7.32 4 1 -1 o 6.551 5.270 0.00 1.70910 2.55 2 1 4 o 18.737 18.391 180.00 1.70879 7.28 3 1 3 o 9.480 4.541 0.00 1.70409 3.65 3 2 -3 o 4.327 0.126 180.00 1.69210 1.63 2 2 -4 o 22.331 20.754 0.00 1.68641 8.34 2 3 3 o 1.078 1.123 180.00 1.68449 0.40 3 3 -2 o 12.850 10.796 180.00 1.67717 4.72 4 1 1 o 7.725 6.671 180.00 1.66818 2.79 2 4 -2 o 6.573 5.920 0.00 1.66711 2.37 0 4 3 o 0.368 0.332 180.00 1.66701 0.13 0 3 4 o 10.327 9.357 0.00 1.66659 3.72 4 0 -2 o 0.000 3.339 180.00 1.66047 0.00 1 3 -4 o 0.000 0.707 180.00 1.64032 0.00 1 4 -3 o 21.474 18.846 0.00 1.63604 7.32 0 5 1 o 1.465 1.421 0.00 1.63511 0.50 0 1 5 o 0.106 0.146 180.00 1.63376 0.04 2 4 2 o 19.786 23.759 0.00 1.62906 6.65 4 1 -2 o 25.485 28.457 0.00 1.62849 8.56 4 2 0 o 1.293 1.033 180.00 1.62309 0.43 1 5 0 o 5.398 4.230 0.00 1.62276 1.79 3 3 2 o 11.314 12.159 180.00 1.62006 3.74 1 1 -5 o 45.950 56.571 180.00 1.61342 15.01 4 2 -1 o 16.782 18.139 180.00 1.61060 5.45 2 2 4 o 2.545 2.669 0.00 1.61034 0.83 3 0 -4 o 21.834 20.577 0.00 1.60910 3.54 1 4 3 o 9.076 8.432 180.00 1.60882 2.94 3 2 3 o 5.666 4.488 0.00 1.60641 1.83 1 3 4 o 7.269 3.985 180.00 1.60404 2.33 1 5 -1 o 19.235 11.713 180.00 1.59713 6.09 1 5 1 o 61.728 56.873 180.00 1.58854 19.24 4 0 2 o 11.016 10.650 180.00 1.58771 1.71 3 1 -4 o 14.384 11.764 180.00 1.57994 4.41 4 2 1 o 0.650 0.100 180.00 1.57622 0.20 1 1 5 o 24.827 22.926 180.00 1.57056 7.48 4 1 2 o 13.843 16.416 180.00 1.55968 4.08 3 4 0 o 3.594 4.392 180.00 1.55925 1.06 0 5 2 o 0.000 1.308 0.00 1.54809 0.00 0 2 5 o 0.074 0.431 0.00 1.54708 0.02 3 4 -1 o 3.900 6.755 180.00 1.54424 1.12 4 2 -2 o 0.274 0.375 0.00 1.54261 0.08 3 3 -3 o 23.673 23.937 180.00 1.54086 6.73 2 3 -4 o 7.726 11.346 180.00 1.53657 2.18 1 2 -5 o 1.682 1.697 180.00 1.52978 0.47 2 4 -3 o 11.308 10.474 0.00 1.52924 3.14 3 4 1 o 0.502 0.540 180.00 1.52128 0.14 1 5 -2 o 6.477 4.988 0.00 1.51945 1.76 2 1 -5 o 6.206 3.370 180.00 1.51810 1.69 3 0 4 o 7.229 11.620 180.00 1.51233 0.97 2 5 0 o 2.296 3.853 0.00 1.50733 0.61 4 1 -3 o 4.806 6.312 180.00 1.50648 1.28 1 5 2 o 0.390 0.418 180.00 1.50476 0.10 3 2 -4 o 1.166 0.251 180.00 1.50116 0.31 1 2 5 o 1.747 8.107 180.00 1.49310 0.45 2 5 -1 o 0.000 0.001 180.00 1.49023 0.00 4 3 0 o 4.588 7.627 0.00 1.48821 1.17 3 1 4 o 19.843 31.847 0.00 1.48805 5.08 2 4 3 o 6.101 7.934 0.00 1.48558 1.55 4 2 2 o 4.182 10.852 180.00 1.48375 1.06 3 4 -2 o 1.658 2.628 180.00 1.48055 0.42 4 3 -1 o 5.241 5.624 180.00 1.47857 1.31 2 3 4 o 21.349 22.388 0.00 1.47837 5.35 2 5 1 o 26.501 22.612 0.00 1.47636 6.62 3 3 3 o 12.105 9.115 180.00 1.47532 3.02 0 4 4 o 9.738 6.723 180.00 1.47326 2.42 1 4 -4 o 0.505 2.113 0.00 1.45501 0.12 4 3 1 o 12.433 15.802 0.00 1.45183 2.95 2 1 5 o 4.985 6.927 180.00 1.44880 1.18 2 2 -5 o 20.817 20.750 0.00 1.44781 4.90 3 4 2 o 10.327 7.646 180.00 1.44082 2.39 4 2 -3 o 8.138 9.394 0.00 1.43772 1.88 1 3 -5 o 0.064 0.008 180.00 1.41530 0.01 1 5 -3 o 0.949 1.472 0.00 1.40990 0.21 5 0 0 o 1.799 3.279 0.00 1.40970 0.20 2 5 2 o 20.650 17.249 180.00 1.40542 4.44 3 3 -4 o 0.682 0.669 0.00 1.39254 0.14 1 5 3 o 1.329 1.343 180.00 1.39236 0.28 5 1 0 o 0.003 0.002 0.00 1.38998 0.00 0 6 0 o 0.413 0.361 180.00 1.38963 0.04 4 0 -4 o 111.999 102.427 180.00 1.38860 11.61 0 0 6 o 15.051 13.718 0.00 1.38838 1.56 2 2 5 o 15.388 13.581 180.00 1.38732 3.18 1 3 5 o 8.894 8.118 0.00 1.38611 1.83 5 1 -1 o 1.679 1.686 180.00 1.38492 0.35 3 4 -3 o 48.492 51.261 0.00 1.38425 9.96 3 1 -5 o 0.296 0.334 180.00 1.38155 0.06 2 4 -4 o 8.115 8.649 0.00 1.38114 1.65 4 3 2 o 4.858 4.270 180.00 1.37861 0.99 1 0 -6 o 31.060 27.300 0.00 1.37861 3.15 0 6 1 o 2.371 0.255 0.00 1.37069 0.47 4 1 -4 o 0.417 0.059 180.00 1.36973 0.08 0 1 6 o 5.979 0.859 180.00 1.36952 1.19 4 2 3 o 0.023 0.002 180.00 1.36744 0.00 1 6 0 o 41.632 35.814 180.00 1.36338 8.16 5 0 -2 o 1.148 1.067 180.00 1.36134 0.11 1 1 -6 o 0.424 0.427 180.00 1.36014 0.08 3 5 0 o 10.131 10.388 0.00 1.35986 1.97 5 1 1 o 11.608 12.925 180.00 1.35753 2.25 3 5 -1 o 33.037 23.197 180.00 1.34986 6.28 2 3 -5 o 4.999 3.497 180.00 1.34964 0.95 1 6 -1 o 0.015 0.010 180.00 1.34808 0.00 1 0 6 o 52.468 43.539 0.00 1.34637 4.95 4 4 0 o 3.038 2.728 0.00 1.34570 0.57 5 1 -2 o 15.178 12.599 180.00 1.34355 2.85 1 6 1 o 9.593 7.377 0.00 1.34290 1.80 4 3 -3 o 1.290 0.991 0.00 1.34146 0.24 2 5 -3 o 1.442 1.407 180.00 1.33981 0.27 4 4 -1 o 26.174 27.322 180.00 1.33856 4.85 2 4 4 o 1.944 2.040 0.00 1.33841 0.36 3 4 3 o 1.303 1.963 180.00 1.33615 0.24 5 2 0 o 0.836 1.589 0.00 1.33542 0.15 3 5 1 o 5.997 15.624 180.00 1.33445 1.10 5 2 -1 o 1.189 1.555 180.00 1.33094 0.22 1 1 6 o 2.263 3.137 0.00 1.32915 0.41 3 3 4 o 1.377 2.163 180.00 1.32840 0.25 3 2 -5 o 8.959 15.905 180.00 1.32794 1.62 2 0 -6 o 16.849 19.989 180.00 1.32015 1.50 4 4 1 o 6.946 8.270 0.00 1.31863 1.23 0 6 2 o 4.391 5.148 0.00 1.31820 0.78 4 2 -4 o 1.731 1.951 0.00 1.31744 0.31 0 2 6 o 22.634 25.273 0.00 1.31725 4.00 5 0 2 o 1.371 1.472 180.00 1.31069 0.12 2 5 3 o 12.575 14.878 0.00 1.31016 2.18 1 2 -6 o 0.062 0.085 180.00 1.30890 0.01 3 5 -2 o 7.441 9.228 0.00 1.30670 1.28 5 2 1 o 32.323 39.651 0.00 1.30657 5.57 4 0 4 o 0.214 0.251 0.00 1.30563 0.02 3 1 5 o 13.346 15.491 180.00 1.30445 2.29 2 1 -6 o 8.200 9.438 0.00 1.30391 1.40 0 5 4 o 1.569 1.881 180.00 1.30168 0.27 0 4 5 o 5.058 6.042 0.00 1.30142 0.86 1 6 -2 o 0.391 0.458 0.00 1.30038 0.07 2 3 5 o 7.230 8.486 180.00 1.30024 1.23 4 4 -2 o 16.787 19.837 0.00 1.29876 2.84 5 1 2 o 10.954 14.753 180.00 1.29479 1.83 5 2 -2 o 0.055 0.070 180.00 1.29409 0.01 2 6 0 o 32.261 33.079 180.00 1.29276 5.38 1 6 2 o 30.495 22.371 0.00 1.29113 5.06 1 4 -5 o 5.841 4.245 180.00 1.29108 0.97 4 1 4 o 36.862 24.699 180.00 1.28991 6.10 1 5 -4 o 2.754 1.997 180.00 1.28905 0.46 4 3 3 o 4.027 5.713 0.00 1.28383 0.66 2 6 -1 o 13.502 18.266 180.00 1.28192 2.19 1 2 6 o 1.903 2.632 0.00 1.28121 0.31 3 5 2 o 8.133 12.039 180.00 1.27915 1.31 5 1 -3 o 0.626 0.672 180.00 1.27473 0.10 3 4 -4 o 8.991 8.266 180.00 1.27373 1.43 2 6 1 o 2.861 2.497 180.00 1.27306 0.46 1 5 4 o 5.960 4.074 0.00 1.27121 0.94 1 4 5 o 18.131 5.600 180.00 1.26880 2.85 2 0 6 o 21.332 16.841 180.00 1.26512 1.66 4 4 2 o 0.037 0.047 0.00 1.26304 0.01 3 2 5 o 1.047 0.888 180.00 1.25905 0.16 2 2 -6 o 8.439 9.696 0.00 1.25855 1.30 5 3 0 o 31.952 52.364 0.00 1.25722 4.89 5 3 -1 o 15.044 25.584 0.00 1.25348 2.28 3 3 -5 o 0.379 0.267 180.00 1.25098 0.06 2 1 6 o 20.405 13.595 180.00 1.25080 3.07 5 2 2 o 5.368 3.176 0.00 1.25035 0.81 4 2 4 o 7.812 7.187 0.00 1.24595 1.16 2 6 -2 o 2.036 2.059 180.00 1.24274 0.30 0 6 3 o 16.638 16.779 180.00 1.24270 2.46 4 3 -4 o 61.272 59.641 180.00 1.24218 9.04 0 3 6 o 36.247 34.940 180.00 1.24203 5.35 2 4 -5 o 8.588 8.063 180.00 1.24065 1.26 3 5 -3 o 0.100 0.075 180.00 1.23907 0.01 2 5 -4 o 0.998 0.621 180.00 1.23683 0.15 4 1 -5 o 0.570 0.415 0.00 1.23636 0.08 1 3 -6 o 39.204 39.299 0.00 1.23502 5.68 4 4 -3 o 0.007 0.006 0.00 1.23429 0.00 5 3 1 o 0.027 0.017 180.00 1.23306 0.00 5 2 -3 o 9.078 4.766 180.00 1.23226 1.31 1 6 -3 o 4.154 1.998 180.00 1.22971 0.59 3 0 -6 o 2.307 1.073 180.00 1.22935 0.16 2 6 2 o 42.447 16.616 0.00 1.22673 6.03 3 4 4 o 16.613 6.456 0.00 1.22409 2.34 5 3 -2 o 2.860 1.110 0.00 1.22256 0.40 1 6 3 o 112.210 77.347 0.00 1.21802 15.59 3 1 -6 o 18.069 5.337 180.00 1.21620 2.50 5 1 3 o 3.214 0.507 0.00 1.21342 0.44 1 3 6 o 26.638 14.708 180.00 1.21168 3.64 4 5 0 o 28.708 20.834 0.00 1.21119 3.92 2 2 6 o 0.003 0.003 0.00 1.21060 0.00 4 5 -1 o 44.180 41.241 180.00 1.20598 5.95 2 5 4 o 0.611 0.577 0.00 1.20587 0.08 3 5 3 o 2.158 2.056 180.00 1.20421 0.29 5 0 -4 o 0.275 0.253 0.00 1.20275 0.02 2 4 5 o 2.578 2.693 0.00 1.20196 0.34 4 2 -5 o 2.981 1.756 0.00 1.19750 0.39 3 6 0 o 17.141 16.741 180.00 1.19608 2.25 3 3 5 o 13.499 16.600 180.00 1.19288 1.76 2 3 -6 o 42.827 50.530 0.00 1.19246 5.57 4 5 1 o 5.107 5.302 0.00 1.19134 0.66 5 1 -4 o 4.175 3.943 180.00 1.19043 0.54 3 6 -1 o 33.824 29.721 180.00 1.18926 4.37 4 4 3 o 4.076 3.589 0.00 1.18896 0.53 5 3 2 o 1.794 2.046 180.00 1.18548 0.23 2 6 -3 o 6.770 7.101 0.00 1.18237 0.86 4 3 4 o 0.314 0.291 0.00 1.18173 0.04 3 2 -6 o 16.476 25.448 180.00 1.17915 2.07 0 7 1 o 3.547 5.497 180.00 1.17912 0.45 3 6 1 o 0.474 0.759 180.00 1.17868 0.06 0 5 5 o 0.116 0.186 0.00 1.17861 0.01 0 1 7 o 0.373 0.623 0.00 1.17810 0.05 4 5 -2 o 0.213 0.450 180.00 1.17663 0.03 5 2 3 o 0.378 0.797 0.00 1.17662 0.05 6 0 0 o 17.737 23.528 0.00 1.17475 1.10 1 7 0 o 3.837 4.799 0.00 1.17446 0.48 1 1 -7 o 3.789 4.454 0.00 1.17383 0.47 1 5 -5 o 31.297 29.700 0.00 1.17090 3.85 5 3 -3 o 0.334 0.283 0.00 1.17002 0.04 5 4 0 o 2.023 1.583 0.00 1.16773 0.25 5 4 -1 o 1.667 1.615 0.00 1.16473 0.20 1 7 -1 o 26.448 25.714 0.00 1.16463 3.20 3 0 6 o 46.025 45.017 0.00 1.16390 2.78 6 1 0 o 10.649 10.425 0.00 1.16326 1.28 4 1 5 o 10.933 10.715 180.00 1.16310 1.32 3 4 -5 o 0.372 0.366 180.00 1.16272 0.04 6 1 -1 o 92.571 93.293 0.00 1.16196 11.12 2 6 3 o 31.340 31.784 180.00 1.16184 3.76 1 7 1 o 18.784 19.806 0.00 1.16129 2.25 3 6 -2 o 7.269 7.787 0.00 1.15943 0.87 3 5 -4 o 20.866 16.928 180.00 1.15792 2.48 0 6 4 o 0.385 0.310 0.00 1.15592 0.05 4 4 -4 o 1.654 1.385 0.00 1.15565 0.20 5 2 -4 o 5.608 4.716 0.00 1.15562 0.66 0 4 6 o 0.279 0.238 0.00 1.15552 0.03 1 5 5 o 28.751 28.979 0.00 1.15421 3.38 3 1 6 o 34.463 42.137 0.00 1.15272 4.04 2 3 6 o 1.333 1.536 180.00 1.15143 0.16 1 1 7 o 7.853 7.868 0.00 1.15048 0.92 4 5 2 o 24.722 22.780 180.00 1.14987 2.88 1 4 -6 o 12.268 11.303 0.00 1.14987 1.43 6 0 -2 o 0.000 0.000 0.00 1.14954 0.00 5 4 1 o 9.074 6.962 0.00 1.14829 1.05 1 6 -4 o 3.940 2.695 0.00 1.14704 0.45 0 7 2 o 0.199 0.139 0.00 1.14520 0.02 0 2 7 o 2.887 2.098 180.00 1.14433 0.33 6 1 1 o 9.122 7.202 180.00 1.14246 1.04 1 2 -7 o 0.105 0.118 180.00 1.14041 0.01 4 3 -5 o 3.005 3.616 0.00 1.14014 0.34 3 6 2 o 3.748 4.599 0.00 1.14005 0.42 5 4 -2 o 5.720 7.325 180.00 1.13979 0.65 6 1 -2 o 12.649 16.695 0.00 1.13876 1.43 2 1 -7 o 1.495 1.975 0.00 1.13867 0.17 5 0 4 o 50.714 76.613 180.00 1.13499 2.83 1 6 4 o 0.706 1.007 180.00 1.13442 0.08 1 7 -2 o 10.544 13.451 0.00 1.13346 1.17 2 5 -5 o 3.321 3.895 180.00 1.13290 0.37 1 4 6 o 12.675 12.673 180.00 1.13096 1.40 6 2 0 o 23.034 23.285 180.00 1.13072 2.54 4 2 5 o 59.573 60.816 180.00 1.13057 6.58 6 2 -1 o 2.090 2.354 180.00 1.12952 0.23 2 7 0 o 2.749 3.182 180.00 1.12840 0.30 4 5 -3 o 3.964 4.466 0.00 1.12805 0.43 1 7 2 o 0.013 0.014 180.00 1.12732 0.00 4 0 -6 o 36.013 35.421 180.00 1.12521 1.96 5 1 4 o 13.932 14.223 0.00 1.12462 1.51 3 3 -6 o 60.110 63.044 0.00 1.12427 6.52 5 3 3 o 1.873 3.072 0.00 1.12208 0.20 2 7 -1 o 1.287 2.574 0.00 1.12117 0.14 3 2 6 o 0.327 0.677 0.00 1.12103 0.04 3 5 4 o 0.006 0.019 0.00 1.12025 0.00 1 2 7 o 0.160 2.328 180.00 1.11897 0.02 3 4 5 o 39.739 47.235 180.00 1.11563 4.21 2 4 -6 o 5.296 6.218 180.00 1.11529 0.56 2 7 1 o 4.473 5.250 180.00 1.11523 0.47 4 1 -6 o 3.341 3.925 0.00 1.11510 0.35 6 0 2 o 27.181 36.929 0.00 1.11265 1.43 6 2 1 o 6.384 8.412 0.00 1.11158 0.67 3 6 -3 o 0.020 0.026 180.00 1.11140 0.00 2 6 -4 o 3.312 3.904 0.00 1.10979 0.35 5 4 2 o 1.482 1.713 0.00 1.10957 0.15 6 2 -2 o 15.261 16.946 180.00 1.10818 1.58 2 2 -7 o 34.577 38.541 0.00 1.10809 3.59 4 4 4 o 6.446 9.466 180.00 1.10649 0.67 5 3 -4 o 0.726 1.598 0.00 1.10382 0.07 2 5 5 o 10.838 20.909 0.00 1.10321 1.11 6 1 2 o 0.548 0.933 0.00 1.10287 0.06 5 1 -5 o 3.702 4.612 180.00 1.10115 0.38 6 1 -3 o 0.278 0.355 180.00 1.09735 0.03 2 1 7 o 13.113 16.218 0.00 1.09713 1.32 5 4 -3 o 28.397 33.657 0.00 1.09687 2.86 5 2 4 o 0.973 1.026 180.00 1.09513 0.10 2 7 -2 o 2.570 2.763 180.00 1.09468 0.26 0 7 3 o 17.038 18.343 180.00 1.09465 1.70 0 3 7 o 0.365 0.409 0.00 1.09397 0.04 4 5 3 o 12.630 14.417 0.00 1.09313 1.26 4 6 0 o 3.938 4.015 180.00 1.09115 0.39 1 3 -7 o 3.391 3.614 180.00 1.09055 0.33 4 6 -1 o 2.233 3.246 0.00 1.08734 0.22 2 6 4 o 6.062 8.566 0.00 1.08726 0.59 4 2 -6 o 0.029 0.033 0.00 1.08634 0.00 3 6 3 o 48.162 51.983 0.00 1.08604 4.70 1 7 -3 o 4.159 4.290 180.00 1.08574 0.41 2 7 2 o 13.618 12.234 180.00 1.08369 1.32 6 3 0 o 3.073 3.667 0.00 1.08206 0.30 4 3 5 o 2.768 3.403 180.00 1.08193 0.27 2 4 6 o 0.946 1.289 0.00 1.08151 0.09 6 3 -1 o 4.089 6.430 180.00 1.08101 0.39 3 1 -7 o 8.327 17.601 0.00 1.08020 0.80 1 7 3 o 0.057 0.080 0.00 1.07767 0.01 4 6 1 o 27.886 25.000 0.00 1.07657 2.65 5 5 0 o 0.611 0.547 0.00 1.07656 0.06 6 2 2 o 0.374 0.345 180.00 1.07502 0.04 5 5 -1 o 8.281 8.627 180.00 1.07421 0.78 3 3 6 o 5.647 6.020 180.00 1.07356 0.53 5 2 -5 o 0.296 0.315 180.00 1.07342 0.03 3 5 -5 o 57.997 62.230 0.00 1.07263 5.44 4 4 -5 o 21.879 24.616 180.00 1.07213 2.05 1 3 7 o 0.480 0.580 180.00 1.07175 0.04 6 2 -3 o 1.400 3.722 0.00 1.06990 0.13 2 2 7 o 0.010 0.029 0.00 1.06970 0.00 0 6 5 o 0.074 0.144 180.00 1.06715 0.01 4 5 -4 o 0.639 1.235 0.00 1.06707 0.06 0 5 6 o 3.226 6.108 180.00 1.06697 0.30 4 6 -2 o 0.976 1.186 0.00 1.06568 0.09 6 3 1 o 8.472 9.392 180.00 1.06525 0.78 1 5 -6 o 5.045 6.906 0.00 1.06252 0.46 3 7 0 o 1.086 1.477 0.00 1.06238 0.10 6 3 -2 o 10.110 13.666 180.00 1.06226 0.92 2 3 -7 o 19.737 26.561 0.00 1.06218 1.80 1 6 -5 o 0.851 1.107 180.00 1.06142 0.08 5 5 1 o 7.509 9.760 180.00 1.06127 0.68 3 4 -6 o 0.029 0.048 180.00 1.05891 0.00 4 0 6 o 0.599 0.985 180.00 1.05890 0.03 3 7 -1 o 0.091 0.389 0.00 1.05760 0.01 5 4 3 o 0.000 0.038 180.00 1.05707 0.00 5 5 -2 o 0.000 0.030 0.00 1.05455 0.00 3 2 -7 o 0.246 9.994 180.00 1.05399 0.02 2 7 -3 o 3.651 6.385 180.00 1.05274 0.32 3 6 -4 o 0.842 1.060 0.00 1.05172 0.07 6 0 -4 o 5.852 7.293 0.00 1.05165 0.26 5 3 4 o 2.449 2.896 0.00 1.05075 0.22 4 1 6 o 17.451 20.892 180.00 1.05047 1.53 3 7 1 o 30.001 36.926 0.00 1.05014 2.63 6 1 3 o 0.224 0.279 0.00 1.05005 0.02 1 6 5 o 10.035 15.552 0.00 1.04894 0.88 1 5 6 o 0.006 0.016 0.00 1.04755 0.00 4 6 2 o 0.338 1.378 180.00 1.04568 0.03 6 1 -4 o 0.047 0.121 180.00 1.04339 0.00 4 3 -6 o 3.269 7.118 0.00 1.04297 0.28 0 8 0 o 0.139 0.242 0.00 1.04222 0.01 5 4 -4 o 4.204 6.730 180.00 1.04177 0.36 0 0 8 o 0.644 0.915 180.00 1.04128 0.03 1 0 -8 o 6.741 4.768 0.00 1.03952 0.29 2 7 3 o 102.654 68.861 180.00 1.03817 8.70 3 7 -2 o 3.631 3.212 0.00 1.03645 0.31 5 1 5 o 1.247 1.114 0.00 1.03640 0.11 3 5 5 o 3.282 3.519 0.00 1.03533 0.28 2 5 -6 o 2.879 3.229 0.00 1.03506 0.24 0 8 1 o 8.246 10.576 180.00 1.03416 0.69 0 7 4 o 0.212 0.279 180.00 1.03394 0.02 0 4 7 o 0.030 0.040 180.00 1.03347 0.00 0 1 8 o 29.449 40.097 0.00 1.03326 2.46 6 3 2 o 1.266 1.711 0.00 1.03295 0.11 2 6 -5 o 0.213 0.286 180.00 1.03286 0.02 1 1 -8 o 0.687 0.731 0.00 1.03154 0.06 5 3 -5 o 1.127 1.197 180.00 1.03153 0.09 1 8 0 o 25.725 24.821 180.00 1.03101 2.13 1 4 -7 o 0.247 0.228 180.00 1.03058 0.02 5 5 2 o 3.873 3.555 180.00 1.03048 0.32 4 6 -3 o 40.511 38.226 0.00 1.02918 3.34 6 3 -3 o 10.071 9.850 180.00 1.02841 0.83 2 3 7 o 13.070 12.887 0.00 1.02823 1.07 4 5 4 o 8.192 8.153 0.00 1.02801 0.67 3 1 7 o 23.837 23.748 0.00 1.02799 1.96 1 7 -4 o 0.941 0.953 0.00 1.02758 0.08 4 2 6 o 19.411 20.133 0.00 1.02631 1.59 6 2 3 o 1.811 1.875 0.00 1.02592 0.15 1 8 -1 o 11.759 10.641 0.00 1.02434 0.96 6 4 0 o 1.378 1.073 0.00 1.02341 0.11 4 4 5 o 0.045 0.035 180.00 1.02330 0.00 3 6 4 o 11.745 8.967 0.00 1.02325 0.95 3 7 2 o 1.880 1.365 180.00 1.02254 0.15 6 4 -1 o 26.502 19.224 180.00 1.02252 2.14 1 8 1 o 18.944 13.680 180.00 1.02207 1.53 5 0 -6 o 27.134 19.920 180.00 1.02156 1.09 1 0 8 o 18.351 14.037 0.00 1.02093 0.74 5 5 -3 o 12.892 10.262 0.00 1.02028 1.03 6 2 -4 o 31.191 25.178 0.00 1.01971 2.50 1 7 4 o 1.854 1.468 0.00 1.01847 0.15 3 4 6 o 18.490 15.938 180.00 1.01621 1.47 2 0 -8 o 9.430 8.243 180.00 1.01598 0.37 1 4 7 o 0.712 0.616 0.00 1.01468 0.06 3 3 -7 o 12.865 10.933 180.00 1.01425 1.01 5 1 -6 o 0.049 0.041 0.00 1.01398 0.00 1 1 8 o 5.590 4.784 180.00 1.01337 0.44 5 2 5 o 10.987 9.487 180.00 1.01319 0.86 0 8 2 o 1.555 1.450 0.00 1.01105 0.12 0 2 8 o 0.198 0.175 0.00 1.01025 0.02 2 6 5 o 24.159 21.428 180.00 1.01021 1.88 6 4 1 o 0.264 0.231 0.00 1.00916 0.02 1 2 -8 o 42.495 37.041 180.00 1.00864 3.29 4 1 -7 o 2.348 2.044 180.00 1.00858 0.18 2 1 -8 o 8.442 7.341 180.00 1.00852 0.65 2 5 6 o 0.856 0.724 0.00 1.00788 0.07 7 0 0 o 15.180 11.835 180.00 1.00693 0.58 6 4 -2 o 4.077 3.053 180.00 1.00661 0.31 2 4 -7 o 3.401 2.524 180.00 1.00655 0.26 3 2 7 o 19.347 11.787 0.00 1.00532 1.48 1 8 -2 o 5.688 3.069 0.00 1.00294 0.43 4 6 3 o 0.478 0.259 180.00 1.00246 0.04 3 7 -3 o 5.737 3.249 180.00 1.00172 0.43 2 7 -4 o 0.314 0.221 180.00 1.00053 0.02 4 5 -5 o 8.375 6.220 0.00 1.00029 0.63 7 1 -1 o 6.332 5.114 0.00 0.99990 0.48 7 1 0 o 0.920 0.777 180.00 0.99967 0.07 2 8 0 o 14.350 12.569 180.00 0.99943 1.08 1 8 2 o 36.271 34.010 0.00 0.99868 2.72 6 0 4 o 0.660 0.703 0.00 0.99692 0.02 5 4 4 o 4.775 5.130 0.00 0.99680 0.36 2 8 -1 o 7.295 5.386 0.00 0.99440 0.54 7 0 -2 o 12.941 10.196 180.00 0.99299 0.48 5 2 -6 o 1.955 1.717 180.00 0.99221 0.14 1 2 8 o 12.815 11.574 180.00 0.99163 0.94 2 8 1 o 1.055 0.900 180.00 0.99025 0.08 4 4 -6 o 1.578 1.343 180.00 0.99016 0.12 6 1 4 o 0.234 0.198 180.00 0.98987 0.02 5 6 0 o 0.034 0.029 0.00 0.98964 0.00 3 5 -6 o 10.016 8.540 0.00 0.98952 0.73 4 3 6 o 3.312 2.824 180.00 0.98952 0.24 6 3 3 o 9.649 8.375 180.00 0.98917 0.70 5 5 3 o 2.230 2.140 0.00 0.98802 0.16 5 6 -1 o 50.549 49.379 180.00 0.98781 3.67 4 2 -7 o 8.247 8.402 0.00 0.98715 0.60 2 2 -8 o 1.308 1.337 0.00 0.98709 0.09 4 7 0 o 1.391 1.433 0.00 0.98681 0.10 3 6 -5 o 2.575 2.661 180.00 0.98658 0.19 7 1 -2 o 3.667 3.749 180.00 0.98602 0.26 7 1 1 o 19.298 19.000 180.00 0.98535 1.39 4 7 -1 o 3.642 3.315 180.00 0.98399 0.26 2 7 4 o 0.369 0.334 180.00 0.98393 0.03 6 3 -4 o 24.633 21.602 180.00 0.98359 1.76 3 7 3 o 0.047 0.038 180.00 0.98303 0.00 6 1 -5 o 3.536 2.685 180.00 0.98271 0.25 4 6 -4 o 1.316 0.918 180.00 0.98225 0.09 0 6 6 o 2.030 1.396 180.00 0.98217 0.14 2 0 8 o 16.943 11.495 180.00 0.98209 0.60 6 4 2 o 11.896 7.442 0.00 0.98156 0.85 5 4 -5 o 0.191 0.108 0.00 0.98035 0.01 7 2 -1 o 3.763 2.401 180.00 0.97900 0.27 7 2 0 o 0.236 0.156 180.00 0.97878 0.02 1 6 -6 o 0.929 0.625 0.00 0.97870 0.07 5 3 5 o 1.690 1.319 180.00 0.97773 0.12 5 6 1 o 10.988 8.592 180.00 0.97772 0.77 6 4 -3 o 3.499 2.758 180.00 0.97767 0.25 2 4 7 o 10.519 8.474 0.00 0.97751 0.74 4 7 1 o 0.086 0.087 180.00 0.97599 0.01 2 8 -2 o 1.559 1.633 180.00 0.97577 0.11 0 8 3 o 0.334 0.351 180.00 0.97575 0.02 5 5 -4 o 27.033 29.002 180.00 0.97549 1.89 2 1 8 o 3.472 3.757 0.00 0.97535 0.24 0 3 8 o 13.999 15.338 0.00 0.97509 0.98 3 0 -8 o 53.059 58.844 0.00 0.97477 1.85 1 3 -8 o 0.724 0.856 180.00 0.97365 0.05 5 6 -2 o 0.543 0.601 180.00 0.97246 0.04 3 3 7 o 0.520 0.396 0.00 0.97066 0.04 6 2 4 o 4.532 3.666 180.00 0.96958 0.31 1 8 -3 o 10.287 8.358 0.00 0.96943 0.70 0 7 5 o 43.157 35.154 0.00 0.96895 2.95 0 5 7 o 58.350 47.481 180.00 0.96867 3.98 3 1 -8 o 4.798 3.918 180.00 0.96818 0.33 2 8 2 o 2.829 2.323 0.00 0.96797 0.19 4 7 -2 o 3.674 3.028 0.00 0.96785 0.25 1 6 6 o 12.943 11.406 180.00 0.96696 0.88 1 5 -7 o 1.299 1.256 0.00 0.96629 0.09 7 2 -2 o 0.748 0.759 0.00 0.96597 0.05 3 4 -7 o 0.472 0.505 0.00 0.96547 0.03 7 2 1 o 2.416 2.609 0.00 0.96534 0.16 7 0 2 o 2.464 2.683 180.00 0.96508 0.08 1 7 -5 o 21.771 23.691 180.00 0.96466 1.47 1 8 3 o 18.896 20.127 180.00 0.96367 1.27 6 2 -5 o 2.141 2.118 180.00 0.96285 0.14 6 5 0 o 4.257 3.907 0.00 0.96037 0.28 4 5 5 o 0.000 0.000 180.00 0.96028 0.00 7 1 -3 o 5.400 5.949 180.00 0.95971 0.36 5 0 6 o 15.013 16.565 0.00 0.95970 0.50 6 5 -1 o 4.019 4.505 180.00 0.95964 0.27 5 3 -6 o 22.053 28.607 0.00 0.95884 1.46 7 1 2 o 21.868 28.982 180.00 0.95868 1.44 1 3 8 o 0.012 0.017 180.00 0.95832 0.00 3 7 -4 o 2.473 3.601 180.00 0.95736 0.16 3 6 5 o 0.788 1.147 0.00 0.95732 0.05 2 6 -6 o 0.368 0.538 180.00 0.95711 0.02 2 2 8 o 3.168 4.460 180.00 0.95593 0.21 1 7 5 o 3.437 4.655 0.00 0.95526 0.22 3 5 6 o 1.121 1.456 180.00 0.95441 0.07 4 3 -7 o 5.423 6.983 0.00 0.95428 0.35 2 3 -8 o 9.218 11.823 180.00 0.95422 0.60 5 6 2 o 0.002 0.002 0.00 0.95348 0.00 5 1 6 o 14.354 16.549 0.00 0.95341 0.93 1 5 7 o 9.424 10.260 180.00 0.95314 0.61 4 7 2 o 2.299 2.285 180.00 0.95279 0.15 3 8 0 o 6.449 6.227 180.00 0.95269 0.42 4 1 7 o 0.993 0.924 0.00 0.95257 0.06 4 6 4 o 0.540 0.368 0.00 0.95153 0.03 3 8 -1 o 8.911 6.326 0.00 0.94924 0.57 3 2 -8 o 1.292 0.931 180.00 0.94917 0.08 6 5 1 o 3.743 3.158 0.00 0.94856 0.24 7 3 -1 o 32.640 41.120 0.00 0.94691 2.07 7 3 0 o 6.166 7.937 0.00 0.94671 0.39 6 5 -2 o 0.263 0.345 0.00 0.94645 0.02 2 5 -7 o 11.870 15.644 180.00 0.94639 0.75 2 8 -3 o 0.011 0.015 180.00 0.94572 0.00 5 6 -3 o 3.673 4.983 180.00 0.94539 0.23 4 4 6 o 0.080 0.097 0.00 0.94407 0.01 3 8 1 o 3.785 4.366 180.00 0.94383 0.24 6 4 3 o 0.281 0.320 180.00 0.94377 0.02 2 7 -5 o 23.453 24.451 0.00 0.94307 1.47 7 2 -3 o 24.171 29.168 180.00 0.94119 1.51 4 7 -3 o 0.125 0.143 0.00 0.94027 0.01 7 2 2 o 17.302 19.606 0.00 0.94022 1.08 6 4 -4 o 0.016 0.014 180.00 0.93892 0.00 6 3 4 o 2.613 1.909 0.00 0.93838 0.16 5 5 4 o 5.418 3.835 0.00 0.93828 0.33 3 7 4 o 2.006 1.367 0.00 0.93573 0.12 2 6 6 o 9.134 6.484 180.00 0.93550 0.56 5 2 6 o 0.000 0.000 180.00 0.93524 0.00 2 8 3 o 7.539 5.702 0.00 0.93512 0.46 7 3 -2 o 5.717 4.338 180.00 0.93510 0.35 7 3 1 o 8.056 6.689 0.00 0.93453 0.49 4 2 7 o 0.567 0.476 0.00 0.93445 0.03 3 8 -2 o 17.011 15.540 0.00 0.93386 1.03 5 4 5 o 30.733 28.207 180.00 0.93382 1.87 5 1 -7 o 10.631 11.071 0.00 0.93278 0.64 4 5 -6 o 7.810 8.189 0.00 0.93273 0.47 6 3 -5 o 4.166 4.702 180.00 0.93227 0.25 0 8 4 o 0.470 0.554 180.00 0.93202 0.03 0 4 8 o 0.607 0.770 180.00 0.93152 0.04 3 0 8 o 0.612 0.747 0.00 0.93071 0.02 1 4 -8 o 1.895 2.062 0.00 0.93026 0.11 7 0 -4 o 6.043 5.535 0.00 0.92954 0.18 4 6 -5 o 9.161 8.238 0.00 0.92941 0.55 3 4 7 o 1.483 1.498 0.00 0.92765 0.09 1 8 -4 o 0.116 0.120 180.00 0.92735 0.01 6 1 5 o 7.453 7.755 0.00 0.92727 0.44 2 3 8 o 6.197 5.922 0.00 0.92598 0.37 2 7 5 o 8.454 7.751 0.00 0.92573 0.50 6 0 -6 o 0.527 0.483 180.00 0.92573 0.02 6 5 2 o 23.726 21.001 180.00 0.92554 1.40 3 1 8 o 2.592 2.077 0.00 0.92497 0.15 5 5 -5 o 15.819 11.977 0.00 0.92452 0.93 7 1 -4 o 0.000 0.000 0.00 0.92382 0.00 3 8 2 o 6.128 4.660 0.00 0.92364 0.36 7 1 3 o 5.025 4.959 180.00 0.92253 0.29 6 5 -3 o 4.365 4.688 0.00 0.92227 0.26 2 5 7 o 5.167 5.770 180.00 0.92214 0.30 4 0 -8 o 2.908 3.363 0.00 0.92201 0.08 3 6 -6 o 0.122 0.154 0.00 0.92076 0.01 0 9 1 o 5.321 6.702 0.00 0.92074 0.31 1 8 4 o 0.355 0.440 180.00 0.92064 0.02 6 1 -6 o 1.200 1.348 180.00 0.92008 0.07 0 1 9 o 0.165 0.181 0.00 0.91993 0.01 3 3 -8 o 3.818 4.136 180.00 0.91984 0.22 4 7 3 o 2.451 2.628 180.00 0.91976 0.14 5 6 3 o 3.329 3.508 0.00 0.91955 0.19 1 1 -9 o 2.174 2.291 0.00 0.91954 0.13 1 9 0 o 3.046 3.540 180.00 0.91852 0.18 5 4 -6 o 10.801 15.046 0.00 0.91732 0.62 1 4 8 o 0.941 1.292 0.00 0.91687 0.05 4 1 -8 o 0.397 0.514 180.00 0.91643 0.02 5 2 -7 o 1.591 1.732 0.00 0.91574 0.09 1 9 -1 o 0.002 0.002 0.00 0.91379 0.00 4 4 -7 o 8.352 8.149 180.00 0.91332 0.47 2 4 -8 o 6.591 6.493 180.00 0.91327 0.37 7 3 -3 o 2.250 2.467 180.00 0.91256 0.13 1 9 1 o 3.010 3.418 180.00 0.91218 0.17 3 5 -7 o 0.288 0.333 0.00 0.91201 0.02 7 3 2 o 7.724 9.255 180.00 0.91168 0.44 6 2 5 o 7.936 11.238 180.00 0.91053 0.45 5 7 0 o 3.163 4.391 180.00 0.90982 0.18 5 6 -4 o 1.523 1.992 180.00 0.90942 0.09 5 7 -1 o 3.025 3.362 180.00 0.90840 0.17 3 2 8 o 24.655 27.221 180.00 0.90835 1.37 3 8 -3 o 11.709 12.715 0.00 0.90821 0.65 3 7 -5 o 1.602 1.641 180.00 0.90745 0.09 2 8 -4 o 0.710 0.726 0.00 0.90733 0.04 7 2 -4 o 11.744 11.998 0.00 0.90726 0.65 5 3 6 o 7.691 7.868 180.00 0.90714 0.43 7 4 -1 o 2.307 2.391 0.00 0.90686 0.13 7 4 0 o 7.527 7.908 180.00 0.90668 0.42 4 3 7 o 1.545 1.665 0.00 0.90642 0.09 7 2 3 o 0.081 0.090 0.00 0.90605 0.00 1 1 9 o 0.000 0.000 0.00 0.90502 0.00 0 9 2 o 0.010 0.007 0.00 0.90432 0.00 4 7 -4 o 7.963 4.793 0.00 0.90407 0.44 0 7 6 o 1.063 0.626 0.00 0.90401 0.06 2 1 -9 o 4.936 2.816 180.00 0.90391 0.27 0 6 7 o 0.932 0.528 180.00 0.90389 0.05 6 2 -6 o 0.161 0.087 180.00 0.90372 0.01 0 2 9 o 3.857 2.025 0.00 0.90358 0.21 1 2 -9 o 3.687 1.843 0.00 0.90321 0.20 1 6 -7 o 22.076 11.922 0.00 0.90195 1.20 1 7 -6 o 0.028 0.017 180.00 0.90130 0.00 5 7 1 o 22.630 17.087 0.00 0.90054 1.23 4 2 -8 o 9.285 7.675 0.00 0.90026 0.50 6 4 4 o 9.929 11.255 180.00 0.89935 0.54 1 9 -2 o 2.356 3.268 180.00 0.89850 0.13 6 6 0 o 0.179 0.197 180.00 0.89714 0.01 4 6 5 o 12.583 13.529 180.00 0.89706 0.67 4 8 0 o 0.313 0.337 180.00 0.89706 0.02 6 6 -1 o 1.867 1.758 0.00 0.89654 0.10 7 4 -2 o 0.083 0.078 180.00 0.89646 0.00 5 7 -2 o 0.307 0.283 180.00 0.89642 0.02 2 9 0 o 0.010 0.009 0.00 0.89598 0.00 7 4 1 o 1.161 1.032 0.00 0.89596 0.06 1 9 2 o 0.602 0.568 180.00 0.89544 0.03 4 8 -1 o 1.217 1.323 180.00 0.89493 0.06 2 8 4 o 0.060 0.066 180.00 0.89489 0.00 3 8 3 o 6.948 9.069 180.00 0.89421 0.37 6 4 -5 o 4.232 5.607 180.00 0.89397 0.22 4 5 6 o 3.265 4.325 0.00 0.89391 0.17 6 5 3 o 1.020 1.329 0.00 0.89365 0.05 2 9 -1 o 5.320 6.135 0.00 0.89235 0.28 3 6 6 o 2.795 3.222 180.00 0.89227 0.15 1 7 6 o 0.959 1.107 0.00 0.89211 0.05 1 6 7 o 0.056 0.066 0.00 0.89123 0.00 6 5 -4 o 3.325 4.544 0.00 0.88953 0.17 1 2 9 o 2.540 3.510 180.00 0.88944 0.13 2 9 1 o 0.339 0.474 0.00 0.88934 0.02 5 3 -7 o 1.904 2.667 180.00 0.88932 0.10 4 8 1 o 6.855 9.903 180.00 0.88890 0.36 2 4 8 o 1.950 2.838 0.00 0.88842 0.10 2 2 -9 o 0.328 0.477 0.00 0.88839 0.02 6 6 1 o 12.904 18.648 0.00 0.88749 0.67 _reflns_number_observed 710 _reflns_limit_h_min 0 _reflns_limit_h_max 10 _reflns_limit_k_min 0 _reflns_limit_k_max 11 _reflns_limit_l_min -11 _reflns_limit_l_max 11 _reflns_d_resolution_high 0.887 _reflns_d_resolution_low 3.373 data_FINAL_p_03 _pd_block_id 2004-05-29T19:48|FINAL_H_03|Li2BeH4|STADIP #============================================================================== # 9. INSTRUMENT CHARACTERIZATION _pd_instr_location "STADI/P STOE Department of Chemistry, MSU, 119992 Moscow, Russia" _pd_calibration_special_details # description of the method used # to calibrate the instrument "Si external standard" _diffrn_ambient_temperature 293 _diffrn_source "sealed X-Ray tube" _diffrn_source_target Cu _diffrn_source_type "Cu K\a~1~" _diffrn_measurement_device_type "STADI/P STOE" _diffrn_detector point _diffrn_detector_type "scintillation" # make or model of detector _pd_meas_scan_method step # options are 'step', 'cont', # 'tof', 'fixed' or # 'disp' (= dispersive) _pd_meas_special_details ; ? ; # The following two items identify the program(s) used (if appropriate). _computing_data_collection "WinXPow STOE" _computing_data_reduction "WinXPow STOE" # Describe any processing performed on the data, prior to refinement. # For example: a manual Lp correction or a precomputed absorption correction _pd_proc_info_data_reduction ? # The following item is used for angular dispersive measurements only. _diffrn_radiation_monochromator "Ge primiry beam" # The following items are used to define the size of the instrument. # Not all distances are appropriate for all instrument types. _pd_instr_dist_src/mono 260 _pd_instr_dist_mono/spec 130 _pd_instr_dist_src/spec ? _pd_instr_dist_spec/anal ? _pd_instr_dist_anal/detc ? _pd_instr_dist_spec/detc 130 # 10. Specimen size and mounting information # The next three fields give the specimen dimensions in mm. The equatorial # plane contains the incident and diffracted beam. _pd_spec_size_axial 10 # perpendicular to # equatorial plane _pd_spec_size_equat 1 # parallel to # scattering vector # in transmission _pd_spec_size_thick ? # parallel to # scattering vector # in reflection _pd_spec_mounting # This field should be # used to give details of the # container. "glass capyllary" _pd_spec_mount_mode transmission # options are 'reflection' # or 'transmission' _pd_spec_shape cylinder # options are 'cylinder' # 'flat_sheet' or 'irregular' # phase table loop_ _pd_phase_id _pd_phase_block_id _pd_phase_mass_% _pd_proc_ls_profile_function _pd_proc_ls_peak_cutoff 1 2004-05-29T19:48|FINAL_phase1|Li2BeH4|| ? ; CW Profile function number 2 with 18 terms Profile coefficients for Simpson's rule integration of pseudovoigt function C.J. Howard (1982). J. Appl. Cryst.,15,615-620. P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83. #1(GU) = 657.930 #2(GV) = -105.720 #3(GW) = 52.180 #4(LX) = 0.000 #5(LY) = 2.945 #6(trns) = 0.000 #7(asym) = -3.8817 #8(shft) = 0.0000 #9(GP) = 0.000 #10(stec)= 0.00 #11(ptec)= 0.00 #12(sfec)= 0.00 #13(L11) = 0.000 #14(L22) = 0.000 #15(L33) = 0.000 #16(L12) = 0.000 #17(L13) = 0.000 #18(L23) = 0.000 Peak tails are ignored where the intensity is below 0.0020 times the peak Aniso. broadening axis 0.0 0.0 1.0 ; 0.00200 loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source LI 0.001 0.000 1.12820 3.95460 0.75080 1.05240 0.61750 85.3905 0.46530 168.261 0.03770 International_Tables_Vol_C BE 0.003 0.001 1.59190 43.6427 1.12780 1.86230 0.53910 103.483 0.70290 0.54200 0.03850 International_Tables_Vol_C D 0.000 0.000 0.49300 10.5109 0.32291 26.1257 0.14019 3.14236 0.04081 57.7997 0.00304 International_Tables_Vol_C _diffrn_radiation_probe x-ray _diffrn_radiation_polarisn_ratio 0.444 _diffrn_radiation_wavelength 1.5406 _diffrn_radiation_type ? _pd_proc_ls_prof_R_factor 0.0530 _pd_proc_ls_prof_wR_factor 0.0669 _pd_proc_ls_prof_wR_expected 0.0497 _refine_ls_R_Fsqd_factor 0.18648 _pd_proc_ls_background_function ; GSAS Background function number 2 with 20 terms. Cosine Fourier series 1: 152.796 2: 308.523 3: -5.43492 4: -42.4156 5: 3.65136 6: -36.8199 7: -67.7226 8: -43.0493 9: -18.9205 10: -35.0868 11: -18.1441 12: 18.2920 13: 15.8062 14: 1.58846 15: 17.6228 16: 19.3610 17: -5.42733 18: -4.00267 19: 16.1004 20: -16.5413 ; _exptl_absorpt_process_details ; GSAS Absorption/surface roughness correction: function number 0 No correction is applied. ; _exptl_absorpt_correction_T_min 1.00000 _exptl_absorpt_correction_T_max 1.00000 # Extinction correction _gsas_exptl_extinct_corr_T_min 1.00000 _gsas_exptl_extinct_corr_T_max 1.00000 _pd_proc_info_datetime 2004-05-29T19:48:32 _pd_calc_method "Rietveld Refinement" #---- raw/calc data loop ----- _pd_meas_2theta_range_min 10.0 _pd_meas_2theta_range_max 100.0 _pd_meas_2theta_range_inc 0.02 _pd_proc_2theta_range_min 10.0 _pd_proc_2theta_range_max 100.0 _pd_proc_2theta_range_inc 0.02 loop_ _pd_meas_counts_total _pd_proc_ls_weight _pd_proc_intensity_bkg_calc _pd_calc_intensity_total # ; # ; ? ? ? ? _pd_meas_number_of_points 4500 _pd_proc_number_of_points 4500 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_observed_status _refln_F_squared_meas _refln_F_squared_calc _refln_phase_calc _refln_d_spacing _gsas_i100_meas 1 0 0 o 4.054 0.143 0.00 7.04852 3.14 0 1 1 o -0.001 1.262 180.00 5.89303 0.00 1 1 0 o 14.885 20.200 0.00 5.38281 13.25 1 1 -1 o 3.468 5.454 180.00 4.62259 2.25 1 1 1 o 27.030 20.777 180.00 4.42596 16.01 0 2 0 o 29.006 25.155 0.00 4.16888 7.56 0 0 2 o 52.437 43.657 0.00 4.16513 13.64 0 2 1 o 23.992 19.932 0.00 3.72809 9.87 0 1 2 o 17.566 14.607 180.00 3.72608 7.23 1 0 -2 o 238.639 208.504 180.00 3.68805 47.97 1 2 0 o 119.635 99.890 0.00 3.58824 45.35 2 0 0 o 457.258 434.427 0.00 3.52426 83.32 1 0 2 o 33.983 42.374 180.00 3.49170 6.08 1 1 -2 o 70.530 74.165 180.00 3.37282 23.37 1 2 -1 o 7.956 9.691 180.00 3.33421 2.58 1 2 1 o 20.117 18.343 0.00 3.25812 6.19 2 1 0 o 23.582 23.868 180.00 3.24618 7.18 1 1 2 o -0.023 10.113 0.00 3.22068 0.00 2 1 -1 o -0.004 1.015 0.00 3.08522 0.00 2 1 1 o 11.008 22.248 0.00 2.96750 2.75 0 2 2 o 266.212 254.863 180.00 2.94652 65.47 2 0 -2 o 929.508 913.612 180.00 2.77720 100.02 1 2 -2 o 9.097 5.009 0.00 2.76227 1.93 2 2 0 o 64.883 48.582 180.00 2.69141 13.00 1 2 2 o 0.170 0.055 180.00 2.67682 0.03 0 3 1 o 37.559 30.542 180.00 2.63639 7.19 2 1 -2 o 82.254 68.604 0.00 2.63488 15.72 0 1 3 o 11.866 9.957 0.00 2.63450 2.27 2 0 2 o 75.267 105.151 0.00 2.61126 7.05 2 2 -1 o 1.254 1.367 180.00 2.59752 0.23 1 3 0 o 325.245 355.212 0.00 2.58552 59.49 2 2 1 o 258.391 269.851 0.00 2.52608 44.80 1 1 -3 o 1.629 1.608 180.00 2.51711 0.28 2 1 2 o 117.860 113.924 180.00 2.49191 19.81 1 3 -1 o 72.591 76.244 0.00 2.48547 12.12 1 3 1 o 31.464 55.039 0.00 2.45347 5.11 1 1 3 o 367.602 379.032 0.00 2.42120 57.75 3 0 0 o -0.016 3.539 180.00 2.34951 0.00 0 3 2 o 0.095 0.088 0.00 2.31184 0.01 2 2 -2 o 159.183 148.065 180.00 2.31129 22.44 0 2 3 o 281.283 261.987 180.00 2.31104 39.63 3 1 0 o 6.980 0.248 180.00 2.26143 0.93 1 2 -3 o 8.109 5.603 180.00 2.23057 1.05 1 3 -2 o 138.955 172.860 0.00 2.21958 17.81 3 1 -1 o 1.404 1.782 180.00 2.21636 0.18 2 2 2 o 84.483 106.073 180.00 2.21298 10.74 2 3 0 o 62.876 49.648 0.00 2.18231 7.71 1 3 2 o 122.957 106.018 180.00 2.17451 14.98 2 1 -3 o 25.534 22.392 0.00 2.17267 3.11 1 2 3 o 43.200 40.264 180.00 2.16301 5.19 3 1 1 o 163.874 197.519 180.00 2.15004 19.44 2 3 -1 o 27.141 22.087 180.00 2.13135 3.15 3 0 -2 o 83.261 35.959 180.00 2.10331 4.68 2 3 1 o 2.515 0.604 0.00 2.09135 0.28 0 4 0 o 23.197 5.840 180.00 2.08444 1.27 0 0 4 o 64.381 16.385 180.00 2.08257 3.52 2 1 3 o 0.877 0.401 0.00 2.05263 0.09 3 2 0 o 108.221 91.798 0.00 2.04682 11.39 3 1 -2 o 180.803 174.227 180.00 2.03942 18.84 1 0 -4 o 117.415 104.771 180.00 2.03196 6.05 0 4 1 o 111.498 95.444 0.00 2.02210 11.38 0 1 4 o 0.047 0.041 0.00 2.02049 0.00 3 2 -1 o 24.565 19.289 180.00 2.01322 2.48 1 4 0 o 13.081 6.360 0.00 1.99887 1.29 3 0 2 o 57.689 29.399 180.00 1.99384 2.84 2 2 -3 o 66.754 50.484 0.00 1.98031 6.47 1 1 -4 o 82.407 80.268 180.00 1.97418 7.93 2 3 -2 o 4.523 5.269 0.00 1.96450 0.43 0 3 3 o 0.623 0.728 180.00 1.96434 0.06 1 0 4 o 49.668 58.017 180.00 1.96419 2.35 3 2 1 o 188.297 221.470 0.00 1.96313 17.85 1 4 -1 o 11.712 9.891 180.00 1.95154 1.10 3 1 2 o 11.014 10.513 180.00 1.93916 1.01 1 4 1 o 19.635 22.743 180.00 1.93594 1.79 1 3 -3 o 0.578 0.686 0.00 1.91421 0.05 1 1 4 o 113.432 136.701 0.00 1.91185 10.09 2 3 2 o 33.528 36.034 0.00 1.90306 2.93 2 2 3 o 50.245 44.951 0.00 1.88814 4.31 3 2 -2 o 29.411 26.478 0.00 1.87784 2.49 1 3 3 o 75.239 73.015 0.00 1.87100 6.33 0 4 2 o 9.134 9.992 0.00 1.86404 0.76 0 2 4 o 3.788 4.047 0.00 1.86304 0.32 2 0 -4 o 69.423 53.877 180.00 1.84403 2.81 1 2 -4 o 12.177 10.818 0.00 1.82655 0.96 1 4 -2 o 14.018 19.475 180.00 1.81466 1.09 3 1 -3 o 1.064 4.831 180.00 1.80744 0.08 2 1 -4 o 13.503 27.866 0.00 1.80052 1.03 3 2 2 o 0.038 0.068 0.00 1.79870 0.00 3 3 0 o 124.243 179.394 0.00 1.79427 9.40 2 4 0 o 1.431 2.062 0.00 1.79412 0.11 1 4 2 o 1.412 1.562 0.00 1.78978 0.11 1 2 4 o 3.841 1.492 180.00 1.77685 0.28 3 3 -1 o 0.015 0.009 180.00 1.77150 0.00 2 4 -1 o 114.576 108.455 180.00 1.76548 8.32 4 0 0 o 0.798 1.036 180.00 1.76213 0.03 2 3 -3 o 5.919 8.008 180.00 1.74896 0.42 2 0 4 o 72.245 98.324 0.00 1.74585 2.55 2 4 1 o 117.482 164.614 0.00 1.74255 8.25 3 3 1 o 0.022 0.028 180.00 1.73709 0.00 4 1 0 o 8.611 9.999 0.00 1.72405 0.59 4 1 -1 o 2.252 3.632 180.00 1.70910 0.15 2 1 4 o 29.639 47.234 180.00 1.70879 1.98 3 1 3 o 16.882 26.494 0.00 1.70409 1.12 3 2 -3 o 10.018 10.975 180.00 1.69210 0.65 2 2 -4 o 92.950 82.530 0.00 1.68641 5.99 2 3 3 o 3.477 3.175 0.00 1.68449 0.22 3 3 -2 o 170.909 169.252 180.00 1.67717 10.84 4 1 1 o 9.674 9.268 180.00 1.66818 0.61 2 4 -2 o 33.688 31.449 0.00 1.66711 2.11 0 4 3 o 64.568 60.143 180.00 1.66701 4.03 0 3 4 o 6.913 6.342 0.00 1.66659 0.44 4 0 -2 o 1.749 0.819 180.00 1.66047 0.05 1 3 -4 o -0.001 0.384 180.00 1.64032 0.00 1 4 -3 o 0.085 0.137 0.00 1.63604 0.01 0 5 1 o 0.784 0.892 0.00 1.63511 0.05 0 1 5 o 7.356 6.502 180.00 1.63376 0.44 2 4 2 o 51.101 35.692 0.00 1.62906 3.01 4 1 -2 o 200.615 140.143 0.00 1.62849 11.80 4 2 0 o 3.318 2.793 180.00 1.62309 0.19 1 5 0 o 71.993 61.326 0.00 1.62276 4.20 3 3 2 o 2.094 1.832 180.00 1.62006 0.12 1 1 -5 o 385.813 280.711 180.00 1.61342 22.15 4 2 -1 o 156.573 114.734 180.00 1.61060 8.95 2 2 4 o 2.127 1.566 180.00 1.61034 0.12 3 0 -4 o 7.243 5.512 0.00 1.60910 0.21 1 4 3 o 55.746 42.865 180.00 1.60882 3.18 3 2 3 o 6.172 5.208 0.00 1.60641 0.35 1 3 4 o 27.667 24.788 180.00 1.60404 1.56 1 5 -1 o 76.179 58.500 180.00 1.59713 4.26 1 5 1 o 235.185 206.587 180.00 1.58854 12.97 4 0 2 o 10.734 9.560 180.00 1.58771 0.29 3 1 -4 o 27.552 29.087 180.00 1.57994 1.50 4 2 1 o 21.506 25.329 180.00 1.57622 1.16 1 1 5 o 57.456 63.496 180.00 1.57056 3.08 4 1 2 o 43.499 39.840 180.00 1.55968 2.29 3 4 0 o 35.498 32.343 180.00 1.55925 1.87 0 5 2 o 0.015 0.012 0.00 1.54809 0.00 0 2 5 o 54.433 42.762 180.00 1.54708 2.80 3 4 -1 o 3.700 2.853 180.00 1.54424 0.19 4 2 -2 o 1.357 1.052 0.00 1.54261 0.07 3 3 -3 o 24.807 19.144 180.00 1.54086 1.26 2 3 -4 o 138.785 113.121 180.00 1.53657 7.02 1 2 -5 o 7.289 17.831 180.00 1.52978 0.37 2 4 -3 o 1.403 4.047 0.00 1.52924 0.07 3 4 1 o 2.818 8.747 0.00 1.52128 0.14 1 5 -2 o 10.640 23.603 0.00 1.51945 0.52 2 1 -5 o 0.637 1.245 180.00 1.51810 0.03 3 0 4 o 89.266 116.247 0.00 1.51233 2.16 2 5 0 o 3.340 2.409 180.00 1.50733 0.16 4 1 -3 o 11.929 7.728 0.00 1.50648 0.57 1 5 2 o 31.262 16.667 180.00 1.50476 1.50 3 2 -4 o 1.321 0.552 0.00 1.50116 0.06 1 2 5 o 3.103 2.302 180.00 1.49310 0.14 2 5 -1 o 60.916 50.900 0.00 1.49023 2.84 4 3 0 o 2.655 2.259 0.00 1.48821 0.12 3 1 4 o 149.320 127.293 0.00 1.48805 6.94 2 4 3 o 103.739 94.450 0.00 1.48558 4.80 4 2 2 o 24.151 24.256 180.00 1.48375 1.12 3 4 -2 o 13.196 16.750 180.00 1.48055 0.61 4 3 -1 o 27.278 38.763 180.00 1.47857 1.25 2 3 4 o 0.798 1.139 180.00 1.47837 0.04 2 5 1 o 0.180 0.313 0.00 1.47636 0.01 3 3 3 o 9.712 19.991 0.00 1.47532 0.44 0 4 4 o 0.074 4.765 180.00 1.47326 0.00 1 4 -4 o 1.020 0.827 180.00 1.45501 0.04 4 3 1 o 20.156 24.407 180.00 1.45183 0.88 2 1 5 o 16.195 18.115 180.00 1.44880 0.70 2 2 -5 o 89.668 97.145 180.00 1.44781 3.88 3 4 2 o 6.482 6.870 180.00 1.44082 0.28 4 2 -3 o 2.892 3.053 0.00 1.43772 0.12 2 5 -2 o 0.621 0.946 0.00 1.42963 0.03 0 5 3 o 17.865 27.147 0.00 1.42957 0.75 1 4 4 o 0.654 0.995 0.00 1.42951 0.03 0 3 5 o 10.611 16.319 180.00 1.42897 0.44 4 1 3 o 16.315 30.543 0.00 1.42620 0.68 4 3 -2 o 14.854 30.712 180.00 1.42544 0.62 3 2 4 o 3.385 11.106 0.00 1.42167 0.14 1 3 -5 o 28.794 45.536 180.00 1.41530 1.18 1 5 -3 o 16.982 21.449 0.00 1.40990 0.68 5 0 0 o 13.588 17.158 180.00 1.40970 0.27 2 5 2 o 14.944 16.309 180.00 1.40542 0.60 3 3 -4 o 52.784 52.799 180.00 1.39254 2.06 1 5 3 o 239.675 238.393 180.00 1.39236 9.38 5 1 0 o 0.209 0.198 0.00 1.38998 0.01 0 6 0 o 303.463 286.488 180.00 1.38963 5.91 4 0 -4 o 126.893 118.210 0.00 1.38860 2.47 0 0 6 o 138.472 128.642 180.00 1.38838 2.69 2 2 5 o 109.461 100.438 180.00 1.38732 4.24 1 3 5 o 6.515 5.923 180.00 1.38611 0.25 5 1 -1 o 117.210 106.910 0.00 1.38492 4.52 3 4 -3 o 110.550 101.746 0.00 1.38425 4.27 3 1 -5 o 15.173 15.513 0.00 1.38155 0.58 2 4 -4 o 1.944 2.037 180.00 1.38114 0.07 4 3 2 o 26.172 31.323 0.00 1.37861 1.00 1 0 -6 o 43.732 52.368 0.00 1.37861 0.83 0 6 1 o 0.397 0.370 180.00 1.37069 0.01 4 1 -4 o 30.447 27.656 0.00 1.36973 1.14 0 1 6 o 1.169 1.056 180.00 1.36952 0.04 4 2 3 o 33.056 29.631 0.00 1.36744 1.23 1 6 0 o 13.852 13.263 180.00 1.36338 0.51 5 0 -2 o 58.507 55.112 180.00 1.36134 1.08 1 1 -6 o 0.655 0.607 0.00 1.36014 0.02 3 5 0 o 20.609 19.015 0.00 1.35986 0.76 5 1 1 o 25.535 23.853 180.00 1.35753 0.94 3 5 -1 o 0.003 0.004 0.00 1.34986 0.00 2 3 -5 o 0.757 0.985 180.00 1.34964 0.03 1 6 -1 o 0.383 0.379 0.00 1.34808 0.01 1 0 6 o 10.772 9.309 180.00 1.34637 0.19 4 4 0 o 2.945 2.538 0.00 1.34570 0.11 5 1 -2 o 12.974 12.547 180.00 1.34355 0.47 1 6 1 o 15.901 16.113 0.00 1.34290 0.57 4 3 -3 o 0.444 0.486 0.00 1.34146 0.02 2 5 -3 o 3.473 3.890 0.00 1.33981 0.12 4 4 -1 o 136.618 150.475 180.00 1.33856 4.84 2 4 4 o 1.434 1.575 0.00 1.33841 0.05 3 4 3 o 54.051 57.378 180.00 1.33615 1.91 5 2 0 o 65.773 69.640 0.00 1.33542 2.32 3 5 1 o 21.341 22.642 0.00 1.33445 0.75 5 2 -1 o 109.067 118.507 180.00 1.33094 3.81 1 1 6 o 0.506 0.553 0.00 1.32915 0.02 3 3 4 o 64.102 69.948 0.00 1.32840 2.23 3 2 -5 o 7.690 8.367 180.00 1.32794 0.27 2 0 -6 o 73.587 55.897 180.00 1.32015 1.26 4 4 1 o 43.254 33.034 180.00 1.31863 1.47 0 6 2 o 5.759 4.452 0.00 1.31820 0.20 4 2 -4 o 89.005 71.267 0.00 1.31744 3.03 0 2 6 o 33.352 26.993 0.00 1.31725 1.14 5 0 2 o 233.721 264.443 180.00 1.31069 3.93 2 5 3 o 2.962 3.294 180.00 1.31016 0.10 1 2 -6 o 4.496 4.722 0.00 1.30890 0.15 3 5 -2 o 47.022 45.288 180.00 1.30670 1.57 5 2 1 o 20.734 19.920 0.00 1.30657 0.69 4 0 4 o 36.897 35.263 180.00 1.30563 0.61 3 1 5 o 7.292 7.172 180.00 1.30445 0.24 2 1 -6 o 68.988 69.621 0.00 1.30391 2.29 0 5 4 o 1.658 1.927 0.00 1.30168 0.06 0 4 5 o 5.904 6.945 0.00 1.30142 0.20 1 6 -2 o 0.793 0.952 0.00 1.30038 0.03 2 3 5 o 0.022 0.026 0.00 1.30024 0.00 4 4 -2 o 0.003 0.003 0.00 1.29876 0.00 5 1 2 o 35.674 25.256 180.00 1.29479 1.16 5 2 -2 o 14.307 9.917 180.00 1.29409 0.47 2 6 0 o 11.839 8.308 180.00 1.29276 0.39 1 6 2 o 2.529 1.878 0.00 1.29113 0.08 1 4 -5 o 5.596 4.162 0.00 1.29108 0.18 4 1 4 o 30.963 23.253 180.00 1.28991 1.00 1 5 -4 o 46.591 33.865 180.00 1.28905 1.51 4 3 3 o 0.006 0.003 0.00 1.28383 0.00 2 6 -1 o 7.911 3.486 0.00 1.28192 0.25 1 2 6 o 12.549 5.410 180.00 1.28121 0.40 3 5 2 o 46.483 19.503 180.00 1.27915 1.47 5 1 -3 o 1.977 1.030 0.00 1.27473 0.06 3 4 -4 o 1.378 0.730 180.00 1.27373 0.04 2 6 1 o 50.222 26.307 0.00 1.27306 1.57 1 5 4 o 88.562 42.482 0.00 1.27121 2.77 1 4 5 o 10.033 4.144 180.00 1.26880 0.31 2 0 6 o 108.497 35.781 0.00 1.26512 1.68 4 4 2 o 16.555 5.600 0.00 1.26304 0.51 3 2 5 o 0.701 0.337 180.00 1.25905 0.02 2 2 -6 o 16.345 8.424 0.00 1.25855 0.50 5 3 0 o 4.879 3.216 0.00 1.25722 0.15 5 3 -1 o 18.374 20.288 0.00 1.25348 0.56 3 3 -5 o 3.298 3.164 180.00 1.25098 0.10 2 1 6 o 12.800 12.248 180.00 1.25080 0.39 5 2 2 o 7.538 7.222 0.00 1.25035 0.23 4 2 4 o 48.411 59.092 180.00 1.24595 1.45 2 6 -2 o 170.116 178.018 0.00 1.24274 5.06 0 6 3 o 144.046 150.380 180.00 1.24270 4.28 4 3 -4 o 142.813 144.877 180.00 1.24218 4.24 0 3 6 o 14.238 14.329 0.00 1.24203 0.42 2 4 -5 o 175.267 167.165 180.00 1.24065 5.19 3 5 -3 o 12.390 11.398 0.00 1.23907 0.37 2 5 -4 o 2.693 2.325 180.00 1.23683 0.08 4 1 -5 o 43.925 37.251 180.00 1.23636 1.29 1 3 -6 o 26.144 21.043 0.00 1.23502 0.77 4 4 -3 o 0.382 0.300 0.00 1.23429 0.01 5 3 1 o 0.205 0.157 180.00 1.23306 0.01 1 6 -3 o 3.725 2.604 180.00 1.22971 0.11 3 0 -6 o 88.538 61.509 0.00 1.22935 1.28 5 2 -3 o 0.950 0.710 180.00 1.23226 0.03 2 6 2 o 0.100 0.071 180.00 1.22673 0.00 3 4 4 o 0.046 0.032 180.00 1.22409 0.00 5 3 -2 o 22.708 14.740 180.00 1.22256 0.65 1 6 3 o 5.533 5.890 0.00 1.21802 0.16 3 1 -6 o 0.585 0.876 0.00 1.21620 0.02 5 1 3 o 0.284 0.329 180.00 1.21342 0.01 1 3 6 o 288.106 270.433 180.00 1.21168 8.11 4 5 0 o 9.360 8.525 0.00 1.21119 0.26 2 2 6 o 66.419 59.411 0.00 1.21060 1.87 4 5 -1 o 35.640 43.711 0.00 1.20598 0.99 2 5 4 o 1.170 1.444 180.00 1.20587 0.03 3 5 3 o 47.266 61.916 180.00 1.20421 1.32 5 0 -4 o 83.364 105.469 0.00 1.20275 1.16 2 4 5 o 1.112 1.343 0.00 1.20196 0.03 4 2 -5 o 1.559 1.483 180.00 1.19750 0.04 3 6 0 o 10.256 11.179 180.00 1.19608 0.28 3 3 5 o 0.020 0.036 180.00 1.19288 0.00 2 3 -6 o 0.248 0.458 0.00 1.19246 0.01 4 5 1 o 47.830 87.029 0.00 1.19134 1.31 5 1 -4 o 0.434 0.737 0.00 1.19043 0.01 3 6 -1 o 13.290 20.686 180.00 1.18926 0.36 4 4 3 o 21.840 33.092 0.00 1.18896 0.59 5 3 2 o 64.199 74.377 180.00 1.18548 1.73 2 6 -3 o 55.925 55.578 0.00 1.18237 1.50 4 3 4 o 156.624 153.468 0.00 1.18173 4.20 3 2 -6 o 26.832 26.862 180.00 1.17915 0.72 0 7 1 o 0.707 0.709 180.00 1.17912 0.02 3 6 1 o 30.999 31.537 0.00 1.17868 0.83 0 5 5 o 7.586 7.740 0.00 1.17861 0.20 0 1 7 o 1.091 1.136 0.00 1.17810 0.03 4 5 -2 o 7.886 8.610 0.00 1.17663 0.21 5 2 3 o 17.824 19.466 0.00 1.17662 0.47 6 0 0 o 50.594 53.594 0.00 1.17475 0.67 1 7 0 o 1.314 1.368 180.00 1.17446 0.03 1 1 -7 o 45.496 45.320 0.00 1.17383 1.21 1 5 -5 o 238.775 193.962 0.00 1.17090 6.29 5 3 -3 o 1.293 1.039 0.00 1.17002 0.03 5 4 0 o 11.437 10.544 180.00 1.16773 0.30 5 4 -1 o 4.230 4.823 180.00 1.16473 0.11 1 7 -1 o 21.873 24.941 0.00 1.16463 0.57 3 0 6 o 53.582 60.224 0.00 1.16390 0.70 6 1 0 o 32.262 35.310 0.00 1.16326 0.84 4 1 5 o 0.681 0.740 180.00 1.16310 0.02 3 4 -5 o 35.452 37.782 0.00 1.16272 0.92 6 1 -1 o 49.023 50.626 0.00 1.16196 1.27 2 6 3 o 17.617 18.123 180.00 1.16184 0.46 1 7 1 o 52.792 53.658 0.00 1.16129 1.37 3 6 -2 o 15.748 16.451 0.00 1.15943 0.41 3 5 -4 o 23.404 25.949 180.00 1.15792 0.61 0 6 4 o 0.104 0.118 180.00 1.15592 0.00 4 4 -4 o 7.619 8.616 180.00 1.15565 0.20 5 2 -4 o 0.178 0.201 180.00 1.15562 0.00 0 4 6 o 2.491 2.814 180.00 1.15552 0.06 1 5 5 o 36.237 40.473 0.00 1.15421 0.93 3 1 6 o 40.627 45.744 0.00 1.15272 1.04 2 3 6 o 26.319 29.884 180.00 1.15143 0.67 1 1 7 o 17.120 19.225 0.00 1.15048 0.44 4 5 2 o 7.848 8.647 180.00 1.14987 0.20 1 4 -6 o 0.043 0.048 180.00 1.14987 0.00 6 0 -2 o 29.030 31.508 0.00 1.14954 0.37 5 4 1 o 17.325 17.493 0.00 1.14829 0.44 1 6 -4 o 3.547 3.279 0.00 1.14704 0.09 0 7 2 o 0.811 0.663 180.00 1.14520 0.02 0 2 7 o 9.050 7.080 0.00 1.14433 0.23 6 1 1 o 35.297 25.940 180.00 1.14246 0.89 1 2 -7 o 24.620 18.821 180.00 1.14041 0.62 4 3 -5 o 10.177 7.938 0.00 1.14014 0.26 3 6 2 o 0.738 0.580 0.00 1.14005 0.02 5 4 -2 o 0.001 0.001 180.00 1.13979 0.00 6 1 -2 o 31.563 29.113 0.00 1.13876 0.79 2 1 -7 o 7.426 6.951 0.00 1.13867 0.19 5 0 4 o 24.525 36.853 180.00 1.13499 0.31 1 6 4 o 0.907 1.365 0.00 1.13442 0.02 1 7 -2 o 1.015 1.501 180.00 1.13346 0.03 2 5 -5 o 0.645 0.932 180.00 1.13290 0.02 1 4 6 o 0.749 0.935 0.00 1.13096 0.02 6 2 0 o 4.073 4.931 180.00 1.13072 0.10 4 2 5 o 19.339 22.948 180.00 1.13057 0.48 6 2 -1 o 10.763 10.853 0.00 1.12952 0.27 2 7 0 o 0.001 0.001 0.00 1.12840 0.00 4 5 -3 o 1.120 0.886 180.00 1.12805 0.03 1 7 2 o 0.081 0.058 0.00 1.12732 0.00 4 0 -6 o 15.663 10.050 180.00 1.12521 0.19 5 1 4 o 3.294 2.138 0.00 1.12462 0.08 3 3 -6 o 20.410 13.449 0.00 1.12427 0.50 5 3 3 o 4.249 3.178 0.00 1.12208 0.10 2 7 -1 o 11.504 9.033 180.00 1.12117 0.28 3 2 6 o 5.949 4.709 180.00 1.12103 0.15 3 5 4 o 72.106 59.310 0.00 1.12025 1.77 1 2 7 o 9.185 8.047 0.00 1.11897 0.23 3 4 5 o 42.006 40.394 180.00 1.11563 1.03 2 4 -6 o 4.758 4.579 180.00 1.11529 0.12 2 7 1 o 22.252 21.418 180.00 1.11523 0.54 4 1 -6 o 22.676 21.828 0.00 1.11510 0.55 6 0 2 o 80.613 77.171 0.00 1.11265 0.98 6 2 1 o 12.723 12.146 180.00 1.11158 0.31 3 6 -3 o 20.594 19.651 180.00 1.11140 0.50 2 6 -4 o 0.656 0.631 180.00 1.10979 0.02 5 4 2 o 1.558 1.504 180.00 1.10957 0.04 6 2 -2 o 8.237 8.132 180.00 1.10818 0.20 2 2 -7 o 1.389 1.373 180.00 1.10809 0.03 4 4 4 o 9.661 9.674 0.00 1.10649 0.23 5 3 -4 o 81.366 81.222 0.00 1.10382 1.96 2 5 5 o 0.044 0.045 0.00 1.10321 0.00 6 1 2 o 11.433 11.717 180.00 1.10287 0.28 5 1 -5 o 1.338 1.448 0.00 1.10115 0.03 6 1 -3 o 1.001 0.688 0.00 1.09735 0.02 2 1 7 o 5.275 3.504 180.00 1.09713 0.13 5 4 -3 o 159.913 102.220 0.00 1.09687 3.82 5 2 4 o 0.427 0.225 0.00 1.09513 0.01 2 7 -2 o 0.199 0.100 0.00 1.09468 0.00 0 7 3 o 5.922 2.986 180.00 1.09465 0.14 0 3 7 o 6.036 2.878 0.00 1.09397 0.14 4 5 3 o 0.697 0.313 0.00 1.09313 0.02 4 6 0 o 4.851 2.035 0.00 1.09115 0.11 1 3 -7 o 11.162 4.728 180.00 1.09055 0.27 4 6 -1 o 0.826 0.455 180.00 1.08734 0.02 2 6 4 o 10.714 5.939 180.00 1.08726 0.25 4 2 -6 o 0.079 0.048 180.00 1.08634 0.00 3 6 3 o 53.881 33.068 0.00 1.08604 1.27 1 7 -3 o 0.048 0.030 180.00 1.08574 0.00 2 7 2 o 3.953 3.140 180.00 1.08369 0.09 6 3 0 o 5.611 5.360 180.00 1.08206 0.13 4 3 5 o 0.705 0.680 0.00 1.08193 0.02 2 4 6 o 9.342 9.255 180.00 1.08151 0.22 6 3 -1 o 0.157 0.158 180.00 1.08101 0.00 3 1 -7 o 90.661 91.744 0.00 1.08020 2.14 1 7 3 o 50.716 47.476 180.00 1.07767 1.19 4 6 1 o 3.306 2.975 0.00 1.07657 0.08 5 5 0 o 3.256 2.928 0.00 1.07656 0.08 6 2 2 o 6.344 5.409 0.00 1.07502 0.15 5 5 -1 o 80.748 66.870 180.00 1.07421 1.89 3 3 6 o 34.462 27.918 180.00 1.07356 0.81 5 2 -5 o 15.604 12.583 180.00 1.07342 0.37 3 5 -5 o 2.263 1.783 0.00 1.07263 0.05 4 4 -5 o 31.820 24.809 180.00 1.07213 0.75 1 3 7 o 14.439 11.193 180.00 1.07175 0.34 6 2 -3 o 68.670 53.079 0.00 1.06990 1.61 2 2 7 o 0.025 0.019 0.00 1.06970 0.00 0 6 5 o 35.644 28.427 180.00 1.06715 0.83 4 5 -4 o 0.561 0.448 180.00 1.06707 0.01 0 5 6 o 0.322 0.257 180.00 1.06697 0.01 4 6 -2 o 0.839 0.684 0.00 1.06568 0.02 6 3 1 o 38.797 31.876 180.00 1.06525 0.90 1 5 -6 o 13.313 11.336 0.00 1.06252 0.31 3 7 0 o 0.018 0.016 0.00 1.06238 0.00 6 3 -2 o 57.073 48.934 180.00 1.06226 1.33 2 3 -7 o 32.215 27.683 0.00 1.06218 0.75 1 6 -5 o 22.630 20.001 180.00 1.06142 0.53 5 5 1 o 0.056 0.050 180.00 1.06127 0.00 3 4 -6 o 4.422 4.430 0.00 1.05891 0.10 4 0 6 o 43.888 43.969 0.00 1.05890 0.51 3 7 -1 o 0.769 0.824 0.00 1.05760 0.02 5 4 3 o 3.692 4.086 180.00 1.05707 0.09 5 5 -2 o 6.460 8.149 180.00 1.05455 0.15 3 2 -7 o 1.286 1.587 180.00 1.05399 0.03 2 7 -3 o 39.258 41.385 180.00 1.05274 0.91 3 6 -4 o 0.771 0.666 180.00 1.05172 0.02 6 0 -4 o 0.695 0.594 0.00 1.05165 0.01 5 3 4 o 0.000 0.000 180.00 1.05075 0.00 4 1 6 o 46.219 32.583 180.00 1.05047 1.07 3 7 1 o 282.946 192.733 0.00 1.05014 6.54 6 1 3 o 9.803 6.620 0.00 1.05005 0.23 1 6 5 o 4.338 2.864 0.00 1.04894 0.10 1 5 6 o 35.387 27.591 180.00 1.04755 0.82 4 6 2 o 3.180 3.819 0.00 1.04568 0.07 6 1 -4 o 1.945 2.854 0.00 1.04339 0.05 4 3 -6 o 11.745 16.690 0.00 1.04297 0.27 0 8 0 o 104.419 138.443 180.00 1.04222 1.21 5 4 -4 o 0.861 1.100 0.00 1.04177 0.02 0 0 8 o 119.823 149.062 180.00 1.04128 1.38 1 0 -8 o 24.026 32.239 0.00 1.03952 0.28 2 7 3 o 8.434 14.386 180.00 1.03817 0.20 3 7 -2 o 0.327 0.800 0.00 1.03645 0.01 5 1 5 o 1.866 4.653 180.00 1.03640 0.04 3 5 5 o 0.398 1.138 180.00 1.03533 0.01 2 5 -6 o 6.870 20.418 0.00 1.03506 0.16 0 8 1 o 0.475 1.437 0.00 1.03416 0.01 0 7 4 o 0.040 0.120 180.00 1.03394 0.00 0 4 7 o 4.314 12.747 0.00 1.03347 0.10 0 1 8 o 0.115 0.333 0.00 1.03326 0.00 6 3 2 o 19.075 54.103 180.00 1.03295 0.44 2 6 -5 o 1.100 3.070 180.00 1.03286 0.03 1 1 -8 o 0.527 1.340 180.00 1.03154 0.01 5 3 -5 o 0.129 0.333 180.00 1.03153 0.00 1 8 0 o 1.067 2.646 180.00 1.03101 0.02 1 4 -7 o 0.004 0.010 0.00 1.03058 0.00 5 5 2 o 12.125 29.677 180.00 1.03048 0.28 4 6 -3 o 6.616 16.609 0.00 1.02918 0.15 6 3 -3 o 0.758 2.012 0.00 1.02841 0.02 2 3 7 o 1.764 4.815 0.00 1.02823 0.04 4 5 4 o 3.932 11.052 0.00 1.02801 0.09 3 1 7 o 5.741 16.203 0.00 1.02799 0.13 1 7 -4 o 0.511 1.588 180.00 1.02758 0.01 4 2 6 o 1.997 12.638 0.00 1.02631 0.05 6 2 3 o 0.003 0.031 180.00 1.02592 0.00 1 8 -1 o 0.002 0.120 180.00 1.02434 0.00 6 4 0 o -0.004 0.592 0.00 1.02341 0.00 4 4 5 o 0.000 0.004 180.00 1.02330 0.00 3 6 4 o -0.023 16.924 180.00 1.02325 0.00 3 7 2 o -0.002 1.025 180.00 1.02254 0.00 6 4 -1 o 0.011 1.121 0.00 1.02252 0.00 1 8 1 o -0.012 2.647 180.00 1.02207 0.00 5 0 -6 o -0.021 6.602 0.00 1.02156 0.00 1 0 8 o -0.001 0.370 180.00 1.02093 0.00 5 5 -3 o -0.005 3.318 180.00 1.02028 0.00 6 2 -4 o -0.010 0.724 0.00 1.01971 0.00 1 7 4 o 3.388 5.058 0.00 1.01847 0.08 3 4 6 o 2.053 1.160 0.00 1.01621 0.05 2 0 -8 o 2.614 1.435 0.00 1.01598 0.03 1 4 7 o 9.165 4.615 0.00 1.01468 0.21 3 3 -7 o 0.029 0.015 180.00 1.01425 0.00 5 1 -6 o 0.285 0.145 180.00 1.01398 0.01 1 1 8 o 0.000 0.000 0.00 1.01337 0.00 5 2 5 o 35.857 18.928 0.00 1.01319 0.82 0 2 8 o 0.396 0.187 0.00 1.01025 0.01 2 6 5 o 131.916 62.333 180.00 1.01021 3.04 6 4 1 o 10.322 4.328 180.00 1.00916 0.24 0 8 2 o 3.679 1.881 0.00 1.01105 0.08 1 2 -8 o 46.304 18.327 180.00 1.00864 1.07 4 1 -7 o 2.652 1.041 0.00 1.00858 0.06 2 1 -8 o 1.741 0.685 0.00 1.00852 0.04 2 5 6 o 26.130 9.614 180.00 1.00788 0.60 7 0 0 o 22.248 7.640 0.00 1.00693 0.26 6 4 -2 o 0.532 0.178 0.00 1.00661 0.01 2 4 -7 o 1.547 0.517 180.00 1.00655 0.04 3 2 7 o 9.800 3.134 180.00 1.00532 0.23 _reflns_number_observed 507 _reflns_limit_h_min 0 _reflns_limit_h_max 7 _reflns_limit_k_min 0 _reflns_limit_k_max 8 _reflns_limit_l_min -8 _reflns_limit_l_max 8 _reflns_d_resolution_high 1.005 _reflns_d_resolution_low 7.049 # The following lines are used to test the character set of files sent by # network email or other means. They are not part of the CIF data set. # abcdefghijklmnopqrstuvwxyzABCDEFGHIJKLMNOPQRSTUVWXYZ0123456789 # !@#$%^&*()_+{}:"~<>?|\-=[];'`,./