Crystallography Open Database

Information card for entry 4311901

4311900 << 4311901 >> 4311902

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Coordinates	4311901.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H40 N2 Si2 Sn
Calculated formula	C24 H40 N2 Si2 Sn
SMILES	[Sn](N([Si](C)(C)C)c1c(cc(cc1C)C)C)N([Si](C)(C)C)c1c(cc(cc1C)C)C
Title of publication	Syntheses and Structural Characterization of a Monomeric Tin(II) Diamide and a Novel Chlorotin(II) Amide Trimer
Authors of publication	Yongjun Tang; Ana M. Felix; Lev N. Zakharov; Arnold L. Rheingold; Richard A. Kemp
Journal of publication	Inorganic Chemistry
Year of publication	2004
Journal volume	43
Pages of publication	7239 - 7242
a	11.4745 ± 0.0009 Å
b	14.5719 ± 0.0012 Å
c	17.1003 ± 0.0013 Å
α	100.277 ± 0.001°
β	95.159 ± 0.002°
γ	90.172 ± 0.001°
Cell volume	2801.5 ± 0.4 Å³
Cell temperature	213 ± 2 K
Ambient diffraction temperature	213 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.058
Residual factor for significantly intense reflections	0.0458
Weighted residual factors for significantly intense reflections	0.1166
Weighted residual factors for all reflections included in the refinement	0.125
Goodness-of-fit parameter for all reflections included in the refinement	1.021
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179158 (current)	2016-03-23	cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/19.	4311901.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4311901.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4311901.cif
5312	2011-01-03	cif/ Adding files, updated with the 'cif_fix_enum' program and the cif_core.dic dictionary. The enumerator values were fixed, mostly incorrect case, but also some values that had extra underscores, dashes or spaces. Unfortunately, 22 had non-ASCII characters with the 8-th bit set, and these got incorrectly interpreted as latin1 characters and converted to their UTF8 equivalents by Perl. To fix the structures, however, they need to be redeposited from the original files with the new CIFParser/cif_filter version.	4311901.cif
3403	2010-11-15	../uploads/cif-deposit/cod/cif Adding structures of 4311901 via cif-deposit CGI script.	4311901.cif