Crystallography Open Database

Information card for entry 4313597

Preview

Coordinates	4313597.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C211 H182 Cl34 N20 Rh4
Calculated formula	C211 H132 Cl34 N20 Rh4
Title of publication	Synthesis and Properties of Rhodium(III) Porphyrin Cyclic Tetramer and Cofacial Dimer
Authors of publication	Keiko Fukushima; Kenji Funatsu; Akio Ichimura; Yoichi Sasaki; Masamitsu Suzuki; Tetsuaki Fujihara; Kiyoshi Tsuge; Taira Imamura
Journal of publication	Inorganic Chemistry
Year of publication	2003
Journal volume	42
Pages of publication	3187 - 3193
a	15.972 ± 0.001 Å
b	17.631 ± 0.002 Å
c	19.856 ± 0.002 Å
α	86.924 ± 0.003°
β	86.302 ± 0.001°
γ	81.108 ± 0.001°
Cell volume	5507.4 ± 0.9 Å³
Cell temperature	120 K
Ambient diffraction temperature	120 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for significantly intense reflections	0.1015
Weighted residual factors for all reflections included in the refinement	0.2335
Goodness-of-fit parameter for all reflections included in the refinement	2.596
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4313597.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4313597.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4313597.cif
6666	2011-01-12	../uploads/cif-deposit/cod/cif Adding structures of 4313597 via cif-deposit CGI script.	4313597.cif