Crystallography Open Database

Information card for entry 4316061

Preview

Coordinates	4316061.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H34 Cu7 N40 O2
Calculated formula	C24 H34 Cu7 N40 O2
Title of publication	A Unique Example of Structural and Magnetic Diversity in Four Interconvertible Copper(II)-Azide Complexes with the Same Schiff Base Ligand: A Monomer, a Dimer, a Chain, and a Layer
Authors of publication	Subrata Naiya; Chaitali Biswas; Michael G. B. Drew; Carlos J. Gómez-García; Juan M. Clemente-Juan; Ashutosh Ghosh
Journal of publication	Inorganic Chemistry
Year of publication	2010
Journal volume	49
Pages of publication	6616 - 6627
a	10.3496 ± 0.0011 Å
b	11.3763 ± 0.001 Å
c	11.7155 ± 0.001 Å
α	98.344 ± 0.008°
β	115.39 ± 0.01°
γ	98.852 ± 0.008°
Cell volume	1196.4 ± 0.2 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.2828
Residual factor for significantly intense reflections	0.0839
Weighted residual factors for significantly intense reflections	0.1151
Weighted residual factors for all reflections included in the refinement	0.166
Goodness-of-fit parameter for all reflections included in the refinement	0.816
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179240 (current)	2016-03-23	cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/60.	4316061.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4316061.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4316061.cif
9236	2011-02-09	../uploads/cif-deposit/cod/cif Adding structures of 4316061 via cif-deposit CGI script.	4316061.cif