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Information card for entry 4316140
Preview
| Coordinates | 4316140.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | {(2,6-dimesitylphenyl)imidotin(II)}2 |
|---|---|
| Formula | C48 H50 N2 Sn2 |
| Calculated formula | C48 H50 N2 Sn2 |
| SMILES | [Sn]1N(c2c(cccc2c2c(cc(cc2C)C)C)c2c(cc(cc2C)C)C)[Sn]N1c1c(cccc1c1c(cc(cc1C)C)C)c1c(cc(cc1C)C)C |
| Title of publication | Synthesis and Structural Characterization of a Series of Dimeric Metal(II) Imido Complexes {M(μ-NAr#)}2 [M = Ge, Sn, Pb; Ar#= C6H3-2,6-(C6H2-2,4,6-Me3)2] and the Related Monomeric Primary Amido Derivatives M{N(H)Ar#}2 (M = Ge, Sn, Pb): Spectroscopic Manifestations of Secondary Metal-Ligand Interactions |
| Authors of publication | William A. Merrill; Robert J. Wright; Corneliu S. Stanciu; Marilyn M. Olmstead; James C. Fettinger; Philip P. Power |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 2010 |
| Journal volume | 49 |
| Pages of publication | 7097 - 7105 |
| a | 12.6268 ± 0.0011 Å |
| b | 21.102 ± 0.0019 Å |
| c | 16.2797 ± 0.0014 Å |
| α | 90° |
| β | 111.47 ± 0.003° |
| γ | 90° |
| Cell volume | 4036.7 ± 0.6 Å3 |
| Cell temperature | 90 ± 2 K |
| Ambient diffraction temperature | 90 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.083 |
| Residual factor for significantly intense reflections | 0.0449 |
| Weighted residual factors for significantly intense reflections | 0.0999 |
| Weighted residual factors for all reflections included in the refinement | 0.1177 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.022 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 179241 (current) | 2016-03-23 | cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/61. |
4316140.cif |
| 91935 | 2013-12-29 | cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs. |
4316140.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4316140.cif |
| 9330 | 2011-02-09 | ../uploads/cif-deposit/cod/cif Adding structures of 4316140 via cif-deposit CGI script. |
4316140.cif |
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