Crystallography Open Database

Information card for entry 4317518

Preview

Coordinates	4317518.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C82 H116 Al2 Cl8 N4 O8 P2
Calculated formula	C81.88 H115.76 Al2 Cl7.76 N4 O8 P2
Title of publication	Ligand-Tetrahydrofuran Coupling in Chelated Aluminum Phosphinates
Authors of publication	Y. Wang; S. Parkin; D. Atwood
Journal of publication	Inorganic Chemistry
Year of publication	2002
Journal volume	41
Pages of publication	558 - 565
a	9.337 ± 0.001 Å
b	16.245 ± 0.002 Å
c	16.297 ± 0.002 Å
α	66.953 ± 0.01°
β	73.913 ± 0.01°
γ	78.892 ± 0.01°
Cell volume	2175.6 ± 0.5 Å³
Cell temperature	173 ± 1 K
Ambient diffraction temperature	173 ± 1 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0632
Residual factor for significantly intense reflections	0.0425
Weighted residual factors for significantly intense reflections	0.1031
Weighted residual factors for all reflections included in the refinement	0.1124
Goodness-of-fit parameter for all reflections included in the refinement	1.033
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179255 (current)	2016-03-23	cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/75.	4317518.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4317518.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4317518.cif
12268	2011-03-05	../uploads/cif-deposit/cod/cif Adding structures of 4317518 via cif-deposit CGI script.	4317518.cif