Crystallography Open Database

Information card for entry 4317541

Preview

Coordinates	4317541.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C63 H69 Cl2 N11 O18 Zn4
Calculated formula	C63 H69 Cl2 N11 O18 Zn4
Title of publication	Formation of Molecular Ladder Elements with Macrocyclic Platforms via Linear Bifunctional Ligands
Authors of publication	Wei Huang; Shaohua Gou; Dahua Hu; Suchada Chantrapromma; Hoong-Kun Fun; Qingjin Meng
Journal of publication	Inorganic Chemistry
Year of publication	2002
Journal volume	41
Pages of publication	864 - 868
a	11.652 ± 0.0003 Å
b	12.1394 ± 0.0003 Å
c	13.8462 ± 0.0003 Å
α	66.9563 ± 0.0008°
β	80.5638 ± 0.0008°
γ	76.6348 ± 0.0008°
Cell volume	1747.52 ± 0.07 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0901
Residual factor for significantly intense reflections	0.0601
Weighted residual factors for significantly intense reflections	0.1487
Weighted residual factors for all reflections included in the refinement	0.1619
Goodness-of-fit parameter for all reflections included in the refinement	0.925
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179255 (current)	2016-03-23	cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/75.	4317541.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4317541.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4317541.cif
13816	2011-03-07	../uploads/cif-deposit/cod/cif Adding structures of 4317541 via cif-deposit CGI script.	4317541.cif