Crystallography Open Database

Information card for entry 4317681

Preview

Coordinates	4317681.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C42 H37 Cl3 Cr N8 Ni O14.5
Calculated formula	C42 H36 Cl3 Cr N8 Ni O14.5
Title of publication	Synthesis, Structures, and Magnetic Properties of Heterodimetal Bis(μ-hydroxo)chromium(III)nickel(II) Complexes with Tpa Derivatives Having Sterically Bulky Substituents
Authors of publication	Kazushi Shiren; Shuhei Fujinami; Masatatsu Suzuki; Akira Uehara
Journal of publication	Inorganic Chemistry
Year of publication	2002
Journal volume	41
Pages of publication	1598 - 1605
a	12.07 ± 0.002 Å
b	17.503 ± 0.002 Å
c	21.844 ± 0.002 Å
α	90°
β	94.97 ± 0.01°
γ	90°
Cell volume	4597.4 ± 1 Å³
Cell temperature	293.2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for significantly intense reflections	0.0565
Weighted residual factors for all reflections included in the refinement	0.0812
Goodness-of-fit parameter for all reflections included in the refinement	1.55
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4317681.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4317681.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4317681.cif
13959	2011-03-07	../uploads/cif-deposit/cod/cif Adding structures of 4317681 via cif-deposit CGI script.	4317681.cif