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Information card for entry 4317684
Preview
| Coordinates | 4317684.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C45 H54 Cl15 N9 Sb2 |
|---|---|
| Calculated formula | C45 H54 Cl15 N9 Sb2 |
| Title of publication | Structures of Sb(OC6H3Me2-2,6)3 and Sb(OEt)5.NH3: The First Authenticated Monomeric Sb(OR)n (n= 3, 5) |
| Authors of publication | Graeme A. Horley; Mary F. Mahon; Kieran C. Molloy; Monica M. Venter; Peter W. Haycock; Christopher P. Myers |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 2002 |
| Journal volume | 41 |
| Pages of publication | 1652 - 1657 |
| a | 13.43 ± 0.0002 Å |
| b | 14.418 ± 0.0002 Å |
| c | 17.418 ± 0.0003 Å |
| α | 82.765 ± 0.0007° |
| β | 77.557 ± 0.0007° |
| γ | 70.767 ± 0.0007° |
| Cell volume | 3104.14 ± 0.08 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0842 |
| Residual factor for significantly intense reflections | 0.0417 |
| Weighted residual factors for significantly intense reflections | 0.1035 |
| Weighted residual factors for all reflections included in the refinement | 0.1281 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.844 |
| Diffraction radiation wavelength | 0.71069 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 288183 (current) | 2023-12-08 | cod/ Corrected misspelt data names in multiple entries using the 'cif_correct_tags' program and a data names replacement file from cod-tools revision 9827. This change affected only the misspelt variants of the '_atom_site_symmetry_multiplicity' data name. |
4317684.cif |
| 179256 | 2016-03-23 | cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/76. |
4317684.cif |
| 120093 | 2014-07-12 | Adding DOIs to range 4/31 structures. | 4317684.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4317684.cif |
| 17004 | 2011-03-31 | cif/ Commiting CIFs, that were updated with the 'cif_fix_values' script, using options '--fix-misspelled replacement_values.lst', '--fix-temperature' and '--fix-enums' with built-in table of enum values. The following cmd was used: > (set -x; find ? -name \*.cif | sort | xargs -i sh -c 'if !( > cif_fix_values --fix-misspelled ~/../inputs/replacament_values.lst {} | > cif_filter --add-cif-header {} | > sponge {} ) 2>&1 | grep NOTE; then svn revert {}; > fi' ) & |
4317684.cif |
| 13962 | 2011-03-07 | ../uploads/cif-deposit/cod/cif Adding structures of 4317684 via cif-deposit CGI script. |
4317684.cif |
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