Crystallography Open Database

Information card for entry 4318807

Preview

Coordinates	4318807.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C12 H29 F2 N3 Si
Calculated formula	C12 H29 F2 N3 Si
Title of publication	Hexaalkylguanidinium and 2-(Dialkylamino)-1,3-dimethylimidazolinium Trimethyldifluorosiliconates and Perfluoroalkoxides. Accidental Isolation and Molecular Structure of [C(NMe2)3]+F-.6CH2Cl2
Authors of publication	Alexander A. Kolomeitsev; German Bissky; Jan Barten; Natalya Kalinovich; Enno Lork; Gerd-Volker Röschenthaler
Journal of publication	Inorganic Chemistry
Year of publication	2002
Journal volume	41
Pages of publication	6118 - 6124
a	9.135 ± 0.002 Å
b	8.6 ± 0.002 Å
c	10.58 ± 0.002 Å
α	90°
β	96.99 ± 0.03°
γ	90°
Cell volume	825 ± 0.3 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	13
Hermann-Mauguin space group symbol	P 1 2/n 1
Hall space group symbol	-P 2yac
Residual factor for all reflections	0.0657
Residual factor for significantly intense reflections	0.0496
Weighted residual factors for significantly intense reflections	0.1377
Weighted residual factors for all reflections included in the refinement	0.1456
Goodness-of-fit parameter for all reflections included in the refinement	1.07
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179268 (current)	2016-03-23	cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/88.	4318807.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4318807.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4318807.cif
15533	2011-03-16	../uploads/cif-deposit/cod/cif Adding structures of 4318807 via cif-deposit CGI script.	4318807.cif